#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2011408.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011408_Fobs loop_ _publ_author_name 'Gomes, Ligia' 'Sousa, Carla' 'Freire, Cristina' 'de Castro, Baltazar' _publ_section_title ; Diaqua{6,6'-dimethoxy-2,2'-[propane-1,3-diylbis(nitrilomethylidyne-N)]diphenolato-O,O'}nickel(II) ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1201 _journal_page_last 1203 _journal_volume 56 _journal_year 2000 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _exptl_crystal_F_000 912.00 _[local]_cod_data_source_file da1141Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' IP1170' _shelx_refln_list_code 4 _shelx_f_calc_maximum 184.83 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 7264.94 6519.86 231.31 o 6 0 0 830.28 852.41 17.88 o 8 0 0 127.34 152.58 22.07 o 2 1 0 28793.48 25573.86 122.23 o 4 1 0 19513.18 18818.87 361.41 o 6 1 0 3839.94 3892.77 129.21 o 8 1 0 864.82 1069.59 21.04 x 2 2 0 20487.23 19596.67 322.11 o 4 2 0 28370.86 27510.73 777.65 o 6 2 0 1755.26 1694.11 25.68 o 8 2 0 274.32 314.39 15.21 o 2 3 0 19139.47 19064.61 508.94 o 4 3 0 535.72 595.22 13.78 o 6 3 0 416.37 389.67 15.98 o 8 3 0 752.67 814.93 26.29 o 0 4 0 1608.21 2275.76 46.29 x 2 4 0 12519.27 12627.45 321.85 o 4 4 0 949.62 904.04 25.47 o 6 4 0 4730.67 4759.45 208.61 o 8 4 0 2170.80 2378.65 143.93 o 2 5 0 572.66 563.00 13.55 o 4 5 0 476.00 454.06 12.96 o 6 5 0 665.67 626.58 26.41 o 8 5 0 135.93 169.48 13.95 o 0 6 0 7294.93 9921.60 73.81 x 2 6 0 18.32 21.02 16.42 o 4 6 0 889.67 892.74 42.19 o 6 6 0 338.49 298.20 15.51 o 8 6 0 2.83 6.80 16.83 o 2 7 0 1442.98 1587.76 75.57 o 4 7 0 8421.68 8834.93 431.82 o 6 7 0 2189.54 2248.60 79.27 o 8 7 0 4.30 6.95 14.58 o 2 8 0 1054.18 1165.81 91.74 o 4 8 0 699.09 660.75 41.21 o 6 8 0 113.37 106.58 12.11 o 8 8 0 209.23 219.62 15.47 o 2 9 0 5373.87 6472.30 537.39 o 4 9 0 1850.58 1792.62 102.22 o 6 9 0 324.89 322.21 15.80 o 8 9 0 862.02 844.92 83.99 o 0 10 0 2565.80 2823.81 34.67 o 2 10 0 26.94 70.80 15.17 o 4 10 0 2103.82 1993.31 120.54 o 6 10 0 608.77 614.29 51.31 o 8 10 0 379.47 386.27 18.73 o 2 11 0 2391.40 3368.67 298.88 x 4 11 0 21.91 6.12 9.71 o 6 11 0 295.71 285.93 15.69 o 8 11 0 310.80 313.56 14.67 o 0 12 0 3175.77 3484.20 34.87 o 2 12 0 152.68 148.73 29.33 o 4 12 0 3649.38 3830.52 291.79 o 6 12 0 799.12 892.79 64.40 o 8 12 0 257.41 244.39 18.14 o 2 13 0 1564.74 1990.18 201.98 o 4 13 0 752.92 749.05 87.10 o 6 13 0 68.24 84.36 20.79 o 8 13 0 103.48 156.25 73.93 o 0 14 0 29938.36 40917.33 101.72 x 2 14 0 6009.21 7151.44 785.78 o 4 14 0 2272.61 2307.34 242.80 o 6 14 0 308.57 318.89 31.03 o 2 15 0 960.59 1045.18 23.39 o 4 15 0 2849.04 3330.00 324.04 o 6 15 0 926.69 899.56 41.43 o 0 16 0 16796.79 21417.29 73.06 x 2 16 0 8014.66 8599.67 50.61 o 4 16 0 9198.11 9349.02 954.06 o 6 16 0 1750.52 1662.26 251.16 o 2 17 0 18.70 25.43 23.74 o 4 17 0 986.30 980.95 142.89 o 6 17 0 1793.41 1686.64 171.17 o 0 18 0 13322.91 15417.23 59.60 o 2 18 0 4565.93 4408.83 41.82 o 4 18 0 3771.52 3687.74 379.14 o 6 18 0 719.19 716.30 69.51 o 2 19 0 993.84 869.79 74.90 o 4 19 0 1018.40 937.03 176.85 o 6 19 0 16.92 24.32 16.14 o 0 20 0 5537.62 5878.67 40.28 o 2 20 0 598.10 723.68 93.75 o 4 20 0 438.53 405.00 20.07 o 6 20 0 130.50 116.14 25.42 o 2 21 0 52.76 56.65 14.91 o 4 21 0 12.12 33.08 28.96 o 0 22 0 18.97 -43.01 26.62 o 2 22 0 35.49 4.57 17.96 o 4 22 0 934.10 770.56 31.24 o 2 23 0 41.94 42.39 21.26 o 4 23 0 10.60 43.16 28.26 o 0 24 0 1958.38 1999.16 29.40 o 2 24 0 24.47 15.73 17.54 o 4 24 0 44.35 23.22 43.56 o 2 25 0 494.10 395.25 58.71 o 0 26 0 2090.87 1767.21 29.01 o 2 26 0 1047.99 996.37 125.36 o 1 0 1 17335.04 13929.06 279.51 x 2 0 1 23437.98 22150.75 339.38 o 3 0 1 9009.78 7958.31 73.88 o 4 0 1 2977.06 2914.55 29.87 o 5 0 1 710.49 691.16 14.37 o 6 0 1 204.63 216.53 10.01 o 7 0 1 876.50 913.81 13.78 o 8 0 1 394.12 436.83 13.41 o 9 0 1 35.02 47.47 13.66 o 1 1 1 251.78 209.89 12.63 o 2 1 1 6484.91 5916.14 53.40 o 3 1 1 2307.60 2123.19 31.03 o 4 1 1 3188.65 2776.66 32.03 o 5 1 1 602.77 602.29 9.74 o 6 1 1 307.80 288.27 7.33 o 7 1 1 1076.15 1086.83 14.18 o 8 1 1 28.60 33.84 8.26 o 9 1 1 145.18 147.28 10.91 o 1 2 1 16114.73 14350.85 139.75 o 2 2 1 10341.12 9783.20 111.48 o 3 2 1 13905.16 12713.30 205.83 o 4 2 1 1007.63 903.68 15.39 o 5 2 1 1347.34 1235.56 23.40 o 6 2 1 1146.06 1172.79 18.49 o 7 2 1 782.86 801.76 14.87 o 8 2 1 177.16 184.88 8.97 o 9 2 1 50.38 46.84 11.31 o 0 3 1 3126.99 3955.30 60.99 x 1 3 1 165.10 159.09 13.11 o 2 3 1 211.39 215.05 9.81 o 3 3 1 1378.43 1317.99 14.75 o 4 3 1 6711.64 6242.32 104.53 o 5 3 1 623.26 611.17 12.33 o 6 3 1 1667.82 1647.85 38.13 o 7 3 1 1237.67 1309.45 20.81 o 8 3 1 260.49 281.95 12.78 o 9 3 1 212.40 284.81 31.74 o 1 4 1 11815.98 12965.03 587.29 o 2 4 1 6.76 9.93 7.66 o 3 4 1 7688.09 6921.87 117.45 o 4 4 1 1296.50 1395.21 28.48 o 5 4 1 1043.56 962.72 20.20 o 6 4 1 116.51 137.69 8.71 o 7 4 1 1052.96 1043.04 21.98 o 8 4 1 537.55 545.55 18.09 o 9 4 1 55.82 77.55 16.64 o 0 5 1 6694.43 8748.63 57.69 x 1 5 1 216.15 240.53 14.09 o 2 5 1 281.87 341.59 10.09 o 3 5 1 1195.54 1072.53 20.61 o 4 5 1 66.85 41.09 7.09 o 5 5 1 127.79 114.35 7.95 o 6 5 1 655.64 648.65 9.39 o 7 5 1 634.27 698.60 21.75 o 8 5 1 432.53 444.41 12.39 o 1 6 1 365.40 339.11 12.66 o 2 6 1 427.14 410.84 14.79 o 3 6 1 2516.36 2233.98 56.84 o 4 6 1 1801.84 1662.64 33.94 o 5 6 1 52.24 45.20 7.55 o 6 6 1 329.22 327.32 9.28 o 7 6 1 315.25 335.60 12.92 o 8 6 1 4.72 20.24 11.06 o 0 7 1 2871.90 3630.28 45.84 x 1 7 1 8.31 9.00 11.03 o 2 7 1 1676.06 1753.46 73.67 o 3 7 1 279.23 291.95 10.35 o 4 7 1 2709.97 2653.31 67.27 o 5 7 1 19.92 25.30 7.41 o 6 7 1 61.90 76.22 9.25 o 7 7 1 187.36 196.10 12.35 o 8 7 1 146.70 126.21 9.90 o 1 8 1 21.53 43.65 9.67 o 2 8 1 774.48 949.39 44.18 o 3 8 1 402.84 324.79 9.50 o 4 8 1 1212.77 1237.36 43.24 o 5 8 1 6.23 1.89 7.39 o 6 8 1 709.91 749.96 25.98 o 7 8 1 182.47 182.12 9.80 o 8 8 1 372.61 382.63 14.65 o 0 9 1 11205.04 14238.74 71.92 x 1 9 1 64.69 67.39 12.46 o 2 9 1 432.74 410.22 19.99 o 3 9 1 160.36 146.19 10.35 o 4 9 1 442.63 404.90 14.43 o 5 9 1 3.15 4.81 6.36 o 6 9 1 531.64 525.50 24.66 o 7 9 1 331.28 318.27 9.84 o 8 9 1 65.73 56.81 9.47 o 1 10 1 640.55 596.44 23.90 o 2 10 1 275.06 324.26 13.94 o 3 10 1 1737.81 1651.37 83.87 o 4 10 1 127.43 113.37 9.17 o 5 10 1 208.68 210.90 9.72 o 6 10 1 139.05 143.79 9.29 o 7 10 1 355.73 355.48 9.62 o 8 10 1 391.16 381.68 12.27 o 0 11 1 12.86 114.51 13.62 o 1 11 1 21.25 13.34 10.55 o 2 11 1 90.74 66.32 10.31 o 3 11 1 541.93 535.21 29.28 o 4 11 1 2769.15 2827.02 137.66 o 5 11 1 298.44 282.45 11.93 o 6 11 1 429.54 429.99 19.32 o 7 11 1 676.71 724.33 36.41 o 8 11 1 92.16 91.36 9.40 o 1 12 1 5195.88 6359.49 256.02 o 2 12 1 480.90 629.62 33.36 o 3 12 1 4406.14 4475.69 294.64 o 4 12 1 5.82 4.77 8.09 o 5 12 1 643.65 683.17 34.63 o 6 12 1 99.18 114.77 8.68 o 7 12 1 591.21 614.13 24.94 o 8 12 1 66.58 68.41 11.31 o 0 13 1 4007.19 5173.83 112.47 x 1 13 1 241.63 279.58 15.81 o 2 13 1 326.01 327.46 18.75 o 3 13 1 1302.66 1414.31 96.80 o 4 13 1 469.15 477.84 22.93 o 5 13 1 389.50 421.52 23.50 o 6 13 1 245.67 262.41 13.67 o 7 13 1 722.88 784.48 41.15 o 8 13 1 129.74 134.71 16.89 o 1 14 1 7516.92 8973.69 400.72 o 2 14 1 251.93 296.52 23.81 o 3 14 1 4949.09 5188.01 354.98 o 4 14 1 319.82 317.53 19.79 o 5 14 1 811.12 790.07 47.39 o 6 14 1 1.99 1.24 9.48 o 7 14 1 610.08 622.77 45.22 o 0 15 1 2967.55 3593.97 95.12 o 1 15 1 74.96 69.64 13.09 o 2 15 1 1384.99 1598.24 88.10 o 3 15 1 830.06 902.95 77.87 o 4 15 1 1619.21 1760.12 135.50 o 5 15 1 611.88 588.53 31.95 o 6 15 1 316.90 284.44 12.33 o 7 15 1 848.54 872.29 62.68 o 1 16 1 4415.01 5003.42 168.36 o 2 16 1 99.50 84.63 12.05 o 3 16 1 3773.12 3685.36 295.71 o 4 16 1 129.14 157.45 22.64 o 5 16 1 667.55 689.03 54.48 o 6 16 1 562.26 550.57 41.72 o 7 16 1 281.10 284.76 12.66 o 0 17 1 2387.99 3019.65 46.84 x 1 17 1 58.22 60.27 11.01 o 2 17 1 1251.72 1248.44 69.38 o 3 17 1 503.10 556.75 61.03 o 4 17 1 2781.43 2717.46 244.61 o 5 17 1 283.26 270.78 19.97 o 6 17 1 770.46 734.92 58.15 o 7 17 1 516.16 488.31 38.82 o 1 18 1 1860.36 2117.93 73.04 o 2 18 1 89.02 99.45 18.36 o 3 18 1 1471.21 1493.78 134.90 o 4 18 1 602.17 577.06 45.68 o 5 18 1 256.48 286.29 26.31 o 6 18 1 298.36 293.79 20.59 o 0 19 1 3543.36 3881.31 108.28 o 1 19 1 2.02 -4.74 10.59 o 2 19 1 1087.35 1083.38 90.03 o 3 19 1 72.25 82.49 13.12 o 4 19 1 291.77 290.66 23.25 o 5 19 1 4.13 -2.78 10.40 o 6 19 1 17.35 20.25 10.10 o 1 20 1 426.92 522.19 23.53 o 2 20 1 249.09 208.22 16.28 o 3 20 1 779.94 809.77 97.70 o 4 20 1 176.25 167.37 12.20 o 5 20 1 224.08 224.03 11.10 o 6 20 1 12.48 0.87 12.34 o 0 21 1 78.14 129.62 13.41 o 1 21 1 1.81 13.40 11.72 o 2 21 1 3.76 6.04 12.91 o 3 21 1 16.05 18.59 11.50 o 4 21 1 404.26 408.14 47.65 o 5 21 1 5.64 -3.96 10.84 o 1 22 1 655.39 714.92 28.25 o 2 22 1 592.79 545.99 32.27 o 3 22 1 670.51 722.30 82.80 o 4 22 1 13.12 4.28 12.00 o 5 22 1 100.64 91.48 11.81 o 0 23 1 7.24 21.70 14.71 o 1 23 1 49.00 59.97 12.20 o 2 23 1 8.79 -6.01 12.40 o 3 23 1 313.39 263.72 72.05 o 4 23 1 199.71 182.64 13.53 o 1 24 1 994.70 1033.67 37.83 o 2 24 1 129.89 131.49 11.75 o 3 24 1 670.86 665.05 56.06 o 4 24 1 11.41 9.55 15.03 o 0 25 1 1403.74 1247.47 19.03 o 1 25 1 16.06 15.56 13.55 o 2 25 1 215.37 210.92 11.79 o 3 25 1 223.96 193.13 12.78 o 1 26 1 374.80 334.28 20.60 o 2 26 1 10.73 -0.67 14.14 o 0 27 1 663.13 657.12 28.11 o 0 0 2 579.19 540.92 27.31 o 1 0 2 376.59 333.07 18.61 o 2 0 2 1556.59 1296.30 18.20 x 3 0 2 430.88 425.00 13.96 o 4 0 2 1854.91 1792.41 38.91 o 5 0 2 18.83 18.16 8.61 o 6 0 2 65.65 63.83 9.18 o 7 0 2 853.03 882.65 31.31 o 8 0 2 14.38 23.22 12.55 o 9 0 2 129.43 155.25 14.12 o 1 1 2 658.92 649.16 16.24 o 2 1 2 355.62 322.75 10.10 o 3 1 2 5891.01 5090.02 44.78 o 4 1 2 668.63 629.94 8.30 o 5 1 2 522.30 479.13 8.43 o 6 1 2 445.14 451.29 9.55 o 7 1 2 773.17 769.85 10.59 o 8 1 2 125.77 125.78 10.10 o 9 1 2 37.35 16.40 15.19 o 0 2 2 4327.28 4531.92 196.17 o 1 2 2 125.76 124.76 13.15 o 2 2 2 518.92 468.64 11.37 o 3 2 2 401.07 362.84 9.59 o 4 2 2 7.79 0.75 6.93 o 5 2 2 421.63 366.66 7.49 o 6 2 2 106.97 110.98 6.46 o 7 2 2 1052.14 1092.31 11.49 o 8 2 2 14.53 14.24 10.32 o 9 2 2 130.91 157.48 22.36 o 1 3 2 2108.34 2222.47 86.37 o 2 3 2 120.29 108.61 8.31 o 3 3 2 9590.75 8940.09 117.83 o 4 3 2 13.72 15.36 7.28 o 5 3 2 1069.55 1078.01 15.65 o 6 3 2 7.89 8.54 6.48 o 7 3 2 931.01 940.36 26.87 o 8 3 2 61.01 59.96 9.39 o 0 4 2 5964.82 6800.41 266.79 o 1 4 2 152.31 146.05 11.46 o 2 4 2 414.70 397.60 12.11 o 3 4 2 1002.50 911.95 18.14 o 4 4 2 1067.73 1065.93 21.81 o 5 4 2 371.42 366.22 9.55 o 6 4 2 6.18 4.45 6.95 o 7 4 2 1522.00 1613.10 22.65 o 8 4 2 19.85 21.70 8.86 o 1 5 2 9145.75 11179.64 775.34 o 2 5 2 1462.43 1531.99 64.44 o 3 5 2 10278.91 9966.13 249.67 o 4 5 2 116.97 127.29 7.85 o 5 5 2 1290.53 1287.42 35.51 o 6 5 2 33.08 34.16 7.84 o 7 5 2 1083.70 1127.18 27.75 o 8 5 2 6.69 14.79 8.80 o 0 6 2 5728.52 7778.74 342.27 x 1 6 2 24.91 37.17 9.84 o 2 6 2 21.40 37.59 9.94 o 3 6 2 1154.83 1193.30 35.58 o 4 6 2 505.69 508.06 10.47 o 5 6 2 864.44 814.81 22.99 o 6 6 2 434.05 480.27 14.22 o 7 6 2 1133.69 1159.84 22.77 o 8 6 2 95.87 96.99 10.60 o 1 7 2 8461.86 11116.80 420.06 x 2 7 2 324.71 318.94 14.10 o 3 7 2 9083.10 9022.09 426.92 o 4 7 2 25.08 19.77 8.38 o 5 7 2 897.39 867.38 27.48 o 6 7 2 1.47 6.86 8.13 o 7 7 2 684.03 745.00 30.51 o 8 7 2 21.96 10.02 10.29 o 0 8 2 4323.31 5882.93 189.76 x 1 8 2 84.91 91.19 11.58 o 2 8 2 2352.52 2542.79 140.37 o 3 8 2 619.50 636.03 27.80 o 4 8 2 1944.90 1897.05 73.58 o 5 8 2 264.56 256.06 8.65 o 6 8 2 69.65 61.80 8.78 o 7 8 2 974.64 956.26 18.79 o 8 8 2 105.27 108.68 10.66 o 1 9 2 3703.59 4796.57 160.36 x 2 9 2 106.82 111.63 9.39 o 3 9 2 5218.05 5432.50 282.41 o 4 9 2 189.84 177.52 7.94 o 5 9 2 1137.25 1166.98 38.40 o 6 9 2 125.25 133.10 10.75 o 7 9 2 1110.05 1063.28 22.72 o 8 9 2 0.53 -0.65 9.18 o 0 10 2 2891.70 3552.99 36.36 o 1 10 2 108.78 134.24 12.22 o 2 10 2 474.94 526.93 25.01 o 3 10 2 33.44 33.15 8.71 o 4 10 2 1011.85 1016.86 40.50 o 5 10 2 231.85 223.19 9.78 o 6 10 2 420.51 425.86 13.50 o 7 10 2 1037.87 1069.81 33.98 o 8 10 2 98.43 89.95 10.07 o 1 11 2 2967.81 3742.79 119.46 x 2 11 2 5.45 8.03 13.93 o 3 11 2 5851.01 6018.25 371.82 o 4 11 2 20.30 18.13 8.17 o 5 11 2 1167.21 1189.99 64.85 o 6 11 2 14.38 12.30 8.54 o 7 11 2 743.56 771.75 40.88 o 8 11 2 97.00 89.48 10.46 o 0 12 2 335.29 418.71 20.51 o 1 12 2 55.29 35.14 11.69 o 2 12 2 96.25 94.96 11.04 o 3 12 2 486.75 522.30 32.15 o 4 12 2 823.52 823.48 46.82 o 5 12 2 292.56 330.08 19.45 o 6 12 2 121.51 123.51 10.01 o 7 12 2 704.68 747.57 55.68 o 8 12 2 73.27 75.27 11.27 o 1 13 2 5779.54 7050.20 257.79 x 2 13 2 56.59 58.72 12.03 o 3 13 2 3846.88 3990.54 231.64 o 4 13 2 121.66 128.46 12.77 o 5 13 2 558.01 611.75 33.16 o 6 13 2 235.59 231.52 14.08 o 7 13 2 697.84 728.35 65.06 o 0 14 2 855.13 996.23 62.28 o 1 14 2 106.58 113.17 9.80 o 2 14 2 44.16 42.68 10.83 o 3 14 2 699.63 663.48 37.93 o 4 14 2 238.26 250.86 11.20 o 5 14 2 353.09 344.55 21.08 o 6 14 2 40.26 40.92 8.35 o 7 14 2 647.75 666.30 38.51 o 1 15 2 2287.31 2790.33 108.90 o 2 15 2 256.08 314.61 27.35 o 3 15 2 3422.08 3216.18 186.59 o 4 15 2 241.91 260.96 17.91 o 5 15 2 601.06 634.48 44.59 o 6 15 2 243.47 252.34 19.99 o 7 15 2 412.61 414.81 18.61 o 0 16 2 303.56 380.72 19.22 o 1 16 2 0.21 5.40 14.62 o 2 16 2 38.15 36.23 11.61 o 3 16 2 128.39 145.47 13.09 o 4 16 2 70.44 93.43 11.99 o 5 16 2 238.40 230.41 15.57 o 6 16 2 63.46 62.44 10.61 o 7 16 2 695.01 673.15 36.39 o 1 17 2 867.48 1078.08 30.54 x 2 17 2 0.14 -14.92 9.33 o 3 17 2 1565.44 1597.95 147.56 o 4 17 2 109.70 91.67 10.66 o 5 17 2 395.75 395.40 31.35 o 6 17 2 14.26 15.96 11.10 o 7 17 2 409.46 393.00 77.14 o 0 18 2 5.92 7.40 13.37 o 1 18 2 8.17 15.16 10.06 o 2 18 2 154.22 151.94 24.07 o 3 18 2 88.66 93.04 13.51 o 4 18 2 3.66 13.97 10.15 o 5 18 2 50.18 59.74 10.56 o 6 18 2 22.48 10.14 9.76 o 1 19 2 835.93 1007.00 39.21 o 2 19 2 55.34 74.05 10.88 o 3 19 2 1337.94 1410.88 127.16 o 4 19 2 157.85 145.43 11.32 o 5 19 2 284.68 299.30 22.15 o 6 19 2 0.56 2.36 10.76 o 0 20 2 67.77 59.80 15.79 o 1 20 2 12.35 2.49 10.23 o 2 20 2 30.80 13.01 10.88 o 3 20 2 167.10 168.34 12.18 o 4 20 2 172.65 151.68 34.20 o 5 20 2 166.67 150.60 10.57 o 6 20 2 15.95 11.06 13.75 o 1 21 2 1712.33 1956.42 55.25 o 2 21 2 27.24 31.13 12.68 o 3 21 2 1797.19 1672.26 178.29 o 4 21 2 18.75 6.26 10.03 o 5 21 2 344.40 310.37 15.90 o 0 22 2 851.36 940.23 19.45 o 1 22 2 45.88 47.88 10.82 o 2 22 2 99.01 75.38 31.88 o 3 22 2 347.21 347.24 44.55 o 4 22 2 54.70 39.48 11.24 o 5 22 2 243.55 221.30 32.46 o 1 23 2 1722.18 1814.43 66.19 o 2 23 2 81.45 72.82 13.64 o 3 23 2 1567.50 1580.57 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13 354.43 348.03 13.14 o 3 1 13 0.14 9.88 14.34 o 1 2 13 6.49 10.26 12.09 o 2 2 13 0.41 1.61 13.04 o 3 2 13 12.38 5.17 14.62 o 0 3 13 679.29 832.74 66.79 o 1 3 13 26.97 26.14 12.76 o 2 3 13 421.24 447.05 19.83 o 3 3 13 0.15 12.83 14.89 o 1 4 13 187.98 248.01 15.72 o 2 4 13 1.05 6.89 13.08 o 3 4 13 171.08 163.67 12.64 o 0 5 13 1013.65 1248.66 122.62 o 1 5 13 116.52 134.66 11.31 o 2 5 13 632.97 709.08 30.22 o 3 5 13 62.23 69.14 15.33 o 1 6 13 457.79 506.33 37.03 o 2 6 13 29.78 37.33 13.49 o 3 6 13 168.80 156.11 24.83 o 0 7 13 1080.83 1255.90 165.05 o 1 7 13 24.62 12.34 13.87 o 2 7 13 601.72 657.39 51.38 o 1 8 13 252.93 265.77 21.47 o 2 8 13 21.34 23.87 16.90 o 0 9 13 551.34 637.02 101.36 o 1 9 13 34.58 46.97 14.04 o 2 9 13 312.63 337.61 30.69 o 1 10 13 578.52 600.04 41.21 o 0 0 14 214.31 220.15 24.93 o 1 0 14 19.38 33.98 19.61 o 1 1 14 180.13 233.61 14.94 o 0 2 14 290.60 337.65 23.86 o 1 2 14 7.09 6.01 18.34 o 1 3 14 376.98 454.74 80.88 o 0 4 14 1009.28 1067.13 40.48 o