#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2011278.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011278_Fobs loop_ _publ_author_name 'Ng, Seik Weng' 'Shanmuga Sundara Raj, S.' 'Fun, Hoong-Kun' 'Razak, Ibrahim Abdul' 'Hook, James M.' _publ_section_title ; Linear chains in polymeric dicyclohexylammonium tributyl(4-oxo-4H-pyran-2,6-dicarboxylato)stannate and methylphenylammonium tributyl(pyridine-2,6-dicarboxylato)stannate containing trigonal bipyramidal tin ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 966 _journal_page_last 968 _journal_volume 56 _journal_year 2000 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.454 _cell_angle_gamma 90.000 _cell_length_a 18.1212 _cell_length_b 18.0363 _cell_length_c 21.8937 _exptl_crystal_F_000 2752.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file sk1382Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Dicyclohexylammonium chelidonicatotributylstannate in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 769.32 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 26.59 9.15 11.68 o 2 0 0 48895.01 47235.65 1599.21 o 3 0 0 2.13 275.83 43.56 o 4 0 0 591846.75 564901.63 25560.50 o 5 0 0 82.24 0.32 36.61 o 6 0 0 1391.48 1298.73 111.26 o 7 0 0 602.01 554.60 53.52 o 8 0 0 49818.40 48881.31 1668.68 o 9 0 0 1216.18 1010.19 74.33 o 10 0 0 19814.19 18786.37 662.19 o 11 0 0 365.40 359.32 62.70 o 12 0 0 3085.81 3780.30 167.14 o 13 0 0 441.23 376.18 67.72 o 14 0 0 2475.19 2216.23 122.68 o 15 0 0 51.71 24.11 61.82 o 16 0 0 533.11 664.80 83.32 o 17 0 0 86.50 263.59 75.32 o 18 0 0 455.45 491.64 77.55 o 19 0 0 9.93 -22.60 84.28 o 20 0 0 0.62 48.92 84.28 o 21 0 0 11.21 249.99 102.90 o 1 1 0 3.54 7.93 8.94 o 3 1 0 5.43 101.69 14.64 o 4 1 0 30950.05 35765.35 861.45 o 5 1 0 91.51 24.48 53.30 o 6 1 0 157249.95 166876.28 3984.18 o 7 1 0 668.78 722.20 40.17 o 8 1 0 2178.74 2510.22 80.94 o 9 1 0 65.61 40.46 35.05 o 10 1 0 25184.28 27346.39 671.47 o 11 1 0 192.83 220.71 38.31 o 12 1 0 2364.18 1897.48 77.20 o 13 1 0 1.49 -5.89 38.29 o 14 1 0 1685.28 1702.00 78.60 o 15 1 0 195.60 148.36 70.25 o 16 1 0 1039.68 902.08 64.61 o 17 1 0 18.00 34.11 39.77 o 18 1 0 87.53 126.43 47.79 o 19 1 0 58.07 105.45 61.97 o 20 1 0 196.37 372.69 74.40 o 21 1 0 7.51 143.36 98.16 o 1 2 0 1126.18 919.11 31.00 o 2 2 0 11193.73 15130.18 378.66 o 3 2 0 2113.19 1875.85 58.28 o 4 2 0 89653.94 94527.59 2326.51 o 5 2 0 286.62 198.24 28.66 o 6 2 0 62410.45 67860.98 1628.57 o 7 2 0 123.72 217.06 35.17 o 8 2 0 29458.55 25941.64 634.37 o 9 2 0 23.89 98.24 36.02 o 10 2 0 26261.08 25313.62 622.98 o 11 2 0 16.09 38.35 33.34 o 12 2 0 3416.72 3321.24 109.16 o 13 2 0 214.55 228.90 44.52 o 14 2 0 1804.17 1575.94 78.15 o 15 2 0 26.17 16.42 41.85 o 16 2 0 643.35 778.86 59.32 o 17 2 0 73.08 96.04 56.58 o 18 2 0 298.90 269.67 56.47 o 19 2 0 7.99 102.31 54.32 o 20 2 0 1.57 113.51 56.59 o 21 2 0 5.50 237.09 67.19 o 1 3 0 5026.50 4323.06 102.48 o 2 3 0 163258.73 136147.08 3006.90 o 3 3 0 350.66 524.13 28.30 o 4 3 0 83537.61 88308.32 2175.93 o 5 3 0 42.17 -5.32 28.23 o 6 3 0 53250.45 53239.71 1453.96 o 7 3 0 433.79 353.40 31.61 o 8 3 0 31578.89 30724.30 748.56 o 9 3 0 243.06 208.05 33.19 o 10 3 0 5983.53 5823.44 233.34 o 11 3 0 304.40 196.53 35.49 o 12 3 0 2634.75 2408.72 87.86 o 13 3 0 1.26 -9.57 41.19 o 14 3 0 1591.02 1798.38 80.43 o 15 3 0 108.85 170.34 48.14 o 16 3 0 805.23 703.94 59.71 o 17 3 0 15.74 -33.16 54.67 o 18 3 0 108.10 232.02 111.38 o 19 3 0 11.72 104.34 76.75 o 20 3 0 58.73 127.92 68.61 o 21 3 0 0.32 154.62 58.07 o 0 4 0 113132.55 129479.82 3785.42 o 1 4 0 1500.36 1118.16 43.35 o 2 4 0 4048.26 5414.52 133.20 o 3 4 0 44.03 76.59 40.86 o 4 4 0 35533.88 35173.16 874.61 o 5 4 0 2233.60 1810.53 62.15 o 6 4 0 10047.14 9645.69 253.43 o 7 4 0 203.54 49.48 27.81 o 8 4 0 4599.59 4495.28 127.03 o 9 4 0 1623.03 1445.73 73.00 o 10 4 0 5284.88 4594.26 196.14 o 11 4 0 21.55 59.55 43.62 o 12 4 0 2892.37 3036.04 102.26 o 13 4 0 534.71 412.72 48.36 o 14 4 0 1681.85 1493.04 79.86 o 15 4 0 21.12 40.39 47.31 o 16 4 0 134.80 223.16 56.15 o 17 4 0 43.56 155.89 55.73 o 18 4 0 174.06 210.83 57.89 o 19 4 0 5.01 204.34 58.56 o 20 4 0 2.20 44.79 51.92 o 1 5 0 674.99 653.14 46.41 o 2 5 0 54225.03 59195.45 1313.68 o 3 5 0 3872.25 4507.75 110.72 o 4 5 0 20401.43 21477.49 539.59 o 5 5 0 81.81 4.52 18.86 o 6 5 0 14622.77 13642.41 351.31 o 7 5 0 372.56 490.23 37.82 o 8 5 0 4118.05 3817.87 129.25 o 9 5 0 6.51 -17.26 25.88 o 10 5 0 1549.48 1506.41 62.56 o 11 5 0 111.26 69.85 33.82 o 12 5 0 741.51 735.83 56.33 o 13 5 0 38.25 32.88 52.72 o 14 5 0 118.40 65.74 37.80 o 15 5 0 13.50 18.32 60.60 o 16 5 0 328.54 436.94 62.38 o 17 5 0 6.20 56.86 51.49 o 18 5 0 7.82 61.60 73.70 o 19 5 0 33.76 46.86 71.08 o 20 5 0 10.73 76.29 71.34 o 0 6 0 38816.60 40684.71 1198.96 o 1 6 0 116.61 188.74 18.76 o 2 6 0 2716.04 3495.02 88.91 o 3 6 0 130.93 315.42 35.78 o 4 6 0 28712.27 28834.74 647.42 o 5 6 0 161.33 312.34 26.00 o 6 6 0 4559.15 4635.94 132.76 o 7 6 0 114.62 111.50 30.43 o 8 6 0 4267.13 4368.09 225.44 o 9 6 0 872.56 973.31 52.48 o 10 6 0 26.30 -1.89 39.77 o 11 6 0 42.03 33.76 32.51 o 12 6 0 2181.14 2278.91 85.99 o 13 6 0 314.82 136.50 42.78 o 14 6 0 230.83 161.64 52.27 o 15 6 0 62.67 20.60 53.72 o 16 6 0 0.71 53.78 50.16 o 17 6 0 43.30 79.21 73.84 o 18 6 0 25.64 58.87 91.22 o 19 6 0 4.35 82.07 128.62 o 20 6 0 14.71 86.49 104.63 o 1 7 0 1251.01 1239.55 39.10 o 2 7 0 12833.00 14250.16 325.83 o 3 7 0 5150.61 5059.63 124.97 o 4 7 0 1816.23 2212.07 76.70 o 5 7 0 1.08 13.02 14.80 o 6 7 0 6152.68 5523.29 235.43 o 7 7 0 989.66 717.79 79.04 o 8 7 0 306.43 150.49 53.64 o 9 7 0 16.11 24.62 67.70 o 10 7 0 1396.08 1548.89 77.94 o 11 7 0 655.38 534.30 42.66 o 12 7 0 476.99 392.31 41.19 o 13 7 0 13.79 -39.14 69.76 o 14 7 0 172.72 224.20 57.96 o 15 7 0 169.31 56.64 75.06 o 16 7 0 2.61 -31.26 67.23 o 18 7 0 0.24 -29.10 71.97 o 19 7 0 19.18 156.74 85.69 o 20 7 0 0.39 43.68 102.27 o 0 8 0 11697.21 12425.21 379.28 o 1 8 0 1767.91 2034.37 56.06 o 2 8 0 615.49 1068.17 40.18 o 3 8 0 1194.39 1346.60 46.14 o 4 8 0 2950.17 2439.26 70.13 o 5 8 0 3469.94 3682.89 115.83 o 6 8 0 709.21 863.73 42.90 o 7 8 0 52.57 19.47 22.24 o 8 8 0 289.92 308.31 58.50 o 9 8 0 656.76 606.70 69.61 o 10 8 0 881.11 700.26 48.17 o 11 8 0 261.28 164.51 40.27 o 12 8 0 1.91 -1.26 39.77 o 13 8 0 285.46 195.19 77.91 o 14 8 0 101.02 77.02 107.63 o 15 8 0 12.97 -83.96 70.07 o 16 8 0 24.12 -61.48 63.60 o 17 8 0 34.65 -26.87 81.44 o 18 8 0 1.14 37.33 76.38 o 19 8 0 6.26 49.94 67.47 o 1 9 0 353.19 423.79 28.38 o 2 9 0 4075.01 4622.28 110.12 o 3 9 0 1169.92 1084.91 42.05 o 4 9 0 23.02 -7.93 17.68 o 5 9 0 561.61 539.56 35.40 o 6 9 0 41.76 110.79 59.69 o 7 9 0 1874.65 1527.11 175.02 o 8 9 0 28.59 31.93 24.42 o 9 9 0 41.76 64.38 28.75 o 10 9 0 734.84 934.14 84.48 o 11 9 0 109.86 115.20 63.54 o 12 9 0 35.31 -109.53 83.64 o 13 9 0 85.66 222.11 78.63 o 14 9 0 38.60 85.18 73.09 o 15 9 0 167.84 161.09 80.93 o 16 9 0 9.60 -52.40 75.44 o 17 9 0 2.73 88.52 76.51 o 18 9 0 42.24 -39.80 59.69 o 19 9 0 26.05 57.76 93.74 o 0 10 0 3974.72 3623.87 128.86 o 1 10 0 3313.42 3009.97 78.41 o 2 10 0 4433.94 4152.64 101.82 o 3 10 0 1583.37 1737.42 57.06 o 4 10 0 61.84 70.66 20.55 o 5 10 0 1006.29 1092.74 42.85 o 6 10 0 118.37 162.17 22.54 o 7 10 0 442.62 486.64 64.24 o 8 10 0 648.87 726.62 74.63 o 9 10 0 1197.79 1066.61 83.08 o 10 10 0 672.15 561.53 75.13 o 11 10 0 0.26 -11.81 61.71 o 12 10 0 1.74 82.56 77.96 o 13 10 0 411.13 435.05 91.77 o 14 10 0 51.16 85.02 71.06 o 15 10 0 0.91 -1.56 70.33 o 16 10 0 188.86 180.09 118.84 o 17 10 0 94.54 85.06 80.65 o 18 10 0 60.07 209.97 91.16 o 1 11 0 2491.96 2222.44 64.57 o 2 11 0 57.46 10.58 28.36 o 3 11 0 2246.42 2192.50 64.09 o 4 11 0 25.38 -2.79 38.27 o 5 11 0 533.51 519.24 45.91 o 6 11 0 501.36 460.87 45.50 o 7 11 0 746.39 625.75 67.91 o 8 11 0 31.11 -9.78 80.17 o 9 11 0 317.21 253.32 64.64 o 10 11 0 1220.06 1069.81 89.96 o 11 11 0 499.43 425.82 78.99 o 12 11 0 136.10 135.94 76.76 o 13 11 0 28.76 105.28 73.86 o 14 11 0 191.57 286.31 91.80 o 15 11 0 178.25 181.77 93.58 o 16 11 0 139.80 170.44 99.27 o 17 11 0 6.67 82.52 92.32 o 18 11 0 13.26 136.78 88.34 o 0 12 0 2763.05 2339.39 98.34 o 1 12 0 2172.78 2166.81 66.48 o 2 12 0 9.82 16.60 59.12 o 3 12 0 2052.37 2369.01 70.20 o 4 12 0 254.39 323.02 38.25 o 5 12 0 1563.60 1550.29 75.04 o 6 12 0 440.81 503.17 47.28 o 7 12 0 198.21 180.31 60.05 o 8 12 0 140.27 156.29 62.54 o 9 12 0 863.52 847.94 88.98 o 10 12 0 24.93 -3.27 53.12 o 11 12 0 31.73 58.84 57.44 o 12 12 0 106.88 18.11 67.43 o 13 12 0 230.42 282.19 86.45 o 14 12 0 89.24 -8.95 68.59 o 15 12 0 11.08 38.82 94.06 o 16 12 0 80.54 115.04 87.41 o 17 12 0 22.71 174.79 87.41 o 1 13 0 835.15 1040.70 47.27 o 2 13 0 156.42 89.63 27.73 o 3 13 0 1113.48 1241.35 59.23 o 4 13 0 58.52 -6.15 28.07 o 5 13 0 864.18 953.78 61.73 o 6 13 0 247.35 249.93 43.45 o 7 13 0 1061.49 1049.68 91.21 o 8 13 0 0.77 19.57 101.32 o 9 13 0 257.40 265.86 97.51 o 10 13 0 350.40 361.09 129.30 o 11 13 0 294.65 428.19 73.54 o 12 13 0 0.67 13.76 63.79 o 13 13 0 13.67 176.43 89.62 o 14 13 0 104.92 81.44 75.00 o 15 13 0 58.64 338.88 98.29 o 16 13 0 7.26 128.67 80.49 o 0 14 0 650.17 670.68 63.67 o 1 14 0 1972.25 2035.05 76.97 o 2 14 0 20.89 -19.70 33.62 o 3 14 0 721.29 793.47 51.65 o 4 14 0 73.91 34.57 31.65 o 5 14 0 961.27 967.04 58.95 o 6 14 0 3.73 -32.91 31.53 o 7 14 0 229.87 239.33 65.32 o 8 14 0 324.09 243.09 65.61 o 9 14 0 418.07 417.88 73.49 o 10 14 0 7.55 10.41 56.11 o 11 14 0 55.26 145.70 68.20 o 12 14 0 81.77 89.31 65.25 o 13 14 0 120.86 172.25 69.97 o 14 14 0 1.14 146.15 84.87 o 15 14 0 3.08 136.10 77.45 o 16 14 0 11.44 21.51 72.39 o 1 15 0 812.94 702.27 58.78 o 2 15 0 24.03 3.57 32.71 o 3 15 0 816.59 824.18 54.73 o 4 15 0 134.44 49.98 34.28 o 5 15 0 458.82 506.72 50.45 o 6 15 0 27.57 0.46 40.89 o 7 15 0 337.78 451.40 72.29 o 8 15 0 7.01 17.72 70.62 o 9 15 0 130.23 129.90 64.81 o 10 15 0 0.18 146.87 82.79 o 11 15 0 172.07 221.93 72.34 o 12 15 0 5.62 77.24 120.89 o 13 15 0 1.34 180.76 67.79 o 14 15 0 7.79 24.78 71.04 o 15 15 0 36.55 56.98 78.49 o 0 16 0 69.04 66.69 70.55 o 1 16 0 231.48 188.08 45.56 o 2 16 0 150.95 35.32 36.46 o 3 16 0 351.38 313.96 47.17 o 4 16 0 0.47 26.49 33.97 o 5 16 0 425.74 479.58 59.09 o 6 16 0 71.52 25.67 41.24 o 7 16 0 54.93 133.70 48.14 o 8 16 0 46.47 87.12 80.50 o 9 16 0 359.73 400.28 75.70 o 10 16 0 18.22 75.80 61.51 o 11 16 0 3.65 105.20 63.85 o 12 16 0 1.40 52.94 64.95 o 13 16 0 86.39 164.17 72.64 o 14 16 0 26.54 185.41 88.58 o 1 17 0 106.77 132.86 69.75 o 2 17 0 47.20 20.14 39.85 o 3 17 0 244.08 301.77 55.31 o 4 17 0 2.89 -47.59 42.00 o 5 17 0 80.27 88.71 54.21 o 6 17 0 94.28 143.85 50.61 o 7 17 0 303.80 353.61 59.47 o 8 17 0 5.03 60.10 53.98 o 9 17 0 17.39 35.28 62.51 o 10 17 0 1.53 24.91 60.85 o 11 17 0 95.08 134.62 66.63 o 12 17 0 1.75 24.55 72.48 o 0 18 0 254.89 226.28 111.42 o 1 18 0 146.56 183.10 48.27 o 2 18 0 28.86 69.84 44.05 o 3 18 0 128.94 113.84 56.76 o 4 18 0 130.78 111.23 103.29 o 5 18 0 219.74 185.08 63.07 o 6 18 0 1.10 136.77 79.43 o 7 18 0 33.16 169.13 52.97 o 8 18 0 4.18 115.84 50.20 o 9 18 0 84.42 136.24 53.60 o 10 18 0 1.58 143.24 56.17 o 11 18 0 6.81 85.40 80.76 o 1 19 0 90.64 204.20 75.54 o 2 19 0 66.69 53.98 51.78 o 3 19 0 56.54 70.38 83.33 o 4 19 0 1.58 42.10 54.60 o 5 19 0 69.51 138.00 68.36 o 6 19 0 5.05 93.35 137.15 o 7 19 0 38.63 99.80 76.50 o 8 19 0 0.26 9.23 57.08 o 9 19 0 12.46 64.25 72.28 o 0 20 0 3.08 72.81 66.28 o 1 20 0 40.86 68.46 66.38 o 2 20 0 5.01 90.34 108.90 o 3 20 0 73.89 53.81 52.96 o 4 20 0 3.10 -9.68 60.68 o 5 20 0 23.68 64.50 122.63 o 6 20 0 27.24 29.08 57.26 o 7 20 0 27.78 37.46 66.78 o 1 21 0 22.27 -4.16 49.43 o 2 21 0 0.88 70.61 86.33 o 3 21 0 20.11 174.23 71.57 o 4 21 0 12.29 23.01 53.54 o -21 1 1 0.34 209.61 80.01 o -20 1 1 0.02 10.68 48.15 o -19 1 1 0.18 32.26 47.79 o -18 1 1 33.18 -46.53 38.29 o -17 1 1 2.61 41.92 63.14 o -16 1 1 14.48 3.90 39.48 o -15 1 1 0.06 35.04 42.20 o -14 1 1 81.99 48.32 71.64 o -13 1 1 4.97 9.81 42.25 o -12 1 1 422.24 482.79 60.46 o -11 1 1 159.96 224.55 41.07 o -10 1 1 2242.60 2531.75 85.00 o -9 1 1 3.53 20.82 27.19 o -8 1 1 12067.39 12912.76 324.72 o -7 1 1 0.36 127.12 27.42 o -6 1 1 3202.50 3277.91 94.38 o -5 1 1 1222.10 1796.37 60.09 o -4 1 1 5710.19 6488.24 188.97 o -3 1 1 5531.38 5115.67 148.84 o -2 1 1 1903.44 1562.40 50.85 o -1 1 1 766.85 273.99 30.68 o 0 1 1 1872.35 435.77 264.16 o 1 1 1 364.22 44.09 8.29 o 2 1 1 2272.03 3130.84 77.30 o 3 1 1 18537.33 20485.42 459.34 o 4 1 1 31741.76 35410.99 852.87 o 5 1 1 1777.44 2328.52 71.49 o 6 1 1 2975.40 3038.39 88.80 o 7 1 1 1740.65 1129.26 48.01 o 8 1 1 419.96 772.80 44.04 o 9 1 1 202.34 165.69 32.53 o 10 1 1 1897.63 2079.04 75.79 o 11 1 1 212.67 286.32 39.13 o 12 1 1 30.94 -23.70 30.68 o 13 1 1 0.50 60.23 57.07 o 14 1 1 1.85 -21.86 54.33 o 15 1 1 0.56 -50.41 36.62 o 16 1 1 0.07 -41.19 39.94 o 17 1 1 0.01 50.68 50.02 o 18 1 1 4.41 -7.47 55.24 o 19 1 1 1.50 38.79 73.07 o 20 1 1 0.18 81.13 66.71 o 21 1 1 0.19 187.71 142.04 o -21 2 1 1.94 250.57 68.75 o -20 2 1 22.66 95.55 57.71 o -19 2 1 0.35 105.39 58.32 o -18 2 1 10.29 0.60 36.99 o -17 2 1 2.59 60.24 46.39 o -16 2 1 243.14 245.05 53.04 o -15 2 1 0.06 37.91 42.54 o -14 2 1 36.82 98.38 58.04 o -13 2 1 218.92 239.23 45.25 o -12 2 1 7.89 -26.83 70.07 o -11 2 1 688.15 596.26 46.30 o -10 2 1 1079.40 1403.13 61.77 o -9 2 1 276.10 322.82 37.06 o -8 2 1 548.30 444.73 51.34 o -7 2 1 1047.20 995.59 44.87 o -6 2 1 5132.86 4477.42 139.64 o -5 2 1 113.43 76.68 49.40 o -4 2 1 31365.16 32136.51 880.14 o -3 2 1 39584.96 45779.09 1130.90 o -2 2 1 2818.81 1230.75 87.65 o -1 2 1 143.33 356.02 18.09 o 0 2 1 3131.20 4370.03 95.36 o 1 2 1 2607.05 2098.61 52.62 o 2 2 1 53320.80 46798.89 1155.03 o 3 2 1 6572.70 11937.37 303.26 o 4 2 1 32923.46 33501.45 747.94 o 5 2 1 1245.83 967.00 38.65 o 6 2 1 8460.37 9350.50 236.90 o 7 2 1 1949.03 1977.90 65.88 o 8 2 1 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