#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/14/2011474.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2011474_Fobs
loop_
_publ_author_name
'K\"onig, Uwe-Christoph'
'Berkei, Michael'
'Hirsch, Claudia'
'Preut, Hans'
'Mitchell, Terence Nigel'
_publ_section_title
;
 Chlorodimethyl(<i>N</i>-methylpyrrolidinone)tin(IV)-\m-chloro-dichlorodimethyltin(IV)
;
_journal_issue                   10
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              e450
_journal_page_last               e451
_journal_volume                  56
_journal_year                    2000
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                78.448
_cell_angle_beta                 84.361
_cell_angle_gamma                84.378
_cell_length_a                   7.3650
_cell_length_b                   10.3110
_cell_length_c                   12.3110
_exptl_crystal_F_000             516.00
_reflns_d_resolution_high        0.7811
_[local]_cod_data_source_file    qd0036Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' ccd1141 in P-1'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            211.73
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 0 0 3026.63 3104.93 114.40 o
2 0 0 12981.25 12724.63 468.07 o
3 0 0 2558.67 2577.05 78.88 o
4 0 0 124.89 102.96 23.29 o
5 0 0 53.20 70.45 23.09 o
6 0 0 190.25 176.80 34.82 o
7 0 0 2912.77 2753.84 190.20 o
8 0 0 186.87 92.42 107.15 o
9 0 0 790.72 759.45 199.57 o
-9 1 0 25.02 -62.95 150.01 o
-8 1 0 1183.53 1196.10 175.46 o
-7 1 0 441.29 478.17 65.63 o
-6 1 0 614.14 535.77 44.20 o
-5 1 0 1632.20 1705.08 57.59 o
-4 1 0 65.38 84.38 21.43 o
-3 1 0 48.92 53.58 16.07 o
-2 1 0 12602.73 12795.47 331.32 o
-1 1 0 32935.58 31693.54 1260.96 o
1 1 0 21523.11 21158.91 885.94 o
2 1 0 20118.73 19827.71 663.18 o
3 1 0 0.07 5.36 24.11 o
4 1 0 8197.05 8405.67 217.75 o
5 1 0 626.54 575.69 37.74 o
6 1 0 1511.66 1562.38 67.52 o
7 1 0 590.36 521.03 60.27 o
8 1 0 487.94 358.96 96.44 o
9 1 0 873.69 850.53 211.63 o
-9 2 0 141.26 162.07 140.64 o
-8 2 0 519.79 574.61 127.24 o
-7 2 0 90.68 155.37 61.61 o
-6 2 0 4407.16 4532.59 229.04 o
-5 2 0 1225.86 1141.18 45.54 o
-4 2 0 4766.93 4914.32 136.62 o
-3 2 0 1497.02 1630.30 41.81 o
-2 2 0 2139.86 2350.43 64.32 o
-1 2 0 6381.78 6110.87 178.49 o
0 2 0 124.51 271.49 20.76 o
1 2 0 24926.75 22145.52 924.17 o
2 2 0 13891.92 13790.30 510.32 o
3 2 0 10763.52 10865.32 360.30 o
4 2 0 1832.44 1780.92 52.56 o
5 2 0 623.62 586.19 34.48 o
6 2 0 5.82 15.92 36.17 o
7 2 0 310.48 118.77 74.34 o
8 2 0 777.73 759.45 137.96 o
9 2 0 355.54 464.78 141.98 o
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-7 3 0 1555.18 1493.45 152.69 o
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-4 3 0 2395.18 2361.32 93.09 o
-3 3 0 1325.21 1304.35 47.55 o
-2 3 0 406.67 444.79 20.84 o
-1 3 0 2005.44 2071.02 81.63 o
0 3 0 2514.97 2363.40 88.18 o
1 3 0 25046.29 22414.12 1066.80 o
2 3 0 1794.99 1749.50 88.38 o
3 3 0 12577.45 12801.43 532.42 o
4 3 0 877.51 893.04 42.86 o
5 3 0 2045.83 2093.51 91.65 o
6 3 0 729.07 694.70 47.95 o
7 3 0 93.46 101.14 53.35 o
8 3 0 41.82 31.93 61.45 o
-8 4 0 7.88 -9.38 119.21 o
-7 4 0 1136.87 940.27 117.87 o
-6 4 0 377.02 389.77 87.06 o
-5 4 0 6392.90 6454.87 266.75 o
-4 4 0 2546.55 2651.17 84.65 o
-3 4 0 2605.56 2658.97 164.08 o
-2 4 0 641.32 649.50 26.98 o
-1 4 0 4790.11 4730.15 182.83 o
0 4 0 1184.46 1201.74 44.73 o
1 4 0 297.30 248.02 23.19 o
2 4 0 18312.88 16863.89 695.58 o
3 4 0 2476.07 2520.71 82.28 o
4 4 0 3715.51 3749.03 180.82 o
5 4 0 2852.40 3061.45 134.46 o
6 4 0 0.75 21.19 44.22 o
7 4 0 1096.75 1034.18 75.95 o
8 4 0 6.81 44.20 84.38 o
9 4 0 37.57 -25.45 131.26 o
-8 5 0 164.14 168.77 141.98 o
-7 5 0 10.71 1.34 105.81 o
-6 5 0 1564.75 1548.97 100.92 o
-5 5 0 3832.88 3807.43 216.87 o
-4 5 0 653.12 594.91 34.38 o
-3 5 0 11582.98 12244.95 652.97 o
-2 5 0 702.33 675.55 49.56 o
-1 5 0 4662.95 4584.95 219.66 o
0 5 0 215.53 229.77 41.52 o
1 5 0 1223.82 1217.08 117.20 o
2 5 0 5261.53 4795.24 163.55 o
3 5 0 693.38 672.39 62.95 o
4 5 0 2587.26 2526.55 88.91 o
5 5 0 5.45 -26.24 33.79 o
6 5 0 4631.81 5062.89 270.35 o
7 5 0 451.76 467.40 76.24 o
8 5 0 112.60 182.16 91.08 o
-7 6 0 37.75 -60.27 120.55 o
-6 6 0 801.10 723.92 90.36 o
-5 6 0 151.05 165.87 58.26 o
-4 6 0 8641.21 8570.29 767.49 o
-3 6 0 3634.23 3748.08 371.69 o
-2 6 0 5209.83 5034.00 250.47 o
-1 6 0 2936.97 2886.61 158.05 o
0 6 0 305.64 283.58 42.19 o
1 6 0 135.27 109.13 32.58 o
2 6 0 321.08 288.78 37.57 o
3 6 0 2513.81 2350.52 98.48 o
4 6 0 1222.89 1179.61 71.66 o
5 6 0 2041.33 2078.86 112.45 o
6 6 0 1500.58 1572.17 96.74 o
7 6 0 193.54 146.00 92.42 o
8 6 0 446.44 356.28 120.55 o
-7 7 0 7.53 54.92 141.98 o
-6 7 0 77.89 76.47 80.03 o
-5 7 0 1458.22 1484.01 177.47 o
-4 7 0 6983.21 6972.22 712.57 o
-3 7 0 123.20 89.94 44.09 o
-2 7 0 8184.01 8289.06 740.03 o
-1 7 0 418.58 379.18 40.87 o
0 7 0 3443.45 3474.64 177.47 o
1 7 0 1324.67 1217.91 70.86 o
2 7 0 335.02 301.39 42.34 o
3 7 0 2336.70 2208.49 121.97 o
4 7 0 170.51 155.42 37.82 o
5 7 0 2883.01 3006.06 251.81 o
6 7 0 39.00 25.84 53.26 o
7 7 0 1205.77 1292.54 166.09 o
8 7 0 1013.15 920.18 289.31 o
-6 8 0 87.88 120.87 95.15 o
-5 8 0 304.31 294.69 85.10 o
-4 8 0 83.75 63.58 68.96 o
-3 8 0 3640.99 3747.56 386.42 o
-2 8 0 2462.87 2389.47 383.74 o
-1 8 0 2038.87 1963.69 209.62 o
0 8 0 4871.20 4969.13 384.41 o
1 8 0 102.24 97.16 46.88 o
2 8 0 12.79 5.87 46.90 o
3 8 0 21.11 19.93 46.34 o
4 8 0 2074.64 2042.18 142.78 o
5 8 0 485.53 414.36 60.81 o
6 8 0 600.29 547.82 91.08 o
7 8 0 2250.34 2090.83 329.50 o
-6 9 0 352.75 143.32 172.78 o
-5 9 0 4.91 34.03 98.16 o
-4 9 0 128.60 99.01 84.67 o
-3 9 0 1683.97 1659.12 326.15 o
-2 9 0 91.32 189.12 68.85 o
-1 9 0 3735.00 4042.75 338.87 o
0 9 0 5.02 18.99 50.50 o
1 9 0 2440.26 2542.74 275.92 o
2 9 0 482.75 516.92 77.69 o
3 9 0 322.59 286.09 72.07 o
4 9 0 74.24 146.91 99.12 o
5 9 0 1.02 -36.61 97.11 o
6 9 0 667.30 601.40 100.46 o
7 9 0 282.25 454.06 226.36 o
-5 10 0 96.29 185.08 130.02 o
-4 10 0 35.37 102.49 104.31 o
-3 10 0 600.09 528.42 140.64 o
-2 10 0 881.15 956.84 123.38 o
-1 10 0 1470.05 1807.99 136.99 o
0 10 0 1464.39 1558.02 126.44 o
1 10 0 1377.25 1559.85 124.08 o
2 10 0 0.18 -38.84 88.40 o
3 10 0 492.34 417.80 174.12 o
4 10 0 14.32 12.05 69.65 o
5 10 0 3.03 -38.84 92.42 o
-4 11 0 7.02 -5.36 191.54 o
-3 11 0 21.57 -50.62 113.88 o
-2 11 0 1318.74 1420.74 190.45 o
-1 11 0 0.04 -47.07 81.39 o
0 11 0 1387.98 1593.39 172.37 o
1 11 0 136.50 134.32 116.53 o
2 11 0 909.68 878.66 155.37 o
3 11 0 534.20 474.15 131.26 o
4 11 0 92.74 119.21 77.69 o
5 11 0 0.44 -148.68 168.77 o
-2 12 0 92.68 263.87 239.76 o
-1 12 0 198.91 199.13 104.33 o
0 12 0 284.20 412.64 123.08 o
1 12 0 466.86 500.49 127.39 o
2 12 0 1520.32 1916.71 462.10 o
3 12 0 14.90 93.76 135.28 o
4 12 0 364.64 419.24 135.28 o
-3 -12 1 90.83 91.08 132.60 o
-2 -12 1 0.24 -81.70 132.60 o
-1 -12 1 245.58 151.70 120.59 o
0 -12 1 2.93 37.94 189.53 o
1 -12 1 698.18 911.08 193.38 o
2 -12 1 832.29 961.71 241.25 o
-5 -11 1 284.48 255.83 195.55 o
-4 -11 1 377.95 405.84 109.83 o
-3 -11 1 3.11 42.86 105.81 o
-2 -11 1 0.77 6.70 100.46 o
-1 -11 1 0.20 81.65 89.40 o
0 -11 1 36.71 6.04 94.06 o
1 -11 1 1181.38 1275.99 155.44 o
2 -11 1 4.25 -7.63 87.60 o
3 -11 1 1043.75 1383.62 330.84 o
4 -11 1 10.22 75.01 214.31 o
-5 -10 1 2077.22 2077.44 254.49 o
-4 -10 1 653.34 632.20 95.10 o
-3 -10 1 123.33 118.90 69.65 o
-2 -10 1 519.30 456.91 117.87 o
-1 -10 1 82.18 159.39 93.76 o
0 -10 1 6.72 7.19 72.85 o
1 -10 1 223.20 223.73 82.60 o
2 -10 1 829.77 927.45 122.43 o
3 -10 1 1394.58 1480.33 343.56 o
4 -10 1 45.62 7.07 105.46 o
5 -10 1 615.91 535.77 235.74 o
-7 -9 1 137.97 -111.17 199.57 o
-6 -9 1 1396.04 1401.03 233.06 o
-5 -9 1 2138.43 2069.40 202.25 o
-4 -9 1 74.39 60.95 70.72 o
-3 -9 1 3776.67 3701.41 256.54 o
-2 -9 1 164.03 153.45 56.83 o
-1 -9 1 1206.36 1311.91 103.68 o
0 -9 1 223.01 218.43 53.35 o
1 -9 1 217.73 172.38 65.27 o
2 -9 1 1280.86 1195.35 104.50 o
3 -9 1 100.65 114.62 63.88 o
4 -9 1 1694.83 1509.48 284.63 o
5 -9 1 518.92 413.13 143.99 o
6 -9 1 1268.11 918.84 302.71 o
-7 -8 1 13.12 -48.22 125.91 o
-6 -8 1 741.32 774.18 108.49 o
-5 -8 1 224.47 181.19 53.73 o
-4 -8 1 4677.77 4768.11 289.65 o
-3 -8 1 3430.46 3375.42 219.86 o
-2 -8 1 362.42 370.01 51.86 o
-1 -8 1 2587.46 2605.65 280.61 o
0 -8 1 297.87 264.64 50.91 o
1 -8 1 110.77 128.64 44.99 o
2 -8 1 7.26 29.18 45.15 o
3 -8 1 547.90 487.71 71.66 o
4 -8 1 2620.23 2775.27 251.81 o
5 -8 1 606.28 588.03 105.14 o
6 -8 1 2343.44 2049.59 490.23 o
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-5 -7 1 343.62 302.32 47.80 o
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-3 -7 1 176.21 164.80 46.34 o
-2 -7 1 2716.00 2574.00 145.32 o
-1 -7 1 2254.09 2297.06 109.75 o
0 -7 1 2227.30 2168.09 208.95 o
1 -7 1 3820.69 3863.46 295.34 o
2 -7 1 16.67 15.81 33.43 o
3 -7 1 1747.11 1646.55 236.41 o
4 -7 1 550.85 437.15 65.78 o
5 -7 1 2564.53 2479.26 368.34 o
6 -7 1 412.95 407.73 88.89 o
7 -7 1 1092.39 1086.29 189.21 o
-8 -6 1 240.44 186.18 87.06 o
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-5 -6 1 1760.38 1753.85 98.16 o
-4 -6 1 173.10 141.12 36.34 o
-3 -6 1 1874.14 1700.53 89.94 o
-2 -6 1 7523.88 7605.21 455.40 o
-1 -6 1 30.48 47.38 30.13 o
0 -6 1 8307.90 8360.81 378.45 o
1 -6 1 17.84 15.07 30.13 o
2 -6 1 924.10 810.11 98.45 o
3 -6 1 238.40 197.08 39.55 o
4 -6 1 264.52 246.22 70.99 o
5 -6 1 1621.45 1551.27 131.93 o
6 -6 1 8.45 42.51 65.70 o
7 -6 1 2788.88 3379.35 541.12 o
-8 -5 1 824.01 742.04 131.26 o
-7 -5 1 10.58 24.11 58.93 o
-6 -5 1 1.78 -32.40 44.35 o
-5 -5 1 21.12 2.68 42.86 o
-4 -5 1 619.42 568.00 40.85 o
-3 -5 1 3019.88 2820.76 149.06 o
-2 -5 1 2887.80 2688.35 114.99 o
-1 -5 1 8390.30 8519.60 291.83 o
0 -5 1 2489.57 2417.77 82.89 o
1 -5 1 5847.80 5749.49 216.32 o
2 -5 1 5396.52 5214.36 224.35 o
3 -5 1 0.87 -3.64 30.47 o
4 -5 1 0.25 -5.05 36.36 o
5 -5 1 1527.77 1346.90 93.09 o
6 -5 1 950.82 967.15 72.38 o
7 -5 1 1037.19 1102.34 178.14 o
8 -5 1 789.51 671.05 234.40 o
-8 -4 1 858.96 912.14 136.62 o
-7 -4 1 241.76 258.81 55.02 o
-6 -4 1 764.43 809.95 60.10 o
-5 -4 1 106.00 117.87 31.63 o
-4 -4 1 186.24 183.92 23.81 o
-3 -4 1 1592.49 1552.64 54.23 o
-2 -4 1 2835.98 2617.32 99.24 o
-1 -4 1 6591.03 6316.88 260.04 o
0 -4 1 479.70 462.86 26.52 o
1 -4 1 11760.08 10850.82 349.59 o
2 -4 1 3168.49 3165.55 104.40 o
3 -4 1 5729.92 5625.27 143.03 o
4 -4 1 364.64 354.31 31.82 o
5 -4 1 348.69 301.49 35.91 o
6 -4 1 1108.51 1054.12 88.40 o
7 -4 1 43.24 38.84 77.69 o
8 -4 1 1822.57 1841.70 412.54 o
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-6 -3 1 1160.95 1168.15 72.35 o
-5 -3 1 1745.40 1787.78 110.50 o
-4 -3 1 775.11 793.27 38.84 o
-3 -3 1 1145.97 1206.81 54.92 o
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-1 -3 1 1050.38 941.11 51.09 o
0 -3 1 522.00 569.33 23.68 o
1 -3 1 11855.00 11191.18 320.18 o
2 -3 1 9935.99 9734.52 332.85 o
3 -3 1 9799.03 9952.43 259.73 o
4 -3 1 535.63 569.25 30.72 o
5 -3 1 82.84 75.01 32.15 o
6 -3 1 250.31 204.93 54.92 o
7 -3 1 95.32 76.35 88.40 o
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-8 -2 1 1234.32 1392.99 191.54 o
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0 -2 1 26956.40 25766.49 1084.55 o
1 -2 1 66.23 87.64 11.88 o
2 -2 1 44829.66 44100.14 1202.12 o
3 -2 1 4802.67 5071.78 124.83 o
4 -2 1 3052.61 3292.08 94.26 o
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6 -2 1 1406.17 1446.57 100.46 o
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-1 -1 1 5722.35 5564.58 260.28 o
0 -1 1 1997.22 1959.61 86.23 o
1 -1 1 29346.50 27977.43 1373.57 o
2 -1 1 12432.56 12518.68 314.33 o
3 -1 1 7679.23 7948.42 208.65 o
4 -1 1 23363.13 23815.18 1022.65 o
5 -1 1 258.57 218.32 29.47 o
6 -1 1 1814.43 1788.12 75.01 o
7 -1 1 0.26 -14.73 54.92 o
8 -1 1 93.38 97.78 97.78 o
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1 0 1 5217.57 5185.02 178.06 o
2 0 1 35.08 43.52 8.92 o
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4 0 1 13721.95 13943.44 349.68 o
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0 1 1 551.14 550.12 19.95 o
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8 1 1 501.48 513.00 111.17 o
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-4 2 1 107.92 104.47 22.77 o
-3 2 1 5869.67 6015.72 143.45 o
-2 2 1 8852.57 9034.46 243.72 o
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0 2 1 362.30 338.60 14.12 o
1 2 1 2406.35 2456.98 88.19 o
2 2 1 577.98 562.73 22.29 o
3 2 1 1113.70 1153.51 39.25 o
4 2 1 17255.22 17768.50 607.43 o
5 2 1 5196.94 5519.52 172.20 o
6 2 1 486.28 452.85 52.81 o
7 2 1 1739.69 1799.97 129.28 o
8 2 1 8.95 21.25 72.41 o
9 2 1 314.04 313.42 128.58 o
-8 3 1 148.83 167.43 132.60 o
-7 3 1 25.77 30.81 64.29 o
-6 3 1 1310.37 1339.42 99.12 o
-5 3 1 227.43 265.20 36.16 o
-4 3 1 1545.60 1589.40 94.43 o
-3 3 1 9670.18 10030.42 268.69 o
-2 3 1 318.75 288.76 17.92 o
-1 3 1 16077.84 15624.02 508.31 o
0 3 1 2.27 6.05 13.51 o
1 3 1 3465.76 3265.82 121.47 o
2 3 1 3919.67 3926.19 153.02 o
3 3 1 345.36 368.92 24.74 o
4 3 1 5294.30 5384.26 216.32 o
5 3 1 107.87 113.35 40.18 o
6 3 1 5512.88 5558.28 254.51 o
7 3 1 368.86 409.86 93.76 o
8 3 1 1784.10 1982.34 269.22 o
9 3 1 355.00 333.21 116.48 o
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