#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/14/2011497.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011497_Fobs loop_ _publ_author_name 'Chun, Hyungphil' 'Bernal, Ivan' _publ_section_title ; Triazidocobalt(III) complexes with tridentate amine ligands ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1326 _journal_page_last 1329 _journal_volume 56 _journal_year 2000 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _exptl_crystal_F_000 624.00 _[local]_cod_data_source_file da1147Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 'H. Chun and I. Bernal; m-Co(aepn)(N3)3' _shelx_refln_list_code 4 _shelx_f_calc_maximum 138.54 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10088.27 9945.62 77.41 o 4 0 0 9226.24 9337.45 108.89 o 6 0 0 234.85 241.57 20.17 o 8 0 0 65.56 62.19 43.60 o 10 0 0 325.47 418.64 55.75 o 1 1 0 3572.13 3917.17 160.56 o 2 1 0 9010.79 9317.21 298.42 o 3 1 0 1113.69 1113.09 42.56 o 4 1 0 959.30 1012.90 43.04 o 5 1 0 483.17 532.14 16.87 o 6 1 0 1034.71 1037.84 24.60 o 7 1 0 36.85 24.12 39.64 o 8 1 0 172.20 187.29 30.02 o 9 1 0 447.83 494.28 31.03 o 10 1 0 484.07 539.34 36.76 o 0 2 0 9502.45 14053.18 116.89 o 1 2 0 7751.50 8989.57 76.39 o 2 2 0 3194.56 3392.26 146.75 o 3 2 0 54.80 41.95 12.55 o 4 2 0 3040.17 3021.57 63.99 o 5 2 0 414.01 433.28 17.00 o 6 2 0 197.47 220.59 33.35 o 7 2 0 710.43 652.94 69.24 o 8 2 0 278.31 267.97 26.00 o 9 2 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921.36 985.36 43.89 o 0 10 0 1333.84 1513.22 48.92 o 1 10 0 1322.77 1641.75 35.03 o 2 10 0 194.62 274.90 52.73 o 3 10 0 2323.31 2804.00 99.10 o 4 10 0 30.82 116.70 58.76 o 5 10 0 83.10 71.48 35.73 o 6 10 0 5.95 25.41 54.40 o 7 10 0 1040.80 1049.81 102.91 o 8 10 0 0.47 64.54 64.67 o 1 11 0 1423.46 1848.97 50.35 o 2 11 0 2609.43 3122.18 124.51 o 3 11 0 118.35 152.02 81.79 o 4 11 0 604.94 685.43 30.93 o 5 11 0 547.61 647.96 31.60 o 6 11 0 377.41 375.04 32.19 o 7 11 0 157.26 147.63 70.67 o 8 11 0 257.27 330.42 55.75 o 0 12 0 2956.45 3790.03 113.40 o 1 12 0 2.93 63.30 53.69 o 2 12 0 160.79 204.08 26.61 o 3 12 0 27.66 30.28 48.39 o 4 12 0 2316.73 2556.66 54.87 o 5 12 0 25.99 34.44 53.11 o 6 12 0 438.30 490.37 34.46 o 7 12 0 17.07 31.76 70.54 o 8 12 0 600.56 650.93 41.82 o 1 13 0 4.09 20.96 31.15 o 2 13 0 4275.61 4776.55 229.65 o 3 13 0 409.10 484.46 31.20 o 4 13 0 7.07 68.67 60.07 o 5 13 0 29.10 27.32 62.49 o 6 13 0 762.96 798.04 39.66 o 7 13 0 0.08 33.35 65.53 o 0 14 0 2421.43 2772.33 76.55 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