#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/15/2011508.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011508_Fobs loop_ _publ_author_name 'Paix\~ao, J. A.' 'Matos Beja, A.' 'Ramos Silva, M.' 'Alte da Veiga, L.' 'Serra, A. C.' _publ_section_title ; 3-Hydroxybenzaldehyde ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1348 _journal_page_last 1350 _journal_volume 56 _journal_year 2000 _space_group_IT_number 33 _symmetry_space_group_name_Hall 'P 2c -2n' _symmetry_space_group_name_H-M 'P n a 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 18.8580 _cell_length_b 3.8640 _cell_length_c 8.1900 _exptl_crystal_F_000 256.00 _reflns_d_resolution_high 0.7129 _[local]_cod_data_source_file gd1106Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' m-HYDROXYBENZALDEHYDE' _shelx_refln_list_code 4 _shelx_f_calc_maximum 74.91 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 1623.30 1543.67 9.40 o 8 0 0 874.99 841.36 13.20 o 10 0 0 426.80 477.41 8.93 o 12 0 0 1.85 2.49 1.10 o 14 0 0 73.84 82.51 2.51 o 16 0 0 16.42 13.85 1.63 o 18 0 0 46.31 49.45 1.08 o 20 0 0 1.03 1.00 2.97 o 22 0 0 22.08 20.72 1.18 o 24 0 0 4.51 0.13 3.52 o 26 0 0 0.00 2.74 3.86 o 1 1 0 4208.29 4056.66 23.53 o 2 1 0 5179.74 5010.02 60.47 o 3 1 0 4035.99 4005.66 21.11 o 4 1 0 5610.87 5458.17 42.66 o 5 1 0 64.50 69.42 0.43 o 6 1 0 85.49 90.82 0.57 o 7 1 0 56.21 54.32 0.79 o 8 1 0 307.73 335.38 1.78 o 9 1 0 85.63 84.99 0.76 o 10 1 0 60.24 56.62 0.54 o 11 1 0 220.86 242.36 1.76 o 12 1 0 6.20 3.65 1.07 o 13 1 0 101.48 99.61 0.74 o 14 1 0 0.06 -0.51 1.42 o 15 1 0 25.97 24.54 0.71 o 16 1 0 12.12 12.29 0.69 o 17 1 0 16.21 15.73 0.69 o 18 1 0 6.41 6.58 1.96 o 19 1 0 10.14 9.30 0.73 o 20 1 0 3.02 3.80 0.98 o 21 1 0 13.74 15.01 0.81 o 22 1 0 0.01 -1.36 1.36 o 23 1 0 0.02 0.01 2.42 o 24 1 0 0.99 -0.29 1.67 o 25 1 0 1.77 3.00 3.68 o 26 1 0 0.43 1.43 2.76 o 0 2 0 10.18 7.44 0.61 o 1 2 0 81.53 84.08 0.74 o 2 2 0 870.76 833.44 5.07 o 3 2 0 1606.17 1574.30 6.55 o 4 2 0 27.55 24.59 0.49 o 5 2 0 1.85 -1.29 1.38 o 6 2 0 794.89 787.42 4.87 o 7 2 0 738.90 754.91 3.57 o 8 2 0 35.06 32.92 0.60 o 9 2 0 1.01 -0.67 1.84 o 10 2 0 38.31 33.71 0.65 o 11 2 0 15.75 14.82 0.65 o 12 2 0 1.58 2.38 1.15 o 13 2 0 39.99 40.10 0.73 o 14 2 0 69.60 68.69 0.78 o 15 2 0 6.38 3.88 0.78 o 16 2 0 0.85 0.89 1.96 o 17 2 0 9.07 8.82 0.73 o 18 2 0 11.78 8.67 0.85 o 19 2 0 4.27 -0.92 2.24 o 20 2 0 0.88 -0.28 1.37 o 21 2 0 0.00 -0.67 1.42 o 22 2 0 0.35 1.59 1.48 o 23 2 0 0.02 0.06 3.35 o 24 2 0 0.94 -4.07 4.07 o 1 3 0 68.37 73.03 1.11 o 2 3 0 4.55 2.40 1.10 o 3 3 0 18.71 20.19 0.67 o 4 3 0 3.00 2.56 0.74 o 5 3 0 232.65 224.60 1.79 o 6 3 0 257.10 243.45 2.20 o 7 3 0 56.01 58.07 0.78 o 8 3 0 1.18 0.16 1.15 o 9 3 0 74.68 69.71 1.13 o 10 3 0 73.20 73.11 1.06 o 11 3 0 2.41 1.04 1.24 o 12 3 0 20.28 21.22 0.74 o 13 3 0 0.01 -2.08 2.08 o 14 3 0 0.75 1.25 1.08 o 15 3 0 1.45 1.57 2.34 o 16 3 0 21.56 19.24 0.83 o 17 3 0 8.43 7.33 1.25 o 18 3 0 0.02 -1.27 2.37 o 19 3 0 0.05 -2.38 2.49 o 20 3 0 0.79 -2.88 3.58 o 21 3 0 0.73 4.45 3.69 o 22 3 0 0.43 -1.28 5.62 o 0 4 0 0.96 0.00 1.95 o 1 4 0 23.91 24.29 0.75 o 2 4 0 0.14 -0.81 1.42 o 3 4 0 5.01 5.60 1.00 o 4 4 0 7.69 8.24 0.72 o 5 4 0 3.72 3.75 1.12 o 6 4 0 17.13 14.83 0.76 o 7 4 0 1.89 0.32 0.99 o 8 4 0 29.96 28.76 0.84 o 9 4 0 33.39 29.02 0.85 o 10 4 0 29.86 28.28 0.87 o 11 4 0 1.41 0.94 2.33 o 12 4 0 14.72 14.39 0.87 o 13 4 0 1.36 2.65 1.13 o 14 4 0 1.61 2.03 0.99 o 6 0 1 1460.32 1417.35 14.51 o 8 0 1 354.58 360.04 3.75 o 10 0 1 366.44 388.41 1.95 o 12 0 1 237.45 258.31 1.90 o 14 0 1 3.58 2.75 1.48 o 16 0 1 26.20 26.50 0.71 o 18 0 1 36.52 34.44 0.74 o 20 0 1 26.83 24.56 0.78 o 22 0 1 18.88 18.15 0.84 o 24 0 1 6.40 7.66 1.25 o 26 0 1 0.95 2.47 1.65 o 0 1 1 35.86 33.89 0.38 o 1 1 1 825.43 783.03 2.61 o 2 1 1 436.96 427.33 2.95 o 3 1 1 283.40 272.55 1.35 o 4 1 1 162.22 160.98 1.45 o 5 1 1 11.06 11.31 0.25 o 6 1 1 82.66 89.48 0.66 o 7 1 1 427.41 429.60 3.12 o 8 1 1 254.23 264.78 1.50 o 9 1 1 172.88 182.50 1.10 o 10 1 1 126.64 124.35 0.72 o 11 1 1 67.46 73.89 0.62 o 12 1 1 53.57 54.50 0.49 o 13 1 1 3.33 3.17 0.75 o 14 1 1 2.81 3.30 0.71 o 15 1 1 28.36 27.34 0.66 o 16 1 1 6.21 6.98 0.50 o 17 1 1 24.76 23.98 0.61 o 18 1 1 16.59 13.58 0.51 o 19 1 1 4.41 2.76 0.95 o 20 1 1 17.96 17.51 0.71 o 21 1 1 7.11 6.56 0.76 o 22 1 1 2.35 1.55 1.14 o 23 1 1 2.03 -0.06 1.26 o 24 1 1 10.02 10.76 0.92 o 25 1 1 3.29 6.25 2.08 o 1 2 1 34.26 36.35 0.44 o 2 2 1 19.94 20.68 0.35 o 3 2 1 88.27 87.35 0.83 o 4 2 1 350.79 354.67 1.54 o 5 2 1 206.07 215.96 1.21 o 6 2 1 72.73 74.70 0.52 o 7 2 1 1.63 0.55 0.79 o 8 2 1 33.85 36.38 0.43 o 9 2 1 33.18 34.72 0.48 o 10 2 1 5.11 10.00 3.10 o 11 2 1 1.17 1.00 0.94 o 12 2 1 4.74 3.77 0.91 o 13 2 1 13.91 16.00 0.52 o 14 2 1 65.27 63.88 0.55 o 15 2 1 13.87 12.70 0.64 o 16 2 1 14.70 14.20 0.55 o 17 2 1 5.05 3.55 0.62 o 18 2 1 6.99 3.39 1.23 o 19 2 1 1.02 0.82 0.94 o 20 2 1 0.02 -0.04 0.97 o 21 2 1 9.08 11.35 0.81 o 22 2 1 7.40 10.98 0.64 o 23 2 1 1.61 -1.52 2.67 o 24 2 1 4.85 2.83 1.31 o 0 3 1 91.35 95.34 0.84 o 1 3 1 5.90 5.99 1.16 o 2 3 1 22.07 24.08 0.48 o 3 3 1 29.58 32.59 0.49 o 4 3 1 4.55 3.77 0.57 o 5 3 1 22.26 20.03 0.50 o 6 3 1 8.97 10.34 0.64 o 7 3 1 37.55 36.28 0.52 o 8 3 1 26.30 26.53 0.50 o 9 3 1 3.10 1.91 0.75 o 10 3 1 10.34 9.93 0.95 o 11 3 1 11.34 11.16 0.49 o 12 3 1 18.82 18.44 0.52 o 13 3 1 2.08 0.83 0.75 o 14 3 1 6.42 4.65 0.80 o 15 3 1 6.21 3.59 0.62 o 16 3 1 5.18 4.37 0.89 o 17 3 1 0.36 -0.98 0.98 o 18 3 1 8.17 9.47 0.82 o 19 3 1 2.84 4.28 0.71 o 20 3 1 0.73 1.26 3.61 o 21 3 1 2.62 1.71 1.60 o 1 4 1 9.09 9.44 0.66 o 2 4 1 7.65 8.24 0.52 o 3 4 1 5.62 3.31 0.88 o 4 4 1 0.88 1.40 1.07 o 5 4 1 0.82 0.61 0.82 o 6 4 1 1.55 1.05 0.63 o 7 4 1 10.50 9.79 1.18 o 8 4 1 8.83 9.47 0.56 o 9 4 1 3.56 2.09 0.95 o 10 4 1 8.97 8.99 0.61 o 11 4 1 5.37 4.55 0.78 o 12 4 1 4.15 3.57 1.28 o 13 4 1 2.36 1.28 1.34 o 14 4 1 2.37 1.52 0.83 o 2 0 2 467.47 466.27 2.01 o 4 0 2 401.61 380.38 2.49 o 6 0 2 188.60 185.11 1.96 o 8 0 2 334.42 323.46 2.15 o 10 0 2 322.43 323.92 4.18 o 12 0 2 88.20 82.56 0.80 o 14 0 2 21.74 19.87 0.66 o 16 0 2 155.81 150.81 0.94 o 18 0 2 24.47 25.17 0.91 o 20 0 2 30.25 27.73 0.80 o 22 0 2 21.59 22.99 0.86 o 24 0 2 7.99 11.95 0.91 o 26 0 2 7.69 9.80 1.43 o 1 1 2 136.21 136.10 0.48 o 2 1 2 242.27 229.31 1.40 o 3 1 2 31.66 32.32 1.21 o 4 1 2 96.61 91.12 0.74 o 5 1 2 150.88 151.55 1.21 o 6 1 2 286.80 284.28 1.55 o 7 1 2 46.91 50.26 0.58 o 8 1 2 60.99 56.82 0.48 o 9 1 2 114.29 106.82 0.54 o 10 1 2 11.68 10.88 0.40 o 11 1 2 10.63 8.93 0.42 o 12 1 2 50.31 51.19 0.47 o 13 1 2 44.03 41.94 0.49 o 14 1 2 59.19 55.25 0.70 o 15 1 2 58.97 59.72 0.59 o 16 1 2 4.94 4.97 0.96 o 17 1 2 29.21 28.69 0.52 o 18 1 2 32.41 32.55 0.55 o 19 1 2 25.06 23.68 0.57 o 20 1 2 12.46 15.06 0.70 o 21 1 2 1.97 2.81 1.09 o 22 1 2 7.68 7.82 0.91 o 23 1 2 1.86 -1.80 1.80 o 24 1 2 12.62 16.49 1.04 o 25 1 2 1.48 1.90 2.18 o 0 2 2 48.58 49.02 0.53 o 1 2 2 46.52 47.47 0.37 o 2 2 2 41.10 38.35 0.37 o 3 2 2 94.11 90.74 0.49 o 4 2 2 2.20 1.73 0.86 o 5 2 2 7.33 6.18 0.59 o 6 2 2 45.90 41.48 0.62 o 7 2 2 16.81 15.42 0.53 o 8 2 2 5.67 6.09 1.27 o 9 2 2 43.25 45.98 0.48 o 10 2 2 34.19 32.60 0.48 o 11 2 2 19.91 20.47 0.50 o 12 2 2 45.78 46.02 0.53 o 13 2 2 45.73 43.87 0.53 o 14 2 2 10.72 10.21 1.44 o 15 2 2 6.08 6.32 0.86 o 16 2 2 3.14 1.65 1.04 o 17 2 2 5.02 2.62 1.88 o 18 2 2 11.38 12.20 0.69 o 19 2 2 19.02 20.22 0.59 o 20 2 2 12.29 12.34 0.60 o 21 2 2 4.70 6.56 0.62 o 22 2 2 12.51 14.33 0.93 o 23 2 2 9.19 11.09 0.95 o 24 2 2 2.27 2.69 2.77 o 1 3 2 6.13 7.24 0.54 o 2 3 2 3.58 1.75 0.98 o 3 3 2 3.89 3.98 0.59 o 4 3 2 16.27 17.01 0.49 o 5 3 2 10.55 11.27 0.52 o 6 3 2 3.79 2.85 0.83 o 7 3 2 19.44 21.42 0.49 o 8 3 2 13.83 16.42 0.82 o 9 3 2 19.10 17.88 0.50 o 10 3 2 12.22 11.45 1.17 o 11 3 2 23.56 23.41 0.52 o 12 3 2 1.00 -0.06 0.86 o 13 3 2 4.90 4.25 0.86 o 14 3 2 1.64 1.03 1.08 o 15 3 2 4.51 3.54 0.95 o 16 3 2 13.25 12.91 1.03 o 17 3 2 4.63 5.74 0.85 o 18 3 2 1.07 1.97 0.91 o 19 3 2 3.26 3.64 0.95 o 20 3 2 2.01 3.80 4.35 o 21 3 2 13.59 17.35 1.01 o 0 4 2 2.43 3.85 1.24 o 1 4 2 0.88 1.45 0.75 o 2 4 2 2.01 1.23 0.82 o 3 4 2 4.71 5.02 0.59 o 4 4 2 2.06 0.93 1.09 o 5 4 2 1.88 0.65 0.70 o 6 4 2 7.58 8.89 0.55 o 7 4 2 10.22 10.85 0.56 o 8 4 2 6.68 6.83 0.64 o 9 4 2 1.99 1.54 0.96 o 10 4 2 5.02 5.51 0.75 o 11 4 2 1.73 -0.32 1.62 o 12 4 2 1.59 1.87 1.05 o 13 4 2 4.19 2.21 0.83 o 2 0 3 1299.96 1353.70 19.18 o 4 0 3 1148.87 1137.71 8.18 o 6 0 3 1188.77 1278.90 7.15 o 8 0 3 168.65 179.30 1.06 o 10 0 3 81.76 84.62 1.31 o 12 0 3 291.17 280.96 3.06 o 14 0 3 128.98 132.82 0.88 o 16 0 3 422.72 427.97 4.48 o 18 0 3 60.75 63.27 0.84 o 20 0 3 22.38 21.66 1.10 o 22 0 3 4.02 4.48 1.70 o 24 0 3 1.92 1.25 3.71 o 0 1 3 659.22 661.40 5.60 o 1 1 3 403.03 421.99 1.95 o 2 1 3 367.86 384.50 2.75 o 3 1 3 254.90 277.93 2.24 o 4 1 3 41.81 44.80 0.35 o 5 1 3 549.72 571.80 2.69 o 6 1 3 108.44 106.55 0.60 o 7 1 3 9.65 7.45 0.35 o 8 1 3 384.32 383.32 1.90 o 9 1 3 29.23 33.44 0.42 o 10 1 3 146.06 146.10 0.95 o 11 1 3 17.38 14.35 0.45 o 12 1 3 190.74 188.46 1.14 o 13 1 3 117.83 116.24 0.60 o 14 1 3 75.71 75.87 0.64 o 15 1 3 141.32 140.18 0.69 o 16 1 3 38.30 42.69 0.54 o 17 1 3 30.41 29.26 0.58 o 18 1 3 35.23 38.36 0.57 o 19 1 3 39.06 38.49 0.59 o 20 1 3 22.24 23.00 0.60 o 21 1 3 1.44 0.89 0.99 o 22 1 3 11.62 12.75 1.20 o 23 1 3 0.95 0.58 2.54 o 24 1 3 0.91 1.15 1.59 o 25 1 3 3.50 3.11 1.23 o 1 2 3 44.49 45.08 0.42 o 2 2 3 334.70 347.27 1.78 o 3 2 3 78.80 83.75 0.81 o 4 2 3 81.91 82.96 0.89 o 5 2 3 19.13 18.73 0.43 o 6 2 3 82.71 81.62 0.50 o 7 2 3 14.01 13.75 0.44 o 8 2 3 19.08 19.29 0.47 o 9 2 3 202.11 200.66 1.33 o 10 2 3 131.35 130.17 1.12 o 11 2 3 28.15 29.07 0.52 o 12 2 3 59.63 60.46 0.60 o 13 2 3 107.37 103.48 0.61 o 14 2 3 17.36 17.92 0.51 o 15 2 3 8.55 9.39 0.56 o 16 2 3 3.20 0.75 1.50 o 17 2 3 2.79 2.19 0.80 o 18 2 3 17.09 17.75 0.74 o 19 2 3 34.77 35.32 0.64 o 20 2 3 5.10 4.71 1.12 o 21 2 3 4.97 4.14 1.17 o 22 2 3 5.83 4.25 1.05 o 23 2 3 6.62 3.53 1.32 o 0 3 3 117.06 120.89 1.10 o 1 3 3 29.64 31.32 0.52 o 2 3 3 15.34 15.48 0.50 o 3 3 3 0.27 -0.97 1.04 o 4 3 3 23.83 23.50 0.50 o 5 3 3 0.12 -0.62 0.88 o 6 3 3 42.16 43.68 0.54 o 7 3 3 51.17 54.19 0.55 o 8 3 3 27.74 28.72 0.53 o 9 3 3 27.51 27.15 0.57 o 10 3 3 29.50 31.17 0.54 o 11 3 3 53.43 50.15 0.58 o 12 3 3 15.88 14.62 0.54 o 13 3 3 7.98 7.33 0.80 o 14 3 3 2.58 1.59 0.94 o 15 3 3 5.36 4.84 0.61 o 16 3 3 1.18 1.72 0.87 o 17 3 3 5.43 5.15 0.70 o 18 3 3 0.38 1.35 1.81 o 20 3 3 0.27 -3.44 3.85 o 1 4 3 5.51 4.91 1.07 o 2 4 3 4.25 5.08 0.94 o 3 4 3 0.35 -1.07 1.32 o 4 4 3 32.25 33.25 0.60 o 5 4 3 6.61 7.95 0.83 o 6 4 3 18.18 18.47 0.59 o 7 4 3 7.95 8.97 0.87 o 8 4 3 11.75 12.01 0.66 o 9 4 3 5.64 5.23 1.02 o 10 4 3 9.46 8.43 0.81 o 11 4 3 0.26 0.53 1.24 o 12 4 3 0.72 -1.29 1.29 o 13 4 3 2.28 2.10 1.70 o 0 0 4 142.18 153.25 1.60 o 2 0 4 242.91 261.83 1.41 o 4 0 4 535.84 616.33 6.58 o 6 0 4 222.24 236.27 1.88 o 8 0 4 409.65 422.93 4.07 o 10 0 4 169.91 163.01 1.38 o 12 0 4 429.41 410.95 6.22 o 14 0 4 321.36 311.28 6.05 o 16 0 4 89.55 88.45 0.87 o 18 0 4 39.52 38.85 0.82 o 20 0 4 2.59 3.32 1.13 o 22 0 4 21.71 24.77 0.94 o 24 0 4 3.63 3.09 1.77 o 1 1 4 134.53 156.16 0.63 o 2 1 4 5.94 5.70 0.38 o 3 1 4 181.35 194.05 0.80 o 4 1 4 210.77 227.08 1.08 o 5 1 4 37.83 41.92 0.43 o 6 1 4 266.12 277.68 1.46 o 7 1 4 48.58 56.33 0.46 o 8 1 4 112.06 107.71 0.57 o 9 1 4 174.52 169.63 1.01 o 10 1 4 179.02 170.31 0.87 o 11 1 4 86.99 83.87 0.72 o 12 1 4 137.98 132.22 0.79 o 13 1 4 123.22 121.78 0.87 o 14 1 4 56.83 57.46 0.56 o 15 1 4 64.06 64.47 0.58 o 16 1 4 40.50 41.72 0.56 o 17 1 4 41.94 41.06 0.58 o 18 1 4 36.79 38.01 0.59 o 19 1 4 2.27 1.07 1.20 o 20 1 4 11.88 13.15 0.60 o 21 1 4 1.11 -0.91 1.27 o 22 1 4 2.83 2.21 0.78 o 23 1 4 1.91 -0.54 2.69 o 24 1 4 0.23 0.38 1.19 o 0 2 4 308.11 328.02 1.65 o 1 2 4 50.69 53.90 0.51 o 2 2 4 21.35 22.25 0.46 o 3 2 4 28.62 28.71 0.47 o 4 2 4 15.36 15.69 0.49 o 5 2 4 39.72 38.87 0.56 o 6 2 4 52.54 53.66 0.62 o 7 2 4 93.96 90.40 0.82 o 8 2 4 128.95 130.26 0.87 o 9 2 4 74.71 72.66 0.58 o 10 2 4 88.87 87.21 0.59 o 11 2 4 99.76 97.67 0.60 o 12 2 4 19.64 18.76 0.51 o 13 2 4 1.65 1.21 0.66 o 14 2 4 0.44 -0.87 0.87 o 15 2 4 39.35 41.34 0.82 o 16 2 4 21.39 22.99 0.57 o 17 2 4 12.21 12.35 0.59 o 18 2 4 9.73 10.89 0.81 o 19 2 4 13.65 14.87 1.10 o 20 2 4 9.99 9.77 0.82 o 21 2 4 10.65 10.63 0.94 o 22 2 4 0.19 -1.06 2.69 o 1 3 4 2.77 1.52 0.77 o 2 3 4 54.05 54.20 0.55 o 3 3 4 11.77 13.17 0.50 o 4 3 4 43.23 46.10 0.58 o 5 3 4 59.82 61.94 0.80 o 6 3 4 33.88 34.93 0.74 o 7 3 4 25.27 25.23 0.53 o 8 3 4 22.41 22.01 0.54 o 9 3 4 52.54 50.19 0.62 o 10 3 4 4.30 3.48 0.64 o 11 3 4 8.42 7.77 0.74 o 12 3 4 4.30 4.01 0.84 o 13 3 4 6.81 5.64 0.60 o 14 3 4 4.84 4.23 0.86 o 15 3 4 3.65 3.99 1.13 o 16 3 4 3.32 2.89 0.92 o 17 3 4 5.41 5.83 0.84 o 20 3 4 5.02 3.37 3.99 o 0 4 4 10.98 11.13 1.40 o 1 4 4 1.05 0.92 0.96 o 2 4 4 17.57 19.56 0.78 o 3 4 4 14.14 15.39 0.59 o 4 4 4 9.51 8.41 0.77 o 5 4 4 4.00 4.98 0.98 o 6 4 4 27.65 28.98 0.63 o 7 4 4 7.12 7.37 1.11 o 8 4 4 5.06 3.98 0.68 o 9 4 4 1.51 0.58 0.74 o 10 4 4 0.72 -1.62 1.79 o 11 4 4 0.43 -1.33 1.33 o 2 0 5 14.47 17.35 0.59 o 4 0 5 59.17 54.64 1.29 o 6 0 5 366.90 370.49 3.80 o 8 0 5 6.01 6.92 0.67 o 10 0 5 38.48 41.21 0.75 o 12 0 5 18.06 18.49 0.73 o 14 0 5 112.92 108.12 1.26 o 16 0 5 11.65 11.72 0.76 o 18 0 5 3.73 1.07 2.32 o 20 0 5 21.04 23.34 1.49 o 22 0 5 4.41 0.00 4.12 o 0 1 5 51.72 55.39 0.75 o 1 1 5 5.80 5.55 0.67 o 2 1 5 53.27 55.24 0.48 o 3 1 5 91.15 91.69 0.52 o 4 1 5 18.33 18.47 0.49 o 5 1 5 12.63 13.17 0.82 o 6 1 5 18.19 18.96 0.48 o 7 1 5 34.19 37.20 0.51 o 8 1 5 24.84 25.91 0.51 o 9 1 5 16.18 15.68 0.52 o 10 1 5 73.83 74.21 0.59 o 11 1 5 18.68 17.39 0.52 o 12 1 5 8.69 8.76 0.50 o 13 1 5 31.94 32.43 0.69 o 14 1 5 0.72 0.13 0.75 o 15 1 5 7.11 7.16 0.88 o 16 1 5 14.51 14.54 0.60 o 17 1 5 14.48 15.08 0.58 o 18 1 5 7.49 6.30 0.95 o 19 1 5 2.58 -1.73 1.73 o 20 1 5 10.64 11.86 1.22 o 21 1 5 7.74 8.36 1.25 o 22 1 5 2.15 -0.44 2.71 o 23 1 5 7.39 10.01 1.01 o 1 2 5 21.68 22.13 0.51 o 2 2 5 16.13 15.76 0.53 o 3 2 5 21.90 22.98 0.53 o 4 2 5 24.68 24.13 0.53 o 5 2 5 0.06 -0.46 0.87 o 6 2 5 0.83 0.11 1.45 o 7 2 5 27.30 29.26 0.53 o 8 2 5 23.01 22.82 0.52 o 9 2 5 10.24 10.71 0.51 o 10 2 5 4.32 3.59 0.62 o 11 2 5 13.78 13.18 0.52 o 12 2 5 15.88 15.86 0.96 o 13 2 5 0.09 -0.29 0.95 o 14 2 5 0.77 -0.79 1.38 o 15 2 5 0.87 -0.90 1.17 o 16 2 5 9.42 10.54 0.59 o 17 2 5 16.43 17.03 0.62 o 18 2 5 12.18 13.88 1.03 o 19 2 5 2.62 2.14 0.86 o 20 2 5 5.95 8.60 2.36 o 21 2 5 2.27 2.88 2.74 o 0 3 5 22.06 22.84 0.75 o 1 3 5 0.03 -0.40 0.86 o 2 3 5 1.53 0.99 0.87 o 3 3 5 6.30 6.26 0.93 o 4 3 5 2.31 1.92 0.88 o 5 3 5 4.06 3.86 0.77 o 6 3 5 2.19 0.02 1.09 o 7 3 5 8.10 7.79 0.75 o 8 3 5 14.14 14.46 0.54 o 9 3 5 8.99 8.89 0.83 o 10 3 5 2.05 0.52 1.15 o 11 3 5 0.36 -0.54 0.98 o 12 3 5 1.00 0.57 0.90 o 13 3 5 3.68 3.34 0.73 o 14 3 5 5.40 6.14 1.02 o 15 3 5 2.58 -0.04 1.83 o 1 4 5 0.60 0.76 1.23 o 2 4 5 1.50 -0.32 1.02 o 3 4 5 2.24 2.49 0.80 o 4 4 5 5.12 2.52 0.82 o 5 4 5 7.91 8.75 1.25 o 6 4 5 3.00 1.50 1.06 o 7 4 5 0.58 -1.39 1.39 o 8 4 5 0.26 -1.08 1.80 o 9 4 5 0.30 -1.65 1.65 o 0 0 6 219.52 223.56 1.63 o 2 0 6 142.17 131.98 1.65 o 4 0 6 97.07 85.51 1.15 o 6 0 6 25.95 22.70 0.76 o 8 0 6 33.58 30.56 1.21 o 10 0 6 129.98 116.79 0.90 o 12 0 6 105.09 100.73 0.90 o 14 0 6 16.71 15.63 0.78 o 16 0 6 31.00 30.06 0.87 o 18 0 6 1.31 -1.12 2.42 o 20 0 6 5.60 7.66 1.45 o 22 0 6 5.28 6.36 1.86 o 1 1 6 72.35 73.22 0.57 o 2 1 6 19.96 20.92 0.53 o 3 1 6 120.77 119.63 0.77 o 4 1 6 19.45 18.24 0.53 o 5 1 6 2.43 1.46 0.66 o 6 1 6 111.06 104.09 0.63 o 7 1 6 2.77 1.35 0.90 o 8 1 6 46.51 42.80 0.56 o 9 1 6 20.36 19.87 0.53 o 10 1 6 32.20 30.91 0.55 o 11 1 6 17.40 14.36 0.53 o 12 1 6 16.27 15.13 0.54 o 13 1 6 35.99 32.97 0.58 o 14 1 6 30.01 32.20 0.65 o 15 1 6 9.55 9.64 0.74 o 16 1 6 5.60 6.80 0.69 o 17 1 6 3.15 1.74 0.89 o 18 1 6 0.92 1.23 0.86 o 19 1 6 3.02 1.68 1.10 o 20 1 6 1.62 1.83 2.37 o 21 1 6 5.99 10.67 1.45 o 22 1 6 3.79 6.41 1.01 o 0 2 6 90.15 92.85 0.86 o 1 2 6 5.51 4.35 0.69 o 2 2 6 5.58 5.43 0.94 o 3 2 6 64.90 70.27 0.62 o 4 2 6 3.46 1.86 0.96 o 5 2 6 6.57 6.60 1.33 o 6 2 6 41.08 43.40 0.57 o 7 2 6 45.01 42.38 0.56 o 8 2 6 24.53 22.37 0.65 o 9 2 6 25.64 23.84 0.56 o 10 2 6 27.78 25.70 0.57 o 11 2 6 1.62 0.62 0.81 o 12 2 6 2.06 2.41 1.35 o 13 2 6 6.84 7.25 1.07 o 14 2 6 2.28 2.38 0.97 o 15 2 6 2.30 -0.25 1.76 o 16 2 6 5.83 7.44 0.82 o 17 2 6 0.02 0.97 1.32 o 20 2 6 0.62 -6.56 6.56 o 1 3 6 11.45 12.68 0.98 o 2 3 6 1.92 1.24 0.73 o 3 3 6 2.10 1.94 0.82 o 4 3 6 24.23 25.73 0.58 o 5 3 6 30.71 32.02 0.64 o 6 3 6 9.07 9.87 0.97 o 7 3 6 19.18 20.74 0.60 o 8 3 6 1.13 1.84 0.88 o 9 3 6 14.23 13.39 1.04 o 10 3 6 3.14 3.34 0.80 o 11 3 6 5.81 6.56 0.69 o 12 3 6 2.63 1.89 0.94 o 13 3 6 0.13 -1.11 1.11 o 0 4 6 2.66 2.77 1.55 o 1 4 6 2.97 3.29 0.79 o 2 4 6 1.02 -0.24 0.95 o 3 4 6 7.20 7.34 0.75 o 4 4 6 0.43 0.47 1.35 o 5 4 6 1.20 -1.37 1.37 o 2 0 7 924.27 882.60 8.58 o 4 0 7 498.42 479.50 5.49 o 6 0 7 27.43 24.78 0.80 o 8 0 7 87.87 73.77 0.99 o 10 0 7 13.50 9.69 1.07 o 12 0 7 35.58 31.93 0.86 o 14 0 7 1.85 -0.46 1.78 o 16 0 7 27.33 27.71 0.92 o 18 0 7 7.49 10.14 1.13 o 20 0 7 13.00 -0.26 5.90 o 0 1 7 545.69 541.64 2.79 o 1 1 7 196.28 203.52 0.98 o 2 1 7 102.33 102.38 0.74 o 3 1 7 134.84 130.46 0.67 o 4 1 7 91.42 85.10 0.80 o 5 1 7 48.38 50.83 0.60 o 6 1 7 186.54 175.16 0.73 o 7 1 7 75.68 71.23 0.66 o 8 1 7 34.56 35.60 0.78 o 9 1 7 10.17 8.44 0.83 o 10 1 7 6.91 5.06 0.59 o 11 1 7 14.98 15.57 0.83 o 12 1 7 0.64 1.20 0.95 o 13 1 7 19.15 17.53 1.30 o 14 1 7 3.46 4.48 0.78 o 15 1 7 17.61 18.61 1.33 o 16 1 7 2.31 1.42 0.84 o 17 1 7 5.11 4.90 0.80 o 20 1 7 0.02 -4.05 4.05 o 1 2 7 107.38 102.76 0.71 o 2 2 7 61.86 62.50 0.62 o 3 2 7 16.63 16.63 0.57 o 4 2 7 87.92 89.27 1.20 o 5 2 7 125.93 122.95 0.83 o 6 2 7 26.60 28.55 0.62 o 7 2 7 16.14 16.41 0.58 o 8 2 7 11.13 11.10 0.58 o 9 2 7 46.14 44.57 0.63 o 10 2 7 28.51 30.50 0.63 o 11 2 7 7.28 3.96 1.05 o 12 2 7 15.92 16.85 0.63 o 13 2 7 7.95 9.16 0.71 o 14 2 7 0.75 -0.95 0.95 o 15 2 7 3.72 3.55 1.32 o 0 3 7 0.93 -2.43 2.43 o 1 3 7 14.96 15.07 0.62 o 2 3 7 10.28 11.93 0.83 o 3 3 7 38.10 38.46 0.66 o 4 3 7 10.93 11.58 0.72 o 5 3 7 6.12 5.42 0.98 o 6 3 7 3.66 2.11 0.99 o 7 3 7 28.21 28.36 0.71 o 8 3 7 33.57 35.55 0.69 o 9 3 7 7.25 5.47 1.12 o 10 3 7 12.72 14.99 0.68 o 11 3 7 7.89 7.68 0.91 o 0 0 8 57.78 54.32 1.26 o 2 0 8 5.77 7.65 1.46 o 4 0 8 18.63 17.35 0.82 o 6 0 8 5.57 3.83 1.10 o 8 0 8 99.83 86.22 0.98 o 10 0 8 2.95 -0.48 1.47 o 12 0 8 0.11 -0.55 1.49 o 14 0 8 0.40 -1.55 1.55 o 16 0 8 15.97 19.15 1.00 o 1 1 8 1.23 0.24 0.85 o 2 1 8 0.96 -0.53 1.65 o 3 1 8 11.45 13.17 1.36 o 4 1 8 29.16 26.82 0.60 o 5 1 8 39.52 37.90 0.62 o 6 1 8 10.33 8.91 1.10 o 7 1 8 4.78 4.61 1.38 o 8 1 8 4.36 2.60 0.67 o 9 1 8 8.50 5.79 0.81 o 10 1 8 2.75 1.46 1.17 o 11 1 8 6.88 5.64 0.96 o 12 1 8 6.96 7.14 0.99 o 13 1 8 3.07 3.18 1.02 o 14 1 8 1.93 0.13 1.91 o 15 1 8 2.40 1.77 1.07 o 0 2 8 7.39 6.99 2.11 o 1 2 8 11.57 11.49 0.60 o 2 2 8 17.79 16.93 0.61 o 3 2 8 0.04 0.20 0.89 o 4 2 8 1.26 0.48 1.29 o 5 2 8 1.95 1.69 0.86 o 6 2 8 13.29 11.05 0.66 o 7 2 8 0.40 -1.97 1.97 o 8 2 8 1.50 0.39 1.07 o 9 2 8 1.03 1.26 0.94 o 10 2 8 5.24 6.30 1.33 o 11 2 8 2.41 1.59 0.81 o 12 2 8 7.23 6.86 0.77 o 1 3 8 1.88 1.60 1.37 o 2 3 8 8.56 10.01 1.00 o 3 3 8 2.15 0.93 1.18 o 4 3 8 0.60 -0.50 0.99 o 5 3 8 2.04 0.79 1.16 o 6 3 8 2.39 2.96 0.90 o 2 0 9 16.35 17.76 2.16 o 4 0 9 11.25 13.30 1.03 o 6 0 9 7.48 6.35 1.03 o 8 0 9 38.65 43.73 1.00 o 10 0 9 0.40 -0.60 2.68 o 12 0 9 8.55 6.91 1.46 o 0 1 9 9.05 9.70 0.90 o 1 1 9 1.60 -1.13 1.31 o 2 1 9 7.61 9.12 0.68 o 3 1 9 2.69 0.73 1.09 o 4 1 9 5.46 5.48 1.02 o 5 1 9 3.98 3.64 1.29 o 6 1 9 6.27 6.24 1.01 o 7 1 9 7.24 8.41 1.52 o 8 1 9 2.94 1.61 1.12 o 9 1 9 5.84 5.19 1.14 o 10 1 9 3.84 0.72 1.20 o 11 1 9 5.35 1.71 1.46 o 12 1 9 6.11 7.33 1.07 o 1 2 9 2.59 1.98 1.38 o 2 2 9 2.82 2.87 1.06 o 3 2 9 0.19 -1.93 1.94 o 4 2 9 3.52 1.28 1.15 o 5 2 9 7.91 7.85 1.26 o 6 2 9 1.58 -0.90 1.42 o 7 2 9 0.68 -1.01 1.17 o 8 2 9 0.41 -1.45 1.45 o 0 0 10 166.28 183.46 1.87 o 2 0 10 9.88 11.60 1.03 o 4 0 10 48.24 53.55 1.11 o 6 0 10 2.23 2.67 1.36 o 8 0 10 26.62 32.36 1.10 o 1 1 10 24.68 29.15 0.88 o 2 1 10 27.46 32.19 1.04 o 3 1 10 28.51 30.60 0.88 o 4 1 10 20.00 22.36 0.76 o 5 1 10 4.84 1.84 1.26 o 6 1 10 11.33 14.53 0.80 o