#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:24:09 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180781 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/12/2011220.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011220_Fobs loop_ _publ_author_name 'Kassem, Tarek' 'Rolland, Val\'erie' 'Martinez, Jean' 'Rolland, Marc' _publ_section_title ; Two key chiral intermediates in a new 4-hydroxyisoleucine synthesis ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1037 _journal_page_last 1039 _journal_volume 56 _journal_year 2000 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cod_data_source_file gs1091IVsup3.hkl _cod_data_source_block IV loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma 0 0 4 461.4 447.7 13.3 0 0 6 1368.7 1267.5 39.7 0 0 8 119.5 125.8 3.3 0 0 10 98.0 107.7 3.7 0 0 12 61.7 70.1 3.3 0 1 2 375.0 445.1 7.3 0 1 3 7.2 4.2 0.4 0 1 4 820.3 837.7 15.4 0 1 5 18.0 26.2 0.7 0 1 6 1768.0 1599.0 30.5 0 1 7 541.7 548.8 9.4 0 1 8 126.4 117.1 2.5 0 1 9 15.9 14.6 0.9 0 1 10 8.5 9.3 1.0 0 1 11 188.7 199.1 4.4 0 1 12 6.7 1.0 1.7 0 1 15 6.9 12.6 2.0 0 2 2 274.7 285.4 5.3 0 2 3 1300.2 1353.4 24.9 0 2 4 496.1 494.7 9.0 0 2 5 60.0 79.7 1.6 0 2 6 1048.9 1041.0 19.2 0 2 7 791.4 756.4 13.6 0 2 8 610.5 564.3 10.9 0 2 9 348.8 305.8 7.4 0 2 10 93.6 87.0 2.7 0 2 11 15.5 13.4 1.6 0 2 12 83.6 84.0 3.9 0 2 13 94.6 99.8 3.2 0 3 1 86.8 84.8 2.2 0 3 2 410.5 397.0 8.5 0 3 3 883.5 899.0 16.7 0 3 4 306.1 311.5 5.7 0 3 5 191.2 172.8 3.6 0 3 6 1380.5 1304.4 24.5 0 3 7 1451.6 1566.2 25.9 0 3 8 266.3 266.4 5.4 0 3 10 27.3 21.3 1.5 0 3 13 69.8 63.0 2.9 0 3 14 15.0 16.5 2.1 0 4 1 427.1 393.3 9.7 0 4 2 1425.7 1428.0 27.5 0 4 3 692.4 656.2 14.9 0 4 4 63.5 57.6 1.5 0 4 5 2279.5 2186.6 40.2 0 4 6 153.2 156.5 3.7 0 4 7 42.8 42.9 1.5 0 4 9 72.2 75.8 2.1 0 4 10 17.2 10.0 1.3 0 4 11 101.7 95.2 3.4 0 4 12 15.3 19.7 1.4 0 4 13 17.9 11.1 2.3 0 4 14 8.0 1.5 2.5 0 4 15 11.3 21.6 3.0 0 5 1 1.8 1.0 0.2 0 5 2 1575.0 1657.8 29.5 0 5 3 171.1 161.4 3.3 0 5 4 324.9 322.9 6.3 0 5 5 194.1 187.7 3.7 0 5 6 111.8 115.3 2.5 0 5 7 27.1 23.5 1.3 0 5 8 20.8 19.1 1.4 0 5 9 561.8 578.5 11.0 0 5 10 41.1 26.5 2.8 0 5 12 11.1 11.7 1.3 0 5 13 48.1 47.8 2.2 0 5 14 9.5 13.6 2.1 0 6 1 503.8 456.2 20.1 0 6 2 450.5 421.3 8.6 0 6 3 187.2 204.2 3.8 0 6 4 16.2 6.4 0.7 0 6 5 502.7 515.6 9.0 0 6 6 16.9 15.0 1.1 0 6 7 14.0 32.9 1.1 0 6 8 687.5 690.7 15.1 0 6 10 32.9 34.7 2.0 0 6 11 10.3 10.9 1.3 0 6 12 8.7 4.2 1.2 0 6 14 11.7 4.9 3.0 0 7 2 179.0 145.7 3.8 0 7 3 26.7 31.9 0.8 0 7 4 217.4 227.7 4.9 0 7 5 199.9 195.2 4.4 0 7 6 116.5 111.7 2.7 0 7 7 2.9 1.6 0.7 0 7 8 247.4 241.8 5.7 0 7 9 57.9 59.1 2.5 0 7 12 19.7 16.0 1.7 0 7 13 19.8 16.7 1.6 0 8 2 361.8 382.7 13.4 0 8 3 8.4 10.2 0.5 0 8 4 16.4 13.4 0.7 0 8 7 3.0 0.1 1.0 0 8 8 122.3 127.2 3.2 0 8 9 83.1 92.3 2.2 0 8 10 4.7 2.5 1.3 0 8 11 24.7 21.1 1.8 0 9 4 79.2 89.5 1.9 0 9 5 13.5 17.5 0.7 0 9 6 3.4 0.9 0.8 0 9 7 7.9 3.9 1.1 0 9 8 19.8 24.2 1.0 0 9 9 49.9 53.2 1.9 0 9 10 5.5 5.6 1.1 0 9 11 13.5 8.8 1.9 0 10 4 1.9 2.6 0.4 0 10 5 10.0 11.4 0.6 0 10 6 7.7 12.6 1.0 0 10 9 67.3 67.5 2.3 0 10 10 12.3 12.4 1.4 0 11 7 12.3 11.2 1.0 0 11 8 3.0 1.7 0.9 1 0 2 507.7 544.8 9.8 1 0 3 12.6 11.3 0.5 1 0 4 1037.6 1067.6 19.2 1 0 5 42.6 50.7 1.3 1 0 6 486.5 470.6 9.1 1 0 7 257.1 251.9 5.6 1 0 8 118.4 98.7 2.6 1 0 10 420.4 390.4 8.1 1 0 12 158.0 165.6 4.2 1 0 13 25.6 22.5 1.4 1 0 14 10.0 10.6 1.5 1 0 15 8.3 7.7 1.7 1 1 3 1439.8 1544.5 18.5 1 1 4 1443.9 1447.0 18.9 1 1 5 3792.5 3814.1 67.6 1 1 6 510.4 474.0 6.5 1 1 7 9.7 10.3 0.7 1 1 8 258.9 264.9 3.5 1 1 9 12.3 9.0 0.7 1 1 10 58.0 57.5 1.4 1 1 11 56.9 63.0 1.4 1 1 12 415.6 433.7 6.2 1 1 13 36.9 38.2 1.5 1 1 14 8.7 8.4 1.1 1 1 15 19.6 24.4 1.6 1 2 0 318.1 343.2 9.6 1 2 2 677.2 662.6 11.1 1 2 3 82.6 101.6 1.4 1 2 4 22.8 25.3 0.6 1 2 5 795.7 751.2 10.2 1 2 6 38.8 33.8 0.9 1 2 7 424.5 422.8 5.7 1 2 8 90.0 79.4 1.6 1 2 9 103.3 95.7 1.9 1 2 10 430.9 426.8 6.0 1 2 11 62.6 54.8 1.9 1 2 12 58.2 56.8 2.5 1 2 13 9.5 8.3 1.2 1 2 14 30.1 26.8 1.4 1 3 0 46.7 45.8 1.1 1 3 1 47.2 42.4 0.8 1 3 2 461.8 482.5 6.3 1 3 3 3297.0 3451.2 116.7 1 3 4 1235.6 1224.2 16.7 1 3 5 1034.4 1004.3 14.3 1 3 6 61.0 48.2 1.2 1 3 7 1.8 3.1 0.4 1 3 8 84.6 99.2 1.4 1 3 9 91.5 90.1 1.7 1 3 10 577.0 565.7 8.1 1 3 11 68.5 74.4 1.7 1 3 12 39.5 45.5 1.4 1 3 13 28.6 22.9 1.5 1 3 14 23.0 21.6 1.5 1 3 15 5.8 7.2 1.8 1 4 0 6.3 4.8 0.9 1 4 1 1569.9 1655.4 30.5 1 4 2 1243.7 1276.7 17.4 1 4 3 517.4 505.1 7.0 1 4 4 424.7 422.8 5.5 1 4 5 26.1 26.2 0.7 1 4 6 53.3 50.2 1.3 1 4 7 26.5 22.8 0.7 1 4 8 225.7 222.6 3.4 1 4 9 412.1 406.1 5.8 1 4 10 784.8 804.3 11.1 1 4 11 36.5 36.8 1.2 1 4 12 39.2 39.5 1.4 1 4 13 18.7 13.8 2.1 1 4 14 22.3 21.1 1.7 1 4 15 8.9 13.0 1.7 1 5 0 361.5 301.3 10.0 1 5 1 1308.0 1324.4 26.6 1 5 2 51.7 63.3 0.9 1 5 3 1199.4 1234.0 16.3 1 5 4 1168.9 1149.3 16.0 1 5 5 255.1 249.5 3.6 1 5 6 2.2 2.6 0.5 1 5 7 172.0 186.8 2.9 1 5 8 260.5 249.1 4.0 1 5 9 75.0 69.9 2.1 1 5 10 292.8 302.4 4.5 1 5 11 43.7 44.2 1.3 1 5 12 24.7 23.0 1.2 1 5 14 15.5 15.2 1.4 1 6 0 79.7 82.0 2.6 1 6 1 781.6 770.0 17.6 1 6 2 249.5 242.7 3.7 1 6 3 146.9 138.6 2.6 1 6 4 777.2 771.5 9.9 1 6 5 31.2 31.6 1.0 1 6 6 27.2 22.5 0.8 1 6 7 73.0 67.4 1.4 1 6 8 16.3 13.7 0.9 1 6 9 32.5 29.4 1.1 1 6 10 198.1 192.5 3.2 1 6 11 10.5 11.9 0.8 1 6 12 3.8 3.9 1.2 1 6 13 3.7 5.1 1.0 1 6 14 7.9 8.7 1.6 1 7 0 33.5 21.3 1.2 1 7 1 400.0 380.8 8.3 1 7 2 13.6 8.8 0.4 1 7 3 97.1 109.6 1.7 1 7 4 632.4 610.2 9.2 1 7 5 1.7 5.7 0.3 1 7 6 50.5 54.0 1.1 1 7 7 35.9 41.2 0.9 1 7 8 2.4 1.4 0.6 1 7 9 43.2 38.1 1.4 1 7 10 32.4 27.0 1.1 1 7 11 3.4 1.2 0.7 1 7 12 34.0 41.7 1.7 1 7 13 12.5 10.6 1.8 1 8 1 10.2 10.4 0.4 1 8 2 132.9 134.3 3.0 1 8 3 341.1 326.8 6.1 1 8 4 28.9 28.9 0.7 1 8 5 132.7 133.2 2.2 1 8 6 20.3 23.7 0.6 1 8 7 110.4 111.6 2.0 1 8 8 20.0 24.6 0.9 1 8 9 23.6 28.1 1.1 1 8 10 36.6 37.0 1.3 1 8 11 7.2 5.5 1.0 1 8 12 26.1 28.8 1.2 1 9 2 134.9 143.6 4.4 1 9 3 383.6 403.8 7.4 1 9 4 23.8 29.1 0.5 1 9 5 57.0 56.4 1.2 1 9 6 37.9 38.8 0.9 1 9 7 48.7 51.2 1.3 1 9 8 43.4 46.1 1.1 1 9 9 33.7 33.1 1.2 1 9 10 4.5 6.1 0.7 1 9 11 8.9 9.7 1.0 1 10 3 56.2 54.5 3.8 1 10 4 12.8 11.1 0.4 1 10 5 30.6 34.4 0.7 1 10 6 11.4 10.6 0.6 1 10 7 14.9 16.3 0.8 1 10 8 43.5 43.9 1.3 1 10 9 18.5 21.5 1.0 1 10 10 16.5 12.9 1.1 1 11 4 27.7 32.1 1.3 1 11 5 11.8 13.8 0.5 1 11 6 9.2 7.6 0.5 1 11 7 6.7 8.2 0.5 1 11 8 24.0 23.9 1.2 1 11 9 13.2 8.5 2.1 2 0 1 477.3 516.2 9.5 2 0 2 1554.8 1610.2 30.5 2 0 4 43.7 38.2 1.1 2 0 5 9.2 10.9 1.0 2 0 6 496.8 461.0 9.6 2 0 7 344.3 388.2 6.6 2 0 8 32.3 25.3 1.3 2 0 9 57.3 51.8 1.8 2 0 10 6.3 6.2 0.8 2 0 11 67.4 79.7 2.2 2 0 12 239.9 239.4 6.7 2 0 13 8.0 11.5 1.3 2 0 14 27.4 25.5 2.0 2 1 1 268.3 277.6 3.5 2 1 2 1038.2 1098.0 14.3 2 1 3 2271.9 2400.1 32.2 2 1 4 648.0 691.4 8.7 2 1 5 2298.3 2283.9 30.3 2 1 6 1125.3 1108.2 14.1 2 1 7 190.0 186.6 2.8 2 1 8 29.0 26.2 0.9 2 1 9 102.8 100.7 1.8 2 1 10 208.7 195.0 3.3 2 1 11 26.2 25.8 1.0 2 1 12 30.1 36.7 1.2 2 1 13 61.2 68.5 1.8 2 1 14 6.2 6.6 1.2 2 1 15 11.2 9.4 1.5 2 2 0 245.1 252.5 5.6 2 2 1 1370.3 1352.8 19.5 2 2 3 68.5 73.9 1.1 2 2 4 1486.7 1538.9 19.6 2 2 5 43.2 68.7 1.0 2 2 6 530.5 531.4 7.0 2 2 7 154.7 160.7 2.5 2 2 8 70.2 66.3 1.6 2 2 9 3.5 5.9 0.6 2 2 10 68.8 62.3 1.5 2 2 11 23.0 24.3 1.2 2 2 12 61.9 61.8 1.9 2 2 13 4.0 1.9 0.8 2 2 14 6.8 5.4 1.3 2 3 0 138.5 156.5 2.8 2 3 1 189.3 185.1 2.7 2 3 2 273.7 265.4 3.9 2 3 3 60.6 77.2 1.3 2 3 4 980.7 987.7 13.0 2 3 5 1080.7 1054.1 14.0 2 3 6 422.2 388.9 5.6 2 3 7 384.2 395.2 5.6 2 3 9 116.2 112.6 2.2 2 3 10 545.2 531.4 7.6 2 3 11 127.3 134.9 2.6 2 3 12 16.3 19.8 1.2 2 3 13 13.6 11.2 1.2 2 3 14 6.1 2.0 1.3 2 3 15 8.3 4.7 1.5 2 4 0 1272.9 1214.0 25.3 2 4 1 311.7 345.1 4.6 2 4 2 851.9 802.0 12.1 2 4 3 1028.3 1141.2 15.0 2 4 4 1135.2 1100.6 15.0 2 4 5 44.1 40.3 0.9 2 4 6 164.4 150.1 2.7 2 4 7 107.8 93.1 1.8 2 4 8 174.6 188.4 2.5 2 4 9 166.9 169.2 2.7 2 4 10 3.1 2.1 0.9 2 4 11 10.0 9.6 1.0 2 4 12 31.4 30.0 1.6 2 4 13 48.5 46.0 2.1 2 4 14 6.8 7.9 1.3 2 4 15 29.2 33.9 2.1 2 5 0 338.7 345.5 7.3 2 5 1 64.0 62.3 1.0 2 5 2 775.4 716.1 11.3 2 5 3 96.6 87.8 1.6 2 5 4 477.2 457.9 6.4 2 5 5 454.8 392.2 6.3 2 5 7 104.9 104.8 2.0 2 5 8 275.3 251.7 4.2 2 5 9 92.6 96.1 1.9 2 5 10 19.3 21.3 0.9 2 5 11 19.6 20.8 0.9 2 5 12 8.5 8.1 0.8 2 5 13 60.0 57.6 2.3 2 5 14 12.6 7.6 1.7 2 6 0 1312.7 1337.8 40.8 2 6 1 150.7 159.0 2.6 2 6 2 516.7 534.6 7.7 2 6 3 739.9 698.9 10.1 2 6 4 25.7 34.9 0.7 2 6 5 112.3 110.8 2.1 2 6 6 139.5 132.3 2.3 2 6 7 19.9 21.4 0.7 2 6 8 435.1 454.3 7.1 2 6 9 309.6 309.8 4.6 2 6 10 21.3 20.4 1.2 2 6 11 52.7 59.3 1.5 2 6 12 3.4 2.8 0.8 2 6 13 29.7 23.4 1.3 2 6 14 12.1 9.4 1.6 2 7 0 2.9 0.5 0.6 2 7 1 98.2 114.1 2.2 2 7 2 104.8 99.8 2.2 2 7 3 4.2 2.2 0.4 2 7 4 162.8 155.6 2.7 2 7 5 178.9 178.1 2.8 2 7 6 104.2 99.6 1.8 2 7 7 133.2 134.7 2.2 2 7 8 197.4 189.1 3.2 2 7 9 18.7 18.5 1.2 2 7 10 54.2 53.8 2.0 2 7 11 11.1 11.3 1.1 2 7 12 8.5 6.7 1.0 2 7 13 11.2 5.9 1.9 2 8 0 17.8 17.6 1.1 2 8 1 128.8 165.3 3.9 2 8 2 109.2 109.7 2.4 2 8 3 180.1 175.5 2.8 2 8 4 1.7 2.0 0.4 2 8 5 46.5 44.1 1.2 2 8 6 9.2 11.1 0.5 2 8 7 56.5 51.0 1.4 2 8 8 177.6 184.7 3.0 2 8 9 24.1 23.1 0.8 2 8 10 23.5 28.0 1.1 2 8 11 6.9 3.0 1.5 2 8 12 8.4 6.4 1.1 2 9 0 6.3 2.9 0.7 2 9 1 6.4 6.4 0.6 2 9 2 483.9 442.3 10.4 2 9 3 29.3 32.4 1.0 2 9 4 43.7 46.3 0.9 2 9 5 112.7 114.9 2.1 2 9 6 31.1 33.3 0.9 2 9 7 38.3 36.6 1.0 2 9 8 8.6 7.0 0.7 2 9 9 70.7 64.9 1.6 2 9 10 11.1 10.1 1.0 2 10 0 90.0 91.8 3.0 2 10 1 77.2 72.8 2.3 2 10 2 4.8 5.8 0.5 2 10 3 60.7 70.1 1.5 2 10 4 97.6 92.3 2.3 2 10 5 47.6 53.9 1.0 2 10 6 16.3 20.2 0.7 2 10 7 25.3 20.9 0.9 2 10 8 15.7 13.3 0.9 2 10 9 9.2 7.1 1.1 2 10 10 14.9 18.0 1.5 2 11 3 6.5 8.2 0.6 2 11 4 30.9 27.9 1.2 2 11 5 53.4 40.7 1.5 2 11 7 8.0 7.6 0.6 2 11 8 10.7 11.9 0.9 2 11 9 9.0 8.0 1.5 2 12 5 4.1 3.4 0.4 3 0 1 31.2 25.6 0.8 3 0 2 188.0 170.6 3.9 3 0 3 611.1 624.1 11.6 3 0 4 494.8 436.1 10.9 3 0 5 3309.4 3251.9 60.0 3 0 6 494.7 517.1 9.5 3 0 7 86.3 84.4 2.3 3 0 8 46.4 32.3 1.7 3 0 9 83.8 91.9 3.3 3 0 10 17.7 14.0 1.2 3 0 11 115.4 118.5 3.5 3 0 12 99.7 102.7 2.8 3 0 13 12.1 15.1 1.5 3 0 14 9.6 5.6 1.9 3 0 15 24.0 28.4 2.0 3 1 0 936.9 876.2 37.7 3 1 1 1914.0 2029.8 26.5 3 1 2 2309.9 2444.8 38.4 3 1 3 1.9 0.9 0.3 3 1 4 663.2 665.8 9.1 3 1 5 837.9 792.4 10.9 3 1 6 682.5 704.3 8.4 3 1 7 114.7 111.8 1.8 3 1 8 184.1 192.5 2.9 3 1 9 537.2 543.8 7.1 3 1 10 131.9 138.5 2.5 3 1 11 28.6 33.7 1.2 3 1 12 16.9 14.5 1.2 3 1 14 11.2 9.6 1.3 3 1 15 9.6 4.0 1.3 3 2 1 2396.9 2443.1 32.3 3 2 2 4456.3 4660.8 176.4 3 2 3 304.8 298.8 4.4 3 2 4 1059.6 996.2 15.4 3 2 5 19.4 18.4 0.6 3 2 6 601.8 573.8 8.3 3 2 7 211.3 187.1 2.9 3 2 8 196.8 203.2 3.2 3 2 9 143.5 137.0 2.4 3 2 10 46.0 49.7 1.2 3 2 11 71.0 67.9 1.6 3 2 12 126.3 127.5 2.6 3 2 13 20.3 23.2 1.2 3 2 14 5.0 0.9 1.2 3 2 15 3.7 3.4 1.2 3 3 0 2404.7 2389.8 46.4 3 3 1 986.0 976.0 15.2 3 3 2 203.4 174.9 3.1 3 3 3 1371.0 1406.7 18.8 3 3 4 346.7 299.0 5.2 3 3 5 248.6 257.8 3.6 3 3 6 52.8 34.1 1.1 3 3 7 26.1 27.1 0.9 3 3 8 257.9 238.9 3.6 3 3 9 135.6 124.9 2.6 3 3 10 65.9 71.0 1.4 3 3 11 44.3 50.7 1.5 3 3 13 30.2 28.7 1.7 3 3 14 20.7 19.4 1.3 3 3 15 7.6 5.1 1.7 3 4 0 112.1 112.2 2.4 3 4 1 228.1 206.3 3.3 3 4 2 1081.8 1050.9 15.6 3 4 3 834.9 741.3 11.0 3 4 4 369.5 346.6 5.3 3 4 5 105.1 118.1 1.7 3 4 6 256.4 262.4 3.8 3 4 7 95.1 99.8 1.8 3 4 8 392.0 396.3 5.5 3 4 9 104.3 93.1 2.0 3 4 10 119.7 115.0 2.6 3 4 11 8.5 9.2 0.7 3 4 12 17.5 21.5 1.2 3 4 13 18.8 20.6 1.5 3 5 0 483.2 481.5 9.8 3 5 1 782.7 810.8 10.8 3 5 2 284.3 261.7 4.0 3 5 3 350.9 348.1 4.7 3 5 4 681.5 615.7 9.8 3 5 5 171.8 143.4 2.7 3 5 6 353.6 357.6 5.2 3 5 7 195.5 199.6 3.3 3 5 8 202.2 191.0 3.3 3 5 9 76.4 81.8 1.6 3 5 10 181.9 185.4 3.3 3 5 11 22.4 22.4 1.0 3 5 12 26.2 27.6 1.2 3 5 13 66.6 64.0 2.4 3 5 14 17.1 16.4 1.4 3 6 0 297.8 285.0 8.1 3 6 1 113.8 103.7 1.8 3 6 2 8.7 14.4 0.4 3 6 3 92.1 90.1 1.6 3 6 4 185.3 188.1 2.9 3 6 5 59.8 67.3 1.3 3 6 6 164.6 178.8 2.7 3 6 7 20.2 23.6 0.7 3 6 8 159.8 176.8 2.7 3 6 9 4.4 4.9 0.7 3 6 10 3.3 0.1 0.9 3 6 11 4.5 2.8 1.2 3 6 12 10.9 12.6 1.1 3 6 13 29.6 24.2 1.5 3 7 0 15.0 7.6 0.6 3 7 1 158.0 145.3 2.5 3 7 2 325.5 303.4 4.9 3 7 3 152.3 180.4 2.3 3 7 4 41.2 38.5 1.0 3 7 5 282.2 282.3 4.5 3 7 6 32.8 29.3 0.8 3 7 7 106.0 123.6 2.0 3 7 8 52.1 58.6 1.5 3 7 9 111.0 111.8 2.3 3 7 10 50.8 46.5 1.8 3 7 12 6.1 6.8 1.3 3 7 13 31.9 22.6 2.0 3 8 0 33.1 35.7 1.2 3 8 1 161.9 145.3 3.7 3 8 2 66.8 70.2 1.4 3 8 3 184.5 193.7 3.0 3 8 4 30.5 31.7 0.8 3 8 5 25.9 26.5 0.7 3 8 6 27.4 33.2 0.9 3 8 7 230.1 237.1 4.4 3 8 8 2.3 0.8 0.6 3 8 9 53.1 52.7 1.6 3 8 10 18.5 18.5 1.1 3 8 11 5.4 4.0 1.4 3 8 12 4.3 1.9 0.9 3 9 0 63.7 66.3 2.8 3 9 1 121.2 126.8 2.9 3 9 2 156.4 170.8 3.6 3 9 3 75.1 83.6 1.6 3 9 4 12.0 9.8 0.5 3 9 5 166.2 176.4 3.0 3 9 6 30.1 29.7 0.8 3 9 7 4.8 8.9 0.6 3 9 8 18.2 21.1 0.8 3 9 9 4.9 1.5 0.8 3 9 10 11.4 7.3 1.1 3 9 11 25.3 24.6 1.3 3 10 0 10.7 6.6 0.9 3 10 1 107.2 98.7 3.3 3 10 2 31.8 31.9 1.0 3 10 3 19.0 16.3 0.8 3 10 4 21.2 16.2 0.7 3 10 5 8.3 9.8 0.6 3 10 6 56.4 59.3 1.5 3 10 7 4.7 8.4 0.6 3 10 8 13.0 12.3 0.9 3 10 9 30.7 34.5 1.4 3 10 10 25.9 26.4 1.2 3 11 2 10.9 8.4 0.8 3 11 3 18.6 21.0 0.8 3 11 4 41.9 45.0 1.5 3 11 5 72.9 76.0 2.5 3 11 6 43.4 36.9 1.9 3 11 7 46.3 49.9 1.6 3 11 8 13.8 10.4 1.1 3 12 3 20.2 15.7 1.1 3 12 4 11.8 13.7 0.7 3 12 6 11.6 14.5 3.1 4 0 0 416.5 445.8 11.1 4 0 1 27.8 26.5 0.9 4 0 2 1.9 2.6 0.5 4 0 3 103.6 87.0 2.7 4 0 4 106.6 111.0 2.5 4 0 5 3.4 0.6 1.1 4 0 6 83.4 66.7 2.5 4 0 7 270.3 268.2 5.9 4 0 8 2.3 2.6 0.7 4 0 9 26.0 21.7 1.2 4 0 11 3.8 0.9 1.2 4 0 12 6.2 0.3 1.8 4 0 13 6.6 5.8 1.6 4 0 14 27.1 27.6 2.2 4 1 0 624.9 668.4 12.5 4 1 1 1604.4 1583.0 22.5 4 1 2 909.2 971.2 13.0 4 1 3 496.2 476.5 7.1 4 1 4 58.1 58.0 1.1 4 1 5 34.0 37.3 0.8 4 1 6 44.2 29.6 1.1 4 1 7 254.2 215.7 4.1 4 1 8 14.1 12.0 0.9 4 1 9 54.4 62.7 1.5 4 1 10 410.4 414.8 6.1 4 1 11 43.1 49.4 1.3 4 1 12 21.1 25.9 1.1 4 1 13 49.6 55.5 1.6 4 1 14 4.2 1.0 1.0 4 2 0 74.6 56.3 1.7 4 2 1 233.5 217.4 3.3 4 2 2 901.4 908.3 12.8 4 2 3 263.3 285.5 4.1 4 2 4 385.9 371.4 5.8 4 2 5 108.2 107.3 1.9 4 2 6 310.5 318.9 5.0 4 2 7 24.6 25.8 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1 31.5 27.6 0.9 8 3 2 44.6 40.9 1.1 8 3 3 326.2 316.4 5.2 8 3 4 97.3 90.7 1.9 8 3 5 63.9 63.7 1.5 8 3 6 10.7 10.9 1.0 8 3 7 53.5 53.3 1.8 8 3 8 134.8 145.3 2.8 8 3 9 18.8 22.6 1.3 8 3 10 29.1 28.6 1.5 8 3 11 30.0 29.1 1.6 8 3 12 5.6 4.0 1.3 8 4 0 145.8 149.4 3.5 8 4 1 87.8 88.7 1.9 8 4 2 157.2 172.3 2.8 8 4 3 98.1 102.7 2.1 8 4 4 110.0 105.5 2.6 8 4 5 73.9 79.4 1.6 8 4 6 209.9 201.1 3.4 8 4 7 19.6 21.6 0.9 8 4 8 81.5 77.0 1.9 8 4 9 4.3 4.6 1.0 8 4 11 17.5 15.0 1.4 8 4 12 15.2 17.5 1.9 8 5 0 2.7 0.2 0.7 8 5 1 125.8 117.0 2.2 8 5 2 36.5 39.4 1.1 8 5 3 405.9 395.8 6.7 8 5 4 57.8 68.9 1.4 8 5 5 71.3 66.8 1.8 8 5 6 14.6 11.1 0.9 8 5 7 10.0 11.1 0.8 8 5 8 31.3 40.4 1.9 8 5 9 102.6 106.3 2.4 8 5 11 21.5 25.3 1.5 8 6 0 102.0 106.8 3.8 8 6 1 51.2 52.1 1.9 8 6 2 378.7 366.8 6.5 8 6 3 112.6 113.1 2.5 8 6 4 264.7 263.0 4.7 8 6 5 28.7 20.4 1.1 8 6 6 30.7 30.9 1.6 8 6 7 21.2 21.0 1.1 8 6 8 56.7 52.8 1.7 8 6 9 39.9 38.1 1.5 8 6 10 6.5 6.7 1.3 8 7 0 31.2 26.1 1.3 8 7 1 93.8 86.9 2.0 8 7 2 17.2 17.8 0.9 8 7 3 81.7 87.9 1.8 8 7 4 71.7 78.0 1.9 8 7 5 36.4 36.3 1.4 8 7 6 5.0 2.8 1.1 8 7 7 3.9 5.5 0.9 8 7 8 41.2 35.3 1.4 8 7 9 19.6 20.8 1.2 8 7 10 11.1 6.1 1.2 8 8 0 5.9 3.8 0.9 8 8 1 71.3 67.6 1.7 8 8 2 29.0 32.7 1.1 8 8 3 9.6 9.8 0.7 8 8 4 43.0 46.5 1.3 8 8 5 4.4 3.9 0.7 8 8 6 2.6 1.6 0.8 8 8 7 19.1 22.9 1.1 8 8 8 3.9 2.8 1.0 8 8 9 4.7 5.3 0.9 8 9 0 6.5 6.5 0.9 8 9 1 2.4 1.1 0.6 8 9 2 12.5 11.3 0.7 8 9 3 2.2 2.6 0.5 8 9 4 17.0 16.9 1.0 8 9 5 17.3 13.8 1.2 8 10 0 238.2 234.2 7.3 8 10 1 48.2 41.6 2.3 8 10 2 3.5 0.9 1.0 8 10 4 5.2 4.0 1.0 8 11 0 33.3 33.0 2.9 8 11 2 7.9 6.3 1.7 9 0 1 3.0 4.2 1.0 9 0 2 128.9 133.5 2.9 9 0 3 159.1 145.4 4.1 9 0 4 9.3 10.7 1.2 9 0 5 47.1 57.7 2.1 9 0 6 411.6 409.0 9.2 9 0 7 14.2 13.5 1.7 9 0 8 43.6 60.3 2.7 9 0 10 7.0 7.4 1.5 9 0 11 21.1 15.8 1.9 9 1 0 6.3 4.3 1.1 9 1 1 594.4 578.3 8.8 9 1 2 56.4 63.9 1.6 9 1 3 223.8 234.4 3.7 9 1 4 34.8 37.2 1.3 9 1 5 17.6 13.4 1.2 9 1 6 10.9 8.9 1.4 9 1 7 160.9 146.4 3.4 9 1 8 58.7 63.4 1.7 9 1 9 53.5 56.4 1.8 9 1 10 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1.5 9 6 9 15.7 12.9 1.4 9 7 0 26.8 24.1 1.2 9 7 1 10.6 7.6 1.0 9 7 2 33.7 39.7 1.3 9 7 3 8.3 9.2 1.7 9 7 4 37.8 40.4 1.4 9 7 5 39.1 42.0 1.3 9 7 7 27.5 25.0 1.2 9 7 8 20.9 18.7 1.4 9 8 0 26.4 17.3 1.4 9 8 1 10.2 8.3 0.8 9 8 2 5.5 4.8 0.9 9 8 3 25.9 25.6 1.2 9 8 4 10.3 8.6 1.0 9 8 5 25.5 24.7 1.6 9 8 7 15.8 14.3 1.1 9 9 1 33.2 25.8 1.4 9 9 2 8.0 4.6 0.9 9 9 3 2.7 1.5 0.7 9 9 5 4.8 4.9 0.9 9 9 6 47.4 48.6 1.8 9 10 0 51.8 45.8 2.4 9 10 1 31.0 31.0 1.7 9 10 2 15.6 13.3 2.0 9 10 3 23.9 24.9 1.4 10 0 0 103.9 114.7 4.5 10 0 1 74.3 84.5 2.2 10 0 2 69.8 74.1 1.9 10 0 3 21.7 22.6 1.3 10 0 4 231.2 243.9 6.0 10 0 6 8.2 9.6 1.3 10 0 7 101.8 106.5 3.7 10 0 8 56.9 73.3 2.4 10 0 9 118.3 111.3 3.8 10 1 0 360.8 373.7 9.2 10 1 1 301.1 299.1 4.8 10 1 2 96.9 108.2 2.1 10 1 3 33.9 37.7 1.3 10 1 4 25.1 33.9 1.7 10 1 5 27.7 27.5 1.5 10 1 6 17.8 19.1 1.0 10 1 7 3.1 2.7 0.9 10 1 8 88.6 88.3 2.3 10 1 10 10.1 9.6 1.6 10 2 0 40.0 44.5 2.0 10 2 1 210.4 204.7 4.5 10 2 2 45.8 46.0 1.7 10 2 3 66.9 69.7 1.8 10 2 4 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11 4 4 35.6 34.7 1.6 11 4 5 19.8 23.3 1.2 11 4 6 18.4 22.3 1.4 11 4 7 10.0 8.6 1.5 11 4 8 6.5 0.7 1.7 11 5 0 54.3 66.4 3.0 11 5 1 5.6 4.0 1.1 11 5 2 43.2 48.7 1.6 11 5 3 3.5 4.4 0.9 11 5 4 6.6 7.9 1.7 11 5 5 70.8 66.6 2.2 11 5 6 65.0 68.7 2.1 11 5 7 13.1 10.0 1.7 11 6 1 8.5 5.8 1.3 11 6 2 9.0 15.0 0.9 11 6 3 50.4 44.4 2.0 11 6 4 7.8 12.5 1.2 11 6 5 17.9 18.5 1.3 11 7 0 23.0 20.9 1.5 11 7 1 5.3 4.8 1.0 11 7 2 23.6 21.9 1.4 11 7 3 13.9 13.4 1.4 11 7 4 5.6 4.0 1.1 11 7 5 3.2 4.7 1.0 11 8 0 26.3 29.1 2.3 11 8 1 29.0 23.6 1.5 12 0 0 17.3 12.0 3.0 12 0 1 46.3 48.9 2.3 12 0 2 15.1 20.8 1.7 12 0 3 133.7 133.9 4.1 12 0 4 17.8 15.6 1.6 12 0 5 28.3 26.4 2.5 12 0 6 4.7 3.8 1.5 12 0 7 10.1 11.6 2.5 12 1 0 38.5 41.0 2.1 12 1 1 38.2 38.6 1.4 12 1 2 16.5 12.9 1.7 12 1 4 7.5 8.3 1.1 12 1 7 22.2 23.1 2.1 12 2 0 38.6 39.1 2.1 12 2 1 33.7 43.2 1.5 12 2 2 27.1 29.4 1.2 12 2 3 14.7 12.8 1.4 12 2 4 30.8 36.8 1.6 12 2 5 28.9 31.5 1.4 12 2 6 14.2 11.8 1.3 12 2 7 5.6 10.2 1.3 12 3 0 35.9 37.8 2.5 12 3 1 187.6 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