#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:27:36 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180784 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/15/2011560.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011560_Fobs loop_ _publ_author_name 'Lynch, Daniel E.' 'McClenaghan, Ian' _publ_section_title ; 2-Chloro-3-morpholino-1,4-naphthoquinone ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first e537 _journal_volume 56 _journal_year 2000 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 67.204 _cell_angle_beta 84.407 _cell_angle_gamma 81.268 _cell_length_a 5.0386 _cell_length_b 10.3948 _cell_length_c 12.7421 _exptl_crystal_F_000 288.00 _reflns_d_resolution_high 0.7689 _cod_data_source_file qa0432Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 2-Chloro-3-(4-morpholino)-1,4-naphthoquinone _shelx_refln_list_code 4 _shelx_f_calc_maximum 65.16 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1924.70 1781.86 46.45 o 2 0 0 157.24 137.73 5.16 o 3 0 0 176.77 151.34 4.13 o 4 0 0 598.54 592.20 29.18 o 5 0 0 22.42 20.94 2.80 o 6 0 0 0.70 0.40 0.69 o -6 1 0 0.00 0.02 1.02 o -5 1 0 36.35 35.98 1.77 o -4 1 0 0.30 0.62 0.34 o -3 1 0 154.72 143.17 4.61 o -2 1 0 173.76 149.42 6.23 o -1 1 0 2963.10 2571.77 66.43 o 1 1 0 121.99 108.70 12.21 o 2 1 0 1.26 1.17 0.24 o 3 1 0 1188.86 1148.70 31.14 o 4 1 0 413.55 419.49 17.87 o 5 1 0 43.66 50.49 2.88 o 6 1 0 6.15 5.54 0.94 o -6 2 0 0.51 0.24 1.12 o -5 2 0 46.47 45.89 1.43 o -4 2 0 8.74 7.66 0.95 o -3 2 0 278.01 256.30 6.79 o -2 2 0 1621.37 1486.95 49.22 o -1 2 0 3705.79 3329.44 91.59 o 0 2 0 16.44 17.55 0.41 o 1 2 0 137.35 141.68 3.47 o 2 2 0 1970.92 1873.60 53.13 o 3 2 0 38.60 35.38 1.14 o 4 2 0 75.23 75.38 2.39 o 5 2 0 21.94 19.48 1.49 o 6 2 0 0.91 0.29 0.66 o -6 3 0 0.43 0.84 0.99 o -5 3 0 113.22 128.81 4.92 o -4 3 0 4.13 3.93 0.38 o -3 3 0 8.30 3.77 1.67 o -2 3 0 353.00 339.81 8.22 o -1 3 0 0.53 0.60 0.20 o 0 3 0 2266.34 2168.29 48.89 o 1 3 0 16.10 15.86 13.90 o 2 3 0 894.13 839.01 17.02 o 3 3 0 5.89 5.03 0.33 o 4 3 0 88.18 91.99 3.49 o 5 3 0 174.02 187.97 10.60 o -5 4 0 144.17 165.84 6.32 o -4 4 0 17.92 18.73 0.88 o -3 4 0 9.79 5.67 0.73 o -2 4 0 5.76 8.27 0.38 o -1 4 0 203.94 191.85 4.82 o 0 4 0 754.13 764.85 15.84 o 1 4 0 3954.26 4282.49 90.29 o 2 4 0 34.67 47.72 1.12 o 3 4 0 131.15 127.38 2.62 o 4 4 0 29.85 26.18 1.39 o 5 4 0 125.71 143.45 6.04 o 6 4 0 0.16 -0.26 0.82 o -5 5 0 14.62 13.37 0.97 o -4 5 0 47.58 41.79 1.76 o -3 5 0 135.43 142.22 6.77 o -2 5 0 77.93 78.11 2.15 o -1 5 0 369.06 366.63 7.71 o 0 5 0 914.05 1031.24 19.83 o 1 5 0 251.49 294.26 5.58 o 2 5 0 182.24 183.36 4.19 o 3 5 0 13.08 12.96 0.48 o 4 5 0 892.21 935.05 26.96 o 5 5 0 95.37 96.33 4.88 o 6 5 0 2.98 2.17 1.05 o -5 6 0 30.75 33.60 2.86 o -4 6 0 0.52 0.30 0.36 o -3 6 0 121.33 114.95 3.80 o -2 6 0 4.23 4.32 0.68 o -1 6 0 169.72 169.35 3.96 o 0 6 0 52.78 58.44 1.95 o 1 6 0 16.89 14.40 0.44 o 2 6 0 128.73 119.16 3.03 o 3 6 0 0.21 0.12 0.21 o 4 6 0 256.80 268.10 7.42 o 5 6 0 11.43 10.39 1.11 o 6 6 0 40.10 42.76 3.49 o -4 7 0 13.67 12.53 0.92 o -3 7 0 14.30 13.89 0.75 o -2 7 0 34.20 34.70 1.24 o -1 7 0 57.83 57.89 2.39 o 0 7 0 87.31 87.77 1.98 o 1 7 0 97.21 100.12 2.06 o 2 7 0 60.80 58.82 1.40 o 3 7 0 0.13 0.38 0.37 o 4 7 0 43.92 37.07 1.36 o 5 7 0 0.12 0.04 0.93 o -4 8 0 45.57 44.40 2.94 o -3 8 0 5.31 4.30 1.17 o -2 8 0 234.82 276.78 9.49 o -1 8 0 36.97 37.11 1.55 o 0 8 0 3.16 1.94 0.33 o 1 8 0 49.52 53.66 1.31 o 2 8 0 117.38 92.99 2.21 o 3 8 0 0.21 0.67 0.32 o 4 8 0 22.85 21.21 1.33 o 5 8 0 42.12 49.28 3.62 o -3 9 0 69.80 77.06 4.70 o -2 9 0 0.01 -0.43 0.47 o -1 9 0 71.91 77.07 3.59 o 0 9 0 1.95 0.87 0.30 o 1 9 0 196.18 166.55 4.80 o 2 9 0 359.75 341.78 7.77 o 3 9 0 12.20 9.50 0.88 o 4 9 0 9.02 7.95 1.29 o 5 9 0 24.44 32.66 2.88 o -3 10 0 33.34 39.65 2.98 o -2 10 0 42.41 36.60 2.43 o -1 10 0 34.65 31.65 1.62 o 0 10 0 23.36 21.18 1.10 o 1 10 0 29.19 22.90 1.02 o 2 10 0 5.21 6.85 1.48 o 3 10 0 1.91 1.77 0.65 o 4 10 0 26.24 22.35 2.56 o -2 11 0 6.28 6.71 1.27 o -1 11 0 8.57 9.38 1.41 o 0 11 0 64.30 67.58 3.56 o 1 11 0 172.43 170.03 6.74 o 2 11 0 9.95 10.85 0.99 o 3 11 0 3.00 4.52 1.65 o 0 12 0 26.40 24.37 1.52 o 1 12 0 14.83 14.02 1.85 o 2 12 0 47.33 43.67 2.33 o -1 -12 1 0.00 0.77 0.75 o 0 -12 1 49.58 52.86 4.39 o -3 -11 1 12.48 12.78 1.84 o -2 -11 1 59.73 68.22 3.45 o -1 -11 1 9.96 9.16 0.86 o 0 -11 1 24.99 22.62 1.41 o 1 -11 1 0.14 1.00 1.00 o -4 -10 1 4.32 3.58 1.26 o -3 -10 1 2.30 2.00 1.11 o -2 -10 1 9.75 11.20 1.72 o -1 -10 1 63.55 66.97 2.69 o 0 -10 1 205.25 217.93 7.38 o 1 -10 1 28.75 29.16 2.18 o 2 -10 1 6.82 2.75 1.01 o -4 -9 1 67.31 68.09 5.30 o -3 -9 1 68.68 74.68 3.24 o -2 -9 1 232.33 211.80 6.64 o -1 -9 1 12.51 11.56 0.64 o 0 -9 1 0.15 0.03 0.32 o 1 -9 1 7.91 6.54 0.84 o 2 -9 1 157.67 174.79 6.72 o 3 -9 1 0.40 0.47 0.94 o -5 -8 1 9.79 7.08 1.38 o -4 -8 1 54.52 62.81 3.85 o -3 -8 1 11.07 6.25 1.60 o -2 -8 1 269.71 264.58 6.66 o -1 -8 1 0.59 0.62 0.26 o 0 -8 1 149.21 163.44 4.34 o 1 -8 1 357.73 375.95 12.33 o 2 -8 1 1029.37 1160.54 48.70 o 3 -8 1 0.41 1.03 0.57 o 4 -8 1 0.88 -0.96 1.14 o -5 -7 1 209.56 250.80 14.79 o -4 -7 1 2.77 3.12 0.47 o -3 -7 1 12.50 12.11 0.53 o -2 -7 1 32.30 40.11 1.14 o -1 -7 1 10.15 10.63 0.45 o 0 -7 1 144.97 145.47 3.38 o 1 -7 1 380.16 402.27 11.07 o 2 -7 1 24.54 24.63 1.24 o 3 -7 1 34.64 32.73 1.38 o 4 -7 1 0.72 2.37 0.96 o -5 -6 1 58.88 62.26 3.36 o -4 -6 1 27.09 27.40 1.14 o -3 -6 1 16.35 15.59 1.12 o -2 -6 1 292.17 299.44 7.23 o -1 -6 1 114.87 127.90 4.13 o 0 -6 1 183.86 187.73 3.54 o 1 -6 1 5.39 4.99 0.38 o 2 -6 1 57.76 61.14 2.17 o 3 -6 1 74.75 83.30 3.44 o 4 -6 1 13.65 14.44 1.46 o 5 -6 1 23.08 28.77 2.49 o -6 -5 1 25.28 27.08 2.33 o -5 -5 1 1.16 0.78 0.71 o -4 -5 1 10.04 8.69 0.37 o -3 -5 1 377.03 380.85 9.47 o -2 -5 1 65.53 67.05 2.29 o -1 -5 1 0.19 1.03 0.24 o 0 -5 1 57.05 52.59 1.05 o 1 -5 1 61.92 69.57 1.90 o 2 -5 1 298.61 323.43 8.17 o 3 -5 1 9.94 13.90 0.75 o 4 -5 1 5.24 4.64 0.91 o 5 -5 1 40.69 44.21 3.28 o -6 -4 1 69.50 69.02 4.97 o -5 -4 1 155.21 176.16 9.76 o -4 -4 1 23.03 22.72 1.84 o -3 -4 1 440.55 454.39 9.19 o -2 -4 1 46.29 64.41 1.75 o -1 -4 1 18.55 24.08 0.57 o 0 -4 1 298.48 299.28 6.05 o 1 -4 1 36.31 44.85 1.34 o 2 -4 1 575.51 588.65 25.86 o 3 -4 1 36.73 42.61 2.38 o 4 -4 1 24.58 26.95 3.45 o 5 -4 1 45.55 47.84 5.32 o -6 -3 1 1.71 2.48 0.94 o -5 -3 1 325.76 373.48 16.32 o -4 -3 1 15.89 13.67 0.72 o -3 -3 1 54.15 57.88 4.99 o -2 -3 1 140.17 153.74 4.69 o -1 -3 1 478.92 487.34 9.32 o 0 -3 1 385.81 394.90 8.30 o 1 -3 1 239.46 243.07 6.04 o 2 -3 1 56.92 60.49 2.35 o 3 -3 1 394.13 406.07 14.40 o 4 -3 1 36.79 34.60 1.31 o 5 -3 1 60.65 61.52 4.31 o 6 -3 1 189.91 190.74 8.85 o -6 -2 1 6.63 5.81 1.32 o -5 -2 1 168.38 189.42 10.30 o -4 -2 1 38.20 33.58 2.36 o -3 -2 1 290.75 315.67 9.32 o -2 -2 1 600.59 612.97 14.77 o -1 -2 1 1066.51 1048.95 23.49 o 0 -2 1 434.00 382.35 7.97 o 1 -2 1 81.69 82.25 2.23 o 2 -2 1 251.95 225.09 6.15 o 3 -2 1 3.07 1.76 0.60 o 4 -2 1 44.09 40.89 1.42 o 5 -2 1 89.97 85.70 3.58 o 6 -2 1 22.26 19.07 1.39 o -6 -1 1 11.09 8.51 1.54 o -5 -1 1 54.47 56.79 3.14 o -4 -1 1 13.05 13.39 1.39 o -3 -1 1 68.49 61.11 2.37 o -2 -1 1 46.68 48.65 1.55 o -1 -1 1 139.67 141.87 4.52 o 0 -1 1 377.80 389.41 8.61 o 1 -1 1 3452.45 3113.57 117.78 o 2 -1 1 1220.70 1141.57 41.99 o 3 -1 1 8.13 8.40 0.41 o 4 -1 1 69.14 70.85 1.92 o 5 -1 1 122.10 120.62 6.26 o 6 -1 1 16.86 15.31 1.08 o -6 0 1 16.63 14.77 1.59 o -5 0 1 5.46 6.44 0.59 o -4 0 1 52.57 64.46 2.93 o -3 0 1 200.84 194.06 3.86 o -2 0 1 0.59 0.37 0.07 o -1 0 1 250.35 244.38 6.71 o 1 0 1 58.04 47.31 1.66 o 2 0 1 24.82 27.74 0.86 o 3 0 1 82.71 83.05 1.89 o 4 0 1 78.04 70.73 2.33 o 5 0 1 126.45 124.67 3.63 o 6 0 1 14.00 10.88 0.95 o -6 1 1 40.66 40.45 2.03 o -5 1 1 118.89 116.39 6.19 o -4 1 1 228.69 207.47 6.69 o -3 1 1 22.17 21.54 1.18 o -2 1 1 20.90 16.22 0.97 o 1 1 1 1532.86 1389.09 24.14 o 2 1 1 194.66 177.25 4.28 o 3 1 1 1275.30 1215.86 30.50 o 4 1 1 393.41 366.44 10.37 o 5 1 1 1.80 1.19 0.48 o 6 1 1 11.64 9.69 0.89 o -6 2 1 7.81 8.01 0.97 o -5 2 1 160.04 156.51 3.98 o -4 2 1 0.01 -0.31 0.31 o -3 2 1 230.05 214.87 5.97 o -2 2 1 315.08 309.84 8.39 o -1 2 1 1606.26 1457.69 36.65 o 0 2 1 3.13 5.92 0.24 o 1 2 1 499.86 466.55 8.24 o 2 2 1 184.86 190.71 3.52 o 3 2 1 279.20 273.41 6.17 o 4 2 1 112.26 117.78 5.03 o 5 2 1 40.84 39.65 2.58 o 6 2 1 28.45 25.68 2.23 o -6 3 1 75.71 91.32 5.74 o -5 3 1 0.13 0.35 0.30 o -4 3 1 4.81 4.39 0.92 o -3 3 1 76.27 70.02 2.02 o -2 3 1 17.93 17.55 0.63 o -1 3 1 191.71 168.85 4.32 o 0 3 1 307.21 313.87 6.58 o 1 3 1 223.08 223.82 4.01 o 2 3 1 1491.26 1489.87 36.06 o 3 3 1 177.08 183.49 4.28 o 4 3 1 26.79 29.69 1.57 o 5 3 1 10.29 10.02 1.12 o 6 3 1 39.60 40.59 3.16 o -5 4 1 37.05 40.08 2.34 o -4 4 1 133.47 134.57 4.40 o -3 4 1 172.32 164.02 4.60 o -2 4 1 6.04 7.06 0.31 o -1 4 1 89.39 78.19 1.82 o 0 4 1 996.59 974.81 20.51 o 1 4 1 62.38 70.65 1.43 o 2 4 1 759.40 827.09 15.82 o 3 4 1 113.93 106.65 2.50 o 4 4 1 517.35 526.07 17.19 o 5 4 1 0.50 0.41 0.67 o 6 4 1 90.65 110.62 5.94 o -5 5 1 40.88 41.68 2.86 o -4 5 1 0.26 -0.12 0.91 o -3 5 1 236.45 271.42 8.72 o -2 5 1 161.70 151.56 4.83 o -1 5 1 263.89 252.23 5.29 o 0 5 1 252.11 270.69 4.85 o 1 5 1 17.19 31.51 0.89 o 2 5 1 2.54 1.26 0.16 o 3 5 1 88.87 85.25 1.87 o 4 5 1 979.68 1007.94 22.67 o 5 5 1 61.14 60.96 5.29 o 6 5 1 14.68 12.99 1.57 o -5 6 1 3.58 5.02 1.40 o -4 6 1 0.03 -0.28 0.36 o -3 6 1 45.00 52.07 2.92 o -2 6 1 20.15 20.47 0.93 o -1 6 1 26.80 23.82 0.81 o 0 6 1 21.93 33.34 0.82 o 1 6 1 40.79 39.45 0.87 o 2 6 1 534.54 527.70 10.97 o 3 6 1 42.69 47.09 1.35 o 4 6 1 47.49 57.10 1.75 o 5 6 1 17.29 14.24 1.38 o 6 6 1 27.04 28.59 2.29 o -4 7 1 7.22 6.95 0.58 o -3 7 1 173.85 205.52 7.63 o -2 7 1 1.19 1.29 0.31 o -1 7 1 145.22 152.82 3.84 o 0 7 1 79.23 82.30 1.65 o 1 7 1 218.01 231.29 5.49 o 2 7 1 334.59 323.72 6.20 o 3 7 1 59.24 57.00 1.41 o 4 7 1 32.14 31.41 2.70 o 5 7 1 2.68 1.71 0.89 o -4 8 1 2.71 2.76 1.20 o -3 8 1 2.17 3.25 0.50 o -2 8 1 66.30 66.57 4.03 o -1 8 1 30.68 32.29 1.35 o 0 8 1 48.39 54.87 1.41 o 1 8 1 45.58 47.49 1.15 o 2 8 1 10.49 10.30 0.40 o 3 8 1 17.13 11.19 1.05 o 4 8 1 256.23 265.08 13.57 o 5 8 1 5.36 4.47 1.57 o -4 9 1 38.63 42.23 3.28 o -3 9 1 145.15 166.63 10.45 o -2 9 1 276.12 297.88 21.99 o -1 9 1 197.40 216.08 16.51 o 0 9 1 0.79 0.73 0.28 o 1 9 1 184.05 198.25 5.75 o 2 9 1 34.51 26.12 0.87 o 3 9 1 42.94 41.46 1.82 o 4 9 1 72.60 76.97 4.76 o 5 9 1 42.27 55.03 3.93 o -3 10 1 233.42 273.02 14.39 o -2 10 1 1.04 1.62 0.83 o -1 10 1 17.18 15.67 1.63 o 0 10 1 0.00 0.29 0.32 o 1 10 1 116.83 109.51 3.60 o 2 10 1 187.51 204.73 7.05 o 3 10 1 110.76 111.31 4.37 o 4 10 1 103.05 126.86 7.71 o -2 11 1 11.63 12.53 1.56 o -1 11 1 61.68 63.10 4.60 o 0 11 1 32.67 28.69 1.78 o 1 11 1 14.10 10.88 0.86 o 2 11 1 0.09 -0.78 1.15 o 3 11 1 14.62 11.72 1.44 o 4 11 1 4.11 3.04 1.22 o -1 12 1 23.22 22.50 2.06 o 0 12 1 0.02 -0.66 0.66 o 1 12 1 90.05 103.97 4.85 o 2 12 1 1.96 3.07 0.83 o -2 -11 2 5.95 5.61 0.93 o -1 -11 2 9.14 7.84 0.90 o 0 -11 2 0.01 -0.57 0.99 o 1 -11 2 0.02 -0.19 1.07 o -3 -10 2 10.07 4.71 1.73 o -2 -10 2 23.40 19.41 1.23 o -1 -10 2 26.55 27.62 1.44 o 0 -10 2 47.86 54.80 2.30 o 1 -10 2 27.06 25.98 2.55 o 2 -10 2 1.71 1.93 1.20 o -4 -9 2 4.99 4.37 1.26 o -3 -9 2 18.69 20.78 1.27 o -2 -9 2 6.47 6.46 0.76 o -1 -9 2 3.52 2.59 0.51 o 0 -9 2 13.34 10.84 0.61 o 1 -9 2 5.96 4.42 0.67 o 2 -9 2 51.04 48.13 3.55 o 3 -9 2 86.12 83.71 5.63 o -5 -8 2 2.78 1.72 1.12 o -4 -8 2 56.93 65.55 3.75 o -3 -8 2 53.12 49.75 2.33 o -2 -8 2 36.03 24.19 1.01 o -1 -8 2 1.77 1.99 0.35 o 0 -8 2 88.81 94.92 2.44 o 1 -8 2 105.80 104.81 3.97 o 2 -8 2 22.93 17.01 1.01 o 3 -8 2 18.35 15.39 0.93 o 4 -8 2 0.04 0.00 1.14 o -5 -7 2 0.08 0.22 1.04 o -4 -7 2 4.41 3.54 1.50 o -3 -7 2 184.10 167.11 6.16 o -2 -7 2 29.39 23.41 1.22 o -1 -7 2 67.81 68.43 1.71 o 0 -7 2 23.34 25.88 0.75 o 1 -7 2 47.40 56.04 1.58 o 2 -7 2 5.80 6.25 0.47 o 3 -7 2 2.96 4.57 1.33 o 4 -7 2 0.48 1.99 1.10 o -5 -6 2 116.30 143.12 8.69 o -4 -6 2 8.66 6.56 0.47 o -3 -6 2 266.27 255.55 8.34 o -2 -6 2 113.73 124.44 3.55 o -1 -6 2 133.85 142.59 3.06 o 0 -6 2 30.72 30.49 0.77 o 1 -6 2 188.75 196.98 4.81 o 2 -6 2 15.02 13.58 0.62 o 3 -6 2 142.57 165.12 6.90 o 4 -6 2 33.69 36.02 1.78 o 5 -6 2 4.25 2.91 2.25 o -5 -5 2 74.19 84.45 5.28 o -4 -5 2 10.01 9.94 0.33 o -3 -5 2 20.97 24.59 0.84 o -2 -5 2 253.01 269.71 6.97 o -1 -5 2 54.32 51.37 1.09 o 0 -5 2 241.70 224.84 4.28 o 1 -5 2 31.06 32.75 1.21 o 2 -5 2 84.22 79.31 2.83 o 3 -5 2 15.13 13.77 0.64 o 4 -5 2 79.12 87.89 3.81 o 5 -5 2 9.34 8.44 0.93 o -6 -4 2 0.52 0.95 1.14 o -5 -4 2 597.07 684.44 43.80 o -4 -4 2 54.68 51.03 1.73 o -3 -4 2 121.47 117.70 2.73 o -2 -4 2 39.12 39.78 1.22 o -1 -4 2 572.52 608.80 12.06 o 0 -4 2 245.02 248.77 4.97 o 1 -4 2 56.61 54.11 1.29 o 2 -4 2 593.98 640.09 14.54 o 3 -4 2 0.33 0.02 0.60 o 4 -4 2 16.07 14.94 1.36 o 5 -4 2 31.56 28.72 2.58 o -6 -3 2 97.79 110.54 6.07 o -5 -3 2 53.42 53.26 2.67 o -4 -3 2 13.81 14.61 2.10 o -3 -3 2 385.57 381.62 8.50 o -2 -3 2 1224.74 1370.55 30.51 o -1 -3 2 648.78 656.96 13.51 o 0 -3 2 1329.83 1370.75 29.77 o 1 -3 2 2.99 3.05 0.19 o 2 -3 2 250.17 226.52 5.82 o 3 -3 2 131.63 136.26 7.17 o 4 -3 2 190.06 205.60 7.13 o 5 -3 2 128.57 128.06 7.41 o -6 -2 2 11.98 14.32 1.38 o -5 -2 2 5.86 4.18 0.59 o -4 -2 2 22.46 22.75 2.02 o -3 -2 2 49.00 42.40 1.51 o -2 -2 2 388.65 428.82 12.67 o -1 -2 2 534.43 502.98 12.12 o 0 -2 2 1.60 2.12 0.18 o 1 -2 2 316.56 304.76 8.14 o 2 -2 2 177.43 210.83 6.01 o 3 -2 2 145.78 153.71 5.67 o 4 -2 2 246.42 257.48 8.46 o 5 -2 2 28.42 26.24 0.94 o 6 -2 2 27.09 21.16 1.38 o -6 -1 2 17.29 16.20 1.14 o -5 -1 2 167.23 197.66 11.64 o -4 -1 2 40.11 37.85 1.44 o -3 -1 2 276.83 274.32 8.34 o -2 -1 2 45.57 49.89 2.03 o -1 -1 2 1751.11 1608.14 42.11 o 0 -1 2 2512.05 2469.51 61.10 o 1 -1 2 2938.03 2793.66 76.64 o 2 -1 2 980.73 878.29 21.22 o 3 -1 2 96.04 93.34 2.53 o 4 -1 2 295.00 288.38 6.83 o 5 -1 2 47.73 47.81 1.72 o 6 -1 2 2.99 2.83 0.68 o -6 0 2 7.96 8.90 0.98 o -5 0 2 110.46 117.28 6.15 o -4 0 2 216.39 233.46 11.48 o -3 0 2 205.01 207.59 6.41 o -2 0 2 108.44 119.00 5.02 o -1 0 2 164.87 146.22 4.46 o 0 0 2 1266.84 1184.90 18.99 o 1 0 2 5.81 6.32 0.21 o 2 0 2 1099.91 1004.90 24.13 o 3 0 2 15.53 14.52 0.73 o 4 0 2 53.29 53.27 1.35 o 5 0 2 97.27 96.75 3.19 o 6 0 2 96.99 105.56 4.88 o -6 1 2 28.32 30.87 4.48 o -5 1 2 144.07 142.20 10.82 o -4 1 2 62.15 58.47 1.86 o -3 1 2 40.08 35.11 1.08 o -2 1 2 3.31 3.89 0.36 o 1 1 2 1009.79 946.11 22.12 o 2 1 2 106.79 92.09 2.50 o 3 1 2 1085.28 1012.32 30.69 o 4 1 2 25.48 25.05 0.81 o 5 1 2 0.40 0.23 0.34 o 6 1 2 67.63 68.72 2.99 o -6 2 2 4.28 6.04 0.78 o -5 2 2 63.19 60.39 2.24 o -4 2 2 119.09 117.82 3.01 o -3 2 2 134.57 135.60 3.70 o -2 2 2 401.63 445.05 11.11 o 0 2 2 398.62 370.51 6.25 o 1 2 2 73.18 71.91 1.19 o 2 2 2 1761.64 1649.31 33.34 o 3 2 2 781.05 787.21 21.59 o 4 2 2 637.76 639.19 24.23 o 5 2 2 17.00 16.37 0.75 o 6 2 2 80.01 87.86 11.54 o -6 3 2 4.17 1.34 1.79 o -5 3 2 9.59 9.65 0.54 o -4 3 2 61.69 62.57 2.74 o -3 3 2 364.14 356.09 11.26 o -2 3 2 7.33 4.26 0.21 o -1 3 2 164.64 146.74 3.62 o 0 3 2 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