#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2011285.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011285_Fobs loop_ _publ_author_name 'Aupers, John H.' 'Ferguson, George' 'Glidewell, Christopher' 'Low, John N.' 'Wardell, James L.' _publ_section_title ; trans-Chloro(2-nitrobenzenethiolato-S)bis(triphenylphosphine-P)palladium(II) monoacetone solvate ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 945 _journal_page_last 947 _journal_volume 56 _journal_year 2000 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.093 _cell_angle_gamma 90.000 _cell_length_a 18.2920 _cell_length_b 10.9690 _cell_length_c 21.3630 _exptl_crystal_F_000 1800.00 _reflns_d_resolution_high 0.7005 _[local]_cod_data_source_file sk1393Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 9905 JWPD P21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 584.06 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, z+1/2' '-x, -y, -z' '-x-1/2, y-1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 28193.84 27292.60 1940.69 o 4 0 0 86231.98 98602.78 2914.65 o 6 0 0 719.96 662.00 46.79 o 8 0 0 3490.28 3624.01 166.39 o 10 0 0 3585.03 3021.29 239.13 o 12 0 0 19720.29 18757.04 1648.99 o 14 0 0 5.46 -7.80 75.11 o 16 0 0 10663.52 11382.44 778.03 o 20 0 0 1.26 -111.86 176.73 o 22 0 0 767.89 993.74 283.16 o 1 1 0 62429.38 54146.29 5335.99 o 2 1 0 3378.66 3419.59 94.23 o 3 1 0 4715.81 4547.29 116.06 o 4 1 0 4620.66 4637.58 91.52 o 5 1 0 2052.82 1775.31 119.93 o 6 1 0 5064.83 5045.62 301.44 o 7 1 0 663.60 524.23 27.02 o 8 1 0 372.18 458.66 38.01 o 9 1 0 413.37 377.62 37.76 o 10 1 0 300.22 262.55 35.26 o 11 1 0 6596.86 6303.43 159.75 o 12 1 0 8.19 58.08 41.02 o 13 1 0 7498.54 7956.37 229.41 o 14 1 0 430.29 330.88 74.75 o 15 1 0 5751.15 5701.90 223.32 o 16 1 0 381.15 241.22 120.92 o 17 1 0 6717.67 6564.02 311.85 o 18 1 0 29.19 -78.39 102.41 o 19 1 0 4.13 -131.43 131.43 o 20 1 0 530.93 509.09 211.61 o 21 1 0 78.16 -146.25 146.25 o 22 1 0 90.47 112.28 277.22 o 23 1 0 1005.16 911.76 203.47 o 24 1 0 40.44 -261.22 261.22 o 0 2 0 49075.57 49908.88 1516.21 o 1 2 0 178.05 196.72 16.29 o 2 2 0 117.21 113.53 18.08 o 3 2 0 424.77 395.77 22.41 o 4 2 0 5.06 16.81 19.20 o 5 2 0 8345.03 8092.62 235.84 o 6 2 0 46371.25 48228.32 1425.99 o 7 2 0 3366.89 3262.71 72.28 o 8 2 0 1441.20 1598.15 101.64 o 9 2 0 315.49 297.63 46.15 o 10 2 0 4497.95 4731.51 133.91 o 11 2 0 35.62 37.39 39.57 o 12 2 0 7728.57 7580.14 192.06 o 13 2 0 3797.01 4114.50 161.18 o 14 2 0 53.76 3.66 52.57 o 15 2 0 155.05 110.38 60.04 o 16 2 0 10383.05 11123.19 311.90 o 17 2 0 75.45 104.81 108.58 o 18 2 0 4790.06 5359.56 258.02 o 19 2 0 85.64 -65.25 209.82 o 20 2 0 332.39 205.83 172.93 o 21 2 0 9.58 145.52 292.54 o 22 2 0 384.06 266.02 166.47 o 23 2 0 0.38 -14.83 194.52 o 1 3 0 14061.54 12737.11 403.99 o 2 3 0 362.60 360.72 20.04 o 3 3 0 4245.52 4065.97 144.93 o 4 3 0 3890.86 3883.60 129.98 o 5 3 0 39789.05 41586.04 1352.30 o 6 3 0 132.47 121.42 22.22 o 7 3 0 12427.25 12632.80 383.94 o 8 3 0 128.33 109.26 25.94 o 9 3 0 2006.05 2176.95 71.19 o 10 3 0 168.29 220.75 52.97 o 11 3 0 19.15 15.49 45.94 o 12 3 0 427.92 389.61 66.09 o 13 3 0 2319.87 2546.19 161.28 o 14 3 0 962.10 933.10 88.50 o 15 3 0 965.99 782.84 90.34 o 16 3 0 126.97 219.08 140.56 o 17 3 0 11546.25 12723.98 402.29 o 18 3 0 105.43 -4.21 156.13 o 19 3 0 563.99 77.49 137.84 o 20 3 0 242.54 112.33 146.18 o 21 3 0 168.36 85.53 410.17 o 22 3 0 4.85 -70.31 221.59 o 23 3 0 78.70 -154.53 313.39 o 0 4 0 14069.25 11162.09 411.76 o 1 4 0 1909.06 2031.59 58.75 o 2 4 0 2812.16 2296.03 168.88 o 3 4 0 647.49 812.66 30.50 o 4 4 0 3548.47 3382.28 97.86 o 5 4 0 294.52 263.56 55.66 o 6 4 0 28376.16 29126.28 1058.79 o 7 4 0 447.23 385.79 61.06 o 8 4 0 654.84 592.73 62.35 o 9 4 0 664.57 725.47 96.72 o 10 4 0 1988.09 1925.32 176.26 o 11 4 0 1174.92 1075.41 68.39 o 12 4 0 1522.96 1330.46 95.08 o 13 4 0 1250.74 1210.91 74.16 o 14 4 0 2068.51 2437.10 130.48 o 15 4 0 875.01 831.29 86.45 o 16 4 0 11995.65 12682.92 491.76 o 17 4 0 439.49 325.74 115.23 o 18 4 0 6410.21 6339.74 305.17 o 19 4 0 71.33 -1.56 119.56 o 20 4 0 48.35 -68.98 144.48 o 21 4 0 4.54 -94.78 148.14 o 22 4 0 25.62 -77.75 322.67 o 23 4 0 45.09 283.06 238.73 o 1 5 0 5281.08 4677.74 113.14 o 2 5 0 2112.93 2125.54 51.48 o 3 5 0 17.32 13.10 22.35 o 4 5 0 6876.96 6980.21 222.50 o 5 5 0 222.37 138.57 51.47 o 6 5 0 928.93 1055.13 53.99 o 7 5 0 2616.01 2687.39 91.54 o 8 5 0 2223.17 2539.39 137.77 o 9 5 0 206.22 190.02 42.09 o 10 5 0 40.60 76.99 45.07 o 11 5 0 2122.64 1995.60 116.02 o 12 5 0 128.20 44.54 44.05 o 13 5 0 2537.42 2768.26 113.09 o 14 5 0 0.13 22.35 70.41 o 15 5 0 1455.67 1334.76 119.56 o 16 5 0 288.31 303.94 90.22 o 17 5 0 5574.53 6026.37 250.71 o 18 5 0 54.97 134.63 95.06 o 19 5 0 566.59 418.57 116.06 o 20 5 0 89.59 60.38 227.36 o 21 5 0 115.14 -81.22 291.05 o 22 5 0 40.01 43.65 190.71 o 0 6 0 48178.58 49553.67 1015.00 o 1 6 0 262.41 287.30 25.58 o 2 6 0 6602.87 6082.69 254.39 o 3 6 0 355.12 431.27 41.67 o 4 6 0 7071.03 6856.37 374.84 o 5 6 0 0.13 -23.15 25.17 o 6 6 0 6645.83 7546.23 368.63 o 7 6 0 79.56 48.97 32.89 o 8 6 0 461.68 510.99 49.20 o 9 6 0 95.13 77.80 45.35 o 10 6 0 880.81 931.75 73.86 o 11 6 0 8.51 -4.91 54.85 o 12 6 0 7084.14 7953.35 243.13 o 13 6 0 275.54 352.42 104.03 o 14 6 0 39.05 60.83 72.70 o 15 6 0 170.82 157.21 89.82 o 16 6 0 4753.68 5143.69 301.34 o 17 6 0 66.29 22.08 152.97 o 18 6 0 2303.68 2285.35 423.50 o 19 6 0 1.86 1.60 209.94 o 20 6 0 2.18 62.20 209.59 o 21 6 0 0.41 38.41 187.22 o 1 7 0 26996.25 27342.43 477.84 o 2 7 0 19.91 58.12 28.46 o 3 7 0 3.89 -29.01 31.73 o 4 7 0 203.96 216.00 37.45 o 5 7 0 3036.88 3276.73 136.12 o 6 7 0 43.33 -14.49 61.19 o 7 7 0 643.40 714.35 81.07 o 8 7 0 6.89 -42.85 54.24 o 9 7 0 38.67 6.60 41.48 o 10 7 0 51.32 17.44 76.40 o 11 7 0 7160.89 8136.82 240.87 o 12 7 0 10.05 5.54 48.68 o 13 7 0 1920.67 1997.84 119.44 o 14 7 0 30.40 10.90 86.53 o 15 7 0 1601.16 1563.70 130.14 o 16 7 0 2.41 -25.60 115.88 o 17 7 0 3370.09 3489.20 306.89 o 18 7 0 104.89 -5.56 91.32 o 19 7 0 270.80 183.64 245.01 o 20 7 0 99.43 126.95 265.45 o 21 7 0 370.36 89.43 425.77 o 0 8 0 44818.37 37666.33 1494.02 o 1 8 0 0.53 18.84 31.64 o 2 8 0 9145.00 9409.97 191.14 o 3 8 0 90.92 88.68 48.10 o 4 8 0 243.37 215.85 31.61 o 5 8 0 145.60 82.57 58.12 o 6 8 0 380.77 354.76 74.08 o 7 8 0 1440.29 1969.45 260.78 o 8 8 0 13.14 51.35 136.66 o 9 8 0 501.92 575.75 99.61 o 10 8 0 1213.23 1101.85 161.47 o 11 8 0 104.43 140.71 55.21 o 12 8 0 5075.52 5494.63 300.63 o 13 8 0 8.11 67.56 67.37 o 14 8 0 170.98 101.31 94.87 o 15 8 0 247.69 266.32 113.84 o 16 8 0 3905.57 4128.28 359.73 o 17 8 0 1.78 -115.82 201.24 o 18 8 0 1568.38 811.30 472.77 o 19 8 0 389.55 935.13 276.83 o 20 8 0 0.51 -23.32 717.24 o 21 8 0 154.11 402.39 802.84 o 1 9 0 18447.17 19113.68 534.32 o 2 9 0 596.83 561.70 51.61 o 3 9 0 411.83 404.92 45.23 o 4 9 0 165.21 170.10 48.54 o 5 9 0 4258.11 4317.07 318.95 o 6 9 0 3.04 -13.61 76.69 o 7 9 0 83.66 239.46 125.92 o 8 9 0 7.31 38.32 98.65 o 9 9 0 109.13 39.86 83.74 o 10 9 0 257.59 173.14 197.47 o 11 9 0 1154.24 1212.50 151.14 o 12 9 0 111.82 68.04 270.20 o 13 9 0 721.20 530.68 275.53 o 14 9 0 262.57 445.05 199.82 o 15 9 0 283.49 134.14 495.74 o 16 9 0 139.26 202.77 208.15 o 17 9 0 3372.37 3095.48 379.83 o 18 9 0 3.20 -159.56 307.76 o 19 9 0 376.23 493.82 559.92 o 20 9 0 11.40 2748.48 1341.19 o 0 10 0 11810.24 12194.32 376.92 o 1 10 0 719.04 818.69 62.71 o 2 10 0 3590.59 3622.41 226.19 o 3 10 0 14.74 46.25 38.36 o 4 10 0 1580.67 1563.01 134.68 o 5 10 0 5.21 -76.25 77.47 o 6 10 0 5635.98 5883.20 530.24 o 7 10 0 115.33 233.39 152.36 o 8 10 0 216.92 244.26 114.31 o 9 10 0 11.39 -42.33 148.12 o 10 10 0 212.82 235.84 149.69 o 11 10 0 266.78 -154.55 154.55 o 12 10 0 989.74 1030.84 402.61 o 13 10 0 11.67 131.77 168.23 o 14 10 0 123.83 226.80 238.20 o 15 10 0 8.90 249.70 217.61 o 16 10 0 4430.25 4625.80 562.55 o 17 10 0 5.58 73.77 327.51 o 18 10 0 1738.40 0.00 828.84 o 1 11 0 343.71 305.17 67.15 o 2 11 0 454.68 453.74 54.59 o 3 11 0 35.59 -13.94 135.08 o 4 11 0 280.07 307.32 88.05 o 5 11 0 3423.61 4143.23 325.33 o 6 11 0 175.82 148.74 107.94 o 7 11 0 3609.56 4093.85 299.05 o 8 11 0 161.13 201.29 107.94 o 9 11 0 1.25 -332.38 332.38 o 10 11 0 52.37 2.82 149.26 o 11 11 0 890.89 1134.52 343.06 o 12 11 0 6.90 -81.96 171.02 o 13 11 0 212.24 534.60 379.08 o 14 11 0 0.03 -131.30 235.62 o 15 11 0 1623.47 1558.89 375.23 o 16 11 0 202.32 617.74 468.00 o 0 12 0 3656.59 3574.48 290.07 o 1 12 0 952.75 984.04 159.48 o 2 12 0 158.11 225.41 113.46 o 3 12 0 4.07 -7.00 97.82 o 4 12 0 2866.54 3036.55 313.27 o 5 12 0 24.81 78.99 147.97 o 6 12 0 1782.11 1401.80 245.60 o 7 12 0 147.17 -109.12 133.39 o 8 12 0 420.51 322.92 239.40 o 9 12 0 5.38 176.88 330.44 o 10 12 0 71.01 12.05 166.16 o 11 12 0 209.61 174.96 437.40 o 12 12 0 913.39 777.91 279.16 o 13 12 0 19.36 -32.98 374.52 o 14 12 0 45.78 450.60 436.54 o 1 13 0 6294.25 5742.88 714.68 o 2 13 0 5.90 -65.12 138.82 o 3 13 0 1280.90 1219.69 284.01 o 4 13 0 339.51 472.29 128.77 o 5 13 0 894.86 1019.55 163.37 o 6 13 0 17.65 105.38 260.40 o 7 13 0 189.11 -6.70 218.26 o 8 13 0 284.63 87.48 394.65 o 9 13 0 10.16 153.86 197.53 o 10 13 0 3.54 225.03 339.86 o 11 13 0 1811.31 2210.08 301.20 o 12 13 0 29.46 188.09 352.80 o 13 13 0 1028.73 793.50 639.85 o 14 13 0 112.55 67.63 326.68 o 2 14 0 1329.62 1209.95 431.85 o 5 14 0 7.05 239.08 412.08 o 6 14 0 102.66 74.68 217.85 o 7 14 0 4.71 -91.98 254.86 o 8 14 0 123.44 26.71 306.16 o 9 14 0 29.19 918.84 806.67 o 10 14 0 524.88 838.00 303.50 o 11 14 0 22.84 258.98 310.90 o -25 0 1 138.85 -66.09 458.76 o -23 0 1 358.63 823.92 283.09 o -21 0 1 3532.08 4138.16 462.70 o -17 0 1 2306.91 2158.69 185.09 o -15 0 1 3759.34 3012.11 286.86 o -13 0 1 2395.43 2208.01 159.09 o -11 0 1 4269.19 4116.70 169.35 o -9 0 1 1015.95 806.60 55.75 o -7 0 1 3602.15 3160.71 177.99 o -5 0 1 24.59 30.79 37.03 o -3 0 1 59370.74 70835.85 1512.35 o -1 0 1 15637.00 -12.30 17.40 o 1 0 1 44102.76 -13.95 13.95 o 3 0 1 9194.89 8392.38 177.02 o 5 0 1 4585.30 4622.85 115.93 o 7 0 1 368.11 375.42 38.25 o 9 0 1 14834.23 15775.12 685.24 o 11 0 1 281.59 205.68 50.91 o 13 0 1 20630.15 23718.37 920.39 o 15 0 1 3988.91 3841.63 213.94 o 17 0 1 914.82 856.59 217.86 o 19 0 1 1544.79 1636.36 414.44 o 23 0 1 21.61 -277.79 277.79 o -24 1 1 7.30 230.14 281.64 o -23 1 1 98.03 43.74 304.21 o -22 1 1 1506.68 1447.21 331.29 o -21 1 1 523.68 594.60 205.14 o -20 1 1 2726.88 2807.82 234.81 o -19 1 1 122.17 13.23 105.47 o -18 1 1 1145.62 1341.52 150.59 o -17 1 1 1.16 -17.06 97.29 o -16 1 1 299.61 216.53 66.21 o -15 1 1 926.05 894.12 77.70 o -14 1 1 4441.54 4204.73 192.26 o -13 1 1 35.10 43.42 49.84 o -12 1 1 494.94 410.53 45.18 o -11 1 1 28.72 11.47 36.21 o -10 1 1 8775.37 8761.55 243.39 o -9 1 1 3382.36 3375.10 87.17 o -8 1 1 3027.62 2866.53 120.49 o -7 1 1 3595.40 3727.20 101.08 o -6 1 1 1822.83 1726.79 58.06 o -5 1 1 4970.28 4951.65 163.20 o -4 1 1 25168.03 24482.47 471.85 o -3 1 1 8269.39 8731.83 152.73 o -2 1 1 76536.24 92951.24 1492.20 o -1 1 1 4163.60 2527.23 154.90 o 0 1 1 4758.96 3287.46 296.38 o 1 1 1 5284.26 4781.61 84.42 o 2 1 1 11314.00 10962.45 390.99 o 3 1 1 6566.64 6225.13 158.66 o 4 1 1 8477.09 7693.35 171.64 o 5 1 1 2447.41 2482.10 99.85 o 6 1 1 151.57 110.98 29.78 o 7 1 1 6.33 -0.12 22.51 o 8 1 1 3646.27 3509.69 89.56 o 9 1 1 2630.38 2317.75 72.05 o 10 1 1 20916.39 23517.20 443.75 o 11 1 1 734.48 727.55 61.74 o 12 1 1 3372.05 3194.11 113.45 o 13 1 1 101.87 35.61 45.24 o 14 1 1 13590.06 14859.30 431.80 o 15 1 1 332.44 295.18 65.78 o 16 1 1 2225.38 1980.71 129.88 o 17 1 1 212.29 202.65 101.82 o 18 1 1 1667.16 1814.47 185.57 o 19 1 1 1033.47 1095.96 195.96 o 20 1 1 509.35 559.58 232.94 o 21 1 1 219.06 149.39 181.51 o 22 1 1 388.67 414.03 185.90 o 23 1 1 99.11 192.90 284.43 o 24 1 1 192.59 432.07 308.17 o -25 2 1 118.39 154.75 330.95 o -23 2 1 25.58 -120.51 280.39 o -22 2 1 119.54 167.36 159.35 o -21 2 1 1372.99 1354.95 303.67 o -20 2 1 449.75 271.19 177.06 o -19 2 1 2999.81 3168.42 265.09 o -18 2 1 353.75 408.93 136.86 o -17 2 1 531.26 511.94 84.71 o -16 2 1 10.07 -49.14 63.87 o -15 2 1 4248.82 4222.16 186.52 o -14 2 1 16.93 -12.53 52.04 o -13 2 1 338.30 364.87 73.62 o -12 2 1 251.74 230.56 54.28 o -11 2 1 17.94 -20.99 44.78 o -10 2 1 1760.68 1644.74 109.62 o -9 2 1 831.42 756.51 62.09 o -8 2 1 1506.88 1494.49 78.04 o -7 2 1 3018.40 2915.56 119.84 o -6 2 1 1776.71 2194.84 70.29 o -5 2 1 3979.33 3981.60 76.73 o -4 2 1 21276.15 21118.32 426.42 o -3 2 1 48902.46 49712.99 1329.70 o -2 2 1 2350.03 2484.58 68.17 o -1 2 1 30813.79 30031.83 636.95 o 0 2 1 409.00 394.20 20.61 o 1 2 1 16343.93 16630.57 342.85 o 2 2 1 183.82 133.86 14.53 o 3 2 1 93236.91 111494.41 1915.58 o 4 2 1 690.91 610.83 29.45 o 5 2 1 64.64 101.29 26.42 o 6 2 1 326.82 287.54 28.16 o 7 2 1 823.35 694.59 45.27 o 8 2 1 5650.70 5489.98 177.89 o 9 2 1 4383.19 4583.52 143.51 o 10 2 1 1.01 45.57 37.41 o 11 2 1 3.23 46.28 37.47 o 12 2 1 70.13 39.00 48.49 o 13 2 1 16748.50 17994.12 682.90 o 14 2 1 4452.01 4226.29 198.21 o 15 2 1 12967.61 13864.96 444.94 o 16 2 1 86.70 68.19 70.25 o 17 2 1 483.82 505.62 138.94 o 18 2 1 3.37 -57.34 112.80 o 19 2 1 3377.64 3517.00 306.22 o 20 2 1 441.50 187.62 152.38 o 21 2 1 365.26 263.29 173.10 o 22 2 1 0.07 22.57 276.00 o 23 2 1 29.14 -193.80 193.80 o -24 3 1 7.61 -87.47 261.14 o -23 3 1 13.38 0.00 328.49 o -22 3 1 2.42 -154.42 154.42 o -21 3 1 3.64 -220.09 220.09 o -20 3 1 4507.95 4513.94 285.45 o -19 3 1 0.78 -96.68 102.49 o -18 3 1 1757.61 1921.14 150.79 o -17 3 1 183.87 273.55 82.73 o -16 3 1 7318.13 8080.96 327.02 o -15 3 1 786.37 891.57 100.73 o -14 3 1 10269.63 11044.76 269.40 o -13 3 1 7.86 -51.01 59.10 o -12 3 1 19.80 46.18 50.09 o -11 3 1 101.55 100.54 41.30 o -10 3 1 883.48 857.87 69.92 o -9 3 1 2586.55 2791.54 95.90 o -8 3 1 6801.07 6780.27 323.00 o -7 3 1 215.18 282.65 32.86 o -6 3 1 1255.55 1451.99 41.14 o -5 3 1 147.96 152.08 32.68 o -4 3 1 42995.38 42225.14 1622.51 o -3 3 1 5696.16 5940.96 209.57 o -2 3 1 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