#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2011555.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011555_Fobs loop_ _publ_author_name 'Kongshaug, Kjell Ove' 'Fjellv\%ag, Helmer' 'Lillerud, Karl Petter' _publ_section_title ; A three-dimensional open-framework zinc arsenate, (C~4~H~12~N~2~)~2~[Zn~7~(AsO~4~)~6~(H~2~O)~2~] ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first e503 _journal_page_last e504 _journal_volume 56 _journal_year 2000 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _exptl_crystal_F_000 2880.00 _[local]_cod_data_source_file qa0423Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' za in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 981.15 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 301835.44 272611.31 2967.15 o 4 0 0 235934.44 241532.88 9329.07 o 6 0 0 13541.23 15533.86 897.46 o 8 0 0 14139.36 13665.33 932.34 o 10 0 0 43914.75 44479.05 4223.82 o 12 0 0 7470.07 9123.58 924.39 o 14 0 0 29118.26 30549.52 1464.60 o 16 0 0 23431.90 23895.73 1516.85 o 18 0 0 1101.59 1873.22 1494.07 o 20 0 0 11297.95 10765.58 1893.85 o 1 1 0 50492.21 51610.70 1841.57 o 3 1 0 13591.64 16193.49 454.72 o 5 1 0 0.84 294.16 432.11 o 7 1 0 46599.25 45650.25 1224.42 o 9 1 0 56831.57 57550.43 2448.70 o 11 1 0 4849.09 4365.65 709.87 o 13 1 0 340.09 948.03 652.85 o 15 1 0 209.60 850.43 743.28 o 17 1 0 5802.86 5682.98 990.27 o 19 1 0 1905.27 653.84 1110.66 o 0 2 0 1867.67 1492.30 1256.68 o 2 2 0 578252.50 490012.06 19642.82 o 4 2 0 651.65 1589.69 434.10 o 6 2 0 1682.66 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