#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/14/2011441.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011441_Fobs loop_ _publ_author_name 'Ferfra, S.' 'Ahabchane, N.' 'Essassi, E. M.' 'Pierrot, M.' _publ_section_title ; 3-(Ethoxycarbonyldihydroxymethyl)-2-oxo-1,2-dihydroquinoxaline ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first e463 _journal_page_last e464 _journal_volume 56 _journal_year 2000 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _[local]_cod_data_source_file qa0354IVsup2.hkl _[local]_cod_data_source_block IV loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma 0 0 4 2912.2 2988.0 78.1 0 0 6 4444.1 4531.3 180.1 0 0 8 1205.8 1234.2 33.4 0 0 12 723.4 701.2 22.1 0 0 14 239.2 241.3 7.1 0 0 20 50.0 46.4 5.1 0 1 4 923.0 1017.1 18.0 0 1 5 10.4 11.7 0.6 0 1 6 3.0 3.5 0.6 0 1 8 1264.5 1243.0 24.3 0 1 9 1128.6 1122.0 20.8 0 1 10 33.2 16.1 2.1 0 1 11 671.6 631.3 12.2 0 1 12 223.2 227.0 4.5 0 1 13 218.9 218.5 5.2 0 1 14 154.5 161.5 3.7 0 1 15 455.1 462.6 9.8 0 1 16 122.4 121.3 4.2 0 1 17 23.1 24.6 2.4 0 1 18 61.0 49.2 3.6 0 1 19 31.0 29.8 2.4 0 1 20 33.8 27.9 2.3 0 2 0 402.9 442.3 12.4 0 2 2 1064.9 1073.9 24.7 0 2 3 255.5 269.9 5.5 0 2 4 1347.7 1343.5 27.5 0 2 5 1995.3 1972.0 53.6 0 2 7 337.9 303.1 8.6 0 2 9 499.0 471.5 10.0 0 2 10 63.9 44.9 1.7 0 2 11 272.8 283.8 5.4 0 2 12 2.4 1.0 0.8 0 2 13 742.5 747.7 14.3 0 2 14 280.3 289.5 7.1 0 2 15 60.4 54.2 2.5 0 2 18 9.0 7.1 2.8 0 2 20 13.9 13.4 2.3 0 2 21 28.0 11.4 8.2 0 3 1 13.0 18.9 0.5 0 3 2 251.0 244.2 5.5 0 3 3 683.2 716.9 14.4 0 3 4 409.3 465.5 9.8 0 3 5 4926.4 4993.6 167.0 0 3 6 255.4 271.6 5.4 0 3 7 2511.0 2578.7 48.9 0 3 8 64.1 53.3 1.7 0 3 9 12.5 9.8 0.8 0 3 10 9.4 9.3 0.9 0 3 11 164.4 143.1 3.8 0 3 12 47.8 40.6 1.9 0 3 13 156.6 153.0 4.4 0 3 15 305.6 303.1 7.8 0 3 16 24.1 28.1 2.5 0 3 19 133.5 133.6 4.8 0 4 0 517.4 533.6 16.8 0 4 1 10.0 17.4 0.4 0 4 2 1.1 0.0 0.3 0 4 3 252.0 246.5 5.3 0 4 4 921.0 937.2 19.5 0 4 5 62.9 88.4 1.5 0 4 7 1037.3 1036.5 21.2 0 4 9 14.1 11.1 1.4 0 4 10 146.5 157.7 4.2 0 4 12 16.0 17.6 1.4 0 4 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7 15 15.5 21.6 1.9 0 7 16 4.9 3.2 1.3 0 7 17 5.9 6.0 1.1 0 8 3 771.1 785.5 31.4 0 8 4 547.4 560.4 22.1 0 8 5 46.5 48.3 2.2 0 8 6 283.3 296.0 9.9 0 8 8 77.8 71.5 3.3 0 8 9 43.8 45.8 1.9 0 8 10 100.7 100.2 3.3 0 8 12 62.5 59.1 2.6 0 8 13 7.8 5.9 1.3 0 8 15 37.1 33.1 2.5 0 9 4 31.5 33.6 1.6 0 9 6 305.5 341.9 16.2 0 9 7 41.6 43.3 2.0 0 9 8 27.1 24.3 4.0 0 9 9 5.1 0.8 1.4 0 9 11 4.7 3.3 1.1 0 9 13 13.8 10.1 2.6 1 0 -14 1018.5 980.5 28.4 1 0 -12 760.9 765.7 19.5 1 0 -10 1195.2 1168.8 30.5 1 0 -8 1556.4 1581.5 44.3 1 0 -6 2493.2 2598.9 77.0 1 0 -4 1165.4 1385.5 42.0 1 0 -2 1179.7 1153.7 54.2 1 0 2 12.1 13.5 1.4 1 0 4 198.2 249.2 5.2 1 0 6 741.6 736.6 25.9 1 0 8 3542.0 3398.2 89.2 1 0 10 87.4 101.3 2.9 1 0 12 29.8 18.9 3.8 1 0 14 48.1 47.9 2.2 1 0 16 185.1 206.0 7.7 1 0 18 33.1 34.3 5.9 1 0 20 214.8 183.9 10.9 1 1 -20 22.8 17.2 3.2 1 1 -18 48.8 53.2 2.7 1 1 -17 418.4 410.3 9.8 1 1 -16 961.3 965.2 19.5 1 1 -15 824.2 837.4 18.3 1 1 -14 311.6 308.2 6.1 1 1 -12 5.0 7.2 1.1 1 1 -11 19.4 21.5 1.1 1 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