#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2011256.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011256_Fobs loop_ _publ_author_name 'Low, John Nicolson' 'Ferguson, George' 'Wardell, James L.' _publ_section_title ; Methyltriphenylstibonium tetrafluoroborate ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first e317 _journal_volume 56 _journal_year 2000 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 98.817 _cell_angle_beta 93.967 _cell_angle_gamma 117.796 _cell_length_a 12.8740 _cell_length_b 13.7600 _cell_length_c 24.9740 _exptl_crystal_F_000 1792.00 _reflns_d_resolution_high 0.8263 _[local]_cod_data_source_file qa0338Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ; ; _shelx_refln_list_code 4 _shelx_f_calc_maximum 412.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 12680.40 13930.46 114.85 o 3 0 0 1005.00 1649.68 47.33 o 4 0 0 181.52 161.23 36.83 o 5 0 0 9686.50 9566.47 104.21 o 6 0 0 4683.68 4355.81 85.53 o 7 0 0 558.90 408.40 55.11 o 8 0 0 816.83 617.09 69.84 o 9 0 0 1586.30 1306.89 88.39 o 10 0 0 959.68 917.73 86.07 o 11 0 0 6.08 74.07 140.50 o 12 0 0 60.05 12.69 156.05 o 13 0 0 225.10 20.73 171.19 o -14 1 0 0.80 15.14 179.92 o -13 1 0 484.10 539.89 94.12 o -12 1 0 139.20 12.14 142.00 o -11 1 0 3.19 10.78 136.00 o -10 1 0 2091.15 2149.87 99.03 o -9 1 0 323.93 318.23 66.57 o -8 1 0 8448.57 7951.85 129.86 o -7 1 0 1653.73 1850.47 68.07 o -6 1 0 7787.13 7550.27 100.53 o -5 1 0 18775.95 19841.56 208.56 o -4 1 0 36320.59 35278.62 295.59 o -3 1 0 1.28 54.56 63.56 o -2 1 0 14750.38 15710.96 138.86 o 1 1 0 1185.86 1976.37 32.74 o 2 1 0 3617.73 2262.41 70.66 o 3 1 0 3572.50 3465.36 60.43 o 4 1 0 4715.59 4394.96 72.16 o 5 1 0 1095.21 988.80 54.83 o 6 1 0 6435.13 6587.94 107.35 o 7 1 0 4086.64 4213.13 100.53 o 8 1 0 4578.21 4672.00 117.04 o 9 1 0 2990.11 3200.05 114.17 o 10 1 0 1755.46 1587.89 102.71 o 11 1 0 119.19 104.76 155.64 o 12 1 0 534.55 655.42 94.53 o 13 1 0 60.35 32.87 180.74 o -14 2 0 15.54 14.46 155.77 o -13 2 0 476.53 487.78 89.35 o -12 2 0 46.90 11.59 138.18 o -11 2 0 266.11 146.50 131.08 o -10 2 0 759.54 995.34 79.66 o -9 2 0 285.59 376.75 62.06 o -8 2 0 1101.17 1303.89 66.97 o -7 2 0 17900.47 18558.54 190.56 o -6 2 0 9139.42 9262.83 105.17 o -5 2 0 293.76 402.94 37.24 o -4 2 0 9076.27 10404.81 104.21 o -3 2 0 19134.35 17362.68 148.82 o -2 2 0 9944.00 8876.26 93.57 o -1 2 0 11658.31 12523.59 122.76 o 0 2 0 10864.77 8061.52 78.16 o 1 2 0 20238.12 22104.79 198.33 o 2 2 0 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106.67 o 9 3 0 1509.89 1588.30 103.12 o 10 3 0 953.82 928.78 100.94 o 11 3 0 441.21 466.09 97.80 o 12 3 0 115.87 155.23 178.83 o -15 4 0 2.71 15.14 156.05 o -14 4 0 114.00 49.65 157.41 o -13 4 0 82.67 12.14 140.36 o -12 4 0 163.32 146.77 72.43 o -11 4 0 2176.70 2350.25 98.76 o -10 4 0 242.11 345.10 65.61 o -9 4 0 330.77 418.76 59.61 o -8 4 0 2844.06 2476.97 75.98 o -7 4 0 895.97 1200.36 56.47 o -6 4 0 2629.24 2925.06 66.16 o -5 4 0 27071.65 27292.39 242.12 o -4 4 0 7953.94 7310.20 80.89 o -3 4 0 3132.61 2844.99 54.70 o -2 4 0 1504.54 1743.12 46.51 o -1 4 0 22063.75 21936.33 185.78 o 0 4 0 4973.64 5129.77 70.79 o 1 4 0 19092.55 19864.21 202.42 o 2 4 0 2013.47 2325.02 61.11 o 3 4 0 10505.68 10687.31 120.72 o 4 4 0 19327.73 19022.86 190.01 o 5 4 0 445.90 569.76 64.52 o 6 4 0 2081.61 1962.32 93.03 o 7 4 0 30.80 26.05 135.04 o 8 4 0 39.73 133.13 152.64 o 9 4 0 322.55 84.98 173.64 o 10 4 0 108.24 40.92 88.66 o 11 4 0 148.35 117.04 106.94 o -15 5 0 89.88 75.43 175.55 o -14 5 0 163.34 184.69 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o 2 7 0 425.00 641.24 65.61 o 3 7 0 4.81 136.40 65.47 o 4 7 0 2703.74 2303.47 103.12 o 5 7 0 42.55 9.96 136.68 o 6 7 0 37.35 11.05 148.82 o 7 7 0 80.67 140.91 159.46 o 8 7 0 37.68 92.21 89.35 o 9 7 0 285.72 458.18 108.99 o -15 8 0 646.52 696.89 103.39 o -14 8 0 119.94 133.95 141.32 o -13 8 0 0.26 26.19 135.72 o -12 8 0 279.46 491.19 71.89 o -11 8 0 531.13 546.57 68.07 o -10 8 0 274.08 398.85 58.79 o -9 8 0 1216.25 1263.65 75.43 o -8 8 0 1.32 42.97 95.35 o -7 8 0 830.61 768.09 58.65 o -6 8 0 24.29 18.69 81.30 o -5 8 0 3549.62 3249.84 80.89 o -4 8 0 7794.50 7148.56 109.94 o -3 8 0 31.86 6.14 85.80 o -2 8 0 1002.37 812.70 57.02 o -1 8 0 11258.15 10656.34 134.90 o 0 8 0 258.70 207.74 56.61 o 1 8 0 3071.70 3277.94 100.12 o 2 8 0 1.29 116.35 131.63 o 3 8 0 8.44 9.14 133.40 o 4 8 0 1174.32 1244.42 90.30 o 5 8 0 131.99 11.19 149.36 o 6 8 0 1184.34 995.89 102.30 o 7 8 0 432.96 401.30 96.57 o 8 8 0 209.76 253.03 108.31 o -15 9 0 132.39 14.46 157.96 o -14 9 0 377.13 544.94 84.03 o -13 9 0 20.43 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