#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/13/2011383.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011383_Fobs loop_ _publ_author_name 'Shanmuga Sundara Raj, S.' 'Surya Prakash Rao, H.' 'Sakthikumar, L.' 'Fun, Hoong-Kun' _publ_section_title ; 2-(Nitromethylene)-1,3-dithietane ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1113 _journal_page_last 1114 _journal_volume 56 _journal_year 2000 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.221 _cell_angle_gamma 90.000 _cell_length_a 3.9198 _cell_length_b 18.3222 _cell_length_c 7.9352 _exptl_crystal_F_000 304.00 _reflns_d_resolution_high 0.7508 _[local]_cod_data_source_file sk1398Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' SK1398 in P2(1)/n ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 102.73 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 60.08 50.40 3.92 o 4 0 0 201.52 175.36 17.14 o 1 1 0 3716.84 3509.24 110.22 o 2 1 0 204.85 172.23 12.57 o 3 1 0 121.49 92.27 11.26 o 4 1 0 158.19 149.58 11.38 o 5 1 0 52.79 51.84 10.17 o 0 2 0 36.25 36.24 1.93 o 1 2 0 10553.20 9431.25 344.24 o 2 2 0 3160.27 2732.31 77.26 o 3 2 0 309.17 254.42 13.16 o 4 2 0 25.38 25.94 4.70 o 5 2 0 12.26 9.45 6.41 o 1 3 0 7401.71 8005.62 292.71 o 2 3 0 1076.27 978.87 37.35 o 3 3 0 276.58 247.51 12.32 o 4 3 0 102.49 91.52 8.24 o 5 3 0 16.95 9.74 6.55 o 0 4 0 7616.61 6794.46 213.17 o 1 4 0 6937.18 5973.26 160.65 o 2 4 0 494.77 493.50 28.20 o 3 4 0 98.77 90.89 6.35 o 4 4 0 0.01 -0.15 2.89 o 5 4 0 11.09 19.38 7.75 o 1 5 0 1525.03 1610.53 81.88 o 2 5 0 5.20 6.78 2.07 o 3 5 0 1423.00 1282.27 48.95 o 4 5 0 23.11 20.28 4.43 o 0 6 0 1270.68 1243.53 45.00 o 1 6 0 136.74 157.11 9.40 o 2 6 0 4318.64 4384.45 162.42 o 3 6 0 88.63 78.39 5.21 o 4 6 0 4.80 4.39 3.48 o 1 7 0 539.92 551.23 16.41 o 2 7 0 353.65 365.28 13.13 o 3 7 0 19.55 20.91 3.00 o 4 7 0 14.62 13.72 4.27 o 0 8 0 6917.20 6892.39 285.56 o 1 8 0 2387.89 2654.29 73.56 o 2 8 0 183.87 192.65 7.78 o 3 8 0 262.08 238.45 12.68 o 4 8 0 162.78 146.19 11.03 o 1 9 0 181.48 188.55 11.09 o 2 9 0 41.75 48.68 3.37 o 3 9 0 90.06 96.00 5.34 o 4 9 0 199.42 199.28 11.01 o 0 10 0 3180.51 3070.26 128.43 o 1 10 0 1104.09 1070.96 31.29 o 2 10 0 18.56 16.54 2.34 o 3 10 0 148.97 165.61 7.61 o 4 10 0 20.24 22.81 4.15 o 1 11 0 1214.37 1304.23 36.94 o 2 11 0 57.22 60.63 3.91 o 3 11 0 1.67 2.89 2.21 o 4 11 0 11.62 11.09 3.40 o 0 12 0 1189.74 1299.22 55.96 o 1 12 0 3.41 1.49 1.35 o 2 12 0 447.27 466.39 16.67 o 3 12 0 3.85 5.19 2.23 o 4 12 0 13.61 10.02 3.33 o 1 13 0 375.42 373.67 13.46 o 2 13 0 63.55 65.54 4.76 o 3 13 0 167.44 171.23 8.95 o 4 13 0 0.13 0.40 2.88 o 0 14 0 0.06 0.84 2.21 o 1 14 0 449.70 470.31 15.86 o 2 14 0 314.09 308.98 22.02 o 3 14 0 1.37 0.34 3.10 o 4 14 0 9.04 10.15 3.81 o 1 15 0 84.62 87.41 5.24 o 2 15 0 17.57 17.89 4.01 o 3 15 0 22.23 21.35 4.35 o 4 15 0 2.10 2.21 4.04 o 0 16 0 112.73 112.71 7.84 o 1 16 0 159.08 147.00 7.26 o 2 16 0 126.12 128.87 8.87 o 3 16 0 190.38 155.59 14.76 o 1 17 0 0.26 1.63 2.27 o 2 17 0 12.03 10.53 3.74 o 3 17 0 0.26 0.58 3.42 o 0 18 0 552.99 546.30 25.95 o 1 18 0 63.58 61.02 6.13 o 2 18 0 2.42 4.87 3.56 o 3 18 0 3.87 3.26 3.75 o 1 19 0 23.20 23.27 4.41 o 2 19 0 69.85 59.44 6.38 o 3 19 0 2.68 2.66 4.12 o 0 20 0 32.81 29.77 4.64 o 1 20 0 3.02 1.19 3.01 o 2 20 0 191.47 221.60 19.04 o 1 21 0 10.73 12.89 4.01 o 2 21 0 11.90 9.69 4.17 o 0 22 0 61.36 56.89 6.25 o 1 22 0 182.64 168.17 11.29 o 2 22 0 1.40 2.35 5.12 o 1 23 0 70.44 73.89 7.42 o 0 24 0 29.91 21.59 6.79 o -5 0 1 17.77 9.77 6.27 o -3 0 1 33.29 28.59 4.35 o -1 0 1 2657.56 2841.66 123.98 o 1 0 1 1556.16 1715.78 159.99 o 3 0 1 9.41 6.06 4.30 o -5 1 1 26.05 20.78 5.12 o -4 1 1 4.51 3.04 3.51 o -3 1 1 344.42 309.01 16.33 o -2 1 1 0.40 2.90 1.35 o -1 1 1 1226.41 1225.11 62.65 o 0 1 1 520.12 545.45 19.85 o 1 1 1 395.09 394.81 13.07 o 2 1 1 9.10 8.63 1.71 o 3 1 1 32.49 27.52 4.15 o 4 1 1 17.62 16.83 4.05 o -5 2 1 5.94 6.48 4.11 o -4 2 1 164.15 153.42 11.45 o -3 2 1 173.16 161.90 9.33 o -2 2 1 25.80 19.43 1.90 o -1 2 1 191.37 183.87 19.12 o 0 2 1 684.62 755.56 26.04 o 1 2 1 349.77 294.12 10.03 o 2 2 1 173.98 128.12 9.64 o 3 2 1 425.62 337.30 14.26 o 4 2 1 113.20 84.75 10.55 o -5 3 1 7.93 12.10 4.63 o -4 3 1 0.41 0.76 3.19 o -3 3 1 34.78 36.28 7.01 o -2 3 1 348.92 326.78 11.25 o -1 3 1 486.84 488.70 13.20 o 0 3 1 702.52 789.66 27.24 o 1 3 1 54.29 53.22 2.85 o 2 3 1 237.49 189.94 14.15 o 3 3 1 38.49 33.07 3.30 o 4 3 1 100.73 82.98 7.87 o -5 4 1 0.05 0.84 3.67 o -4 4 1 3.29 4.21 3.47 o -3 4 1 38.45 39.63 3.64 o -2 4 1 1749.35 1625.23 44.51 o -1 4 1 16.87 23.44 1.80 o 0 4 1 607.65 588.79 44.11 o 1 4 1 168.66 170.14 7.70 o 2 4 1 174.53 147.90 15.07 o 3 4 1 83.99 72.65 4.77 o 4 4 1 18.14 15.80 4.15 o -5 5 1 0.86 -2.27 5.05 o -4 5 1 5.17 4.36 3.73 o -3 5 1 20.71 18.72 2.96 o -2 5 1 221.29 215.21 8.06 o -1 5 1 458.97 450.23 19.85 o 0 5 1 567.76 573.12 28.99 o 1 5 1 63.15 56.96 4.13 o 2 5 1 1292.02 1223.64 46.49 o 3 5 1 5.53 3.24 2.07 o 4 5 1 75.14 69.61 7.11 o -5 6 1 18.40 24.42 8.66 o -4 6 1 164.32 161.61 11.87 o -3 6 1 223.66 209.85 17.60 o -2 6 1 467.78 459.03 12.25 o -1 6 1 0.22 1.30 1.05 o 0 6 1 88.19 81.40 4.45 o 1 6 1 47.66 35.78 3.70 o 2 6 1 92.73 85.20 5.11 o 3 6 1 429.62 412.19 17.50 o 4 6 1 0.89 0.08 3.19 o -4 7 1 33.22 31.60 5.44 o -3 7 1 235.65 220.67 10.45 o -2 7 1 20.94 20.93 1.82 o -1 7 1 320.26 341.83 11.83 o 0 7 1 1902.57 1840.96 50.19 o 1 7 1 19.12 24.13 2.06 o 2 7 1 94.15 86.39 5.18 o 3 7 1 9.53 8.03 2.51 o 4 7 1 25.86 27.09 5.35 o -4 8 1 93.22 97.24 8.86 o -3 8 1 8.47 7.99 2.17 o -2 8 1 9.31 13.42 1.63 o -1 8 1 215.48 216.39 7.08 o 0 8 1 68.16 94.97 4.44 o 1 8 1 1637.97 1664.11 66.17 o 2 8 1 279.27 247.99 9.60 o 3 8 1 49.34 52.69 4.43 o 4 8 1 33.35 35.82 5.72 o -4 9 1 7.11 10.75 2.72 o -3 9 1 610.65 589.65 20.56 o -2 9 1 149.92 153.46 6.00 o -1 9 1 39.20 42.40 2.37 o 0 9 1 3.53 3.45 1.14 o 1 9 1 755.11 712.93 38.58 o 2 9 1 1.47 1.05 1.94 o 3 9 1 16.27 17.00 2.68 o 4 9 1 1.57 1.72 3.63 o -4 10 1 147.75 148.21 10.37 o -3 10 1 13.93 12.45 2.47 o -2 10 1 0.06 1.61 1.61 o -1 10 1 659.09 639.44 18.71 o 0 10 1 99.62 96.21 4.96 o 1 10 1 761.92 674.60 21.60 o 2 10 1 192.53 187.77 7.92 o 3 10 1 71.23 75.91 4.85 o 4 10 1 52.55 57.67 7.13 o -4 11 1 16.20 20.92 3.87 o -3 11 1 2.21 0.67 1.94 o -2 11 1 12.32 11.95 2.14 o -1 11 1 1084.44 968.48 35.53 o 0 11 1 640.78 643.85 20.39 o 1 11 1 20.39 19.38 2.10 o 2 11 1 3.93 8.99 2.75 o 3 11 1 0.26 1.80 2.14 o 4 11 1 34.87 37.33 5.19 o -4 12 1 11.00 15.69 3.53 o -3 12 1 183.87 168.26 8.73 o -2 12 1 282.74 259.34 11.46 o -1 12 1 166.69 159.11 7.23 o 0 12 1 460.26 499.06 16.32 o 1 12 1 0.00 0.65 1.41 o 2 12 1 2.60 5.37 2.04 o 3 12 1 270.43 286.99 11.72 o 4 12 1 5.32 9.23 5.01 o -4 13 1 12.76 14.66 3.67 o -3 13 1 0.08 0.82 2.27 o -2 13 1 797.06 764.68 29.41 o -1 13 1 43.27 39.97 3.98 o 0 13 1 12.64 15.32 2.18 o 1 13 1 2.48 1.58 1.36 o 2 13 1 460.55 468.05 16.81 o 3 13 1 34.87 33.74 4.22 o 4 13 1 59.55 63.73 5.99 o -4 14 1 6.60 8.04 3.32 o -3 14 1 59.20 53.88 4.64 o -2 14 1 400.04 378.14 15.93 o -1 14 1 8.03 9.04 2.10 o 0 14 1 478.98 432.81 27.04 o 1 14 1 129.68 129.16 5.74 o 2 14 1 23.15 20.90 3.88 o 3 14 1 47.02 48.24 5.98 o 4 14 1 12.25 21.25 5.29 o -4 15 1 4.50 6.47 3.63 o -3 15 1 25.07 22.56 3.57 o -2 15 1 21.77 23.75 3.45 o -1 15 1 745.94 725.10 29.94 o 0 15 1 486.25 501.49 16.70 o 1 15 1 63.69 73.17 4.79 o 2 15 1 259.71 241.82 13.61 o 3 15 1 0.13 0.37 3.27 o -3 16 1 17.33 15.12 4.21 o -2 16 1 11.25 7.03 4.99 o -1 16 1 120.86 114.52 7.06 o 0 16 1 0.06 1.15 1.80 o 1 16 1 72.29 77.01 4.98 o 2 16 1 250.39 230.82 20.83 o 3 16 1 98.50 95.95 15.45 o -3 17 1 235.55 245.13 17.29 o -2 17 1 63.02 56.41 5.82 o -1 17 1 3.32 1.60 2.10 o 0 17 1 361.28 347.52 12.42 o 1 17 1 168.84 183.45 11.41 o 2 17 1 4.48 3.95 3.31 o 3 17 1 2.34 1.18 3.41 o -3 18 1 7.78 13.60 4.69 o -2 18 1 5.57 5.17 3.50 o -1 18 1 99.72 94.89 5.78 o 0 18 1 0.01 0.91 1.87 o 1 18 1 721.76 653.13 30.55 o 2 18 1 0.01 0.00 3.16 o 3 18 1 4.71 10.24 4.27 o -3 19 1 149.26 134.73 14.54 o -2 19 1 96.94 96.28 17.41 o -1 19 1 33.80 31.26 4.84 o 0 19 1 231.90 240.23 9.53 o 1 19 1 96.15 91.52 7.70 o 2 19 1 0.17 2.20 3.37 o -2 20 1 37.61 35.76 5.48 o -1 20 1 48.46 52.82 5.97 o 0 20 1 0.25 3.48 2.20 o 1 20 1 39.07 35.31 5.34 o 2 20 1 58.85 64.00 13.53 o -2 21 1 22.74 26.84 5.59 o -1 21 1 259.07 240.52 13.98 o 0 21 1 51.30 48.70 4.08 o 1 21 1 7.04 4.92 3.62 o 2 21 1 80.25 70.80 7.30 o -2 22 1 136.29 126.47 9.68 o -1 22 1 38.75 46.51 10.56 o 0 22 1 127.41 120.21 7.26 o 1 22 1 1.27 2.45 3.58 o -1 23 1 56.18 52.87 6.59 o 0 23 1 15.06 14.66 3.63 o 1 23 1 16.92 11.62 4.82 o 0 24 1 65.10 52.15 8.14 o -4 0 2 5.66 9.06 5.49 o -2 0 2 895.15 750.86 39.74 o 0 0 2 6642.23 6830.08 383.30 o 2 0 2 372.70 334.89 16.48 o 4 0 2 48.93 38.90 7.50 o -5 1 2 1.10 2.31 5.48 o -4 1 2 63.53 64.51 6.98 o -3 1 2 46.04 44.80 3.44 o -2 1 2 84.37 72.29 5.79 o -1 1 2 38.32 39.99 2.35 o 0 1 2 12.87 19.87 1.77 o 1 1 2 1371.51 1131.07 42.08 o 2 1 2 539.73 487.52 27.23 o 3 1 2 82.93 70.50 6.37 o 4 1 2 12.66 10.88 3.93 o -5 2 2 2.58 -2.44 3.57 o -4 2 2 71.77 73.05 10.72 o -3 2 2 371.97 373.05 15.86 o -2 2 2 241.68 237.85 15.66 o -1 2 2 1894.80 1855.12 51.49 o 0 2 2 3.58 2.77 1.25 o 1 2 2 814.88 762.62 21.83 o 2 2 2 497.38 417.62 17.14 o 3 2 2 6.61 3.72 2.68 o 4 2 2 89.15 79.00 7.65 o -5 3 2 20.41 20.51 5.44 o -4 3 2 0.34 3.44 3.55 o -3 3 2 13.04 14.25 2.68 o -2 3 2 340.39 377.04 17.38 o -1 3 2 317.55 344.85 8.91 o 0 3 2 1058.64 1033.21 89.52 o 1 3 2 928.74 1092.80 60.09 o 2 3 2 198.56 175.07 6.80 o 3 3 2 229.20 192.78 9.27 o 4 3 2 162.19 133.66 16.10 o -5 4 2 29.96 29.43 5.82 o -4 4 2 15.83 23.60 5.09 o -3 4 2 23.76 25.45 3.14 o -2 4 2 185.31 181.92 5.76 o -1 4 2 2118.14 2036.29 48.31 o 0 4 2 906.80 971.81 33.50 o 1 4 2 20.40 30.62 3.90 o 2 4 2 36.32 33.73 2.46 o 3 4 2 20.19 19.84 2.94 o 4 4 2 1.20 3.98 3.50 o -5 5 2 34.16 37.23 6.56 o -4 5 2 29.18 33.15 5.56 o -3 5 2 1.40 1.24 1.97 o -2 5 2 74.59 80.64 3.93 o -1 5 2 90.23 88.48 4.36 o 0 5 2 33.76 38.82 4.51 o 1 5 2 115.49 131.70 7.09 o 2 5 2 201.09 188.19 10.58 o 3 5 2 861.95 750.30 29.72 o 4 5 2 6.36 8.71 3.81 o -5 6 2 18.17 9.86 7.40 o -4 6 2 124.06 134.18 10.63 o -3 6 2 238.73 228.47 18.96 o -2 6 2 899.24 903.36 25.96 o -1 6 2 940.42 910.80 23.65 o 0 6 2 250.10 244.48 17.36 o 1 6 2 229.27 235.59 8.39 o 2 6 2 475.40 474.10 19.65 o 3 6 2 125.62 111.31 7.65 o 4 6 2 83.21 74.68 7.84 o -4 7 2 7.29 7.69 4.05 o -3 7 2 44.91 47.60 3.92 o -2 7 2 47.31 51.46 3.08 o -1 7 2 40.37 40.63 2.02 o 0 7 2 16.84 8.59 1.43 o 1 7 2 617.63 670.68 32.99 o 2 7 2 7.00 9.50 2.51 o 3 7 2 33.20 30.81 3.58 o 4 7 2 45.58 41.07 6.01 o -4 8 2 0.77 0.69 2.10 o -3 8 2 582.56 587.54 24.52 o -2 8 2 209.68 201.78 6.91 o -1 8 2 1.19 0.90 0.99 o 0 8 2 751.51 780.18 37.05 o 1 8 2 1158.46 1215.88 59.76 o 2 8 2 471.28 446.33 21.78 o 3 8 2 38.30 37.20 5.72 o 4 8 2 17.38 15.01 4.73 o -4 9 2 155.08 158.00 9.15 o -3 9 2 4.38 4.61 2.04 o -2 9 2 412.95 406.11 14.93 o -1 9 2 4.68 6.71 1.22 o 0 9 2 165.96 167.46 5.68 o 1 9 2 146.53 159.05 7.50 o 2 9 2 957.36 936.06 31.28 o 3 9 2 18.04 21.68 3.57 o 4 9 2 11.74 13.77 4.77 o -4 10 2 0.98 0.27 2.36 o -3 10 2 124.30 139.36 6.64 o -2 10 2 137.47 134.45 5.75 o -1 10 2 988.51 1020.57 29.94 o 0 10 2 413.72 450.90 16.77 o 1 10 2 14.14 14.17 1.97 o 2 10 2 42.92 46.17 4.28 o 3 10 2 15.80 17.92 2.89 o 4 10 2 35.13 44.71 5.58 o -4 11 2 27.52 23.80 4.55 o -3 11 2 37.63 36.81 3.89 o -2 11 2 540.96 533.54 17.65 o -1 11 2 1.37 2.73 1.43 o 0 11 2 1673.82 1856.84 63.54 o 1 11 2 658.45 642.77 21.10 o 2 11 2 37.72 37.32 3.38 o 3 11 2 0.03 1.07 2.27 o 4 11 2 31.90 33.96 5.44 o -4 12 2 42.68 36.02 6.67 o -3 12 2 53.50 55.07 4.60 o -2 12 2 319.80 315.70 17.11 o -1 12 2 332.10 332.71 10.53 o 0 12 2 346.31 347.52 13.57 o 1 12 2 287.07 265.91 17.53 o 2 12 2 1.96 3.05 2.09 o 3 12 2 3.88 6.12 2.58 o 4 12 2 24.41 30.72 5.27 o -4 13 2 15.24 13.36 4.17 o -3 13 2 0.47 -1.29 2.41 o -2 13 2 185.64 174.98 8.60 o -1 13 2 86.83 92.63 4.64 o 0 13 2 334.31 340.52 13.49 o 1 13 2 21.23 19.10 2.71 o 2 13 2 9.08 6.41 2.76 o 3 13 2 260.99 292.29 12.09 o -4 14 2 29.67 28.35 6.34 o -3 14 2 45.60 41.43 5.36 o -2 14 2 107.42 99.04 6.04 o -1 14 2 1814.68 1610.82 44.77 o 0 14 2 7.40 7.99 2.51 o 1 14 2 265.48 260.94 12.87 o 2 14 2 5.89 6.71 2.77 o 3 14 2 44.27 49.13 6.39 o -4 15 2 4.15 6.12 4.10 o -3 15 2 6.88 8.59 2.92 o -2 15 2 10.99 9.23 2.71 o -1 15 2 10.75 10.42 2.01 o 0 15 2 324.51 305.53 15.05 o 1 15 2 83.60 87.25 5.28 o 2 15 2 61.97 68.31 6.45 o 3 15 2 8.23 14.30 4.59 o -3 16 2 458.01 451.52 22.44 o -2 16 2 7.02 10.19 2.89 o -1 16 2 41.16 43.93 3.07 o 0 16 2 0.01 0.74 2.53 o 1 16 2 395.20 394.94 19.90 o 2 16 2 60.19 74.30 10.86 o 3 16 2 96.33 96.58 13.60 o -3 17 2 1.75 0.87 3.46 o -2 17 2 317.92 298.30 17.49 o -1 17 2 21.60 17.38 3.04 o 0 17 2 113.89 108.09 6.20 o 1 17 2 74.23 72.29 8.49 o 2 17 2 367.56 341.27 18.35 o 3 17 2 12.56 19.94 5.00 o -3 18 2 0.46 1.78 3.58 o -2 18 2 198.55 175.36 17.81 o -1 18 2 44.68 48.06 3.97 o 0 18 2 156.82 152.36 10.51 o 1 18 2 3.72 6.15 3.68 o 2 18 2 42.54 44.73 8.53 o 3 18 2 0.23 3.51 5.83 o -3 19 2 15.94 14.77 4.69 o -2 19 2 288.00 300.61 17.19 o -1 19 2 45.01 43.08 3.66 o 0 19 2 313.21 302.31 12.99 o 1 19 2 192.06 184.49 11.62 o 2 19 2 136.89 135.47 10.04 o -2 20 2 47.28 52.26 11.92 o -1 20 2 4.73 5.98 3.47 o 0 20 2 14.52 15.69 3.32 o 1 20 2 117.44 109.27 8.62 o 2 20 2 9.55 9.55 4.51 o -2 21 2 47.43 44.04 6.20 o -1 21 2 1.69 7.99 3.97 o 0 21 2 303.57 286.59 17.15 o 1 21 2 0.01 2.29 5.02 o -2 22 2 19.35 15.43 7.06 o -1 22 2 569.49 545.14 27.02 o 0 22 2 0.41 1.80 2.79 o 1 22 2 72.08 67.01 9.86 o -1 23 2 14.73 14.31 6.47 o 0 23 2 55.35 50.65 14.65 o 1 23 2 2.53 0.48 4.96 o -5 0 3 29.71 27.65 8.37 o -3 0 3 4.54 5.77 2.79 o -1 0 3 6050.67 6438.43 279.57 o 1 0 3 203.09 235.68 15.80 o 3 0 3 89.52 76.62 9.66 o -5 1 3 4.62 6.99 11.13 o -4 1 3 55.29 62.29 6.99 o -3 1 3 442.88 507.89 17.40 o -2 1 3 704.80 752.46 24.51 o -1 1 3 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