#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/13/2011352.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011352_Fobs loop_ _publ_author_name 'Gainsford, Graeme J.' 'Tyler, Peter C.' 'Furneaux, Richard H.' _publ_section_title ; 1,7,8-Tri-O-acetyl-6-O-benzoylcastanospermine ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first e394 _journal_page_last e395 _journal_volume 56 _journal_year 2000 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.0040 _cell_length_b 7.6750 _cell_length_c 45.5640 _exptl_crystal_F_000 888.00 _reflns_d_resolution_high 0.8411 _[local]_cod_data_source_file qa0363Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C45B P TYLER Post Acta review 22/6/2000 (reduce data/para ratio)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 147.62 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1476.19 1413.88 28.86 o 4 0 0 2083.30 1995.01 49.11 o 1 1 0 5820.08 5048.68 39.80 o 2 1 0 136.49 120.67 15.50 o 3 1 0 811.28 823.19 29.17 o 4 1 0 568.53 583.63 30.57 o 5 1 0 67.70 75.74 23.83 o 6 1 0 50.46 79.76 25.94 o 0 2 0 652.80 606.91 21.47 o 1 2 0 403.56 383.53 19.10 o 2 2 0 2075.81 2051.93 37.59 o 3 2 0 2751.58 2664.14 50.33 o 4 2 0 15.93 51.67 18.79 o 5 2 0 155.14 159.62 28.05 o 6 2 0 110.88 143.04 27.79 o 1 3 0 1054.14 968.37 28.41 o 2 3 0 286.51 270.99 22.54 o 3 3 0 176.06 166.24 21.67 o 4 3 0 1581.34 1595.67 49.72 o 0 4 0 68.08 68.35 16.12 o 1 4 0 607.81 581.62 27.52 o 2 4 0 923.14 797.21 31.04 o 3 4 0 152.87 158.05 23.73 o 4 4 0 251.81 215.13 29.82 o 5 4 0 226.65 179.88 30.89 o 1 5 0 1988.52 2039.73 50.60 o 2 5 0 174.05 165.44 25.62 o 3 5 0 77.16 95.48 25.95 o 4 5 0 159.44 149.82 26.15 o 5 5 0 254.89 296.85 30.38 o 0 6 0 1832.71 2088.75 54.99 o 1 6 0 107.53 121.12 26.71 o 2 6 0 262.36 261.85 32.23 o 3 6 0 408.71 381.91 35.68 o 3 7 0 327.33 326.51 38.99 o 1 0 1 2740.36 2632.12 26.61 o 2 0 1 21.96 52.72 13.56 o 3 0 1 139.03 103.76 17.96 o 4 0 1 583.63 544.22 30.49 o 6 0 1 314.83 323.89 31.36 o 0 1 1 409.59 379.08 11.31 o 1 1 1 3702.29 3386.28 33.80 o 2 1 1 565.54 569.18 20.79 o 3 1 1 192.27 204.61 19.88 o 4 1 1 878.36 965.78 36.10 o 5 1 1 63.32 86.19 25.62 o 6 1 1 138.05 107.60 28.84 o 0 2 1 18407.44 17623.05 79.87 o 1 2 1 4501.24 4288.13 44.83 o 2 2 1 122.17 82.38 16.19 o 3 2 1 404.99 435.56 24.68 o 4 2 1 163.20 140.08 23.57 o 5 2 1 514.78 449.09 35.61 o 0 3 1 66.82 78.29 15.05 o 1 3 1 1936.55 1917.93 36.34 o 2 3 1 334.12 337.85 21.35 o 3 3 1 82.31 88.90 19.37 o 4 3 1 407.47 398.30 29.81 o 5 3 1 368.39 352.50 31.94 o 0 4 1 202.36 197.84 19.26 o 1 4 1 224.78 273.38 21.27 o 2 4 1 286.50 270.31 22.17 o 3 4 1 53.37 66.98 20.88 o 4 4 1 360.65 318.31 30.72 o 5 4 1 260.42 278.55 33.24 o 6 4 1 94.19 81.63 32.24 o 0 5 1 132.67 124.11 19.88 o 1 5 1 915.82 924.33 36.58 o 2 5 1 109.90 66.98 25.47 o 3 5 1 344.75 341.67 30.68 o 1 6 1 406.69 472.24 33.36 o 2 6 1 1095.12 1213.99 48.43 o 3 6 1 661.24 670.86 41.37 o 1 7 1 134.93 165.97 27.26 o 2 7 1 248.53 317.57 33.64 o 0 8 1 60.54 85.80 29.59 o 1 8 1 135.38 193.49 30.01 o 1 0 2 13096.15 12559.32 55.80 o 2 0 2 444.14 452.61 19.86 o 3 0 2 489.42 483.58 23.27 o 4 0 2 513.22 530.28 29.62 o 5 0 2 95.46 100.61 29.97 o 0 1 2 11106.38 10817.80 45.31 o 1 1 2 7988.30 7264.80 47.74 o 2 1 2 1668.29 1613.12 31.66 o 3 1 2 823.20 838.74 30.04 o 4 1 2 230.38 224.35 24.86 o 5 1 2 1512.43 1459.49 50.72 o 6 1 2 377.59 428.66 33.93 o 0 2 2 1208.40 1193.84 25.81 o 1 2 2 5808.43 5434.62 50.47 o 2 2 2 1454.60 1438.95 32.27 o 3 2 2 1173.54 1280.66 37.12 o 4 2 2 400.81 387.60 28.18 o 5 2 2 970.49 938.90 43.86 o 6 2 2 223.17 215.74 31.39 o 0 3 2 310.75 313.89 19.11 o 1 3 2 524.19 545.67 22.78 o 2 3 2 1004.78 929.39 30.99 o 3 3 2 1028.48 1088.06 36.95 o 4 3 2 662.48 614.09 33.93 o 5 3 2 209.95 165.44 28.55 o 0 4 2 1830.32 1784.95 40.32 o 1 4 2 1007.38 1079.86 33.40 o 2 4 2 97.02 98.34 18.93 o 3 4 2 263.28 269.62 24.87 o 4 4 2 240.13 219.41 26.73 o 5 4 2 1103.87 951.65 46.72 o 6 4 2 133.19 159.36 31.16 o 0 5 2 72.92 85.61 19.39 o 1 5 2 266.72 267.24 27.47 o 2 5 2 1099.51 1066.27 40.65 o 3 5 2 356.47 391.70 30.79 o 5 5 2 109.04 103.12 27.60 o 1 6 2 394.72 370.24 30.74 o 2 6 2 207.98 181.84 31.89 o 3 6 2 423.82 418.42 34.37 o 4 6 2 103.13 103.97 28.77 o 0 7 2 561.75 578.13 36.41 o 1 7 2 159.07 206.69 26.84 o 2 7 2 106.62 147.04 27.17 o 4 7 2 125.53 113.48 33.59 o 1 0 3 7545.72 7238.30 42.36 o 2 0 3 94.61 73.23 14.20 o 4 0 3 77.51 74.84 20.82 o 5 0 3 1537.27 1424.04 57.15 o 7 0 3 274.66 318.68 34.81 o 1 1 3 17510.49 16517.31 71.99 o 2 1 3 52.26 38.09 14.34 o 3 1 3 2073.35 2084.01 43.56 o 4 1 3 522.39 521.71 31.27 o 5 1 3 370.65 367.05 32.19 o 6 1 3 167.49 147.04 31.44 o 7 1 3 27.76 82.38 24.10 o 0 2 3 1674.53 1724.12 29.29 o 1 2 3 1611.64 1552.87 29.43 o 2 2 3 537.96 495.98 22.18 o 3 2 3 101.58 86.19 19.07 o 4 2 3 1007.02 967.72 37.43 o 5 2 3 551.21 536.03 35.06 o 0 3 3 267.63 236.95 19.16 o 1 3 3 119.75 146.03 16.30 o 2 3 3 827.49 850.19 29.64 o 3 3 3 95.73 80.69 19.01 o 4 3 3 349.42 314.25 27.58 o 5 3 3 294.80 240.48 31.53 o 0 4 3 1036.76 1054.78 32.34 o 1 4 3 457.91 443.83 24.48 o 2 4 3 537.91 559.82 27.49 o 4 4 3 132.46 94.06 26.36 o 2 5 3 289.58 282.03 28.22 o 3 5 3 261.35 289.04 29.63 o 4 5 3 671.83 640.58 40.96 o 2 6 3 1454.89 1552.87 53.96 o 3 6 3 32.38 71.64 23.88 o 4 6 3 54.64 75.20 25.55 o 5 6 3 88.38 112.82 28.43 o 0 7 3 125.27 127.37 26.92 o 1 7 3 400.15 408.71 34.39 o 2 7 3 221.03 229.67 32.70 o 0 8 3 193.69 261.51 28.85 o 3 8 3 124.46 96.09 32.54 o 1 0 4 403.41 400.78 14.54 o 3 0 4 354.77 357.97 21.98 o 4 0 4 2176.09 2160.46 51.11 o 5 0 4 2760.25 2679.16 66.58 o 0 1 4 545.11 517.93 14.16 o 1 1 4 6316.72 5987.90 44.95 o 2 1 4 1230.64 1189.54 28.62 o 3 1 4 709.78 743.67 28.29 o 4 1 4 1016.65 1067.62 37.96 o 5 1 4 81.04 80.13 24.14 o 6 1 4 182.15 188.33 32.74 o 0 2 4 18938.94 18892.70 85.55 o 1 2 4 93.59 109.76 15.00 o 2 2 4 1824.81 1876.37 36.84 o 3 2 4 1004.31 1069.66 34.60 o 4 2 4 99.38 94.67 22.00 o 0 3 4 157.19 151.09 16.32 o 1 3 4 214.14 218.49 17.17 o 2 3 4 816.87 786.70 28.51 o 4 3 4 248.42 278.55 27.35 o 5 3 4 478.65 480.85 33.66 o 1 4 4 1011.42 1018.05 33.10 o 2 4 4 363.15 380.29 24.27 o 3 4 4 77.67 74.12 23.58 o 4 4 4 149.06 111.94 27.22 o 5 4 4 138.02 140.81 27.08 o 6 4 4 163.17 203.72 34.35 o 0 5 4 82.07 82.57 19.79 o 1 5 4 758.62 789.61 34.39 o 2 5 4 408.30 368.25 29.86 o 3 5 4 459.69 506.66 34.09 o 4 5 4 510.07 462.38 36.13 o 0 6 4 124.07 125.50 25.10 o 1 6 4 37.81 75.92 22.41 o 2 6 4 845.49 834.54 41.95 o 3 6 4 414.31 418.42 34.37 o 4 6 4 145.26 213.91 27.91 o 0 7 4 127.81 134.97 28.20 o 2 7 4 71.50 98.54 24.09 o 3 7 4 319.24 279.59 35.38 o 1 8 4 48.49 85.04 25.64 o 1 0 5 3333.69 3199.39 31.68 o 2 0 5 118.06 102.28 15.11 o 3 0 5 562.80 551.99 25.35 o 4 0 5 686.10 651.13 32.82 o 5 0 5 516.35 557.86 35.28 o 6 0 5 295.48 352.50 35.05 o 0 1 5 580.39 578.13 15.46 o 1 1 5 9786.97 9336.04 56.13 o 2 1 5 1515.73 1481.76 31.14 o 3 1 5 771.24 783.80 29.04 o 4 1 5 291.17 319.79 26.34 o 5 1 5 1306.11 1341.50 47.87 o 6 1 5 369.60 388.83 37.64 o 0 2 5 17242.60 17011.54 83.88 o 1 2 5 2827.93 2798.58 37.31 o 2 2 5 394.06 438.17 21.28 o 3 2 5 1856.91 1782.32 42.92 o 4 2 5 36.59 51.38 19.48 o 6 2 5 284.73 274.76 33.36 o 0 3 5 6372.82 6414.22 63.14 o 1 3 5 462.78 469.99 22.94 o 2 3 5 1415.29 1330.89 35.57 o 3 3 5 219.21 196.97 21.84 o 4 3 5 530.68 532.19 32.54 o 5 3 5 387.31 381.91 33.24 o 0 4 5 1646.47 1746.59 40.75 o 1 4 5 706.13 670.33 29.00 o 2 4 5 425.57 382.72 26.38 o 3 4 5 33.91 60.04 19.13 o 4 4 5 271.31 265.21 29.06 o 0 5 5 348.89 348.22 26.71 o 1 5 5 277.32 273.73 26.09 o 2 5 5 109.99 115.48 22.52 o 3 5 5 745.99 811.33 40.18 o 4 5 5 261.11 284.12 30.77 o 5 5 5 193.58 167.04 31.64 o 0 6 5 132.29 134.25 26.20 o 3 6 5 253.28 244.36 35.02 o 4 6 5 152.43 197.26 27.97 o 1 7 5 114.84 113.04 27.79 o 3 7 5 185.85 188.04 32.15 o 0 8 5 187.57 222.18 30.61 o 1 8 5 59.79 86.96 25.34 o 2 8 5 93.88 78.47 29.59 o 3 8 5 75.45 84.46 29.55 o 0 0 6 2737.21 2695.29 23.69 o 1 0 6 104.86 97.51 13.32 o 2 0 6 479.15 411.66 19.78 o 3 0 6 140.39 187.48 17.90 o 5 0 6 280.37 240.48 30.88 o 6 0 6 1347.25 1313.54 55.64 o 1 1 6 6353.10 5879.23 46.13 o 2 1 6 644.30 628.04 21.84 o 3 1 6 1266.46 1415.44 37.46 o 4 1 6 1005.49 1023.35 37.83 o 5 1 6 47.88 61.01 23.50 o 6 1 6 582.34 583.13 41.08 o 0 2 6 80.94 62.48 15.58 o 1 2 6 1313.22 1291.82 27.59 o 2 2 6 285.72 290.80 19.46 o 3 2 6 283.39 340.52 23.35 o 4 2 6 194.72 197.84 24.51 o 5 2 6 226.51 187.19 28.10 o 6 2 6 121.21 142.79 30.24 o 0 3 6 133.39 120.44 16.85 o 1 3 6 155.96 152.62 17.17 o 2 3 6 1715.20 1729.29 39.68 o 3 3 6 132.35 138.36 20.74 o 5 3 6 98.00 99.16 26.24 o 0 4 6 7841.63 8084.15 82.07 o 1 4 6 402.91 371.44 25.19 o 2 4 6 1035.33 966.43 34.18 o 3 4 6 307.12 333.67 27.66 o 4 4 6 669.82 595.72 37.98 o 5 4 6 44.34 61.17 24.01 o 0 5 6 484.41 521.71 29.85 o 1 5 6 262.19 277.52 25.92 o 2 5 6 596.28 554.43 33.71 o 3 5 6 266.62 266.57 28.45 o 4 5 6 100.33 97.11 24.53 o 0 6 6 109.26 93.66 24.09 o 1 6 6 184.88 183.52 27.26 o 2 6 6 136.83 108.24 27.20 o 3 6 6 902.47 896.17 45.34 o 1 7 6 163.56 216.65 27.48 o 2 7 6 26.78 60.68 23.92 o 3 7 6 200.70 188.61 31.63 o 4 7 6 146.38 170.55 31.70 o 0 8 6 123.13 159.88 28.33 o 2 8 6 128.65 151.86 31.19 o 2 0 7 184.18 183.80 16.03 o 3 0 7 1194.83 1158.27 33.89 o 4 0 7 302.21 298.64 24.74 o 0 1 7 2335.09 2377.81 28.33 o 1 1 7 5148.07 4922.71 43.67 o 2 1 7 340.55 336.33 18.64 o 3 1 7 3217.68 3450.56 54.84 o 4 1 7 365.61 326.88 25.51 o 5 1 7 579.62 629.09 35.90 o 6 1 7 304.49 264.20 35.41 o 0 2 7 168.70 153.65 16.72 o 1 2 7 7188.34 7096.04 59.42 o 2 2 7 2540.02 2518.42 41.64 o 3 2 7 900.39 873.34 32.49 o 4 2 7 97.06 91.86 20.68 o 0 3 7 1862.46 1899.80 36.17 o 1 3 7 1076.68 1114.91 31.17 o 2 3 7 756.37 781.47 28.42 o 3 3 7 140.16 119.08 19.47 o 4 3 7 219.58 207.89 26.32 o 0 4 7 106.64 153.14 19.25 o 1 4 7 3783.04 3768.31 58.58 o 2 4 7 835.93 902.39 33.03 o 3 4 7 372.69 329.14 28.60 o 4 4 7 297.98 271.67 31.12 o 5 4 7 109.92 105.03 26.79 o 0 5 7 604.07 581.62 30.02 o 1 5 7 1024.85 1060.86 37.84 o 2 5 7 374.63 399.54 29.03 o 1 6 7 103.57 101.03 25.86 o 2 6 7 308.76 277.86 31.81 o 3 6 7 358.14 426.52 33.85 o 4 6 7 140.83 136.66 27.89 o 0 7 7 307.73 342.06 31.46 o 2 7 7 90.06 110.85 27.30 o 2 8 7 97.99 131.62 27.61 o 0 0 8 652.08 607.93 15.86 o 1 0 8 888.37 865.38 21.97 o 5 0 8 720.48 737.46 40.00 o 6 0 8 237.04 282.38 33.12 o 1 1 8 4903.84 4572.55 43.49 o 3 1 8 1169.50 1185.25 34.28 o 4 1 8 188.25 173.82 22.70 o 5 1 8 57.83 71.12 24.84 o 6 1 8 103.50 116.82 26.91 o 0 2 8 3941.54 4041.81 44.84 o 1 2 8 751.78 695.81 22.44 o 2 2 8 1461.60 1502.60 33.78 o 3 2 8 504.87 472.69 25.26 o 5 2 8 160.12 177.94 25.74 o 0 3 8 232.62 265.89 18.27 o 1 3 8 3486.98 3457.88 50.02 o 2 3 8 186.78 190.04 18.88 o 3 3 8 109.41 117.27 21.57 o 4 3 8 93.99 68.17 25.69 o 0 4 8 1677.59 1709.51 40.31 o 1 4 8 2983.11 3030.37 53.68 o 2 4 8 264.63 237.59 23.66 o 0 5 8 185.34 199.60 24.03 o 1 5 8 286.21 283.42 25.85 o 2 5 8 134.26 130.43 25.11 o 4 5 8 283.44 208.49 31.45 o 1 6 8 97.55 97.92 28.33 o 2 6 8 264.42 289.04 31.39 o 3 6 8 106.36 124.80 27.35 o 1 7 8 96.41 101.24 24.84 o 2 7 8 82.49 75.92 28.20 o 3 7 8 474.10 512.75 38.99 o 0 8 8 84.42 87.35 27.92 o 1 0 9 10444.32 10295.61 61.05 o 2 0 9 199.97 200.77 17.05 o 3 0 9 537.85 568.19 25.71 o 4 0 9 107.29 131.38 22.59 o 5 0 9 974.47 998.29 43.92 o 6 0 9 115.57 132.81 26.54 o 0 1 9 253.83 294.35 16.73 o 2 1 9 884.84 886.26 25.94 o 3 1 9 102.43 102.49 18.90 o 4 1 9 340.75 327.63 27.41 o 5 1 9 195.27 163.31 26.51 o 6 1 9 705.81 731.83 46.02 o 0 2 9 2370.59 2376.80 36.41 o 1 2 9 1900.58 1919.75 33.63 o 2 2 9 5597.85 5769.99 64.61 o 3 2 9 193.39 217.26 21.10 o 4 2 9 195.91 229.67 22.95 o 6 2 9 181.09 196.38 31.40 o 0 3 9 1234.79 1265.86 31.00 o 1 3 9 1028.12 1057.48 31.03 o 2 3 9 44.90 42.98 16.32 o 4 3 9 486.38 547.61 31.07 o 5 3 9 130.93 127.83 25.80 o 1 4 9 1309.08 1339.23 37.96 o 2 4 9 1263.56 1218.34 39.10 o 3 4 9 198.49 222.18 24.74 o 0 5 9 548.47 512.75 29.13 o 2 5 9 318.38 325.76 28.08 o 3 5 9 288.52 221.56 30.57 o 4 5 9 92.79 83.13 27.43 o 2 6 9 576.08 584.63 36.62 o 3 6 9 421.17 466.40 37.63 o 4 6 9 271.29 263.53 32.33 o 0 7 9 126.95 79.95 27.64 o 1 7 9 104.51 134.73 26.97 o 3 7 9 130.22 115.04 30.48 o 4 7 9 161.56 180.44 29.82 o 3 8 9 46.13 75.38 27.38 o 0 0 10 5090.59 5150.90 41.69 o 1 0 10 163.28 166.24 16.32 o 2 0 10 2817.63 2871.48 42.24 o 3 0 10 2234.32 2283.67 46.60 o 5 0 10 770.91 756.74 40.52 o 6 0 10 169.28 193.78 29.46 o 0 1 10 1683.59 1718.96 28.38 o 1 1 10 792.89 765.32 22.38 o 2 1 10 4411.13 4368.66 52.11 o 3 1 10 258.03 236.32 22.01 o 4 1 10 73.35 76.28 20.66 o 5 1 10 341.67 401.62 32.01 o 6 1 10 279.83 280.29 36.12 o 0 2 10 132.28 151.34 15.82 o 1 2 10 342.87 332.91 19.30 o 2 2 10 3016.96 3045.23 46.94 o 3 2 10 136.81 146.53 19.34 o 4 2 10 218.53 205.80 24.11 o 5 2 10 261.51 274.07 27.82 o 0 3 10 273.33 296.49 18.93 o 1 3 10 638.59 679.49 27.04 o 2 3 10 1203.04 1251.87 35.23 o 5 3 10 117.05 145.28 26.51 o 6 3 10 215.62 275.10 33.72 o 0 4 10 2396.61 2316.50 46.93 o 1 4 10 247.20 241.45 22.24 o 3 4 10 19.78 79.76 21.49 o 5 4 10 130.08 177.67 26.82 o 1 5 10 453.87 452.61 29.57 o 3 5 10 687.62 703.49 41.27 o 4 5 10 394.17 423.53 34.16 o 1 6 10 207.53 235.36 28.01 o 2 6 10 53.33 76.64 23.07 o 3 6 10 236.56 226.22 30.27 o 4 6 10 70.66 73.77 26.91 o 2 7 10 55.74 73.41 25.06 o 4 7 10 68.49 78.84 30.39 o 1 8 10 84.37 147.54 28.22 o 1 0 11 113.89 160.15 14.96 o 2 0 11 212.12 232.50 18.03 o 3 0 11 25.71 46.02 16.33 o 4 0 11 184.06 167.31 24.69 o 5 0 11 176.79 167.85 27.15 o 0 1 11 6604.53 6745.71 52.82 o 1 1 11 582.37 539.87 20.73 o 2 1 11 1293.58 1374.38 31.53 o 3 1 11 46.78 49.61 16.36 o 4 1 11 57.92 71.82 18.99 o 5 1 11 221.91 236.00 28.36 o 6 1 11 208.28 173.27 30.58 o 1 2 11 585.81 601.30 22.38 o 2 2 11 237.51 261.18 20.79 o 3 2 11 1488.99 1627.32 43.52 o 4 2 11 96.38 99.99 23.23 o 5 2 11 65.71 73.06 21.99 o 6 2 11 172.49 170.82 30.37 o 0 3 11 306.30 336.33 20.16 o 1 3 11 892.90 940.80 29.91 o 2 3 11 406.45 409.13 23.92 o 3 3 11 520.39 570.67 30.73 o 4 3 11 134.79 133.77 24.71 o 6 3 11 88.28 82.57 31.86 o 1 4 11 30.48 49.61 17.53 o 2 4 11 719.60 659.63 31.97 o 3 4 11 893.64 933.82 39.31 o 4 4 11 239.33 168.39 28.27 o 5 4 11 117.63 101.03 28.98 o 0 5 11 133.14 159.88 23.08 o 1 5 11 275.03 284.12 28.67 o 2 5 11 638.00 653.25 34.47 o 3 5 11 952.79 980.67 46.13 o 4 5 11 224.44 151.60 29.37 o 1 6 11 97.72 109.54 25.62 o 2 6 11 46.05 84.27 22.28 o 3 6 11 269.18 305.49 31.91 o 1 7 11 44.39 57.65 23.00 o 0 8 11 462.15 430.38 40.03 o 2 8 11 81.04 138.12 27.31 o 0 0 12 21792.06 22844.18 90.93 o 1 0 12 660.55 707.35 22.62 o 2 0 12 3437.67 3759.40 49.61 o 3 0 12 85.46 98.13 17.47 o 5 0 12 487.79 431.68 35.34 o 6 0 12 183.42 189.75 26.01 o 0 1 12 3778.34 3708.69 41.69 o 1 1 12 4400.23 4409.89 46.84 o 2 1 12 419.31 415.45 20.72 o 3 1 12 1320.85 1348.35 38.09 o 4 1 12 128.38 141.06 22.18 o 5 1 12 117.19 96.90 25.32 o 6 1 12 178.50 157.53 28.64 o 0 2 12 451.95 457.04 20.85 o 1 2 12 1884.40 1862.91 34.92 o 3 2 12 1458.86 1531.69 42.22 o 4 2 12 104.64 108.03 23.29 o 0 3 12 241.09 248.92 17.67 o 1 3 12 1035.47 1016.07 31.08 o 2 3 12 47.81 53.63 17.62 o 3 3 12 386.19 386.38 27.73 o 4 3 12 433.19 443.39 31.45 o 6 3 12 116.11 134.73 26.73 o 0 4 12 697.70 713.98 28.83 o 1 4 12 928.44 909.88 33.79 o 2 4 12 767.91 733.52 31.46 o 3 4 12 61.71 81.63 22.87 o 4 4 12 81.83 105.24 25.11 o 1 5 12 141.52 129.01 24.27 o 2 5 12 390.42 345.52 30.08 o 3 5 12 264.65 246.31 28.65 o 4 5 12 55.92 85.04 26.21 o 0 6 12 79.04 77.19 24.79 o 1 6 12 372.95 328.01 31.19 o 2 6 12 495.86 504.79 34.03 o 2 7 12 63.65 74.48 26.68 o 3 7 12 135.62 118.85 31.89 o 1 0 13 933.83 956.14 25.02 o 2 0 13 2696.52 2700.67 43.12 o 3 0 13 423.05 372.64 25.23 o 5 0 13 280.74 266.23 30.13 o 0 1 13 1406.62 1437.38 28.32 o 1 1 13 1208.56 1235.78 27.71 o 2 1 13 2263.62 2373.77 41.44 o 3 1 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349.39 27.53 o 4 1 20 525.45 506.19 32.67 o 5 1 20 550.76 516.04 37.70 o 6 1 20 0.36 69.90 24.80 o 0 2 20 102.43 73.77 17.82 o 1 2 20 143.94 148.30 19.20 o 2 2 20 483.93 448.21 25.91 o 4 2 20 215.73 182.96 26.38 o 5 2 20 233.06 235.36 28.64 o 0 3 20 515.11 518.87 26.46 o 1 3 20 874.57 896.17 33.54 o 2 3 20 356.95 352.11 27.64 o 3 3 20 135.35 68.86 24.27 o 4 3 20 281.33 313.15 33.04 o 0 4 20 663.55 680.03 32.46 o 1 4 20 139.98 164.11 22.32 o 3 4 20 186.53 217.87 26.33 o 5 4 20 232.59 118.62 35.70 o 1 5 20 119.62 125.50 24.64 o 2 5 20 102.50 105.67 25.59 o 3 5 20 60.80 76.10 21.72 o 0 6 20 143.84 179.61 28.08 o 2 6 20 214.19 209.69 30.64 o 3 6 20 148.92 176.56 27.57 o 4 6 20 177.29 120.44 31.87 o 0 7 20 498.66 550.04 37.46 o 1 7 20 169.87 136.18 31.23 o 2 7 20 36.09 71.47 26.48 o 1 0 21 2785.24 2982.59 47.59 o 2 0 21 1150.46 1115.60 33.95 o 3 0 21 349.97 343.98 25.78 o 5 0 21 785.51 776.26 42.19 o 1 1 21 2484.27 2484.18 46.53 o 3 1 21 108.33 91.47 21.82 o 4 1 21 120.60 123.42 24.66 o 6 1 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28.42 o 0 2 22 791.54 908.01 31.88 o 1 2 22 638.20 613.06 26.71 o 2 2 22 146.16 99.57 20.70 o 3 2 22 704.60 680.03 35.16 o 4 2 22 367.60 335.95 30.42 o 5 2 22 205.41 173.82 28.99 o 0 3 22 116.96 102.49 21.21 o 1 3 22 400.52 381.10 27.13 o 3 3 22 195.42 186.62 25.51 o 4 3 22 286.75 278.55 28.74 o 5 3 22 85.07 106.31 27.38 o 6 3 22 111.85 134.97 34.71 o 1 4 22 59.68 94.26 20.95 o 4 4 22 243.19 219.10 31.94 o 5 4 22 59.41 75.56 27.41 o 1 5 22 369.05 301.87 31.72 o 2 5 22 55.26 65.63 24.37 o 0 6 22 223.17 192.34 30.21 o 1 6 22 92.32 91.66 25.03 o 2 6 22 319.45 329.14 32.74 o 3 6 22 102.40 104.39 26.28 o 1 7 22 238.09 223.42 33.49 o 1 8 22 101.87 86.57 32.04 o 1 0 23 1019.11 1040.01 32.11 o 3 0 23 178.88 139.34 22.53 o 4 0 23 528.14 571.66 34.23 o 5 0 23 268.97 328.38 31.95 o 6 0 23 178.71 217.26 33.64 o 0 1 23 5382.62 5378.18 71.51 o 3 1 23 66.84 94.87 20.61 o 4 1 23 66.67 91.27 25.76 o 6 1 23 69.70 83.89 27.74 o 0 2 23 390.19 426.52 26.56 o 2 2 23 217.95 203.13 23.65 o 3 2 23 175.61 201.95 25.06 o 1 3 23 774.42 833.34 34.74 o 2 3 23 106.24 81.81 21.77 o 3 3 23 121.28 106.10 25.64 o 4 3 23 195.53 100.20 30.32 o 5 3 23 35.08 64.29 24.95 o 6 3 23 80.59 126.20 29.13 o 0 4 23 796.94 841.15 37.30 o 4 4 23 153.04 117.50 31.26 o 5 4 23 186.43 152.88 34.63 o 2 5 23 564.71 491.37 36.33 o 3 5 23 323.15 301.51 29.54 o 0 6 23 149.67 191.19 26.10 o 1 6 23 117.45 146.53 27.37 o 2 6 23 150.41 100.61 31.21 o 0 0 24 6469.25 7489.30 77.20 o 1 0 24 816.02 858.68 31.00 o 2 0 24 146.83 143.04 19.85 o 4 0 24 685.63 634.82 38.16 o 0 1 24 8979.94 9784.29 90.29 o 1 1 24 357.66 373.04 22.84 o 2 1 24 342.84 331.02 25.67 o 5 1 24 169.90 185.49 27.41 o 1 2 24 227.79 199.89 21.70 o 2 2 24 1372.98 1457.90 42.77 o 4 2 24 164.88 126.43 25.66 o 5 2 24 169.62 187.19 28.95 o 0 3 24 458.54 459.70 28.02 o 1 3 24 598.28 626.49 31.67 o 2 3 24 71.94 61.01 21.39 o 4 3 24 70.34 58.44 22.84 o 5 3 24 207.34 222.18 34.32 o 1 4 24 539.05 572.16 32.75 o 2 4 24 291.37 259.50 28.07 o 4 4 24 200.29 148.80 33.91 o 0 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o 2 0 27 300.29 281.68 25.07 o 3 0 27 456.72 465.06 31.32 o 5 0 27 118.73 75.38 27.74 o 6 0 27 217.44 161.20 32.92 o 0 1 27 1096.42 1110.76 35.95 o 1 1 27 497.84 467.74 29.16 o 2 1 27 412.78 352.50 28.82 o 3 1 27 370.22 400.78 31.15 o 4 1 27 342.49 334.81 33.40 o 5 1 27 282.98 270.99 31.76 o 0 2 27 1830.48 1799.00 47.52 o 1 2 27 242.87 172.45 28.33 o 2 2 27 67.64 86.19 21.76 o 3 2 27 731.59 682.74 39.03 o 4 2 27 396.71 407.46 33.50 o 5 2 27 107.36 94.47 30.25 o 0 3 27 879.45 847.78 40.47 o 1 3 27 180.37 119.30 27.64 o 2 3 27 284.67 254.18 28.78 o 3 3 27 223.55 193.78 29.75 o 4 3 27 282.84 301.87 32.08 o 1 4 27 109.59 75.38 28.10 o 2 4 27 44.84 60.36 23.69 o 4 4 27 397.52 367.05 36.17 o 5 4 27 120.93 132.81 32.51 o 0 5 27 136.47 173.82 27.08 o 2 5 27 349.06 325.38 34.43 o 0 6 27 163.86 195.51 30.46 o 1 6 27 33.89 89.89 21.24 o 2 7 27 168.15 182.12 31.64 o 0 0 28 608.60 586.64 28.14 o 1 0 28 505.86 509.00 27.61 o 2 0 28 1689.54 1685.58 45.99 o 3 0 28 541.11 537.47 33.67 o 4 0 28 472.28 461.48 35.21 o 6 0 28 56.41 82.76 28.31 o 0 1 28 99.41 135.69 21.51 o 1 1 28 220.12 219.10 22.42 o 2 1 28 296.72 277.52 26.96 o 3 1 28 566.25 548.10 33.51 o 4 1 28 295.14 267.58 29.86 o 6 1 28 39.85 75.20 25.55 o 0 2 28 1149.20 1064.24 43.99 o 1 2 28 507.82 472.69 30.67 o 2 2 28 660.65 646.90 33.24 o 3 2 28 460.42 495.51 36.02 o 4 2 28 320.06 321.65 32.37 o 5 2 28 84.82 72.88 27.81 o 0 3 28 275.74 204.61 29.97 o 2 3 28 893.67 822.00 40.45 o 3 3 28 650.31 569.18 39.60 o 4 3 28 105.03 127.13 24.79 o 5 3 28 120.15 168.12 29.05 o 0 4 28 1.33 57.18 21.49 o 1 4 28 218.94 187.48 30.96 o 2 4 28 833.32 806.02 40.05 o 3 4 28 130.69 92.26 28.50 o 0 5 28 144.55 173.27 28.95 o 1 5 28 542.04 543.25 37.23 o 2 5 28 430.23 339.38 35.93 o 3 5 28 87.28 93.26 27.65 o 1 6 28 89.74 117.95 25.68 o 0 7 28 217.70 152.11 34.54 o 1 0 29 2.60 47.44 17.86 o 2 0 29 95.68 125.27 22.52 o 3 0 29 69.73 120.21 23.66 o 5 0 29 118.27 119.53 28.35 o 6 0 29 68.06 79.76 31.13 o 0 1 29 373.44 450.85 30.39 o 2 1 29 37.77 53.02 20.09 o 3 1 29 798.12 768.19 39.10 o 4 1 29 127.30 116.38 26.86 o 0 2 29 216.33 163.05 29.93 o 1 2 29 1959.30 1999.64 51.02 o 2 2 29 263.86 273.04 28.11 o 3 2 29 338.16 382.31 34.48 o 0 3 29 960.39 871.50 41.03 o 1 3 29 223.36 241.12 27.38 o 2 3 29 1008.78 884.41 44.42 o 3 3 29 678.38 656.43 39.33 o 4 3 29 154.18 186.91 30.06 o 5 3 29 16.33 66.47 25.37 o 0 4 29 387.52 364.28 32.47 o 1 4 29 704.22 652.19 40.27 o 5 4 29 122.62 88.51 32.01 o 3 5 29 35.69 65.63 25.21 o 0 6 29 118.36 151.34 28.33 o 2 6 29 65.53 100.20 24.50 o 0 7 29 250.02 222.49 35.90 o 0 0 30 1698.47 1757.88 46.10 o 1 0 30 273.95 305.13 24.64 o 2 0 30 239.09 265.21 26.01 o 3 0 30 127.90 117.05 27.61 o 4 0 30 360.90 409.13 34.83 o 0 1 30 1109.07 1168.88 40.43 o 1 1 30 791.87 861.73 35.32 o 2 1 30 217.44 216.35 25.94 o 3 1 30 691.23 693.07 38.78 o 4 1 30 86.20 70.07 27.09 o 0 2 30 184.93 174.91 26.34 o 1 2 30 94.51 123.42 26.27 o 2 2 30 473.51 429.09 33.52 o 3 2 30 795.49 883.17 42.54 o 4 2 30 387.61 377.06 34.24 o 0 3 30 530.76 511.81 37.08 o 2 3 30 157.59 111.94 31.17 o 3 3 30 212.92 205.50 31.52 o 4 3 30 65.16 66.81 26.11 o 5 3 30 93.43 123.42 28.12 o 0 4 30 197.49 159.88 29.90 o 1 4 30 489.47 449.97 39.61 o 2 4 30 96.18 71.64 25.81 o 4 4 30 194.66 133.53 33.80 o 2 5 30 289.44 332.15 30.63 o 3 5 30 254.20 266.91 33.89 o 1 6 30 180.48 189.47 30.55 o 2 7 30 88.76 117.05 30.75 o 3 0 31 488.16 504.33 34.01 o 4 0 31 146.19 122.96 28.53 o 0 1 31 70.52 145.78 23.04 o 1 1 31 558.69 598.25 31.97 o 2 1 31 735.76 726.79 35.79 o 3 1 31 795.63 743.67 39.60 o 4 1 31 310.28 275.45 32.71 o 0 2 31 213.08 223.11 26.96 o 1 2 31 195.16 211.19 25.32 o 2 2 31 811.55 848.99 39.90 o 3 2 31 245.20 213.31 31.51 o 4 2 31 69.43 83.70 24.86 o 5 2 31 178.52 164.37 31.92 o 1 3 31 1086.24 1046.71 44.30 o 2 3 31 158.52 103.12 29.70 o 4 3 31 155.18 132.81 29.88 o 5 3 31 76.29 86.19 30.43 o 1 4 31 646.46 630.13 40.62 o 2 4 31 919.97 898.03 42.90 o 3 4 31 163.58 156.75 29.09 o 1 5 31 387.39 358.36 33.77 o 2 5 31 137.89 97.31 32.33 o 1 7 31 158.13 188.90 32.22 o 0 0 32 21.77 54.85 19.05 o 1 0 32 38.66 72.00 20.24 o 3 0 32 110.62 115.26 25.84 o 4 0 32 223.56 254.51 31.11 o 0 1 32 205.05 234.72 24.79 o 1 1 32 1179.64 1118.37 40.93 o 2 1 32 1676.55 1721.54 50.79 o 5 1 32 308.46 339.38 37.45 o 0 2 32 63.17 68.35 22.12 o 1 2 32 723.45 767.62 36.79 o 2 2 32 1456.22 1352.16 48.06 o 3 2 32 176.85 156.49 29.33 o 5 2 32 95.31 77.92 29.30 o 1 3 32 682.66 649.54 40.18 o 2 3 32 1489.99 1351.40 51.10 o 4 3 32 121.93 76.28 28.27 o 5 3 32 208.13 193.20 34.31 o 0 4 32 290.85 317.57 31.79 o 1 4 32 198.19 125.73 31.17 o 3 4 32 286.99 233.45 34.87 o 2 5 32 123.43 79.39 28.65 o 4 5 32 142.01 103.55 33.99 o 1 6 32 126.54 137.63 28.23 o 1 0 33 77.99 64.62 22.68 o 2 0 33 701.87 680.03 37.33 o 3 0 33 35.25 73.77 21.56 o 4 0 33 76.14 99.57 23.60 o 0 1 33 147.81 154.42 23.20 o 1 1 33 247.50 284.47 27.64 o 2 1 33 257.25 288.33 31.00 o 3 1 33 728.93 710.11 41.46 o 4 1 33 86.75 95.68 25.37 o 5 1 33 118.67 93.86 30.95 o 0 2 33 276.31 299.72 28.73 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783.95 875.18 47.87 o 0 4 34 275.89 219.41 31.65 o 1 4 34 170.19 136.66 27.40 o 2 4 34 114.68 135.45 27.04 o 3 4 34 86.11 85.04 28.89 o 4 4 34 109.89 81.25 31.04 o 1 5 34 117.60 89.30 29.80 o 3 5 34 265.52 260.50 35.83 o 1 0 35 84.92 114.81 22.45 o 4 0 35 33.31 65.29 24.81 o 0 1 35 94.53 91.47 24.60 o 1 1 35 229.91 237.59 27.18 o 2 1 35 943.20 991.75 42.47 o 3 1 35 902.07 976.78 45.39 o 0 2 35 90.28 103.55 24.07 o 1 2 35 125.10 147.04 23.90 o 2 2 35 328.83 289.74 30.72 o 3 2 35 522.64 525.03 41.36 o 4 2 35 169.95 131.14 31.12 o 5 2 35 132.37 178.22 32.13 o 0 3 35 218.55 220.64 31.43 o 1 3 35 270.42 240.48 31.85 o 3 3 35 646.69 684.91 42.35 o 4 3 35 94.83 152.62 28.70 o 1 4 35 161.75 156.49 27.77 o 3 4 35 349.66 290.45 36.06 o 0 5 35 45.67 61.50 22.94 o 2 5 35 71.12 126.43 24.73 o 0 6 35 83.87 100.82 30.41 o 1 6 35 36.80 79.39 26.99 o 0 0 36 866.18 899.90 39.21 o 2 0 36 1033.67 1007.49 44.12 o 3 0 36 583.82 591.17 37.33 o 5 0 36 52.59 115.93 24.35 o 0 1 36 142.58 158.84 24.84 o 1 1 36 215.84 221.87 27.50 o 2 1 36 490.40 555.41 35.69 o 3 1 36 95.26 90.67 28.05 o 1 2 36 113.01 88.51 27.72 o 2 2 36 347.19 403.28 31.66 o 3 2 36 371.98 363.88 32.85 o 4 2 36 79.31 146.28 27.10 o 0 3 36 1.57 64.29 21.96 o 1 3 36 361.60 331.78 34.76 o 2 3 36 878.33 797.80 42.78 o 3 3 36 121.32 163.05 30.20 o 1 4 36 207.18 146.53 33.90 o 2 4 36 171.18 151.60 29.12 o 4 4 36 123.41 116.38 32.90 o 2 5 36 152.45 125.50 31.61 o 3 5 36 59.22 76.46 28.66 o 0 6 36 167.02 163.58 34.76 o 1 6 36 91.19 103.97 33.00 o 2 0 37 758.71 826.17 41.14 o 3 0 37 376.95 393.34 37.03 o 4 0 37 279.18 322.40 32.41 o 1 1 37 102.85 97.51 26.63 o 2 1 37 553.93 498.75 35.21 o 3 1 37 80.61 75.74 26.18 o 4 1 37 125.74 150.33 31.79 o 1 2 37 429.16 416.72 32.61 o 2 2 37 456.25 451.29 34.38 o 3 2 37 476.46 421.82 39.63 o 0 3 37 153.79 116.82 28.93 o 1 3 37 450.80 406.20 36.38 o 2 3 37 373.44 325.38 34.80 o 3 3 37 50.52 70.42 26.64 o 0 4 37 141.10 166.51 26.77 o 1 4 37 589.62 509.47 40.74 o 3 4 37 148.74 201.36 28.56 o 4 4 37 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39 102.04 116.15 27.72 o 3 0 40 902.12 914.27 47.05 o 1 1 40 178.06 186.62 26.92 o 2 1 40 71.75 71.82 25.67 o 3 1 40 173.82 219.41 32.27 o 1 2 40 106.64 168.93 26.15 o 2 3 40 364.88 367.45 35.39 o 3 3 40 216.84 266.57 30.15 o 4 3 40 159.35 204.91 32.07 o 1 4 40 176.99 197.26 31.18 o 2 4 40 385.35 412.50 37.92 o 0 5 40 326.22 335.95 31.94 o 1 1 41 166.55 152.11 28.15 o 3 1 41 125.65 94.06 30.78 o 0 2 41 125.24 118.17 24.81 o 1 2 41 142.38 153.14 29.52 o 4 2 41 45.04 73.23 26.27 o 0 3 41 251.95 276.48 32.43 o 1 3 41 219.10 206.69 33.70 o 2 3 41 148.66 122.73 29.19 o 3 3 41 80.15 94.06 28.97 o 4 3 41 67.14 76.64 29.60 o 0 4 41 132.67 128.30 28.90 o 3 4 41 55.31 90.28 29.37 o 0 0 42 128.91 128.77 26.13 o 3 0 42 63.75 103.34 25.73 o 4 0 42 109.21 115.26 33.19 o 1 1 42 123.04 158.05 25.04 o 2 1 42 163.84 142.30 27.96 o 3 1 42 44.27 76.83 27.09 o 4 1 42 94.60 102.49 28.77 o 2 2 42 333.18 333.29 32.57 o 4 2 42 46.39 91.07 25.93 o 0 3 42 146.72 219.41 29.81 o 1 3 42 336.16 291.87 34.38 o 2 3 42 149.66 163.84 32.66 o 3 3 42 76.79 99.99 29.66 o 0 4 42 142.16 181.56 29.63 o 1 4 42 77.98 130.43 27.01 o 0 5 42 63.64 81.25 28.99 o 2 0 43 312.05 381.10 31.99 o 2 1 43 21.92 76.28 22.83 o 3 1 43 260.76 291.16 32.21 o 0 2 43 86.50 122.27 24.77 o 2 2 43 131.52 105.67 29.22 o 4 2 43 192.80 204.61 33.83 o 1 4 43 399.32 354.84 36.73 o 0 0 44 443.97 446.02 38.56 o 0 1 44 30.65 60.68 24.24 o 4 1 44 261.83 302.60 37.89 o 0 2 44 131.08 104.82 27.40 o 1 2 44 189.44 171.36 29.60 o 3 2 44 111.47 103.76 30.85 o 0 3 44 70.20 69.73 27.02 o 1 3 44 33.22 87.35 24.24 o 3 3 44 247.22 215.13 37.43 o 1 5 44 96.41 122.04 30.71 o 0 1 45 93.53 84.84 27.90 o 0 2 45 362.79 273.38 33.27 o 1 2 45 102.04 71.47 27.36 o 3 2 45 218.88 226.22 36.20 o 1 3 45 251.91 195.51 33.65 o 3 3 45 74.10 82.19 32.16 o 0 4 45 278.44 340.52 33.69 o 0 0 46 1110.43 1001.57 46.62 o 2 2 46 24.76 86.96 23.99 o 3 2 46 49.78 76.46 27.21 o 2 3 46 80.38 77.92 28.93 o 1 4 46 45.79 92.26 27.50 o 1 0 47 58.61 74.30 26.82 o 3 1 47 51.32 76.64 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