#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:26:34 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180783 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/14/2011495.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011495_Fobs loop_ _publ_author_name 'Liu, Yunqi' 'Fletcher, Michelle O.' 'Fronczek, Frank R.' _publ_section_title ; Tetrakis(diethylamino)phosphonium bromide hemihydrate ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1351 _journal_page_last 1353 _journal_volume 56 _journal_year 2000 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 92.144 _cell_angle_beta 91.799 _cell_angle_gamma 90.246 _cell_length_a 14.2475 _cell_length_b 14.9756 _cell_length_c 20.7125 _exptl_crystal_F_000 1752.00 _reflns_d_resolution_high 0.7697 _cod_data_source_file da1144IIIsup2.hkl _cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' TDEAPB' _shelx_refln_list_code 4 _shelx_f_calc_maximum 347.49 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 26798.77 25207.63 511.59 o 3 0 0 4494.86 3999.09 59.10 o 4 0 0 2563.05 2882.14 43.93 o 5 0 0 31628.11 31835.17 483.96 o 6 0 0 3034.47 2588.02 41.52 o 7 0 0 7.88 -24.12 30.91 o 8 0 0 11188.78 10735.18 169.39 o 9 0 0 1160.62 1227.62 44.86 o 10 0 0 2731.34 2633.43 65.97 o 11 0 0 1442.97 1431.56 61.86 o 12 0 0 544.75 498.43 57.42 o 13 0 0 1258.41 1361.71 68.99 o 14 0 0 47.85 101.57 68.28 o 15 0 0 788.49 728.48 69.31 o 16 0 0 1.90 10.19 95.80 o 17 0 0 74.22 91.38 240.51 o 18 0 0 533.23 356.73 413.81 o -18 1 0 428.51 503.49 292.85 o -17 1 0 311.58 -3.40 213.01 o -16 1 0 477.39 367.60 89.35 o -15 1 0 1027.67 1092.45 84.61 o -14 1 0 367.31 361.14 71.01 o -13 1 0 163.16 152.53 50.28 o -12 1 0 57.75 94.78 54.35 o -11 1 0 2473.34 2543.87 58.82 o -10 1 0 3469.37 3538.97 69.39 o -9 1 0 11371.42 11796.09 190.46 o -8 1 0 3296.51 3470.71 55.12 o -7 1 0 2080.81 2314.60 39.11 o -6 1 0 830.31 806.19 26.51 o -5 1 0 9261.20 8722.82 120.05 o -4 1 0 24783.44 23603.19 344.16 o -3 1 0 7933.82 7694.48 102.87 o -2 1 0 10403.42 10367.69 203.57 o 1 1 0 43.85 -3.40 17.33 o 2 1 0 17220.84 15925.89 253.66 o 3 1 0 7661.95 7640.40 102.49 o 4 1 0 131.50 247.67 16.65 o 5 1 0 419.10 418.64 23.79 o 6 1 0 5074.83 4825.65 72.92 o 7 1 0 8913.14 8617.98 130.04 o 8 1 0 2454.55 2533.04 58.84 o 9 1 0 648.59 747.55 44.51 o 10 1 0 126.28 142.68 44.50 o 11 1 0 1994.08 1958.40 61.87 o 12 1 0 7347.52 7398.30 150.51 o 13 1 0 44.10 87.98 71.00 o 14 1 0 764.24 802.56 72.71 o 15 1 0 2481.56 2537.57 99.94 o 16 1 0 89.63 44.16 95.12 o 17 1 0 2166.09 3041.60 321.53 o 18 1 0 31.07 61.15 294.87 o -18 2 0 66.48 -98.18 285.36 o -17 2 0 922.24 786.25 192.99 o -16 2 0 10.38 13.59 91.04 o -15 2 0 23.13 -10.19 71.68 o -14 2 0 218.54 214.03 68.28 o -13 2 0 2825.29 2561.50 88.40 o -12 2 0 1476.04 1484.87 58.46 o -11 2 0 2969.08 2884.34 62.57 o -10 2 0 4836.77 4827.52 81.00 o -9 2 0 428.95 437.96 34.32 o -8 2 0 8321.60 7972.14 125.15 o -7 2 0 0.79 10.19 23.78 o -6 2 0 6094.85 6380.41 93.42 o -5 2 0 228.60 264.33 16.99 o -4 2 0 6871.62 6841.04 96.69 o -3 2 0 7567.91 7258.62 109.57 o -2 2 0 72652.24 75424.64 1305.95 o -1 2 0 1.19 94.78 10.19 o 0 2 0 32328.75 29451.50 906.82 o 1 2 0 272.44 328.65 12.57 o 2 2 0 67818.22 64736.63 1515.47 o 3 2 0 4693.99 4625.26 79.54 o 4 2 0 3793.86 3650.54 63.39 o 5 2 0 1910.44 1807.60 39.80 o 6 2 0 8524.46 8181.71 147.84 o 7 2 0 2453.95 2417.02 51.70 o 8 2 0 15056.40 15041.67 243.89 o 9 2 0 689.52 585.14 45.19 o 10 2 0 512.84 493.35 41.45 o 11 2 0 274.93 322.41 54.36 o 12 2 0 441.22 428.09 67.61 o 13 2 0 3255.52 3366.35 101.67 o 14 2 0 289.18 328.52 88.67 o 15 2 0 937.33 904.86 105.33 o 16 2 0 1808.17 1539.22 109.77 o 17 2 0 27.93 37.37 159.66 o 18 2 0 327.61 413.79 301.00 o -18 3 0 428.19 258.88 401.23 o -17 3 0 850.30 901.08 178.38 o -16 3 0 815.99 625.18 128.43 o -15 3 0 628.24 549.05 65.57 o -14 3 0 1683.79 1502.88 72.39 o -13 3 0 503.86 447.80 46.89 o -12 3 0 4728.77 4499.33 101.72 o -11 3 0 3775.29 3814.70 79.25 o -10 3 0 600.66 573.89 36.36 o -9 3 0 1056.15 1035.52 41.12 o -8 3 0 18714.73 18089.23 299.04 o -7 3 0 842.20 796.26 26.17 o -6 3 0 1288.10 1231.99 28.56 o -5 3 0 24662.78 24605.07 442.48 o -4 3 0 1292.26 1228.22 36.72 o -3 3 0 72243.59 74493.06 1410.70 o -2 3 0 408.33 421.08 16.65 o -1 3 0 954.13 1025.08 26.19 o 0 3 0 202.38 210.67 16.99 o 1 3 0 2380.24 2572.96 47.36 o 2 3 0 2884.12 2784.61 49.41 o 3 3 0 39139.17 37767.61 760.25 o 4 3 0 1855.65 1744.12 39.12 o 5 3 0 14088.98 13196.08 228.65 o 6 3 0 3203.41 3255.17 66.70 o 7 3 0 1903.48 1851.79 50.32 o 8 3 0 14929.39 14525.72 267.76 o 9 3 0 518.04 554.51 43.83 o 10 3 0 2921.44 2890.95 81.62 o 11 3 0 3828.37 3735.84 92.52 o 12 3 0 29.89 84.93 75.08 o 13 3 0 337.48 315.96 64.21 o 14 3 0 643.11 663.90 99.21 o 15 3 0 733.03 897.67 108.39 o 16 3 0 1594.45 1396.40 126.42 o 17 3 0 1183.66 976.25 131.16 o 18 3 0 28.89 -149.81 425.31 o -18 4 0 531.66 475.30 279.61 o -17 4 0 11.87 -64.54 177.33 o -16 4 0 218.81 268.38 231.01 o -15 4 0 1194.11 1215.16 146.46 o -14 4 0 1016.03 1039.11 75.10 o -13 4 0 24.43 37.37 44.16 o -12 4 0 3166.71 3205.89 85.69 o -11 4 0 361.21 337.03 34.31 o -10 4 0 235.09 243.93 30.92 o -9 4 0 1566.45 1660.82 42.83 o -8 4 0 200.61 129.10 34.31 o -7 4 0 2657.54 2681.97 66.33 o -6 4 0 834.34 1031.80 52.34 o -5 4 0 5004.30 5230.47 118.23 o -4 4 0 933.68 822.95 33.31 o -3 4 0 2422.82 2464.76 46.29 o -2 4 0 16777.58 16243.62 284.33 o -1 4 0 12980.91 12610.56 236.93 o 0 4 0 11795.56 10985.10 208.92 o 1 4 0 7257.98 6761.37 125.19 o 2 4 0 5258.28 5306.47 93.50 o 3 4 0 625.66 654.93 47.58 o 4 4 0 395.34 397.56 46.55 o 5 4 0 1103.03 1159.50 35.69 o 6 4 0 6862.57 6606.39 123.42 o 7 4 0 77.86 145.40 33.63 o 8 4 0 69.38 138.60 43.82 o 9 4 0 10689.21 10387.25 190.35 o 10 4 0 5.64 -13.59 50.96 o 11 4 0 157.30 118.90 61.15 o 12 4 0 562.14 482.80 71.69 o 13 4 0 83.53 94.78 78.13 o 14 4 0 4028.83 4047.97 126.17 o 15 4 0 527.79 562.63 94.11 o 16 4 0 156.38 125.36 152.53 o 17 4 0 506.81 495.69 155.60 o 18 4 0 192.01 640.03 312.54 o -17 5 0 377.79 243.93 207.58 o -16 5 0 2561.59 2496.36 227.07 o -15 5 0 249.72 345.84 175.64 o -14 5 0 261.53 277.90 77.80 o -13 5 0 2068.46 2089.40 106.73 o -12 5 0 1799.68 1641.67 89.73 o -11 5 0 366.34 305.77 65.23 o -10 5 0 20087.38 21005.83 491.58 o -9 5 0 3381.63 3374.18 94.90 o -8 5 0 1297.29 1349.01 59.82 o -7 5 0 1223.49 1069.64 53.36 o -6 5 0 2371.98 2242.31 66.32 o -5 5 0 37539.95 39577.11 726.20 o -4 5 0 944.04 1031.93 29.91 o -3 5 0 19484.98 19181.70 324.84 o -2 5 0 1789.80 1817.74 39.80 o -1 5 0 15413.12 14600.30 283.23 o 0 5 0 314.72 299.69 30.24 o 1 5 0 2184.58 2271.34 50.02 o 2 5 0 655.19 669.88 24.13 o 3 5 0 15797.21 15036.98 272.89 o 4 5 0 160.86 105.32 44.17 o 5 5 0 44755.37 44290.43 869.07 o 6 5 0 520.30 406.73 61.16 o 7 5 0 5532.09 5389.49 102.85 o 8 5 0 133.51 149.82 34.31 o 9 5 0 3073.27 3101.69 77.88 o 10 5 0 10257.73 10716.76 193.30 o 11 5 0 69.34 101.57 54.01 o 12 5 0 0.65 -13.59 64.20 o 13 5 0 193.91 145.40 77.46 o 14 5 0 719.06 709.44 83.92 o 15 5 0 2.53 -26.84 118.56 o 16 5 0 13.54 112.44 149.47 o 17 5 0 43.91 217.41 166.80 o -17 6 0 203.24 200.43 186.51 o -16 6 0 12.99 50.62 193.29 o -15 6 0 59.34 165.78 183.10 o -14 6 0 1594.28 1604.08 83.94 o -13 6 0 2724.91 2741.47 109.81 o -12 6 0 226.34 231.35 63.87 o -11 6 0 1161.51 1227.46 73.40 o -10 6 0 1227.60 1178.92 76.13 o -9 6 0 387.73 455.27 62.17 o -8 6 0 2379.25 2314.18 72.76 o -7 6 0 282.47 322.42 48.24 o -6 6 0 7048.67 6823.60 134.96 o -5 6 0 3550.69 3917.96 87.80 o -4 6 0 7.12 47.22 27.18 o -3 6 0 129.66 138.61 27.52 o -2 6 0 58.75 67.60 23.78 o -1 6 0 126.47 57.41 37.03 o 0 6 0 17998.67 17322.83 370.52 o 1 6 0 5420.27 5558.99 104.31 o 2 6 0 80.07 101.58 27.18 o 3 6 0 3314.93 3430.83 68.41 o 4 6 0 798.45 669.85 63.21 o 5 6 0 793.48 890.72 66.27 o 6 6 0 300.84 187.54 57.42 o 7 6 0 8583.76 8826.39 175.58 o 8 6 0 306.03 361.15 64.21 o 9 6 0 6012.83 6436.39 149.79 o 10 6 0 627.81 576.60 36.36 o 11 6 0 3873.94 3989.25 103.06 o 12 6 0 3031.91 3139.99 97.92 o 13 6 0 5.26 -20.04 64.20 o 14 6 0 745.64 731.53 75.77 o 15 6 0 438.75 568.39 138.95 o 16 6 0 528.82 625.14 151.53 o 17 6 0 431.89 503.49 172.59 o -17 7 0 142.22 81.53 224.21 o -16 7 0 8.77 -129.09 193.29 o -15 7 0 1643.27 1891.23 202.89 o -14 7 0 1976.26 1999.51 104.34 o -13 7 0 8.93 24.12 71.34 o -12 7 0 403.63 447.78 71.69 o -11 7 0 2055.91 1932.43 97.56 o -10 7 0 3921.86 3785.73 114.97 o -9 7 0 1088.06 1119.75 70.35 o -8 7 0 8627.03 8822.72 208.22 o -7 7 0 124.49 135.89 63.87 o -6 7 0 1754.66 1684.84 66.97 o -5 7 0 1946.08 1787.08 49.30 o -4 7 0 177.16 217.43 37.71 o -3 7 0 18410.65 19392.66 326.13 o -2 7 0 1505.11 1340.89 38.42 o -1 7 0 781.40 700.44 40.10 o 0 7 0 736.02 685.13 39.76 o 1 7 0 2341.72 2551.12 58.85 o 2 7 0 1532.05 1344.99 42.84 o 3 7 0 15604.30 15932.09 251.00 o 4 7 0 1347.80 1327.76 84.98 o 5 7 0 2236.78 2000.52 78.21 o 6 7 0 16098.73 15371.73 304.40 o 7 7 0 330.03 401.92 74.74 o 8 7 0 784.44 747.57 82.91 o 9 7 0 72.37 101.57 84.59 o 10 7 0 727.94 757.04 93.10 o 11 7 0 2810.01 2609.12 125.12 o 12 7 0 1953.57 2180.77 119.64 o 13 7 0 51.72 64.54 122.97 o 14 7 0 229.29 238.49 129.77 o 15 7 0 13.27 74.40 145.73 o 16 7 0 42.81 0.00 33.97 o 17 7 0 124.43 182.77 253.77 o -16 8 0 1132.05 1444.47 256.88 o -15 8 0 1058.48 1335.72 174.65 o -14 8 0 23.11 -13.59 175.97 o -13 8 0 3782.72 3966.31 139.42 o -12 8 0 173.28 190.92 78.82 o -11 8 0 2761.03 2865.03 106.07 o -10 8 0 671.87 678.87 69.99 o -9 8 0 21.21 71.34 67.94 o -8 8 0 11276.01 11433.97 287.16 o -7 8 0 19.82 10.19 61.15 o -6 8 0 3024.11 3024.27 83.33 o -5 8 0 2009.64 2052.53 52.70 o -4 8 0 2038.60 1943.17 46.24 o -3 8 0 1555.87 1508.02 45.21 o -2 8 0 22473.18 22310.15 385.26 o -1 8 0 69.99 94.78 47.56 o 0 8 0 6892.69 6491.49 122.37 o 1 8 0 1259.56 1392.29 52.35 o 2 8 0 24766.99 24725.00 497.72 o 3 8 0 1198.52 1163.11 39.77 o 4 8 0 379.96 397.52 81.20 o 5 8 0 41.63 -3.40 65.22 o 6 8 0 1459.78 1422.82 88.03 o 7 8 0 8.56 61.15 74.74 o 8 8 0 1755.02 1762.11 93.14 o 9 8 0 3232.95 3166.69 105.08 o 10 8 0 1876.08 1932.35 107.75 o 11 8 0 959.16 1191.00 104.66 o 12 8 0 719.13 786.23 120.96 o 13 8 0 809.98 883.76 138.63 o 14 8 0 1763.57 1747.20 141.38 o 15 8 0 225.94 251.39 158.99 o 16 8 0 14.93 -47.22 193.29 o -16 9 0 3.50 -30.57 197.37 o -15 9 0 126.17 187.52 201.11 o -14 9 0 1589.91 1646.18 160.74 o -13 9 0 421.03 418.56 104.98 o -12 9 0 2058.38 2235.49 110.13 o -11 9 0 457.87 447.79 91.39 o -10 9 0 226.69 272.12 84.59 o -9 9 0 65.48 54.01 67.60 o -8 9 0 334.01 349.93 67.61 o -7 9 0 10.64 10.19 54.69 o -6 9 0 210.32 275.86 34.99 o -5 9 0 1710.20 1841.40 60.17 o -4 9 0 2438.84 2393.54 57.13 o -3 9 0 4.74 3.40 41.44 o -2 9 0 1188.84 1215.41 44.86 o -1 9 0 67.53 108.71 54.69 o 0 9 0 2346.59 2480.05 69.71 o 1 9 0 694.58 709.52 49.61 o 2 9 0 2016.68 2219.87 60.52 o 3 9 0 68.05 129.09 41.11 o 4 9 0 7550.30 7789.65 154.70 o 5 9 0 1582.17 1679.84 86.00 o 6 9 0 2884.51 2928.64 107.46 o 7 9 0 2928.05 2828.21 99.30 o 8 9 0 2626.36 2675.12 120.70 o 9 9 0 1997.96 2404.24 119.99 o 10 9 0 1116.16 1119.70 120.98 o 11 9 0 1267.70 1340.28 123.70 o 12 9 0 1315.44 1297.79 134.57 o 13 9 0 273.97 203.84 143.03 o 14 9 0 1018.34 1039.08 165.48 o 15 9 0 893.28 1119.56 183.48 o 16 9 0 574.20 428.08 192.98 o -15 10 0 114.87 173.59 235.08 o -14 10 0 435.06 498.40 156.28 o -13 10 0 732.89 904.80 175.32 o -12 10 0 49.44 94.78 92.06 o -11 10 0 1477.46 1453.51 106.71 o -10 10 0 1035.69 1061.89 91.07 o -9 10 0 1014.65 1009.23 89.03 o -8 10 0 1221.92 1268.61 82.92 o -7 10 0 1961.07 1826.41 79.88 o -6 10 0 13294.15 13980.09 290.07 o -5 10 0 1633.29 1557.78 59.82 o -4 10 0 570.31 543.64 40.77 o -3 10 0 1001.25 926.05 46.22 o -2 10 0 795.04 770.01 45.19 o -1 10 0 316.27 435.56 53.68 o 0 10 0 15947.19 16607.08 346.66 o 1 10 0 949.76 969.20 58.11 o 2 10 0 6474.37 6906.08 145.42 o 3 10 0 24.10 64.54 44.16 o 4 10 0 840.07 815.89 53.35 o 5 10 0 466.71 516.78 129.79 o 6 10 0 1969.96 2202.77 109.46 o 7 10 0 188.25 187.53 87.99 o 8 10 0 1933.54 2004.79 119.99 o 9 10 0 1168.33 1178.85 99.91 o 10 10 0 205.41 155.59 101.92 o 11 10 0 491.19 540.88 121.97 o 12 10 0 19.69 -26.84 142.00 o 13 10 0 3.12 57.41 175.63 o 14 10 0 471.62 651.63 154.92 o 15 10 0 182.75 145.40 187.19 o -15 11 0 322.47 435.53 231.02 o -14 11 0 31.05 -44.16 159.66 o -13 11 0 765.70 969.02 199.44 o -12 11 0 357.49 345.85 132.16 o -11 11 0 1026.04 990.85 117.57 o -10 11 0 862.41 796.12 108.39 o -9 11 0 940.17 929.34 74.76 o -8 11 0 105.71 142.68 78.13 o -7 11 0 849.13 782.89 78.15 o -6 11 0 4123.82 4206.05 98.31 o -5 11 0 1578.32 1585.56 60.50 o -4 11 0 90.18 118.90 44.50 o -3 11 0 4193.48 4116.55 89.82 o -2 11 0 2980.05 2947.74 75.84 o -1 11 0 1783.51 1801.61 74.10 o 0 11 0 106.19 84.93 54.69 o 1 11 0 272.24 337.02 53.68 o 2 11 0 2235.15 2236.04 71.74 o 3 11 0 255.98 322.41 54.36 o 4 11 0 1026.05 1131.28 62.87 o 5 11 0 1118.38 1171.06 147.49 o 6 11 0 8465.45 9028.09 232.99 o 7 11 0 597.82 769.91 123.00 o 8 11 0 1220.00 1135.37 125.74 o 9 11 0 903.42 1046.56 124.36 o 10 11 0 5.34 6.79 122.97 o 11 11 0 683.16 672.74 169.20 o 12 11 0 1136.48 1318.77 177.72 o 13 11 0 37.03 -6.79 181.40 o 14 11 0 1638.66 1931.97 204.92 o 15 11 0 456.38 493.30 227.97 o -14 12 0 128.61 142.68 186.50 o -13 12 0 92.09 24.12 173.93 o -12 12 0 165.05 207.23 155.93 o -11 12 0 760.37 753.61 115.18 o -10 12 0 191.15 343.46 105.99 o -9 12 0 20.89 -61.15 101.91 o -8 12 0 322.34 383.56 82.22 o -7 12 0 497.28 482.79 69.31 o -6 12 0 443.13 420.95 50.28 o -5 12 0 1190.33 980.07 62.19 o -4 12 0 7822.43 7703.51 163.81 o -3 12 0 6.07 13.59 40.76 o -2 12 0 1132.23 1119.75 54.71 o -1 12 0 1062.39 1104.10 81.22 o 0 12 0 2684.33 2681.01 90.44 o 1 12 0 2271.26 2398.80 91.45 o 2 12 0 87.27 131.81 68.28 o 3 12 0 2483.28 2462.15 92.48 o 4 12 0 135.92 203.83 61.49 o 5 12 0 185.12 152.54 152.54 o 6 12 0 383.61 337.03 126.38 o 7 12 0 1057.46 1264.43 178.40 o 8 12 0 144.78 160.01 146.08 o 9 12 0 1881.49 1861.18 130.85 o 10 12 0 205.36 231.35 143.70 o 11 12 0 2340.41 2473.16 191.37 o 12 12 0 206.42 200.44 186.51 o 13 12 0 119.05 170.54 173.59 o 14 12 0 551.87 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