#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2011552.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011552_Fobs loop_ _publ_author_name 'Bolte, Michael' 'Hensen, Karl' 'Faber, Alexander' _publ_section_title ; trans-Tetrachlorobis(4-methylpyridine)germanium(IV) ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first e497 _journal_page_last e498 _journal_volume 56 _journal_year 2000 _space_group_IT_number 53 _symmetry_space_group_name_Hall '-P 2ac 2' _symmetry_space_group_name_H-M 'P m n a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.1540 _cell_length_b 7.9330 _cell_length_c 13.7310 _exptl_crystal_F_000 400.00 _reflns_d_resolution_high 0.7507 _[local]_cod_data_source_file qa0414Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' he77 in Pmna' _shelx_refln_list_code 4 _shelx_f_calc_maximum 165.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x+1/2, y, -z+1/2' 'x, -y, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x-1/2, -y, z-1/2' '-x, y, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8642.75 8670.35 181.78 o 4 0 0 27445.70 25812.92 743.90 o 6 0 0 1966.89 1910.75 47.91 o 8 0 0 2721.39 2818.81 100.39 o 0 1 0 10504.76 11120.29 227.18 o 2 1 0 101.56 123.09 5.84 o 4 1 0 4059.59 3848.80 60.24 o 6 1 0 143.15 153.67 9.42 o 8 1 0 463.66 485.92 45.14 o 0 2 0 136.38 131.65 9.04 o 2 2 0 9536.45 9453.30 160.32 o 4 2 0 275.40 247.32 9.59 o 6 2 0 1294.53 1254.91 28.45 o 8 2 0 267.66 256.03 27.64 o 0 3 0 2823.58 3238.82 98.57 o 2 3 0 12720.45 12209.95 206.37 o 4 3 0 166.81 168.22 8.50 o 6 3 0 2078.90 1996.25 40.43 o 8 3 0 77.41 65.54 16.52 o 0 4 0 652.79 922.72 33.44 o 2 4 0 2157.13 1950.97 36.64 o 4 4 0 110.56 126.83 12.21 o 6 4 0 656.22 651.70 24.06 o 8 4 0 5.09 26.37 16.80 o 0 5 0 4126.24 4189.59 127.53 o 2 5 0 62.35 74.71 6.24 o 4 5 0 1603.18 1598.12 32.37 o 6 5 0 245.85 222.60 16.41 o 8 5 0 118.04 107.58 27.78 o 0 6 0 8287.12 7692.29 228.19 o 2 6 0 38.71 36.53 6.08 o 4 6 0 3844.20 3604.82 56.82 o 6 6 0 62.59 78.70 18.36 o 0 7 0 3311.20 3191.07 101.25 o 2 7 0 196.15 195.45 9.87 o 4 7 0 2009.98 1942.05 57.97 o 6 7 0 68.09 65.01 14.61 o 0 8 0 33.19 27.24 12.13 o 2 8 0 595.07 611.44 22.27 o 4 8 0 8.16 9.25 14.05 o 6 8 0 56.02 43.04 15.06 o 0 9 0 46.99 42.64 13.78 o 2 9 0 1985.72 2021.88 41.35 o 4 9 0 4.01 -4.31 11.32 o 0 10 0 4.44 31.91 15.81 o 2 10 0 445.06 406.15 16.27 o 1 0 1 8539.23 8648.21 113.47 o 3 0 1 660.34 668.00 13.99 o 5 0 1 5667.41 5474.43 84.59 o 7 0 1 3.95 4.05 7.28 o 9 0 1 1164.76 1283.02 59.77 o 0 1 1 2053.29 1923.07 34.15 o 1 1 1 7299.19 7372.08 81.72 o 2 1 1 9858.32 10266.97 114.05 o 3 1 1 1565.15 1518.52 22.68 o 4 1 1 365.24 440.13 11.41 o 5 1 1 2892.84 2686.13 42.45 o 6 1 1 850.30 887.85 14.78 o 7 1 1 191.89 204.12 9.27 o 8 1 1 152.02 135.90 13.29 o 9 1 1 631.79 632.20 28.32 o 0 2 1 1649.53 1713.19 31.20 o 1 2 1 910.06 909.93 30.19 o 2 2 1 816.61 846.64 12.44 o 3 2 1 2984.39 2913.33 37.09 o 4 2 1 306.45 315.43 7.66 o 5 2 1 123.91 120.20 6.32 o 6 2 1 52.33 50.49 6.34 o 7 2 1 1112.67 1113.52 23.84 o 8 2 1 13.69 13.30 9.30 o 9 2 1 16.93 35.23 12.77 o 0 3 1 1381.00 1576.96 51.15 o 1 3 1 1884.39 1930.08 30.62 o 2 3 1 884.12 956.20 13.96 o 3 3 1 5122.34 4892.00 60.44 o 4 3 1 314.10 354.00 8.08 o 5 3 1 15.46 12.40 5.05 o 6 3 1 196.38 189.84 9.16 o 7 3 1 2129.69 2147.53 39.71 o 8 3 1 42.01 43.02 18.71 o 9 3 1 6.21 5.25 12.70 o 0 4 1 452.58 460.08 14.34 o 1 4 1 915.81 887.96 14.53 o 2 4 1 626.67 614.46 10.30 o 3 4 1 1452.57 1436.25 20.24 o 4 4 1 109.40 118.63 6.89 o 5 4 1 192.43 198.79 7.29 o 6 4 1 45.18 52.67 7.28 o 7 4 1 646.60 632.87 22.75 o 8 4 1 0.08 -7.73 9.87 o 0 5 1 78.25 63.88 6.98 o 1 5 1 1449.54 1418.88 32.93 o 2 5 1 806.65 840.54 13.23 o 3 5 1 200.54 184.23 6.12 o 4 5 1 24.73 45.72 5.12 o 5 5 1 1422.11 1341.65 25.32 o 6 5 1 157.34 147.61 10.47 o 7 5 1 11.36 2.07 10.91 o 8 5 1 1.37 12.30 11.75 o 0 6 1 38.04 43.65 7.49 o 1 6 1 1830.68 1856.24 32.71 o 2 6 1 30.45 32.09 4.68 o 3 6 1 186.92 193.43 6.04 o 4 6 1 6.74 8.96 4.57 o 5 6 1 1987.08 1953.13 31.03 o 6 6 1 27.50 19.19 8.83 o 7 6 1 4.77 22.27 10.27 o 0 7 1 37.90 54.85 18.06 o 1 7 1 1111.88 1077.97 20.56 o 2 7 1 420.61 388.51 9.88 o 3 7 1 635.56 619.27 12.00 o 4 7 1 1.04 11.78 10.41 o 5 7 1 755.63 729.25 18.53 o 6 7 1 77.58 82.17 10.54 o 7 7 1 123.82 127.37 13.71 o 0 8 1 99.00 97.79 10.38 o 1 8 1 394.09 396.45 11.77 o 2 8 1 139.78 129.10 7.14 o 3 8 1 967.13 979.15 19.07 o 4 8 1 51.76 54.32 10.86 o 5 8 1 31.21 36.70 12.75 o 6 8 1 31.45 24.98 10.35 o 0 9 1 19.41 24.09 9.64 o 1 9 1 192.28 201.50 9.65 o 2 9 1 17.69 5.74 5.57 o 3 9 1 665.62 655.14 15.15 o 4 9 1 23.52 17.47 8.90 o 0 10 1 68.28 65.25 15.14 o 1 10 1 326.26 307.95 12.54 o 2 10 1 37.94 22.19 7.63 o 3 10 1 302.07 299.82 13.91 o 0 0 2 6010.37 6233.95 128.68 o 2 0 2 4439.00 4722.13 71.22 o 4 0 2 2159.55 1987.21 38.60 o 6 0 2 57.80 54.20 7.73 o 8 0 2 175.03 217.81 21.05 o 0 1 2 8681.92 8740.76 146.46 o 1 1 2 59.83 63.76 2.58 o 2 1 2 216.34 233.32 4.58 o 3 1 2 1410.58 1439.19 22.61 o 4 1 2 3215.07 3001.97 81.63 o 5 1 2 262.66 267.72 7.92 o 6 1 2 311.32 330.11 8.85 o 7 1 2 535.60 562.31 13.29 o 8 1 2 487.69 538.01 17.34 o 9 1 2 84.67 91.14 13.91 o 0 2 2 162.85 174.01 9.47 o 1 2 2 1.96 6.06 2.70 o 2 2 2 4981.02 4966.72 60.77 o 3 2 2 770.09 850.50 17.49 o 4 2 2 395.57 397.71 8.54 o 5 2 2 271.68 247.08 10.08 o 6 2 2 1019.46 990.86 19.21 o 7 2 2 424.23 445.73 13.39 o 8 2 2 255.17 269.37 16.88 o 9 2 2 78.31 100.08 26.31 o 0 3 2 133.12 161.55 6.46 o 1 3 2 12.16 27.64 3.82 o 2 3 2 8799.91 8704.84 104.84 o 3 3 2 0.86 5.61 3.44 o 4 3 2 24.07 28.60 4.24 o 5 3 2 22.64 16.19 4.73 o 6 3 2 1602.25 1549.16 27.64 o 7 3 2 0.17 -7.17 7.58 o 8 3 2 101.60 103.89 17.85 o 9 3 2 1.72 10.49 15.12 o 0 4 2 1006.18 1069.41 26.62 o 1 4 2 408.78 454.33 11.80 o 2 4 2 5654.85 5615.09 68.93 o 3 4 2 97.51 92.23 4.72 o 4 4 2 649.22 654.38 11.69 o 5 4 2 699.28 719.21 14.75 o 6 4 2 1674.73 1649.03 27.63 o 7 4 2 163.13 157.73 12.00 o 8 4 2 223.70 192.68 14.82 o 0 5 2 3006.56 2755.78 64.50 o 1 5 2 19.51 30.96 6.05 o 2 5 2 309.77 301.59 7.83 o 3 5 2 393.11 399.03 8.57 o 4 5 2 1284.43 1241.46 18.71 o 5 5 2 97.62 102.33 7.49 o 6 5 2 292.44 297.46 11.03 o 7 5 2 259.37 255.70 13.67 o 8 5 2 150.81 149.31 14.60 o 0 6 2 4567.23 4554.29 99.74 o 1 6 2 44.82 52.28 5.46 o 2 6 2 11.18 15.06 5.77 o 3 6 2 0.01 3.67 4.49 o 4 6 2 2206.89 2139.19 32.77 o 5 6 2 54.24 58.80 7.16 o 6 6 2 64.42 54.41 9.44 o 7 6 2 0.05 7.47 10.09 o 0 7 2 2208.72 2164.21 51.01 o 1 7 2 80.21 78.19 7.22 o 2 7 2 251.55 236.53 7.96 o 3 7 2 74.61 77.98 5.69 o 4 7 2 1367.29 1377.80 21.37 o 5 7 2 314.91 308.25 11.18 o 6 7 2 107.20 91.12 10.78 o 7 7 2 101.39 124.48 13.79 o 0 8 2 401.57 404.20 21.27 o 1 8 2 23.65 19.76 6.28 o 2 8 2 1367.47 1310.23 22.08 o 3 8 2 183.22 151.30 10.46 o 4 8 2 383.29 365.88 12.28 o 5 8 2 9.56 4.87 9.46 o 6 8 2 343.96 316.70 15.36 o 0 9 2 17.97 15.53 18.91 o 1 9 2 11.38 18.09 6.72 o 2 9 2 1413.74 1424.48 24.55 o 3 9 2 64.24 61.22 7.64 o 4 9 2 34.48 28.71 13.40 o 0 10 2 98.34 102.72 13.10 o 1 10 2 53.90 58.26 8.49 o 2 10 2 631.90 665.40 18.02 o 1 0 3 2250.09 2218.84 61.67 o 3 0 3 675.50 724.36 14.35 o 5 0 3 1419.67 1449.68 29.50 o 7 0 3 131.34 156.25 17.47 o 9 0 3 344.31 385.44 33.56 o 0 1 3 7719.72 8332.27 171.50 o 1 1 3 1893.27 1918.11 21.22 o 2 1 3 5370.44 5504.52 74.08 o 3 1 3 1059.78 1019.44 19.84 o 4 1 3 1514.74 1405.78 23.10 o 5 1 3 1084.40 1034.96 15.51 o 6 1 3 294.13 300.27 9.65 o 7 1 3 231.04 239.07 10.70 o 8 1 3 33.30 51.57 10.33 o 9 1 3 218.33 249.55 21.12 o 0 2 3 7457.69 7319.48 151.33 o 1 2 3 1803.09 1770.75 25.19 o 2 2 3 3846.36 3944.33 49.56 o 3 2 3 1777.69 1744.32 21.60 o 4 2 3 1535.24 1440.78 29.95 o 5 2 3 542.66 530.52 10.78 o 6 2 3 359.31 369.82 11.83 o 7 2 3 569.29 577.45 14.98 o 8 2 3 46.00 52.57 10.67 o 9 2 3 90.59 107.53 15.48 o 0 3 3 21.19 37.18 5.74 o 1 3 3 1491.57 1499.23 22.22 o 2 3 3 16.15 19.76 3.30 o 3 3 3 2043.89 1941.98 34.08 o 4 3 3 53.72 61.48 4.73 o 5 3 3 400.11 395.84 10.90 o 6 3 3 0.32 0.24 6.24 o 7 3 3 753.07 718.22 17.07 o 8 3 3 41.02 45.59 13.28 o 9 3 3 61.39 61.87 15.51 o 0 4 3 2627.91 2676.03 69.27 o 1 4 3 2169.38 2141.73 34.19 o 2 4 3 2677.69 2529.24 35.76 o 3 4 3 1816.87 1805.29 27.57 o 4 4 3 683.22 677.33 11.96 o 5 4 3 728.85 702.82 14.84 o 6 4 3 234.33 240.15 10.32 o 7 4 3 576.96 553.95 15.32 o 8 4 3 0.40 6.94 10.78 o 0 5 3 1992.47 1968.53 45.53 o 1 5 3 1799.23 1760.72 26.18 o 2 5 3 1857.95 1858.32 27.66 o 3 5 3 1012.97 1031.09 15.94 o 4 5 3 773.60 785.56 15.35 o 5 5 3 1022.89 993.84 18.71 o 6 5 3 299.65 290.53 11.31 o 7 5 3 238.73 224.17 13.68 o 8 5 3 47.47 53.55 12.92 o 0 6 3 231.02 236.67 11.46 o 1 6 3 1911.13 1838.14 30.90 o 2 6 3 229.85 218.75 6.68 o 3 6 3 964.18 992.86 15.94 o 4 6 3 58.29 60.06 6.76 o 5 6 3 1221.70 1177.88 21.47 o 6 6 3 206.60 201.51 10.60 o 7 6 3 221.28 191.81 13.82 o 0 7 3 791.75 774.41 23.14 o 1 7 3 484.02 510.50 18.59 o 2 7 3 1056.11 1080.53 18.70 o 3 7 3 314.36 315.41 9.26 o 4 7 3 218.79 220.54 9.75 o 5 7 3 283.18 272.36 10.95 o 6 7 3 104.69 118.52 14.48 o 0 8 3 626.08 628.06 21.41 o 1 8 3 555.85 551.76 14.01 o 2 8 3 669.15 639.25 17.58 o 3 8 3 603.18 613.95 16.37 o 4 8 3 306.99 312.33 11.13 o 5 8 3 200.48 200.53 12.61 o 6 8 3 172.14 171.44 13.49 o 0 9 3 20.77 14.50 10.10 o 1 9 3 416.60 376.30 12.31 o 2 9 3 27.39 16.60 7.70 o 3 9 3 509.74 491.63 14.96 o 4 9 3 0.12 -0.62 7.64 o 0 10 3 469.81 481.64 20.75 o 1 10 3 145.10 146.99 11.68 o 2 10 3 120.03 119.87 10.47 o 0 0 4 317.23 327.16 14.61 o 2 0 4 1093.63 1115.76 22.10 o 4 0 4 669.56 709.35 17.63 o 6 0 4 381.42 375.34 18.60 o 8 0 4 254.01 296.32 20.15 o 0 1 4 4322.51 4380.68 95.97 o 1 1 4 0.39 6.32 2.36 o 2 1 4 3500.94 3407.84 42.94 o 3 1 4 1462.98 1513.36 22.03 o 4 1 4 1676.54 1615.72 29.99 o 5 1 4 530.10 522.00 10.07 o 6 1 4 822.00 836.20 15.69 o 7 1 4 770.04 798.96 17.69 o 8 1 4 405.10 417.17 15.86 o 9 1 4 154.13 162.07 15.50 o 0 2 4 3226.72 3103.00 86.81 o 1 2 4 63.39 62.18 3.43 o 2 2 4 2063.37 2012.71 29.12 o 3 2 4 623.96 648.28 12.29 o 4 2 4 1619.94 1604.18 27.11 o 5 2 4 691.85 667.34 14.13 o 6 2 4 773.83 776.84 16.40 o 7 2 4 466.53 460.05 15.40 o 8 2 4 281.05 304.25 18.03 o 9 2 4 227.90 225.95 19.05 o 0 3 4 4432.94 4516.38 95.61 o 1 3 4 300.29 328.23 7.27 o 2 3 4 2494.81 2476.78 31.93 o 3 3 4 285.14 294.42 7.04 o 4 3 4 1783.74 1734.56 26.98 o 5 3 4 31.23 49.09 6.71 o 6 3 4 896.34 866.31 25.57 o 7 3 4 69.40 73.07 9.02 o 8 3 4 314.46 308.80 15.14 o 0 4 4 1737.17 1654.03 31.55 o 1 4 4 131.65 132.64 5.21 o 2 4 4 1504.24 1522.25 23.02 o 3 4 4 471.74 446.49 8.86 o 4 4 4 974.78 967.39 17.36 o 5 4 4 677.88 684.33 17.37 o 6 4 4 517.27 519.03 13.69 o 7 4 4 417.42 393.95 13.32 o 8 4 4 203.11 184.48 16.77 o 0 5 4 1663.36 1673.20 39.76 o 1 5 4 208.71 209.56 7.54 o 2 5 4 1993.01 2031.59 29.95 o 3 5 4 1060.30 1059.26 16.35 o 4 5 4 1009.32 1020.08 20.62 o 5 5 4 31.27 35.25 6.80 o 6 5 4 582.27 576.50 14.75 o 7 5 4 694.40 665.33 17.48 o 8 5 4 305.44 273.53 16.13 o 0 6 4 378.52 375.21 14.38 o 1 6 4 4.26 2.62 5.45 o 2 6 4 583.59 604.31 12.28 o 3 6 4 23.46 24.85 5.73 o 4 6 4 292.52 286.31 9.82 o 5 6 4 22.15 32.52 10.05 o 6 6 4 175.18 173.33 10.67 o 7 6 4 9.42 7.56 11.14 o 0 7 4 200.01 192.50 11.69 o 1 7 4 13.17 20.11 5.51 o 2 7 4 141.09 150.14 7.19 o 3 7 4 570.16 570.30 12.00 o 4 7 4 119.12 129.08 8.76 o 5 7 4 133.59 142.16 9.86 o 6 7 4 59.14 67.66 9.90 o 0 8 4 714.65 724.77 27.76 o 1 8 4 43.41 39.30 9.01 o 2 8 4 382.88 357.98 14.45 o 3 8 4 33.07 40.60 7.40 o 4 8 4 400.29 421.87 12.46 o 5 8 4 184.62 198.74 10.53 o 0 9 4 278.07 293.88 16.21 o 1 9 4 73.74 77.78 9.14 o 2 9 4 156.48 149.36 11.08 o 3 9 4 3.88 11.13 12.35 o 4 9 4 165.35 139.85 10.46 o 0 10 4 318.64 334.36 25.71 o 1 10 4 1.61 11.63 9.39 o 2 10 4 345.32 334.13 13.72 o 1 0 5 1200.80 1192.02 27.75 o 3 0 5 2518.42 2330.46 42.90 o 5 0 5 52.58 48.46 7.96 o 7 0 5 914.65 982.79 32.13 o 9 0 5 4.62 16.72 15.22 o 0 1 5 6335.53 6480.57 134.52 o 1 1 5 874.05 822.96 13.17 o 2 1 5 2271.55 2235.77 64.75 o 3 1 5 1599.36 1534.17 25.35 o 4 1 5 1646.60 1575.12 18.92 o 5 1 5 326.68 342.95 9.11 o 6 1 5 182.63 185.11 9.47 o 7 1 5 593.85 647.14 18.16 o 8 1 5 71.05 96.23 11.58 o 9 1 5 59.41 64.26 15.28 o 0 2 5 5115.06 5017.43 234.41 o 1 2 5 8785.98 9412.00 123.35 o 2 2 5 2306.10 2275.33 33.25 o 3 2 5 3526.40 3549.07 49.59 o 4 2 5 1369.61 1302.23 21.30 o 5 2 5 3356.58 3064.60 44.59 o 6 2 5 299.64 279.20 9.98 o 7 2 5 660.39 660.33 19.95 o 8 2 5 73.81 69.12 11.20 o 0 3 5 5.19 12.43 5.71 o 1 3 5 2088.96 2071.56 26.98 o 2 3 5 0.60 1.54 3.10 o 3 3 5 442.63 458.23 10.21 o 4 3 5 21.46 19.91 5.25 o 5 3 5 1762.97 1714.70 27.65 o 6 3 5 8.51 7.67 6.51 o 7 3 5 34.24 43.05 9.62 o 8 3 5 14.70 24.77 10.67 o 0 4 5 2584.07 2510.25 56.10 o 1 4 5 2706.12 2610.24 36.78 o 2 4 5 1233.31 1203.86 21.22 o 3 4 5 1508.26 1481.75 26.05 o 4 4 5 887.06 898.00 16.80 o 5 4 5 1380.68 1372.59 23.64 o 6 4 5 97.62 82.39 8.15 o 7 4 5 340.27 317.88 12.41 o 8 4 5 30.26 32.79 11.13 o 0 5 5 1908.00 1876.30 47.51 o 1 5 5 1274.96 1269.81 20.06 o 2 5 5 1191.26 1202.52 19.48 o 3 5 5 1759.55 1811.97 28.06 o 4 5 5 788.87 769.46 15.51 o 5 5 5 307.89 305.64 10.70 o 6 5 5 223.86 217.31 10.83 o 7 5 5 638.18 615.55 17.06 o 0 6 5 138.82 133.05 9.98 o 1 6 5 21.45 9.85 4.02 o 2 6 5 40.95 40.19 5.39 o 3 6 5 101.21 102.23 7.15 o 4 6 5 138.73 144.07 9.19 o 5 6 5 119.69 121.19 8.89 o 6 6 5 0.04 3.73 7.62 o 7 6 5 84.45 110.86 11.45 o 0 7 5 1079.93 1079.70 29.58 o 1 7 5 565.06 558.33 15.77 o 2 7 5 361.81 364.58 11.60 o 3 7 5 515.10 502.26 28.59 o 4 7 5 413.66 418.07 13.82 o 5 7 5 229.31 220.30 11.99 o 6 7 5 19.12 31.54 10.29 o 0 8 5 797.85 805.28 25.18 o 1 8 5 404.49 411.84 20.45 o 2 8 5 352.18 342.57 21.20 o 3 8 5 104.24 97.43 8.96 o 4 8 5 423.66 416.68 12.88 o 5 8 5 369.47 378.49 15.33 o 0 9 5 25.77 32.26 31.78 o 1 9 5 438.25 439.76 15.98 o 2 9 5 0.81 11.91 9.42 o 3 9 5 138.69 144.63 12.79 o 4 9 5 43.69 35.69 8.97 o 0 10 5 100.97 115.51 19.26 o 1 10 5 362.43 384.57 18.42 o 0 0 6 488.18 482.29 19.66 o 2 0 6 8778.74 9600.58 163.12 o 4 0 6 11.60 17.37 6.09 o 6 0 6 1446.01 1520.15 42.34 o 8 0 6 162.03 172.45 24.10 o 0 1 6 273.94 277.93 7.79 o 1 1 6 1061.64 1161.85 18.56 o 2 1 6 4605.06 4369.02 127.76 o 3 1 6 48.08 63.64 4.97 o 4 1 6 301.22 299.18 11.33 o 5 1 6 776.46 803.12 15.80 o 6 1 6 1009.39 1042.01 22.81 o 7 1 6 9.08 0.77 7.61 o 8 1 6 187.29 193.99 12.98 o 0 2 6 5449.56 5158.85 108.61 o 1 2 6 220.36 231.57 5.95 o 2 2 6 284.46 297.89 7.37 o 3 2 6 13.38 17.76 4.32 o 4 2 6 2224.65 2119.15 29.07 o 5 2 6 328.90 329.00 9.12 o 6 2 6 354.24 348.54 12.60 o 7 2 6 77.85 65.71 9.51 o 8 2 6 244.17 237.23 16.40 o 0 3 6 7577.03 7150.98 122.34 o 1 3 6 346.60 389.97 7.68 o 2 3 6 105.56 111.03 4.70 o 3 3 6 173.79 208.20 7.38 o 4 3 6 3020.88 2977.41 48.26 o 5 3 6 135.30 143.80 7.89 o 6 3 6 63.45 69.39 7.74 o 7 3 6 37.26 39.61 9.82 o 8 3 6 281.64 294.78 15.73 o 0 4 6 3344.32 3235.32 70.93 o 1 4 6 3.73 12.76 4.20 o 2 4 6 250.49 245.37 7.21 o 3 4 6 269.02 262.18 8.37 o 4 4 6 1735.94 1726.31 27.49 o 5 4 6 67.46 63.93 7.27 o 6 4 6 141.09 142.37 9.32 o 7 4 6 203.31 190.71 12.88 o 8 4 6 333.99 314.82 21.72 o 0 5 6 227.69 241.65 9.78 o 1 5 6 1189.31 1181.14 19.08 o 2 5 6 2588.43 2663.69 38.21 o 3 5 6 367.60 386.14 11.39 o 4 5 6 339.89 361.91 11.00 o 5 5 6 968.26 950.86 18.91 o 6 5 6 529.42 534.07 14.78 o 7 5 6 42.27 38.39 9.51 o 0 6 6 20.19 21.14 11.70 o 1 6 6 1.64 -1.35 4.41 o 2 6 6 3084.99 3177.49 58.86 o 3 6 6 10.88 7.37 10.35 o 4 6 6 11.18 16.55 7.14 o 5 6 6 0.53 6.66 7.78 o 6 6 6 689.83 678.00 18.87 o 7 6 6 4.38 23.75 11.18 o 0 7 6 203.68 215.14 13.34 o 1 7 6 233.36 227.42 9.45 o 2 7 6 1327.34 1395.83 37.34 o 3 7 6 10.61 16.76 7.16 o 4 7 6 122.08 121.09 13.67 o 5 7 6 324.79 312.53 13.81 o 6 7 6 546.38 529.34 18.16 o 0 8 6 1235.59 1236.16 33.87 o 1 8 6 40.49 54.68 8.44 o 2 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