#------------------------------------------------------------------------------
#$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $
#$Revision: 26025 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2011447.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2011447_Fobs
loop_
_publ_author_name
'Farrugia, Louis J.'
'Peacock, Robert D.'
'Stewart, Brian'
_publ_section_title
;
 Lanthanide complexes of 2,2'-oxydiacetate:
 Na~5~[<i>M</i>(C~4~H~4~O~5~)~3~](BF~4~)~2~&#x00B7;6H~2~O (<i>M</i> =
 Nd, Sm or Gd)
;
_journal_issue                   10
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              e435
_journal_page_last               e436
_journal_volume                  56
_journal_year                    2000
_space_group_IT_number           155
_symmetry_space_group_name_Hall  'R 3 2"'
_symmetry_space_group_name_H-M   'R 3 2 :H'
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                120.000
_cell_length_a                   9.7223
_cell_length_b                   9.7223
_cell_length_c                   28.0728
_exptl_crystal_F_000             1389.00
_reflns_d_resolution_high        0.7112
_[local]_cod_data_source_file    qa0369IIsup3.hkl
_[local]_cod_data_source_block   II
#BEGIN Tags that were not found in dictionaries:
_shelx_title
'  Tris(oxodiacetato)samariate(III) (NaBF4)2 (H2O)6'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            450.65
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'y, x, -z'
'x-y, -y, -z'
'-x, -x+y, -z'
'x+2/3, y+1/3, z+1/3'
'-y+2/3, x-y+1/3, z+1/3'
'-x+y+2/3, -x+1/3, z+1/3'
'y+2/3, x+1/3, -z+1/3'
'x-y+2/3, -y+1/3, -z+1/3'
'-x+2/3, -x+y+1/3, -z+1/3'
'x+1/3, y+2/3, z+2/3'
'-y+1/3, x-y+2/3, z+2/3'
'-x+y+1/3, -x+2/3, z+2/3'
'y+1/3, x+2/3, -z+2/3'
'x-y+1/3, -y+2/3, -z+2/3'
'-x+1/3, -x+y+2/3, -z+2/3'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 1 0 42621.24 42927.75 702.53 o
-1 2 0 42713.05 43177.63 193.51 o
0 3 0 34652.36 32344.29 865.06 o
-2 4 0 27204.45 27359.04 210.64 o
1 4 0 34938.06 35772.74 426.09 o
-1 5 0 34805.68 36298.25 622.87 o
-3 6 0 38589.09 36947.03 308.62 o
0 6 0 23748.95 23596.51 377.44 o
-2 7 0 17887.83 17443.08 171.57 o
1 7 0 12471.64 12232.43 231.82 o
-4 8 0 26259.83 26373.00 312.16 o
-1 8 0 11590.15 11616.83 286.95 o
-3 9 0 8446.31 8393.41 186.05 o
0 9 0 2502.68 2519.65 38.26 o
-5 10 0 4394.25 4265.79 76.56 o
-2 10 0 7484.52 7505.46 190.92 o
1 10 0 2896.34 3036.95 82.12 o
-4 11 0 7769.97 7716.02 111.01 o
-1 11 0 3101.76 3213.70 116.07 o
-6 12 0 4243.81 3982.43 79.21 o
-3 12 0 2547.93 2535.74 49.60 o
-5 13 0 1335.86 1375.89 41.89 o
-1 1 1 38152.55 39978.12 907.00 o
-3 2 1 10445.86 11121.40 220.91 o
0 2 1 1053.33 1254.93 16.15 o
-2 3 1 10177.42 11155.91 129.89 o
1 3 1 24904.65 24671.50 509.56 o
-4 4 1 4108.25 4722.45 214.90 o
-1 4 1 24775.48 25003.54 147.57 o
-6 5 1 21796.65 22452.39 364.42 o
-3 5 1 32075.89 31344.84 262.12 o
0 5 1 39321.94 38578.11 871.20 o
-5 6 1 22295.77 23233.10 181.79 o
-2 6 1 24509.65 25099.86 477.54 o
1 6 1 5591.90 5602.21 85.15 o
-7 7 1 9593.02 9520.52 147.15 o
-4 7 1 2822.05 2774.24 40.67 o
-1 7 1 5412.04 5734.90 71.69 o
-9 8 1 5389.62 5498.21 273.79 o
-6 8 1 3141.38 3062.35 72.91 o
-3 8 1 5626.14 5697.88 74.79 o
0 8 1 3519.08 3423.27 49.90 o
-8 9 1 5824.47 6063.26 80.79 o
-5 9 1 4411.35 4425.92 65.77 o
-2 9 1 6477.60 6633.47 226.00 o
1 9 1 3367.13 3473.45 47.88 o
-10 10 1 1850.22 1888.79 36.25 o
-7 10 1 3223.79 3375.88 117.77 o
-4 10 1 1792.63 1751.56 31.19 o
-1 10 1 3825.21 3912.39 108.38 o
-12 11 1 1732.22 1737.98 44.42 o
-9 11 1 3807.08 3827.60 67.22 o
-6 11 1 3473.38 3357.90 50.55 o
-3 11 1 4980.81 4853.51 97.66 o
0 11 1 2014.19 1982.06 51.87 o
-11 12 1 1988.23 1968.80 48.40 o
-8 12 1 2963.88 2812.06 147.28 o
-5 12 1 4206.19 4030.23 106.54 o
-2 12 1 1356.81 1429.90 40.80 o
-10 13 1 1246.17 1254.95 48.76 o
-7 13 1 1342.05 1291.37 39.38 o
-4 13 1 1471.15 1575.19 69.71 o
0 1 2 56206.13 57294.78 747.47 o
-2 2 2 30925.68 31664.99 1139.30 o
1 2 2 16898.58 17106.63 104.53 o
-4 3 2 14815.79 14667.71 409.55 o
-1 3 2 16019.62 16307.94 425.12 o
-3 4 2 12314.26 12424.03 302.96 o
0 4 2 14491.15 14560.62 146.20 o
-5 5 2 17211.80 18099.65 180.09 o
-2 5 2 3168.85 3218.59 64.41 o
1 5 2 3777.20 3831.12 53.69 o
-7 6 2 8670.88 8708.69 209.64 o
-4 6 2 14152.39 14012.64 137.42 o
-1 6 2 4015.69 4312.62 57.32 o
-6 7 2 8409.04 8648.92 163.21 o
-3 7 2 16951.08 16519.37 161.79 o
0 7 2 11611.86 11268.39 205.88 o
-8 8 2 5150.10 5287.09 80.94 o
-5 8 2 6562.14 6279.61 127.62 o
-2 8 2 4690.40 4823.44 58.48 o
1 8 2 2473.84 2578.29 40.58 o
-10 9 2 1864.04 1816.15 49.11 o
-7 9 2 648.54 656.96 21.33 o
-4 9 2 8721.36 8521.26 118.53 o
-1 9 2 2059.89 2061.13 32.88 o
-9 10 2 2092.38 2011.35 62.97 o
-6 10 2 3423.49 3412.99 47.23 o
-3 10 2 4662.11 4532.64 62.94 o
0 10 2 3525.29 3549.18 46.49 o
-11 11 2 2646.18 2812.62 51.50 o
-8 11 2 3616.13 3501.86 51.39 o
-5 11 2 2070.38 2064.91 35.50 o
-2 11 2 1824.41 1755.68 46.02 o
1 11 2 1056.48 1024.28 36.41 o
-10 12 2 1253.14 1266.55 38.50 o
-7 12 2 2452.71 2386.84 114.97 o
-4 12 2 2273.99 2287.54 150.67 o
-1 12 2 1136.17 1090.04 38.90 o
-9 13 2 1271.75 1303.32 59.58 o
-6 13 2 930.58 889.95 72.54 o
-3 13 2 1452.91 1519.11 44.30 o
1 1 3 23237.92 23234.20 283.26 o
-1 2 3 28132.17 29066.55 719.39 o
-3 3 3 1333.02 1522.96 46.51 o
0 3 3 71961.55 73161.95 2156.69 o
-5 4 3 13976.85 14130.71 895.46 o
-2 4 3 27470.68 27243.76 354.25 o
1 4 3 19944.30 19091.92 377.18 o
-4 5 3 14240.16 14283.65 127.70 o
-1 5 3 20858.51 20551.19 514.60 o
-6 6 3 6280.69 6731.40 73.87 o
-3 6 3 937.83 940.84 30.09 o
0 6 3 12790.47 13068.38 143.06 o
-8 7 3 6908.88 7182.20 207.35 o
-5 7 3 6066.92 6240.17 74.19 o
-2 7 3 12129.99 12535.52 146.45 o
1 7 3 3455.55 3192.69 62.42 o
-7 8 3 6189.44 6293.53 84.32 o
-4 8 3 6545.66 6219.09 103.77 o
-1 8 3 3937.60 3920.12 78.99 o
-9 9 3 5789.81 5843.28 83.37 o
-6 9 3 1099.47 1177.88 25.08 o
-3 9 3 3976.54 4013.54 57.85 o
0 9 3 456.85 474.98 21.20 o
-11 10 3 1771.87 1819.70 41.03 o
-8 10 3 4094.86 4160.46 61.75 o
-5 10 3 2867.76 2881.61 41.20 o
-2 10 3 2131.55 2126.08 67.27 o
1 10 3 2111.18 2143.41 76.77 o
-10 11 3 1652.28 1690.63 40.75 o
-7 11 3 2715.88 2552.55 76.10 o
-4 11 3 1683.32 1717.87 96.86 o
-1 11 3 2292.26 2253.92 56.48 o
-9 12 3 1056.22 1064.83 67.75 o
-6 12 3 3122.12 3045.35 50.13 o
-3 12 3 2943.77 3087.75 135.54 o
-8 13 3 1512.99 1522.00 100.60 o
-5 13 3 983.53 1017.57 36.39 o
-1 1 4 51673.73 52964.15 1051.23 o
-3 2 4 32994.49 33321.18 1227.07 o
0 2 4 2968.04 3225.62 67.31 o
-2 3 4 30795.67 31536.82 753.33 o
1 3 4 15120.29 15221.34 117.87 o
-4 4 4 74616.33 73970.27 2417.48 o
-1 4 4 13491.16 13814.77 236.39 o
-6 5 4 8697.40 8817.83 298.37 o
-3 5 4 10684.76 11130.49 111.05 o
0 5 4 2124.56 2576.58 142.11 o
-5 6 4 9763.11 10271.18 123.97 o
-2 6 4 3640.06 3624.80 51.89 o
1 6 4 11512.49 11189.42 141.11 o
-7 7 4 14387.75 14680.92 259.06 o
-4 7 4 12436.21 12614.50 143.47 o
-1 7 4 12694.68 12530.26 148.73 o
-9 8 4 5385.19 5398.44 199.47 o
-6 8 4 2193.46 2361.21 117.21 o
-3 8 4 13737.91 13419.31 245.74 o
0 8 4 4992.07 4912.18 62.85 o
-8 9 4 4990.08 4887.54 72.45 o
-5 9 4 6506.03 6644.12 148.86 o
-2 9 4 7534.77 7566.86 142.48 o
1 9 4 1676.02 1554.61 32.07 o
-10 10 4 2704.34 2795.96 91.65 o
-7 10 4 6130.62 6342.45 167.87 o
-4 10 4 3735.27 3535.25 108.72 o
-1 10 4 1953.94 1903.67 122.15 o
-12 11 4 1839.68 1938.29 46.19 o
-9 11 4 1503.05 1498.70 96.20 o
-6 11 4 4359.92 4209.29 59.64 o
-3 11 4 4246.79 4249.04 110.95 o
0 11 4 4366.33 4355.13 61.66 o
-11 12 4 1774.62 1843.37 46.29 o
-8 12 4 1898.76 1960.13 43.56 o
-5 12 4 2517.50 2343.09 45.21 o
-2 12 4 1496.58 1560.39 42.13 o
-7 13 4 1788.74 1795.59 44.11 o
-4 13 4 850.47 758.27 36.14 o
0 1 5 33765.14 35747.05 275.13 o
-2 2 5 203082.58 191935.28 12377.71 o
1 2 5 29598.00 28635.97 548.24 o
-4 3 5 40485.66 42196.72 950.67 o
-1 3 5 30415.44 29123.57 436.03 o
-3 4 5 39199.75 40546.64 659.60 o
0 4 5 45254.87 45711.27 264.48 o
-5 5 5 6693.26 6704.86 77.25 o
-2 5 5 46605.09 43808.80 227.27 o
1 5 5 40472.79 40586.32 1353.65 o
-7 6 5 10216.29 10533.00 217.28 o
-4 6 5 18755.44 19470.21 165.65 o
-1 6 5 42277.64 43322.98 708.08 o
-6 7 5 11026.04 11665.22 146.99 o
-3 7 5 14424.85 14158.04 153.93 o
0 7 5 3442.35 3734.76 73.37 o
-8 8 5 24652.81 24010.64 370.57 o
-5 8 5 9742.33 9807.23 254.75 o
-2 8 5 15639.91 16253.75 268.75 o
1 8 5 4860.83 4924.03 111.88 o
-10 9 5 4098.26 4019.24 61.29 o
-7 9 5 10853.01 11090.23 191.89 o
-4 9 5 13437.84 13113.37 519.08 o
-1 9 5 5704.16 5834.11 102.12 o
-9 10 5 3944.48 3897.68 87.67 o
-6 10 5 6548.96 7043.55 97.99 o
-3 10 5 5013.40 4824.18 70.86 o
0 10 5 4757.88 4548.03 64.83 o
-11 11 5 2102.24 2040.14 46.37 o
-8 11 5 3170.07 3170.89 46.44 o
-5 11 5 4160.35 3960.13 81.78 o
-2 11 5 2876.60 2913.10 54.72 o
1 11 5 2683.95 2546.48 52.61 o
-10 12 5 2526.84 2514.10 142.25 o
-7 12 5 2141.29 2133.95 44.12 o
-4 12 5 5319.97 5244.42 73.86 o
-1 12 5 2679.28 2646.40 66.18 o
-9 13 5 2550.55 2585.79 164.65 o
-6 13 5 2028.53 2009.07 45.67 o
0 0 6 12120.45 11638.84 242.55 o
1 1 6 12324.98 12881.57 81.63 o
-1 2 6 14986.70 16195.03 99.54 o
-3 3 6 163794.72 160401.44 9313.33 o
0 3 6 9546.48 9735.05 255.99 o
-5 4 6 31208.46 31069.95 1082.56 o
-2 4 6 17521.07 19360.23 510.41 o
1 4 6 8455.06 8569.33 224.59 o
-4 5 6 28816.18 29647.52 191.54 o
-1 5 6 8029.99 8014.05 235.72 o
-6 6 6 2289.04 2108.49 65.85 o
-3 6 6 16214.90 16077.13 151.48 o
0 6 6 7454.54 7205.88 86.99 o
-8 7 6 11690.99 11604.79 138.73 o
-5 7 6 6284.63 6455.44 107.19 o
-2 7 6 7926.55 7898.80 386.61 o
1 7 6 6967.98 6976.76 126.31 o
-7 8 6 11159.97 11322.08 132.96 o
-4 8 6 10091.50 10076.04 260.59 o
-1 8 6 7024.56 7056.92 125.58 o
-9 9 6 3705.52 3652.75 111.06 o
-6 9 6 1848.88 1882.93 30.85 o
-3 9 6 6331.41 5945.43 85.94 o
0 9 6 5992.14 6202.28 86.16 o
-11 10 6 2258.85 2324.89 46.93 o
-8 10 6 2409.65 2437.00 38.10 o
-5 10 6 3120.76 3043.69 66.19 o
-2 10 6 2153.56 2145.87 119.37 o
1 10 6 2881.96 2804.82 50.22 o
-10 11 6 2086.20 2195.89 45.07 o
-7 11 6 4081.30 4178.37 155.08 o
-4 11 6 4878.22 4586.39 67.40 o
-1 11 6 3007.07 3091.76 73.87 o
-9 12 6 3056.02 3079.94 176.76 o
-6 12 6 1708.36 1689.67 82.36 o
-3 12 6 2179.67 2088.04 75.24 o
-8 13 6 1892.44 1942.56 59.31 o
-5 13 6 1276.61 1169.26 166.63 o
-1 1 7 28654.54 28448.22 187.51 o
-3 2 7 44509.83 45489.98 932.27 o
0 2 7 25579.41 25587.35 137.62 o
-2 3 7 52376.49 54511.35 1231.19 o
1 3 7 13373.55 13696.62 414.25 o
-4 4 7 3617.14 4161.39 48.86 o
-1 4 7 13420.54 14019.41 366.11 o
-6 5 7 2385.72 2344.07 34.09 o
-3 5 7 4414.74 4675.71 140.15 o
0 5 7 3429.10 3336.10 129.61 o
-5 6 7 2929.79 2871.70 40.52 o
-2 6 7 12183.34 12122.05 133.55 o
1 6 7 3575.20 3649.95 49.69 o
-7 7 7 2125.31 2156.47 29.95 o
-4 7 7 9185.48 9344.18 126.70 o
-1 7 7 3430.90 3415.70 48.24 o
-9 8 7 6843.46 6590.08 95.49 o
-6 8 7 8112.42 8254.34 95.55 o
-3 8 7 10488.26 9914.37 101.58 o
0 8 7 4049.61 4006.88 95.03 o
-8 9 7 7077.47 6885.54 145.80 o
-5 9 7 6117.40 6077.90 87.36 o
-2 9 7 3935.34 3939.85 56.08 o
1 9 7 1269.88 1289.84 30.45 o
-10 10 7 2270.86 2219.61 99.80 o
-7 10 7 1811.26 1725.11 61.73 o
-4 10 7 1903.84 1861.25 60.57 o
-1 10 7 1696.02 1751.18 34.14 o
-12 11 7 906.07 847.38 36.68 o
-9 11 7 1978.79 1918.46 56.54 o
-6 11 7 3098.10 2955.51 83.52 o
-3 11 7 2728.37 2693.45 43.04 o
0 11 7 1358.85 1315.58 39.54 o
-11 12 7 795.55 790.96 35.99 o
-8 12 7 1869.72 1847.69 43.52 o
-5 12 7 1937.66 1922.58 59.07 o
-2 12 7 2308.89 2320.44 50.23 o
-7 13 7 1025.04 963.20 36.88 o
-4 13 7 1088.99 1125.92 40.32 o
0 1 8 6168.30 6036.23 39.42 o
-2 2 8 937.49 1021.67 33.80 o
1 2 8 18955.53 19275.90 128.84 o
-4 3 8 23453.87 22951.59 510.29 o
-1 3 8 19437.46 19846.00 256.88 o
-3 4 8 25285.68 25198.37 164.87 o
0 4 8 28511.41 28897.51 183.76 o
-5 5 8 13243.16 13470.95 296.66 o
-2 5 8 16263.13 15900.49 398.45 o
1 5 8 576.19 566.28 20.14 o
-7 6 8 2451.90 2416.93 32.19 o
-4 6 8 13449.25 13667.12 145.23 o
-1 6 8 95.33 87.14 41.65 o
-6 7 8 2258.90 2198.02 33.72 o
-3 7 8 8730.78 9029.34 126.74 o
0 7 8 8584.21 8502.21 135.99 o
-8 8 8 7086.11 7124.04 96.03 o
-5 8 8 1957.54 1951.94 109.38 o
-2 8 8 4394.73 4214.67 81.31 o
1 8 8 4706.64 4633.27 122.19 o
-10 9 8 1947.09 2060.62 36.68 o
-7 9 8 2832.00 2904.70 94.52 o
-4 9 8 1361.19 1301.13 26.66 o
-1 9 8 4606.26 4425.03 90.15 o
-9 10 8 2037.70 2160.81 38.21 o
-6 10 8 4286.91 4169.26 198.08 o
-3 10 8 4196.74 3954.93 60.70 o
0 10 8 1624.05 1597.60 38.51 o
-11 11 8 1865.33 1997.73 45.88 o
-8 11 8 2084.19 2215.85 61.98 o
-5 11 8 1175.29 1084.27 37.91 o
-2 11 8 1139.85 1174.78 35.38 o
1 11 8 1248.65 1244.84 39.83 o
-10 12 8 476.34 476.62 39.72 o
-7 12 8 1697.23 1738.68 110.49 o
-4 12 8 2191.05 2109.70 156.74 o
-1 12 8 1140.19 1100.51 37.15 o
-9 13 8 1443.23 1545.98 65.94 o
-6 13 8 1051.91 1000.50 72.96 o
0 0 9 17292.74 16278.70 287.71 o
1 1 9 44197.03 42100.26 402.23 o
-1 2 9 47394.39 44784.46 377.21 o
-3 3 9 2354.51 2831.44 38.64 o
0 3 9 22531.50 22752.52 378.57 o
-5 4 9 10284.88 10847.74 120.08 o
-2 4 9 14080.78 14161.47 162.29 o
1 4 9 18455.58 18059.23 377.24 o
-4 5 9 9755.63 10384.12 299.79 o
-1 5 9 21532.45 21672.63 364.35 o
-6 6 9 433.20 452.26 42.80 o
-3 6 9 12404.64 13383.70 227.27 o
0 6 9 1261.74 1167.00 22.80 o
-8 7 9 10584.09 10492.76 110.84 o
-5 7 9 12087.62 11926.00 257.67 o
-2 7 9 8122.13 8327.54 162.47 o
1 7 9 7825.28 7658.57 133.17 o
-7 8 9 11124.73 11009.87 127.75 o
-4 8 9 9602.98 9576.77 303.06 o
-1 8 9 8320.08 7752.55 210.00 o
-9 9 9 2319.53 2402.48 52.99 o
-6 9 9 7840.37 7668.39 322.42 o
-3 9 9 9987.05 9743.27 238.84 o
0 9 9 6748.17 6672.88 181.55 o
-11 10 9 2277.54 2332.33 54.17 o
-8 10 9 2955.90 3091.89 63.13 o
-5 10 9 6961.78 7314.63 406.59 o
-2 10 9 2191.31 2173.26 61.63 o
1 10 9 1822.53 1711.31 42.13 o
-10 11 9 2190.31 2285.57 73.34 o
-7 11 9 2757.79 2700.90 64.42 o
-4 11 9 2819.74 2772.96 42.24 o
-1 11 9 1633.55 1590.19 41.26 o
-9 12 9 2020.44 2040.25 193.18 o
-6 12 9 1348.03 1303.91 86.57 o
-3 12 9 1723.29 1735.09 45.04 o
-8 13 9 2175.85 2272.24 116.37 o
-5 13 9 1842.55 1801.39 159.47 o
-1 1 10 1503.43 1378.93 14.98 o
-3 2 10 44144.25 44532.05 1113.12 o
0 2 10 40347.24 40062.32 195.68 o
-2 3 10 46344.86 47774.10 221.83 o
1 3 10 66716.28 67267.63 523.74 o
-4 4 10 76775.53 76067.81 2941.77 o
-1 4 10 67671.20 67216.73 1290.46 o
-6 5 10 5729.30 5552.12 69.45 o
-3 5 10 8352.04 8409.53 106.79 o
0 5 10 15515.89 15528.03 324.02 o
-5 6 10 5101.25 5016.52 142.76 o
-2 6 10 15116.27 15470.32 313.24 o
1 6 10 7426.23 7368.97 124.64 o
-7 7 10 20964.66 21569.46 214.94 o
-4 7 10 17429.00 17959.32 812.62 o
-1 7 10 7620.47 7673.19 127.74 o
-9 8 10 3625.84 3737.92 53.58 o
-6 8 10 14289.59 14767.76 723.34 o
-3 8 10 7419.36 7310.21 144.70 o
0 8 10 17826.95 17489.30 214.17 o
-8 9 10 3881.99 3916.68 85.49 o
-5 9 10 5340.96 5280.94 177.71 o
-2 9 10 4228.18 4097.41 76.36 o
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