#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/15/2011546.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011546_Fobs loop_ _publ_author_name 'Alyea, Elmer C.' 'Kannan, Shanmugaperumal' 'Ferguson, George' _publ_section_title ; cis-\m-Chloro-\m-p-toluenethiolato-bis[chloro(triethylphosphine)palladium] ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first e493 _journal_page_last e494 _journal_volume 56 _journal_year 2000 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.132 _cell_angle_gamma 90.000 _cell_length_a 7.8564 _cell_length_b 17.4629 _cell_length_c 9.7865 _exptl_crystal_F_000 680.00 _reflns_d_resolution_high 0.8397 _[local]_cod_data_source_file qa0405Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 9695 PD2 COMPLEX' _shelx_refln_list_code 4 _shelx_f_calc_maximum 206.96 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 27403.46 30152.93 241.54 o 2 0 0 3988.13 4392.44 71.70 o 3 0 0 28.02 4.25 83.40 o 4 0 0 2156.38 2282.05 74.89 o 5 0 0 2389.23 2649.83 91.91 o 6 0 0 1103.47 1117.17 88.26 o 7 0 0 4255.99 4249.79 147.96 o 8 0 0 2355.80 2228.73 135.81 o 9 0 0 125.32 244.13 89.02 o 1 1 0 2037.10 2088.66 35.24 o 2 1 0 2117.06 2160.98 52.56 o 3 1 0 531.56 587.15 42.23 o 4 1 0 1553.84 1538.89 60.77 o 5 1 0 123.18 69.27 124.27 o 6 1 0 541.59 541.72 65.78 o 7 1 0 163.45 288.79 70.34 o 8 1 0 273.64 320.54 78.39 o 9 1 0 184.77 301.55 81.58 o 0 2 0 42830.81 42966.87 257.80 o 1 2 0 25807.37 27703.78 248.83 o 2 2 0 5865.62 5861.60 75.05 o 3 2 0 921.44 941.11 45.88 o 4 2 0 1249.77 1173.84 59.40 o 5 2 0 2064.50 2176.93 79.75 o 6 2 0 1286.74 1353.86 82.19 o 7 2 0 3461.26 3452.24 121.99 o 8 2 0 1704.27 1744.28 109.53 o 9 2 0 243.92 121.68 86.89 o 1 3 0 8749.20 9192.31 98.59 o 2 3 0 3464.63 3439.48 63.20 o 3 3 0 11129.97 11317.43 117.58 o 4 3 0 4965.83 5002.68 94.64 o 5 3 0 188.28 105.43 123.51 o 6 3 0 92.28 144.62 61.53 o 7 3 0 161.29 195.51 147.96 o 8 3 0 962.12 1035.29 88.57 o 9 3 0 428.87 404.70 88.87 o 0 4 0 3497.03 3581.07 56.51 o 1 4 0 4030.73 3754.86 61.98 o 2 4 0 125.15 140.06 35.09 o 3 4 0 3512.24 3544.00 75.20 o 4 4 0 719.69 762.76 51.80 o 5 4 0 616.60 560.56 61.22 o 6 4 0 252.41 22.03 148.72 o 7 4 0 1242.02 1193.89 89.17 o 8 4 0 786.81 684.37 93.12 o 9 4 0 278.84 318.87 83.40 o 1 5 0 11469.74 11662.43 115.91 o 2 5 0 9517.05 9684.21 104.36 o 3 5 0 13531.94 13708.10 138.24 o 4 5 0 7009.28 6824.28 113.33 o 5 5 0 1181.02 1311.32 69.73 o 6 5 0 138.21 10.03 154.65 o 7 5 0 265.61 257.04 65.17 o 8 5 0 563.41 551.90 81.58 o 9 5 0 339.28 259.47 81.58 o 0 6 0 9871.98 10066.58 101.63 o 1 6 0 2360.44 2279.92 57.73 o 2 6 0 1591.91 1590.84 52.26 o 3 6 0 1908.87 2089.88 65.32 o 4 6 0 20.43 7.14 97.38 o 5 6 0 863.89 845.70 67.60 o 6 6 0 1106.77 1190.09 81.73 o 7 6 0 525.86 605.53 71.40 o 8 6 0 723.92 682.09 91.45 o 1 7 0 1681.97 1628.21 54.69 o 2 7 0 7560.85 7545.56 105.12 o 3 7 0 6622.66 6434.62 107.25 o 4 7 0 5008.04 5019.99 106.80 o 5 7 0 968.27 1065.07 74.29 o 6 7 0 244.53 24.31 161.33 o 7 7 0 132.30 114.85 62.74 o 8 7 0 297.31 306.11 78.69 o 0 8 0 6429.52 6328.28 96.16 o 1 8 0 5656.34 5746.60 92.82 o 2 8 0 3788.08 3767.46 84.16 o 3 8 0 59.03 54.54 93.88 o 4 8 0 685.23 715.06 61.07 o 5 8 0 1736.95 1735.46 88.26 o 6 8 0 2136.52 1942.37 102.24 o 7 8 0 1349.80 1285.95 92.67 o 8 8 0 507.18 259.47 87.50 o 1 9 0 1301.21 1251.47 56.51 o 2 9 0 2811.99 2742.65 77.63 o 3 9 0 1432.33 1291.12 65.32 o 4 9 0 1123.02 1169.58 71.25 o 5 9 0 74.45 10.03 126.85 o 6 9 0 3.60 171.97 121.99 o 7 9 0 77.92 203.26 66.69 o 8 9 0 78.80 164.22 66.99 o 0 10 0 13821.00 13552.85 156.32 o 1 10 0 8735.86 8548.65 127.30 o 2 10 0 1718.40 1675.15 70.79 o 3 10 0 1179.81 1200.88 66.08 o 4 10 0 1272.58 1213.64 76.11 o 5 10 0 1348.99 1364.95 87.20 o 6 10 0 1295.85 1191.31 87.05 o 7 10 0 1544.53 1623.50 102.69 o 8 10 0 498.92 571.80 86.59 o 1 11 0 461.15 424.14 51.35 o 2 11 0 227.31 180.93 46.33 o 3 11 0 44.63 119.56 114.54 o 4 11 0 136.18 101.02 141.43 o 5 11 0 128.33 11.24 129.43 o 6 11 0 51.16 102.09 57.12 o 7 11 0 153.26 116.82 73.53 o 0 12 0 11294.00 11119.49 163.00 o 1 12 0 3699.60 3629.83 101.02 o 2 12 0 1088.73 1122.34 68.97 o 3 12 0 468.69 118.64 153.74 o 4 12 0 126.81 156.17 114.54 o 5 12 0 685.86 670.24 72.61 o 6 12 0 629.11 487.49 79.60 o 7 12 0 871.24 1038.33 95.71 o 1 13 0 247.56 359.88 54.23 o 2 13 0 393.20 431.59 61.07 o 3 13 0 564.17 519.70 67.60 o 4 13 0 842.09 804.69 73.22 o 5 13 0 46.88 74.74 53.78 o 6 13 0 53.53 119.40 62.89 o 7 13 0 112.75 116.67 75.96 o 0 14 0 2573.16 2524.20 99.20 o 1 14 0 634.06 696.98 65.47 o 2 14 0 143.34 75.05 56.66 o 3 14 0 55.12 11.09 125.03 o 4 14 0 160.90 123.81 144.93 o 5 14 0 109.68 27.50 66.99 o 6 14 0 119.31 170.14 64.26 o 1 15 0 553.05 583.65 64.11 o 2 15 0 571.98 493.26 69.73 o 3 15 0 1434.07 1451.23 91.00 o 4 15 0 1271.78 1162.14 92.21 o 5 15 0 98.54 32.36 66.69 o 6 15 0 1.85 15.65 62.28 o 0 16 0 21.53 11.55 113.63 o 1 16 0 7.73 11.70 118.04 o 2 16 0 121.69 164.98 125.94 o 3 16 0 318.10 312.94 69.42 o 4 16 0 58.05 22.03 62.74 o 5 16 0 60.53 15.04 62.13 o 1 17 0 230.72 335.88 58.64 o 2 17 0 502.13 517.87 69.58 o 3 17 0 1218.03 1205.59 90.69 o 4 17 0 874.55 979.08 89.02 o 5 17 0 327.31 339.53 78.69 o 0 18 0 285.74 278.91 67.60 o 1 18 0 196.50 179.71 64.26 o 2 18 0 206.37 326.92 64.26 o 3 18 0 171.20 87.50 67.60 o 4 18 0 23.55 15.65 66.54 o 1 19 0 19.49 14.74 59.55 o 2 19 0 349.67 447.69 72.92 o 3 19 0 394.35 525.93 85.68 o 0 20 0 274.24 142.19 71.70 o 1 20 0 280.97 297.75 76.56 o 2 20 0 281.96 180.93 80.51 o -9 0 1 694.82 710.96 95.10 o -8 0 1 4145.30 3830.96 156.32 o -7 0 1 3349.86 3389.20 132.47 o -6 0 1 1709.88 1647.51 98.14 o -5 0 1 246.92 190.35 62.44 o -4 0 1 1271.86 1285.19 67.15 o -3 0 1 4531.90 4832.23 86.29 o -2 0 1 42.55 97.68 102.85 o -1 0 1 26104.07 27065.89 258.25 o 0 0 1 25397.52 26191.47 206.15 o 1 0 1 779.50 994.58 37.37 o 2 0 1 33.96 3.04 100.26 o 3 0 1 10052.28 10757.93 121.38 o 4 0 1 11245.38 11569.61 146.90 o 5 0 1 1968.80 1945.11 88.11 o 6 0 1 204.67 111.20 155.86 o 7 0 1 630.19 747.26 82.03 o 8 0 1 58.11 13.52 78.84 o 9 0 1 90.27 164.67 81.73 o -9 1 1 29.13 21.57 76.87 o -8 1 1 41.06 30.53 72.31 o -7 1 1 464.70 483.39 75.05 o -6 1 1 140.07 63.80 142.80 o -5 1 1 947.49 881.40 66.08 o -4 1 1 1693.15 1576.26 65.02 o -3 1 1 384.26 419.13 43.45 o -2 1 1 180.11 157.69 41.17 o -1 1 1 671.64 714.75 32.66 o 0 1 1 5716.79 5788.07 43.90 o 1 1 1 4455.33 4466.27 54.08 o 2 1 1 1155.56 1154.55 49.68 o 3 1 1 8002.99 8484.39 104.52 o 4 1 1 2406.01 2558.99 75.35 o 5 1 1 424.29 388.14 58.03 o 6 1 1 215.35 267.37 68.21 o 7 1 1 82.77 11.39 150.55 o 8 1 1 187.00 228.78 79.91 o 9 1 1 49.99 101.02 79.91 o -9 2 1 458.95 532.31 79.15 o -8 2 1 2717.28 2610.94 126.24 o -7 2 1 2456.30 2435.94 107.40 o -6 2 1 473.72 579.55 68.51 o -5 2 1 254.06 78.08 128.22 o -4 2 1 2440.91 2477.11 71.40 o -3 2 1 3855.25 3737.54 73.07 o -2 2 1 2087.20 2058.58 54.69 o -1 2 1 6735.05 7222.59 74.44 o 0 2 1 11875.38 12624.20 84.46 o 1 2 1 7774.11 7757.48 78.84 o 2 2 1 630.44 658.39 42.69 o 3 2 1 5168.06 5330.20 84.62 o 4 2 1 9160.50 9336.32 126.09 o 5 2 1 1514.62 1585.68 73.37 o 6 2 1 770.58 769.14 74.89 o 7 2 1 376.73 150.70 170.60 o 8 2 1 159.67 154.50 77.63 o 9 2 1 253.81 342.41 83.40 o -9 3 1 95.08 29.17 75.65 o -8 3 1 47.57 96.31 69.73 o -7 3 1 1414.94 1306.76 88.57 o -6 3 1 995.87 958.58 78.54 o -5 3 1 4735.40 4716.01 108.77 o -4 3 1 8090.55 8125.11 118.80 o -3 3 1 1042.97 1125.99 50.44 o -2 3 1 1115.94 1094.69 47.25 o -1 3 1 3531.22 3536.40 56.97 o 0 3 1 27844.20 28479.60 199.16 o 1 3 1 5314.08 5374.71 67.30 o 2 3 1 12349.35 13039.98 123.81 o 3 3 1 19569.14 20060.84 204.17 o 4 3 1 2892.82 2925.86 79.00 o 5 3 1 557.03 536.41 58.94 o 6 3 1 428.63 527.75 67.15 o 7 3 1 1131.49 1299.93 89.48 o 8 3 1 974.29 955.39 90.54 o 9 3 1 96.65 183.36 76.11 o -9 4 1 77.84 33.27 75.96 o -8 4 1 831.65 699.56 89.33 o -7 4 1 578.59 670.55 72.61 o -6 4 1 99.17 143.86 138.70 o -5 4 1 591.03 568.16 61.98 o -4 4 1 754.90 729.34 53.17 o -3 4 1 2139.53 2046.89 61.07 o -2 4 1 6502.22 6703.50 85.53 o -1 4 1 10251.98 10145.11 104.21 o 0 4 1 10295.47 10268.16 70.79 o 1 4 1 5225.50 5315.77 72.16 o 2 4 1 2103.89 2296.63 56.51 o 3 4 1 3504.72 3484.90 75.35 o 4 4 1 2067.50 2041.87 70.64 o 5 4 1 575.42 636.52 62.59 o 6 4 1 349.75 215.72 162.55 o 7 4 1 591.57 604.62 73.68 o 8 4 1 408.41 502.68 77.78 o 9 4 1 227.27 259.32 81.12 o -9 5 1 87.18 168.93 75.50 o -8 5 1 1.04 13.98 67.75 o -7 5 1 736.03 769.75 77.48 o -6 5 1 3720.55 3875.63 116.52 o -5 5 1 6695.29 6777.79 129.89 o -4 5 1 8213.28 8366.50 126.70 o -3 5 1 4733.07 4681.53 88.26 o -2 5 1 127.28 108.01 35.55 o -1 5 1 1539.89 1405.36 49.07 o 0 5 1 8541.55 8712.72 64.11 o 1 5 1 16838.04 17555.02 165.43 o 2 5 1 18041.71 18605.65 185.03 o 3 5 1 11592.85 11953.50 132.77 o 4 5 1 789.41 831.12 56.36 o 5 5 1 920.14 958.58 69.42 o 6 5 1 1983.12 2023.95 96.92 o 7 5 1 2521.76 2484.55 108.62 o 8 5 1 605.18 754.40 85.98 o 9 5 1 285.91 365.05 81.43 o -8 6 1 652.07 639.56 82.94 o -7 6 1 63.50 12.15 157.38 o -6 6 1 135.47 214.05 64.72 o -5 6 1 759.33 793.90 67.60 o -4 6 1 147.49 7.14 113.18 o -3 6 1 2422.46 2275.06 70.64 o -2 6 1 7195.13 7026.32 97.07 o -1 6 1 960.85 905.71 45.57 o 0 6 1 3659.26 3720.98 48.92 o 1 6 1 1280.01 1293.09 46.94 o 2 6 1 2540.92 2584.21 65.32 o 3 6 1 426.55 347.28 45.27 o 4 6 1 30.60 24.91 96.31 o 5 6 1 559.15 568.31 66.23 o 6 6 1 126.74 10.48 163.92 o 7 6 1 1296.37 1263.77 66.54 o 8 6 1 319.36 200.37 80.21 o -8 7 1 44.44 14.74 70.03 o -7 7 1 472.74 414.12 75.20 o -6 7 1 2198.59 2063.60 100.11 o -5 7 1 4518.81 4484.80 117.89 o -4 7 1 6167.23 5932.39 118.19 o -3 7 1 1750.30 1646.14 62.89 o -2 7 1 218.79 240.78 40.56 o -1 7 1 1617.92 1665.89 54.23 o 0 7 1 3898.46 3930.77 52.56 o 1 7 1 6969.70 6923.02 95.71 o 2 7 1 7780.83 7477.05 105.88 o 3 7 1 7135.90 7397.75 116.67 o 4 7 1 792.33 733.44 61.83 o 5 7 1 430.94 437.36 62.28 o 6 7 1 1656.58 1739.72 91.91 o 7 7 1 1959.66 1911.99 105.88 o 8 7 1 327.50 324.49 78.39 o -8 8 1 636.47 591.55 89.93 o -7 8 1 820.82 966.32 81.73 o -6 8 1 228.13 210.86 63.65 o -5 8 1 11.77 36.92 56.51 o -4 8 1 157.55 92.52 121.23 o -3 8 1 2868.59 2898.52 82.19 o -2 8 1 7919.34 7689.43 114.54 o -1 8 1 3939.97 3969.97 80.36 o 0 8 1 4328.02 4308.43 58.49 o 1 8 1 1811.09 1917.31 61.07 o 2 8 1 1468.47 1577.17 61.37 o 3 8 1 1196.08 1176.57 61.98 o 4 8 1 1040.94 978.63 67.91 o 5 8 1 942.40 962.53 73.07 o 6 8 1 592.07 625.43 68.36 o 7 8 1 436.32 464.25 78.69 o 8 8 1 252.72 217.54 81.73 o -8 9 1 78.10 15.65 77.02 o -7 9 1 244.54 178.80 73.83 o -6 9 1 164.05 119.40 143.56 o -5 9 1 1199.03 1263.32 81.27 o -4 9 1 1563.37 1522.33 78.84 o -3 9 1 334.31 375.38 49.83 o -2 9 1 17.37 6.68 93.73 o -1 9 1 927.38 834.92 51.80 o 0 9 1 2953.72 2827.73 52.87 o 1 9 1 754.15 781.45 47.09 o 2 9 1 2361.94 2270.81 75.05 o 3 9 1 4456.96 4268.78 101.93 o 4 9 1 2484.89 2409.51 90.84 o 5 9 1 819.65 879.89 73.98 o 6 9 1 510.26 518.48 69.12 o 7 9 1 224.96 121.83 72.01 o 8 9 1 148.24 180.78 73.22 o -8 10 1 985.50 1051.40 102.39 o -7 10 1 1410.58 1420.55 100.87 o -6 10 1 579.00 152.83 176.22 o -5 10 1 669.22 570.74 73.37 o -4 10 1 390.48 447.54 58.33 o -3 10 1 2857.89 2762.40 89.78 o -2 10 1 4765.46 4629.12 102.85 o -1 10 1 6412.29 6267.81 113.02 o 0 10 1 5365.33 5282.96 72.16 o 1 10 1 1094.74 1055.35 57.58 o 2 10 1 443.49 440.55 48.31 o 3 10 1 2471.41 2288.58 84.16 o 4 10 1 3536.59 3453.46 108.01 o 5 10 1 624.65 555.25 73.53 o 6 10 1 964.31 1063.70 57.12 o 7 10 1 131.51 14.13 67.15 o 8 10 1 66.10 138.24 72.77 o -7 11 1 61.25 76.87 65.93 o -6 11 1 68.13 96.47 58.03 o -5 11 1 13.28 11.24 107.86 o -4 11 1 188.41 214.50 144.17 o -3 11 1 335.77 235.31 57.58 o -2 11 1 49.86 120.77 40.86 o -1 11 1 322.54 395.89 49.98 o 0 11 1 669.56 688.93 39.95 o 1 11 1 825.34 772.18 56.66 o 2 11 1 90.75 128.97 108.92 o 3 11 1 1158.23 1180.22 73.83 o 4 11 1 809.85 871.07 75.35 o 5 11 1 328.12 333.91 61.37 o 6 11 1 235.48 251.42 66.08 o 7 11 1 30.85 14.74 68.51 o -7 12 1 697.94 673.59 88.41 o -6 12 1 482.33 448.91 74.29 o -5 12 1 278.20 249.75 66.99 o -4 12 1 762.22 691.06 73.68 o -3 12 1 1146.32 1206.80 75.20 o -2 12 1 744.16 723.87 63.96 o -1 12 1 4214.83 4079.04 105.43 o 0 12 1 3556.58 3464.09 70.34 o 1 12 1 43.96 94.64 97.38 o 2 12 1 825.29 876.54 66.23 o 3 12 1 1299.19 1301.14 77.63 o 4 12 1 2397.28 2264.58 102.69 o 5 12 1 976.05 740.12 81.73 o 6 12 1 310.92 397.71 68.21 o 7 12 1 254.37 204.78 73.22 o -7 13 1 130.27 72.92 73.37 o -6 13 1 218.18 372.19 70.94 o -5 13 1 573.97 582.74 75.96 o -4 13 1 1133.08 1230.50 78.84 o -3 13 1 339.15 316.89 62.89 o -2 13 1 164.45 202.50 54.99 o -1 13 1 795.94 837.20 66.08 o 0 13 1 3304.98 3257.49 73.22 o 1 13 1 2874.19 2897.30 97.07 o 2 13 1 1034.51 1085.42 73.22 o 3 13 1 905.60 940.50 78.39 o 4 13 1 239.54 148.57 65.63 o 5 13 1 142.41 183.36 61.07 o 6 13 1 18.94 160.12 62.13 o 7 13 1 192.96 236.07 74.89 o -6 14 1 8.87 14.89 62.44 o -5 14 1 14.75 45.88 59.70 o -4 14 1 366.17 522.43 66.54 o -3 14 1 160.99 37.98 136.87 o -2 14 1 121.36 70.94 126.24 o -1 14 1 1497.53 1468.55 82.79 o 0 14 1 1478.31 1477.51 58.33 o 1 14 1 298.31 56.51 151.31 o 2 14 1 427.26 413.21 64.56 o 3 14 1 1137.07 1181.13 81.43 o 4 14 1 866.19 882.77 80.97 o 5 14 1 153.31 132.77 63.80 o 6 14 1 201.68 175.46 68.82 o -6 15 1 347.14 481.87 75.50 o -5 15 1 853.23 825.65 84.77 o -4 15 1 1501.58 1541.01 97.22 o -3 15 1 536.29 520.15 68.36 o -2 15 1 17.62 11.24 127.46 o -1 15 1 316.25 291.98 57.58 o 0 15 1 2223.23 2227.82 69.73 o 1 15 1 2503.66 2428.80 100.72 o 2 15 1 1425.70 1485.87 85.22 o 3 15 1 1627.47 1651.30 93.28 o 4 15 1 206.54 205.84 71.10 o 5 15 1 34.98 14.28 62.89 o 6 15 1 56.38 32.66 59.85 o -5 16 1 247.39 327.83 69.12 o -4 16 1 48.49 104.52 63.20 o -3 16 1 11.21 12.91 56.66 o -2 16 1 10.94 124.57 115.00 o -1 16 1 27.93 11.70 104.67 o 0 16 1 219.22 209.19 56.51 o 1 16 1 365.51 407.74 64.72 o 2 16 1 97.52 111.05 141.58 o 3 16 1 276.99 271.77 65.32 o 4 16 1 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96.01 65.78 o -2 0 11 9.02 15.65 58.79 o -1 0 11 419.45 477.62 80.97 o 0 0 11 1321.43 1361.91 111.05 o 1 0 11 601.58 718.25 86.14 o 2 0 11 520.26 599.76 86.74 o -3 1 11 45.77 16.25 71.86 o -2 1 11 154.27 284.53 72.01 o -1 1 11 290.75 293.80 76.72 o 0 1 11 59.84 123.51 47.85 o 1 1 11 0.88 15.50 63.65 o 2 1 11 5.99 15.95 70.34 o -3 2 11 54.83 88.57 75.50 o -2 2 11 45.61 50.28 68.36 o -1 2 11 378.81 473.21 85.38 o 0 2 11 575.37 624.52 61.37 o 1 2 11 341.26 298.36 87.35 o 2 2 11 426.36 489.31 76.56 o -3 3 11 236.63 202.81 85.07 o -2 3 11 155.86 179.26 73.83 o -1 3 11 311.46 492.66 76.26 o 0 3 11 149.43 109.99 51.35 o 1 3 11 0.46 15.65 65.63 o 2 3 11 56.02 107.40 62.74 o -2 4 11 74.39 110.44 66.08 o -1 4 11 67.11 170.14 67.91 o 0 4 11 30.50 24.91 45.73 o 1 4 11 84.43 109.38 69.42 o 2 4 11 101.86 173.18 69.88 o -2 5 11 249.05 252.63 83.70 o -1 5 11 221.72 259.32 70.79 o 0 5 11 64.43 44.66 49.68 o 1 5 11 4.29 16.10 68.97 o -1 6 11 26.55 16.25 64.11 o 0 6 11 95.03 62.13 53.32 o 1 6 11 96.72 40.41 71.25 o