#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2011180.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011180_Fobs loop_ _publ_author_name 'Wardell, Solange M. S. V.' 'Wardell, James L.' 'Ward, Mark F.' 'Low, John N.' 'Glidewell, Christopher' _publ_section_title ; Hydrogen-bonded molecular ladders in trans-1,2-bis(2-nitroanilino)cyclohexane ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 865 _journal_page_last 867 _journal_volume 56 _journal_year 2000 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.594 _cell_angle_gamma 90.000 _cell_length_a 13.1140 _cell_length_b 12.7121 _cell_length_c 20.9587 _exptl_crystal_F_000 1504.00 _reflns_d_resolution_high 0.8143 _[local]_cod_data_source_file sk1388Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C18H20N4O4' _shelx_refln_list_code 4 _shelx_f_calc_maximum 442.66 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 44487.68 39584.63 1356.61 o 4 0 0 7.52 32.88 15.85 o 6 0 0 354.52 338.90 37.09 o 8 0 0 1.15 70.50 138.72 o 10 0 0 134.14 184.20 209.22 o 12 0 0 8.97 -138.72 370.68 o 14 0 0 118.85 277.44 391.15 o 1 1 0 182.46 108.14 26.47 o 2 1 0 1443.49 1400.68 40.88 o 3 1 0 811.89 721.49 70.32 o 4 1 0 160.51 150.52 24.73 o 5 1 0 1496.08 1239.28 175.90 o 6 1 0 279.35 243.76 40.52 o 7 1 0 952.78 960.38 52.01 o 8 1 0 150.51 230.39 45.46 o 9 1 0 44.28 106.20 36.91 o 10 1 0 151.07 170.07 33.15 o 11 1 0 98.28 30.29 216.37 o 12 1 0 238.75 66.63 203.75 o 13 1 0 2.45 -210.44 210.44 o 14 1 0 21.68 -106.87 226.73 o 15 1 0 300.55 123.97 576.48 o 0 2 0 14904.12 14657.36 357.71 o 1 2 0 1398.30 1377.72 45.19 o 2 2 0 2860.65 2644.98 71.36 o 3 2 0 30960.92 29571.03 572.97 o 4 2 0 1319.78 1265.02 60.97 o 5 2 0 4037.10 3893.42 94.91 o 6 2 0 201.43 159.69 38.11 o 7 2 0 194.99 129.64 50.54 o 8 2 0 698.76 700.58 63.91 o 9 2 0 100.46 106.25 80.42 o 10 2 0 2419.96 2288.20 147.03 o 11 2 0 227.46 147.51 59.54 o 12 2 0 117.28 501.28 210.44 o 13 2 0 51.63 142.17 210.44 o 14 2 0 3.16 -46.62 228.34 o 15 2 0 15.25 39.99 261.18 o 1 3 0 14705.22 13719.34 270.07 o 2 3 0 45658.32 42948.54 768.88 o 3 3 0 26.96 30.96 25.32 o 4 3 0 245.97 298.24 28.63 o 5 3 0 29.86 38.84 27.09 o 6 3 0 69.46 71.82 29.26 o 7 3 0 16.38 61.78 31.58 o 8 3 0 9.46 14.38 28.74 o 9 3 0 58.27 93.02 70.31 o 10 3 0 235.77 357.22 84.03 o 11 3 0 352.64 276.66 150.00 o 12 3 0 371.07 354.35 243.46 o 13 3 0 384.39 140.29 369.54 o 14 3 0 365.82 218.35 380.91 o 15 3 0 291.09 341.64 278.44 o 0 4 0 33075.83 31483.85 946.98 o 1 4 0 1032.95 1007.38 67.46 o 2 4 0 16345.99 16503.30 308.48 o 3 4 0 1166.82 1224.35 65.47 o 4 4 0 88.18 75.12 41.93 o 5 4 0 1345.54 1501.46 80.77 o 6 4 0 0.07 4.31 36.19 o 7 4 0 532.12 513.42 45.49 o 8 4 0 352.28 436.41 42.88 o 9 4 0 0.80 38.79 45.45 o 10 4 0 3.01 30.32 86.15 o 11 4 0 994.08 910.37 136.51 o 12 4 0 463.43 464.76 143.57 o 13 4 0 106.99 288.45 253.69 o 14 4 0 44.97 99.08 210.44 o 1 5 0 42.38 74.62 56.21 o 2 5 0 1286.54 1299.66 87.29 o 3 5 0 1130.84 1097.89 69.98 o 4 5 0 507.26 623.53 67.81 o 5 5 0 4166.93 4286.85 142.01 o 6 5 0 1190.68 1353.25 78.98 o 7 5 0 540.28 687.57 59.04 o 8 5 0 133.50 246.23 61.10 o 9 5 0 103.71 38.10 36.70 o 10 5 0 503.65 514.42 69.63 o 11 5 0 224.61 155.82 115.78 o 12 5 0 364.99 237.96 120.94 o 13 5 0 105.87 42.21 346.80 o 14 5 0 146.41 669.72 408.44 o 0 6 0 27880.37 28893.49 751.94 o 1 6 0 2626.67 2766.85 101.88 o 2 6 0 1476.58 1274.52 85.37 o 3 6 0 1070.88 1075.00 83.54 o 4 6 0 592.41 695.38 88.41 o 5 6 0 0.00 -11.31 48.92 o 6 6 0 3.36 -3.47 56.07 o 7 6 0 451.46 510.35 61.25 o 8 6 0 148.24 171.57 64.91 o 9 6 0 4.67 -18.74 64.76 o 10 6 0 0.15 -51.07 98.33 o 11 6 0 619.48 821.34 175.97 o 12 6 0 195.84 271.96 186.71 o 13 6 0 277.13 478.29 266.93 o 14 6 0 489.15 615.43 451.41 o 1 7 0 489.41 678.41 112.04 o 2 7 0 1473.94 1460.07 106.04 o 3 7 0 51.74 -34.82 68.21 o 4 7 0 167.33 165.14 69.77 o 5 7 0 140.49 110.63 81.27 o 6 7 0 1165.00 1161.43 101.84 o 7 7 0 7.53 -21.61 67.17 o 8 7 0 54.48 -59.43 138.22 o 9 7 0 120.23 315.31 222.87 o 10 7 0 165.70 256.03 157.43 o 11 7 0 56.07 24.50 184.88 o 12 7 0 7.27 0.67 168.47 o 13 7 0 5.52 -227.62 227.62 o 0 8 0 1317.95 1492.25 151.06 o 1 8 0 557.81 605.66 123.10 o 2 8 0 703.39 678.02 95.71 o 3 8 0 1320.88 1446.71 110.92 o 4 8 0 1404.62 1619.83 175.04 o 5 8 0 0.00 -36.75 100.30 o 6 8 0 221.32 149.64 91.80 o 7 8 0 59.73 36.39 112.03 o 8 8 0 3.89 45.02 91.36 o 9 8 0 7.28 86.67 127.35 o 10 8 0 43.74 -184.20 254.70 o 11 8 0 236.32 207.91 277.18 o 13 8 0 63.93 -370.68 370.68 o 1 9 0 41.87 250.35 326.92 o 2 9 0 3198.03 2889.60 198.75 o 3 9 0 57.62 -23.26 81.10 o 4 9 0 594.76 663.10 132.94 o 5 9 0 165.37 -16.57 99.56 o 6 9 0 209.48 308.76 144.07 o 7 9 0 23.48 41.26 113.87 o 8 9 0 50.78 46.05 163.21 o 9 9 0 48.40 138.72 139.55 o 10 9 0 3.95 68.22 277.44 o 11 9 0 2.72 231.96 370.68 o 12 9 0 7.68 -393.42 393.42 o 0 10 0 27.27 138.72 209.22 o 1 10 0 27.19 -20.64 185.34 o 2 10 0 108.65 189.39 154.42 o 3 10 0 38.39 150.03 147.13 o 4 10 0 6.86 166.56 136.37 o 5 10 0 3616.76 3805.05 332.50 o 6 10 0 97.71 466.34 243.49 o 7 10 0 48.61 23.88 196.18 o 8 10 0 218.84 280.54 185.34 o 9 10 0 1.71 193.60 253.56 o 10 10 0 73.38 368.40 345.66 o 1 11 0 35.44 -22.74 228.34 o 2 11 0 1031.39 1305.72 252.80 o 3 11 0 12.89 300.48 252.80 o 4 11 0 5.82 -210.44 210.44 o 5 11 0 655.97 666.22 233.28 o 6 11 0 2.31 -187.62 187.62 o 7 11 0 225.07 -12.55 160.61 o 8 11 0 2.03 -60.08 180.69 o 9 11 0 30.55 484.38 345.66 o 10 11 0 167.53 461.64 391.15 o 0 12 0 791.60 1364.46 416.16 o 1 12 0 204.12 416.16 194.21 o 2 12 0 710.26 525.80 285.89 o 3 12 0 133.30 321.13 243.33 o 4 12 0 2.02 98.81 222.12 o 5 12 0 8.22 -260.11 260.11 o 6 12 0 33.68 142.48 450.27 o 7 12 0 55.00 264.73 199.98 o 8 12 0 283.06 286.01 194.21 o 9 12 0 70.32 22.74 416.16 o 1 13 0 72.55 312.82 236.69 o 2 13 0 150.31 192.63 226.65 o 3 13 0 31.57 57.99 212.26 o 4 13 0 17.29 219.63 243.49 o 5 13 0 61.18 -138.57 245.22 o 6 13 0 27.88 42.31 292.95 o 7 13 0 110.51 -248.15 248.15 o 8 13 0 16.95 -138.72 368.40 o 0 14 0 4.18 -438.90 625.38 o 1 14 0 2.17 -267.34 269.79 o 2 14 0 390.87 111.21 311.55 o 3 14 0 1523.71 1598.49 404.65 o 4 14 0 0.80 619.24 426.39 o 5 14 0 307.48 150.09 294.27 o 6 14 0 41.65 -59.40 272.74 o 1 15 0 28.76 61.44 351.88 o 2 15 0 41.69 103.80 393.92 o 3 15 0 118.25 68.22 484.38 o 4 15 0 15.88 -300.18 484.38 o -15 0 1 4.44 -206.94 345.66 o -13 0 1 31.93 138.72 254.70 o -11 0 1 519.81 484.38 322.92 o -9 0 1 1082.86 1180.26 325.20 o -7 0 1 11603.61 12978.28 723.16 o -5 0 1 10.98 14.42 45.38 o -3 0 1 1732.36 1727.53 97.20 o -1 0 1 64.84 0.00 22.74 o 1 0 1 698.81 179.56 82.57 o 3 0 1 12617.00 11678.76 437.07 o 5 0 1 924.48 917.06 51.17 o 7 0 1 45.34 71.59 31.33 o 9 0 1 36.71 56.03 35.18 o 11 0 1 329.18 461.64 277.44 o 13 0 1 795.69 277.44 345.66 o 15 0 1 49.35 -115.98 345.66 o -15 1 1 473.12 295.39 249.02 o -14 1 1 74.86 111.56 226.65 o -13 1 1 195.46 -96.62 199.98 o -12 1 1 10.08 128.21 210.44 o -11 1 1 39.61 -205.55 219.86 o -10 1 1 332.53 661.51 173.97 o -9 1 1 16.32 5.38 29.87 o -8 1 1 24.56 43.06 31.09 o -7 1 1 130.43 107.54 49.89 o -6 1 1 155.94 130.92 56.79 o -5 1 1 663.88 614.37 43.53 o -4 1 1 2369.17 2417.97 97.92 o -3 1 1 3695.15 3470.37 88.82 o -2 1 1 9600.71 8372.23 211.02 o -1 1 1 145.40 84.13 56.46 o 0 1 1 86.44 11.37 11.37 o 1 1 1 1850.34 1781.73 48.18 o 2 1 1 708.79 677.55 25.33 o 3 1 1 24042.35 22988.09 501.84 o 4 1 1 136.98 177.82 24.90 o 5 1 1 1232.05 1162.25 52.55 o 6 1 1 656.84 632.82 35.16 o 7 1 1 142.69 187.33 31.19 o 8 1 1 18.25 -9.15 28.39 o 9 1 1 5.06 -12.29 32.15 o 10 1 1 445.73 445.79 52.20 o 11 1 1 802.89 790.05 68.06 o 12 1 1 81.46 31.13 160.61 o 13 1 1 249.61 77.38 183.54 o 14 1 1 113.38 304.19 265.90 o 15 1 1 1125.42 1976.71 391.37 o -15 2 1 78.34 511.90 276.30 o -14 2 1 9.08 163.83 281.37 o -13 2 1 0.09 -177.15 203.75 o -12 2 1 145.66 188.07 203.75 o -11 2 1 6.17 -12.75 116.45 o -10 2 1 40.14 145.58 60.69 o -9 2 1 179.43 151.74 56.46 o -8 2 1 129.92 136.37 31.23 o -7 2 1 830.71 807.32 64.35 o -6 2 1 3761.81 3928.23 137.55 o -5 2 1 1047.44 1025.35 35.98 o -4 2 1 3811.79 3613.29 99.05 o -3 2 1 1574.85 1507.00 42.46 o -2 2 1 4.29 -13.71 13.71 o -1 2 1 2511.80 2499.02 76.87 o 0 2 1 21321.17 20489.71 512.50 o 1 2 1 12182.36 11730.65 327.58 o 2 2 1 50.78 38.45 23.15 o 3 2 1 15821.73 15093.89 365.57 o 4 2 1 714.37 729.78 40.88 o 5 2 1 0.07 -7.13 31.02 o 6 2 1 1217.50 1379.17 72.88 o 7 2 1 226.55 245.89 26.81 o 8 2 1 484.88 479.92 37.11 o 9 2 1 68.51 69.40 47.12 o 10 2 1 1933.20 1839.58 158.87 o 11 2 1 14.06 24.40 65.85 o 12 2 1 236.90 445.26 203.75 o 13 2 1 21.20 138.72 288.81 o 14 2 1 28.77 -211.76 310.96 o 15 2 1 3.06 108.44 363.01 o -15 3 1 22.89 408.60 265.90 o -14 3 1 17.78 -4.42 252.08 o -13 3 1 1.05 417.20 255.12 o -12 3 1 28.28 31.69 105.56 o -11 3 1 0.37 -41.93 66.28 o -10 3 1 228.77 233.34 74.64 o -9 3 1 121.68 192.49 77.83 o -8 3 1 122.84 133.19 106.68 o -7 3 1 4.48 -23.20 23.20 o -6 3 1 811.10 908.34 42.04 o -5 3 1 392.81 342.63 38.28 o -4 3 1 1734.49 1647.51 61.77 o -3 3 1 1866.78 1837.85 66.15 o -2 3 1 101.25 110.36 26.26 o -1 3 1 118.83 93.92 31.29 o 0 3 1 241.30 236.15 32.26 o 1 3 1 834.56 828.82 45.00 o 2 3 1 328.82 304.94 32.97 o 3 3 1 8875.39 8609.54 186.24 o 4 3 1 133.20 78.37 39.49 o 5 3 1 1094.70 1106.63 46.67 o 6 3 1 1926.12 1970.60 64.11 o 7 3 1 28.48 35.91 30.62 o 8 3 1 94.36 145.04 28.62 o 9 3 1 558.98 528.53 70.44 o 10 3 1 198.96 200.13 82.55 o 11 3 1 4.56 -15.90 86.55 o 12 3 1 6.48 0.00 180.10 o 13 3 1 10.55 832.32 370.68 o 14 3 1 4.72 -54.17 404.79 o 15 3 1 0.17 -206.94 322.92 o -15 4 1 0.21 -120.38 299.43 o -14 4 1 17.98 -87.42 259.67 o -13 4 1 141.85 300.18 282.59 o -12 4 1 143.00 161.49 100.79 o -11 4 1 66.26 198.19 95.04 o -10 4 1 6.44 -74.56 74.56 o -9 4 1 125.15 153.71 77.41 o -8 4 1 38.23 69.84 29.73 o -7 4 1 182.93 203.91 81.64 o -6 4 1 1165.56 1239.41 61.18 o -5 4 1 2.48 -5.16 41.19 o 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585.43 570.48 57.99 o 2 5 1 1080.15 1035.13 67.87 o 3 5 1 583.19 624.18 59.29 o 4 5 1 60.46 49.77 50.68 o 5 5 1 196.71 123.04 53.46 o 6 5 1 269.55 300.15 47.92 o 7 5 1 126.27 176.52 54.54 o 8 5 1 839.14 933.33 83.37 o 9 5 1 4.08 12.13 70.65 o 10 5 1 41.94 37.21 39.94 o 11 5 1 252.96 229.89 174.25 o 12 5 1 31.32 -90.89 167.40 o 13 5 1 37.10 243.37 245.22 o 14 5 1 891.82 1088.53 283.19 o -14 6 1 0.04 -243.41 327.23 o -13 6 1 14.30 153.76 259.67 o -12 6 1 2.82 -71.39 140.16 o -11 6 1 14.91 -93.24 254.70 o -10 6 1 406.45 305.92 84.62 o -9 6 1 191.81 261.70 90.98 o -8 6 1 714.49 556.38 71.80 o -7 6 1 25.48 29.77 60.53 o -6 6 1 523.74 594.44 71.59 o -5 6 1 5434.15 5660.55 194.43 o -4 6 1 1114.72 1198.93 106.83 o -3 6 1 108.59 88.47 56.95 o -2 6 1 2085.45 2111.28 97.54 o -1 6 1 43.14 147.12 59.01 o 0 6 1 578.39 632.82 64.24 o 1 6 1 785.39 881.48 76.48 o 2 6 1 491.31 477.02 60.76 o 3 6 1 2130.96 2262.36 111.65 o 4 6 1 4.48 19.70 56.23 o 5 6 1 3202.90 2972.75 123.25 o 6 6 1 396.37 273.28 59.94 o 7 6 1 473.61 520.95 71.34 o 8 6 1 430.47 343.66 64.50 o 9 6 1 1.14 -33.95 60.16 o 10 6 1 1687.68 1657.64 184.06 o 11 6 1 1822.22 1756.09 217.40 o 12 6 1 0.00 117.14 193.43 o 13 6 1 2.15 654.61 250.06 o 14 6 1 0.08 149.93 275.85 o -14 7 1 42.34 -93.24 296.92 o -13 7 1 78.53 392.54 299.04 o -12 7 1 1.59 83.74 153.93 o -11 7 1 406.27 407.82 192.60 o -10 7 1 281.85 151.22 241.05 o -9 7 1 58.02 -95.03 95.03 o -8 7 1 19.84 51.45 73.92 o -7 7 1 127.42 62.23 77.73 o -6 7 1 223.05 180.31 74.43 o -5 7 1 25.70 -55.64 80.25 o -4 7 1 1719.40 1719.78 123.54 o -3 7 1 228.34 235.58 74.33 o -2 7 1 21206.84 21175.87 520.75 o -1 7 1 8920.11 9116.55 258.31 o 0 7 1 725.48 783.58 94.24 o 1 7 1 26928.95 28124.34 699.96 o 2 7 1 2545.61 2478.31 117.75 o 3 7 1 2404.73 2509.90 138.72 o 4 7 1 50.51 42.72 64.23 o 5 7 1 1085.91 1071.42 115.36 o 6 7 1 52.71 23.78 74.01 o 7 7 1 40.37 -1.44 69.44 o 8 7 1 62.04 -50.48 77.87 o 9 7 1 91.72 108.40 106.35 o 10 7 1 27.13 109.79 148.45 o 11 7 1 846.74 811.25 184.19 o 12 7 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