#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2011274.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011274_Fobs loop_ _publ_author_name 'Zeng, Xi-Rui' 'Xu, Yan' 'Xiong, Ren-Geng' 'Zhang, Li-Juan' 'You, Xiao-Zeng' _publ_section_title ; catena-Poly[[diaqua(isonicotinato-O,O')europium(III)]-di-\m-isonicotinato-O:O'] ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first e325 _journal_page_last e326 _journal_volume 56 _journal_year 2000 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.480 _cell_angle_gamma 90.000 _cell_length_a 9.4860 _cell_length_b 18.9740 _cell_length_c 10.7590 _exptl_crystal_F_000 1088.00 _reflns_d_resolution_high 0.8419 _[local]_cod_data_source_file qa0360Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 0525a in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 329.61 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 433.40 415.16 12.34 o 2 0 0 108641.15 76843.87 1114.58 o 3 0 0 1.72 -19.69 19.69 o 4 0 0 17880.96 13914.22 164.39 o 5 0 0 2085.40 2174.51 67.14 o 6 0 0 32709.90 29202.17 297.78 o 7 0 0 869.19 800.79 30.85 o 8 0 0 23459.23 20786.94 309.38 o 9 0 0 469.49 420.74 32.61 o 10 0 0 6785.35 6667.63 179.81 o 11 0 0 5.26 6.17 50.54 o 1 1 0 504.68 513.29 15.13 o 2 1 0 1052.05 896.42 26.74 o 3 1 0 2894.42 2388.25 58.47 o 4 1 0 5.74 27.03 17.92 o 5 1 0 1864.65 1863.36 53.18 o 6 1 0 524.53 560.74 22.92 o 7 1 0 2.78 6.02 12.19 o 8 1 0 139.50 122.37 20.57 o 9 1 0 238.15 206.70 23.65 o 10 1 0 78.73 78.45 24.24 o 11 1 0 294.75 268.69 33.35 o 0 2 0 82934.86 49257.66 584.98 o 1 2 0 3518.64 3645.92 47.89 o 2 2 0 22853.23 19258.53 132.07 o 3 2 0 6184.82 5667.05 88.14 o 4 2 0 10149.45 7635.75 116.20 o 5 2 0 1497.69 1557.06 47.16 o 6 2 0 25935.63 22266.43 250.18 o 7 2 0 11.95 3.09 24.68 o 8 2 0 17086.73 14659.48 248.86 o 9 2 0 2.83 21.89 35.26 o 10 2 0 7330.75 7034.16 206.70 o 11 2 0 231.84 226.82 33.79 o 1 3 0 57.71 93.14 9.11 o 2 3 0 9609.51 9437.99 98.28 o 3 3 0 6011.30 5605.21 89.32 o 4 3 0 185.44 157.63 12.19 o 5 3 0 359.89 355.51 16.31 o 6 3 0 70.60 77.27 13.22 o 7 3 0 744.75 653.44 25.71 o 8 3 0 358.56 327.60 24.83 o 9 3 0 157.10 175.26 21.01 o 10 3 0 159.81 153.66 22.33 o 11 3 0 256.65 254.74 30.85 o 0 4 0 32326.72 29660.52 152.64 o 1 4 0 4.39 24.09 18.80 o 2 4 0 39007.14 35557.92 200.82 o 3 4 0 63.55 65.08 10.14 o 4 4 0 35372.30 30610.56 237.84 o 5 4 0 7.02 26.59 18.80 o 6 4 0 22511.96 19886.99 238.72 o 7 4 0 56.39 79.33 13.07 o 8 4 0 7948.72 7244.53 173.20 o 9 4 0 263.35 267.96 23.36 o 10 4 0 4100.49 4013.04 123.40 o 11 4 0 607.26 592.47 39.37 o 1 5 0 2808.84 3289.97 62.14 o 2 5 0 687.68 687.96 20.13 o 3 5 0 5574.27 5461.83 95.05 o 4 5 0 180.88 191.13 13.37 o 5 5 0 478.70 372.85 18.36 o 6 5 0 0.12 22.04 23.65 o 7 5 0 316.90 236.23 19.69 o 8 5 0 50.42 78.59 16.60 o 9 5 0 298.16 323.34 25.71 o 10 5 0 364.38 270.60 31.00 o 0 6 0 390.53 591.74 17.63 o 1 6 0 2774.94 3143.65 64.34 o 2 6 0 31190.88 29466.46 206.70 o 3 6 0 1776.71 1910.22 51.27 o 4 6 0 33916.14 31676.95 257.82 o 5 6 0 18.28 -23.06 25.41 o 6 6 0 15985.34 14771.57 212.87 o 7 6 0 212.42 189.22 17.78 o 8 6 0 6426.82 6151.85 166.30 o 9 6 0 360.24 351.99 27.32 o 10 6 0 4123.98 4035.81 125.31 o 1 7 0 222.29 177.32 12.19 o 2 7 0 1205.25 1322.30 38.78 o 3 7 0 8990.30 8646.31 129.13 o 4 7 0 12.09 -6.17 24.68 o 5 7 0 4835.11 4825.43 114.29 o 6 7 0 131.54 144.41 15.72 o 7 7 0 1067.57 1017.77 34.52 o 8 7 0 231.89 250.03 24.24 o 9 7 0 1138.55 1155.56 42.31 o 10 7 0 2.65 -46.72 46.72 o 0 8 0 9063.57 8458.86 118.11 o 1 8 0 305.75 359.77 15.72 o 2 8 0 29780.62 29362.74 230.64 o 3 8 0 1954.22 2196.84 60.53 o 4 8 0 22867.31 22259.67 231.96 o 5 8 0 302.34 311.88 18.51 o 6 8 0 6689.50 6411.43 148.82 o 7 8 0 37.55 -32.61 32.61 o 8 8 0 9463.36 9402.00 206.99 o 9 8 0 571.61 527.98 32.47 o 10 8 0 4374.87 4123.81 128.25 o 1 9 0 22124.20 22758.57 207.28 o 2 9 0 7.05 24.68 11.90 o 3 9 0 10799.40 11465.44 162.33 o 4 9 0 125.20 153.22 15.72 o 5 9 0 8876.26 9371.88 169.09 o 6 9 0 1231.94 1213.59 37.02 o 7 9 0 3647.83 3535.74 111.06 o 8 9 0 884.34 871.74 37.02 o 9 9 0 2083.83 2051.69 61.85 o 10 9 0 6.41 0.00 47.16 o 0 10 0 18233.05 18107.08 193.33 o 1 10 0 477.47 542.82 22.92 o 2 10 0 18166.24 18283.95 202.00 o 3 10 0 113.32 147.05 13.96 o 4 10 0 12821.43 12948.02 192.01 o 5 10 0 75.37 65.37 15.43 o 6 10 0 7527.71 7488.69 169.38 o 7 10 0 1176.01 1209.33 39.96 o 8 10 0 6999.91 7334.44 192.45 o 9 10 0 1089.01 1078.29 43.19 o 10 10 0 3598.02 3478.30 107.83 o 1 11 0 15982.12 15839.58 193.62 o 2 11 0 118.85 110.47 16.45 o 3 11 0 8963.73 9095.85 159.10 o 4 11 0 269.40 274.71 18.22 o 5 11 0 7868.26 8050.31 169.53 o 6 11 0 3.57 -17.19 33.79 o 7 11 0 5119.52 4871.41 129.87 o 8 11 0 334.89 322.90 29.97 o 9 11 0 3418.06 3618.01 104.89 o 0 12 0 7650.04 7736.96 141.62 o 1 12 0 75.85 30.12 38.93 o 2 12 0 12255.60 12522.29 186.28 o 3 12 0 8.95 2.79 30.41 o 4 12 0 8267.16 8225.57 168.35 o 5 12 0 157.48 164.68 21.01 o 6 12 0 7443.91 7637.95 178.20 o 7 12 0 113.34 142.06 21.30 o 8 12 0 2779.56 2842.93 83.88 o 9 12 0 17.75 -52.45 52.45 o 1 13 0 10031.09 10377.16 173.20 o 2 13 0 290.76 279.42 21.01 o 3 13 0 13133.21 12909.83 206.55 o 4 13 0 208.66 175.85 21.45 o 5 13 0 10526.97 10996.37 210.96 o 6 13 0 264.82 236.81 24.68 o 7 13 0 3801.98 3697.63 108.86 o 8 13 0 460.69 481.41 32.91 o 9 13 0 3219.56 3176.55 90.64 o 0 14 0 9335.19 9862.55 176.14 o 1 14 0 102.57 57.29 43.19 o 2 14 0 7967.26 8172.83 166.30 o 3 14 0 544.34 525.34 28.50 o 4 14 0 8213.32 8552.73 181.87 o 5 14 0 362.64 387.10 27.77 o 6 14 0 4637.52 4648.55 130.16 o 7 14 0 114.57 157.92 24.09 o 8 14 0 1849.47 1929.76 59.35 o 1 15 0 8086.06 7844.21 167.62 o 2 15 0 0.47 -9.70 37.61 o 3 15 0 13824.19 13013.10 225.79 o 4 15 0 21.75 19.10 35.99 o 5 15 0 10355.92 10651.44 222.42 o 6 15 0 1.90 -8.52 40.11 o 7 15 0 3724.74 3994.53 117.38 o 8 15 0 8.23 70.37 46.28 o 0 16 0 6227.18 6155.81 156.16 o 1 16 0 30.79 -47.45 47.45 o 2 16 0 3832.65 3733.92 110.47 o 3 16 0 266.89 203.47 27.91 o 4 16 0 2922.35 3084.15 94.61 o 5 16 0 56.73 61.41 42.02 o 6 16 0 1836.06 1977.80 58.91 o 7 16 0 9.32 51.86 41.43 o 1 17 0 6050.55 5849.51 158.95 o 2 17 0 6.09 23.65 36.29 o 3 17 0 6727.04 6523.67 176.88 o 4 17 0 124.01 61.11 49.36 o 5 17 0 4793.04 4932.52 142.94 o 6 17 0 92.85 162.18 21.74 o 7 17 0 2889.77 2958.99 93.58 o 0 18 0 4303.64 4487.54 129.87 o 1 18 0 68.12 -65.52 65.52 o 2 18 0 1006.58 967.67 38.05 o 3 18 0 0.10 -55.09 55.09 o 4 18 0 1598.02 1757.44 55.53 o 5 18 0 119.30 0.00 47.45 o 6 18 0 715.87 721.60 39.96 o 1 19 0 11012.90 10872.68 232.55 o 2 19 0 38.95 36.58 42.46 o 3 19 0 7847.52 7896.21 207.58 o 4 19 0 370.01 380.49 31.00 o 5 19 0 3645.67 3416.16 104.30 o 6 19 0 60.41 -47.89 52.89 o 0 20 0 469.22 491.70 32.76 o 1 20 0 597.11 385.04 49.07 o 2 20 0 1954.33 1918.74 60.23 o 3 20 0 1.81 -52.89 52.89 o 4 20 0 1059.41 941.08 46.72 o 5 20 0 18.72 61.55 45.10 o 1 21 0 8965.78 8800.42 232.70 o 2 21 0 1.19 -14.84 41.13 o 3 21 0 3647.55 3650.03 113.85 o 4 21 0 45.99 50.83 42.60 o 0 22 0 108.27 122.23 28.21 o 1 22 0 11.15 -41.43 61.85 o 2 22 0 4.94 61.70 43.04 o -11 1 1 458.75 417.36 32.76 o -10 1 1 3329.40 3001.74 91.96 o -9 1 1 1269.90 1065.07 38.20 o -8 1 1 12951.88 10287.11 200.38 o -7 1 1 4705.22 3749.34 98.57 o -6 1 1 21382.58 16982.66 211.99 o -5 1 1 378.69 235.05 14.69 o -4 1 1 18574.41 13573.84 152.34 o -3 1 1 294.66 308.65 12.78 o -2 1 1 21120.79 18108.54 127.37 o -1 1 1 2406.54 2349.91 39.08 o 0 1 1 76154.41 45248.17 1203.16 o 1 1 1 428.19 493.31 14.25 o 2 1 1 30273.39 28502.01 172.47 o 3 1 1 2795.97 2648.43 66.40 o 4 1 1 10733.64 9259.94 136.62 o 5 1 1 773.91 744.37 23.65 o 6 1 1 19569.91 17576.89 233.43 o 7 1 1 1134.70 1136.47 36.14 o 8 1 1 16406.78 15303.66 266.05 o 9 1 1 17.79 47.45 42.90 o 10 1 1 9239.82 8819.52 241.22 o 11 1 1 5.89 6.17 51.12 o -11 2 1 33.11 -10.43 48.77 o -10 2 1 134.02 84.18 22.33 o -9 2 1 582.73 482.29 28.21 o -8 2 1 51.24 40.84 27.62 o -7 2 1 1156.82 940.64 28.79 o -6 2 1 87.51 79.92 12.63 o -5 2 1 58.93 9.99 25.56 o -4 2 1 805.37 836.78 26.44 o -3 2 1 156.05 126.63 11.02 o -2 2 1 14889.57 13521.99 113.12 o -1 2 1 1657.16 1752.89 37.61 o 0 2 1 127.35 126.48 7.27 o 1 2 1 2309.24 2542.21 47.60 o 2 2 1 2552.76 2850.42 60.23 o 3 2 1 1185.63 1161.88 37.17 o 4 2 1 177.23 253.71 15.13 o 5 2 1 214.68 167.03 14.40 o 6 2 1 1212.74 1121.34 33.35 o 7 2 1 256.67 237.11 20.71 o 8 2 1 55.41 -3.38 33.49 o 9 2 1 1178.89 1138.67 42.75 o 10 2 1 375.72 345.38 34.23 o 11 2 1 284.16 264.73 33.20 o -11 3 1 1340.18 1317.01 50.10 o -10 3 1 4352.45 3851.00 126.63 o -9 3 1 896.64 822.67 34.38 o -8 3 1 8327.44 7300.36 171.29 o -7 3 1 2198.22 1695.30 50.83 o -6 3 1 19265.95 16197.29 206.84 o -5 3 1 4641.16 3996.73 93.29 o -4 3 1 35833.83 30002.22 225.79 o -3 3 1 8754.28 7821.14 103.13 o -2 3 1 43035.80 37657.21 194.80 o -1 3 1 5123.29 5206.94 65.23 o 0 3 1 45936.95 39295.79 743.20 o 1 3 1 11298.01 12207.17 105.33 o 2 3 1 52028.32 46275.91 234.46 o 3 3 1 847.67 808.43 23.50 o 4 3 1 21012.96 19089.88 196.41 o 5 3 1 594.46 581.45 21.01 o 6 3 1 19115.62 17866.15 238.72 o 7 3 1 1167.40 1025.85 33.79 o 8 3 1 9993.89 9099.67 210.08 o 9 3 1 431.16 459.38 29.82 o 10 3 1 6751.13 6653.97 181.43 o 11 3 1 33.72 55.82 53.62 o -11 4 1 257.44 253.85 29.09 o -10 4 1 4.96 9.40 35.11 o -9 4 1 1077.17 888.34 35.26 o -8 4 1 1.23 -3.53 28.21 o -7 4 1 535.64 519.90 22.92 o -6 4 1 1656.93 1506.82 44.22 o -5 4 1 699.28 646.09 20.42 o -4 4 1 3677.51 3448.18 80.21 o -3 4 1 9752.45 9173.85 115.17 o -2 4 1 883.52 1011.60 32.47 o -1 4 1 63302.11 53575.97 221.09 o 0 4 1 4918.78 5274.24 61.63 o 1 4 1 6607.50 6863.02 86.23 o 2 4 1 157.76 192.74 12.49 o 3 4 1 7647.64 7319.16 111.06 o 4 4 1 359.72 428.97 17.33 o 5 4 1 4625.06 4898.00 113.41 o 6 4 1 708.70 683.85 25.71 o 7 4 1 1333.92 1249.44 35.70 o 8 4 1 4.78 -14.10 33.94 o 9 4 1 719.45 735.56 35.70 o 10 4 1 20.86 27.03 43.48 o 11 4 1 678.95 667.69 45.39 o -10 5 1 4445.36 4105.88 119.29 o -9 5 1 1185.33 1120.31 40.11 o -8 5 1 6159.26 5394.25 151.61 o -7 5 1 2566.61 2292.91 70.66 o -6 5 1 20929.24 19238.55 231.23 o -5 5 1 8057.02 8089.25 137.65 o -4 5 1 27342.61 25831.41 221.83 o -3 5 1 13420.17 13176.17 143.38 o -2 5 1 17714.53 16910.08 147.20 o -1 5 1 3608.15 3797.67 66.40 o 0 5 1 31519.47 28799.13 172.03 o 1 5 1 9076.37 9573.44 109.74 o 2 5 1 55801.45 48680.91 264.73 o 3 5 1 454.37 432.93 16.45 o 4 5 1 40857.43 38532.77 286.91 o 5 5 1 370.74 320.26 18.51 o 6 5 1 20164.53 19409.99 251.50 o 7 5 1 340.23 317.61 20.13 o 8 5 1 7518.66 7019.33 183.19 o 9 5 1 363.75 325.10 28.06 o 10 5 1 4022.63 3946.93 117.38 o -10 6 1 124.58 119.88 24.83 o -9 6 1 2006.20 1862.77 54.94 o -8 6 1 59.32 98.43 16.31 o -7 6 1 309.55 277.80 21.01 o -6 6 1 1850.47 1959.88 61.26 o -5 6 1 132.66 99.90 13.37 o -4 6 1 5008.29 5144.36 102.98 o -3 6 1 12975.42 13517.72 152.49 o -2 6 1 866.92 842.36 25.56 o -1 6 1 15157.92 15089.77 138.53 o 0 6 1 4221.87 4494.03 167.25 o 1 6 1 922.43 1167.32 35.26 o 2 6 1 22.53 41.28 9.99 o 3 6 1 3670.13 3663.25 84.47 o 4 6 1 38.10 39.52 23.95 o 5 6 1 7831.67 8204.27 151.31 o 6 6 1 443.42 462.46 22.18 o 7 6 1 1107.68 1050.67 34.38 o 8 6 1 616.79 605.84 31.00 o 9 6 1 299.87 308.36 25.41 o 10 6 1 62.70 86.67 54.21 o -10 7 1 3880.07 3834.69 116.94 o -9 7 1 1998.87 1885.69 60.23 o -8 7 1 8419.90 7823.79 187.16 o -7 7 1 207.07 188.33 19.39 o -6 7 1 16220.83 15130.32 218.45 o -5 7 1 1114.21 1072.86 32.91 o -4 7 1 25836.61 24119.80 229.76 o -3 7 1 413.15 332.01 15.28 o -2 7 1 27586.46 26992.11 208.90 o -1 7 1 244.07 226.82 12.63 o 0 7 1 36416.50 33186.97 197.15 o 1 7 1 7091.81 7809.98 112.97 o 2 7 1 40163.30 37653.98 257.82 o 3 7 1 1353.83 1331.12 39.52 o 4 7 1 29533.00 29883.52 267.81 o 5 7 1 8.08 5.44 30.70 o 6 7 1 10320.59 9963.33 185.54 o 7 7 1 71.47 43.78 37.90 o 8 7 1 11147.42 10909.85 229.76 o 9 7 1 320.62 328.34 26.44 o 10 7 1 6136.39 6238.67 175.11 o -10 8 1 617.10 650.94 40.40 o -9 8 1 1678.67 1590.55 48.63 o -8 8 1 307.66 288.96 23.95 o -7 8 1 355.32 331.57 23.50 o -6 8 1 907.03 919.93 28.79 o -5 8 1 3254.26 3109.42 82.71 o -4 8 1 176.33 207.58 15.87 o -3 8 1 12899.28 12850.92 162.48 o -2 8 1 3572.43 3621.09 83.15 o -1 8 1 13601.96 13961.09 152.93 o 0 8 1 3991.91 4449.84 150.36 o 1 8 1 180.72 221.24 13.22 o 2 8 1 1267.87 1361.53 39.37 o 3 8 1 5976.21 5911.36 115.76 o 4 8 1 512.62 565.30 21.89 o 5 8 1 7384.34 7420.09 151.75 o 6 8 1 179.63 209.49 17.92 o 7 8 1 5455.50 5701.14 156.60 o 8 8 1 35.90 43.04 40.40 o 9 8 1 966.21 866.75 41.28 o 10 8 1 87.28 119.88 26.88 o -10 9 1 4797.25 4521.19 132.51 o -9 9 1 1751.33 1820.02 55.53 o -8 9 1 5890.71 5619.90 145.58 o -7 9 1 2511.43 2442.76 72.28 o -6 9 1 8648.15 8258.48 169.68 o -5 9 1 3390.80 3335.95 90.93 o -4 9 1 11872.49 11613.53 173.35 o -3 9 1 333.66 303.95 16.60 o -2 9 1 11651.89 11322.95 151.75 o -1 9 1 6479.44 6810.87 114.29 o 0 9 1 30664.21 30041.86 167.78 o 1 9 1 4095.28 4520.01 96.52 o 2 9 1 35644.53 35488.43 276.04 o 3 9 1 393.13 407.22 18.51 o 4 9 1 16566.90 17138.52 218.30 o 5 9 1 185.43 213.45 17.63 o 6 9 1 5689.36 5911.80 150.87 o 7 9 1 355.76 396.06 25.71 o 8 9 1 11655.10 11207.92 238.28 o 9 9 1 2.65 31.44 19.69 o 10 9 1 3007.20 3343.29 98.87 o -10 10 1 284.75 264.14 32.32 o -9 10 1 1708.86 1774.19 55.09 o -8 10 1 1911.62 1799.31 49.80 o -7 10 1 6952.64 6875.36 171.29 o -6 10 1 19.94 36.87 31.58 o -5 10 1 2394.73 2258.83 63.17 o -4 10 1 87.99 63.32 14.40 o -3 10 1 5828.91 5966.01 123.11 o -2 10 1 1078.09 1111.64 33.64 o -1 10 1 3736.14 4028.32 93.14 o 0 10 1 293.39 347.24 13.96 o 1 10 1 6782.19 7054.44 126.63 o 2 10 1 95.18 120.46 14.40 o 3 10 1 4130.77 4234.28 107.54 o 4 10 1 3612.04 3905.94 111.94 o 5 10 1 7402.25 7540.55 160.27 o 6 10 1 63.45 92.84 17.19 o 7 10 1 2014.87 2100.76 65.81 o 8 10 1 0.74 36.58 40.84 o 9 10 1 1833.79 1958.26 57.59 o 10 10 1 41.69 63.76 44.51 o -9 11 1 1745.06 1792.99 56.85 o -8 11 1 4367.23 4448.91 136.18 o -7 11 1 1028.74 1044.65 39.81 o -6 11 1 5855.61 6217.51 157.04 o -5 11 1 211.12 228.44 19.83 o -4 11 1 8668.14 8789.25 164.09 o -3 11 1 1541.27 1573.07 49.21 o -2 11 1 27566.64 28031.62 263.11 o -1 11 1 3683.91 3832.20 96.96 o 0 11 1 16678.51 17779.62 176.95 o 1 11 1 478.44 594.97 22.33 o 2 11 1 12423.71 12801.41 182.60 o 3 11 1 1186.88 1303.79 37.90 o 4 11 1 13163.96 13344.52 208.02 o 5 11 1 394.53 394.15 23.06 o 6 11 1 8614.86 9007.70 195.83 o 7 11 1 77.83 133.54 21.30 o 8 11 1 4260.62 4317.57 121.05 o 9 11 1 303.86 330.10 32.32 o -9 12 1 2619.53 2584.37 81.09 o -8 12 1 461.74 470.98 31.00 o -7 12 1 4615.25 4749.77 130.60 o -6 12 1 288.85 296.60 24.83 o -5 12 1 9527.47 9536.13 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