#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/15/2011568.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011568_Fobs loop_ _publ_author_name 'Yao, Yingming' 'Shen, Qi' 'Yu, Kaibei' _publ_section_title ; Tris(2,6-di-tert-butyl-4-methylphenolato-O)(triphenylphosphine oxide-O)samarium(III) ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1330 _journal_page_last 1331 _journal_volume 56 _journal_year 2000 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _exptl_crystal_F_000 2284.00 _[local]_cod_data_source_file sk1411Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C:\XSCANS\Y654 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 453.28 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 7227.00 7326.78 103.23 o 4 0 0 2193.64 2262.03 98.99 o 6 0 0 30419.79 29297.07 348.97 o 8 0 0 1934.09 1729.25 169.18 o 10 0 0 4912.68 4901.85 242.12 o 12 0 0 1703.50 1366.05 240.05 o 1 1 0 22553.86 23079.46 117.48 o 2 1 0 191410.84 181361.34 460.81 o 3 1 0 132.72 145.09 76.22 o 4 1 0 608.86 416.57 81.58 o 5 1 0 10544.10 10924.76 196.87 o 6 1 0 519.58 440.62 118.35 o 7 1 0 15.10 -88.92 115.66 o 8 1 0 7049.64 7115.03 245.53 o 9 1 0 1615.97 1756.59 189.90 o 10 1 0 18.35 -18.05 151.10 o 11 1 0 1254.63 1378.06 212.63 o 12 1 0 915.75 808.36 205.27 o 1 2 0 19507.53 20283.71 119.12 o 2 2 0 420.61 453.36 58.17 o 3 2 0 30411.48 29541.50 234.35 o 4 2 0 5307.02 5319.64 131.84 o 5 2 0 62.75 120.34 85.58 o 6 2 0 319.62 400.49 107.64 o 7 2 0 4974.51 4443.70 187.97 o 8 2 0 199.13 240.02 150.43 o 9 2 0 4949.22 5150.86 244.80 o 10 2 0 1.23 -66.86 157.12 o 11 2 0 515.65 432.58 198.57 o 12 2 0 13.55 84.91 198.57 o 1 3 0 77311.80 78398.49 249.43 o 2 3 0 12611.89 12833.22 136.97 o 3 3 0 410.15 482.09 80.91 o 4 3 0 1744.61 1595.05 96.31 o 5 3 0 11191.38 11362.87 200.90 o 6 3 0 1460.28 1406.94 130.40 o 7 3 0 609.10 431.26 132.39 o 8 3 0 5110.74 5037.46 220.74 o 9 3 0 3983.39 3796.11 224.72 o 10 3 0 330.10 227.99 161.80 o 11 3 0 1416.06 1460.98 201.93 o 12 3 0 779.42 926.69 221.98 o 0 4 0 177065.77 168817.58 1746.54 o 1 4 0 1767.82 2053.61 59.55 o 2 4 0 9860.62 10286.04 132.79 o 3 4 0 643.29 587.10 80.24 o 4 4 0 4093.74 4028.41 124.45 o 5 4 0 29.05 131.04 95.61 o 6 4 0 29010.90 29435.19 352.24 o 7 4 0 486.93 551.60 129.71 o 8 4 0 617.74 714.08 157.79 o 9 4 0 35.66 67.53 159.79 o 10 4 0 3185.83 3379.81 233.39 o 11 4 0 33.97 -28.08 171.82 o 12 4 0 1925.93 1867.57 247.40 o 1 5 0 10116.86 9990.74 111.46 o 2 5 0 24012.60 23817.71 199.31 o 3 5 0 960.78 1061.92 92.28 o 4 5 0 1347.13 1283.97 96.97 o 5 5 0 15090.59 14994.81 232.49 o 6 5 0 1267.25 976.27 129.05 o 7 5 0 1199.74 1196.90 143.76 o 8 5 0 6676.44 6339.36 239.50 o 9 5 0 4023.46 3931.88 234.08 o 10 5 0 1191.43 1186.83 193.90 o 11 5 0 2403.96 2512.26 228.69 o 12 5 0 1118.16 1263.03 239.37 o 0 6 0 16770.40 16430.55 139.39 o 1 6 0 166.43 306.90 56.16 o 2 6 0 95.98 82.91 80.90 o 3 6 0 92025.67 88948.25 429.37 o 4 6 0 616.56 643.24 93.61 o 5 6 0 161.58 257.41 98.28 o 6 6 0 57.26 47.47 110.32 o 7 6 0 4876.50 4683.74 193.32 o 8 6 0 384.36 290.17 154.45 o 9 6 0 7647.43 8253.48 285.66 o 10 6 0 7.74 43.46 155.11 o 11 6 0 1223.63 1301.83 208.61 o 12 6 0 18.91 -246.04 208.60 o 1 7 0 929.72 1134.25 76.24 o 2 7 0 14305.26 14334.48 177.16 o 3 7 0 6197.55 5891.57 140.58 o 4 7 0 618.48 290.19 90.27 o 5 7 0 20370.93 21035.96 279.58 o 6 7 0 4940.78 5046.67 177.94 o 7 7 0 2402.43 2244.30 159.83 o 8 7 0 6458.72 6397.38 235.48 o 9 7 0 420.74 260.09 176.51 o 10 7 0 101.93 60.84 169.82 o 11 7 0 1957.52 2038.77 232.03 o 12 7 0 926.49 1085.16 207.27 o 0 8 0 85215.48 87195.93 359.85 o 1 8 0 24226.68 24839.79 206.04 o 2 8 0 7992.63 8722.38 153.40 o 3 8 0 16198.29 17299.74 214.62 o 4 8 0 42829.63 43376.57 358.12 o 5 8 0 3815.12 4006.16 158.53 o 6 8 0 16625.81 16225.50 284.69 o 7 8 0 853.71 942.11 140.41 o 8 8 0 2671.54 2376.03 194.60 o 9 8 0 810.96 970.84 183.87 o 10 8 0 6480.42 6361.26 280.94 o 11 8 0 1.35 -107.64 181.85 o 12 8 0 1340.22 1671.59 234.69 o 1 9 0 5865.19 6050.06 133.26 o 2 9 0 30401.00 31312.80 264.55 o 3 9 0 1206.33 1263.22 102.98 o 4 9 0 13833.04 14247.15 221.10 o 5 9 0 1310.92 1146.81 118.36 o 6 9 0 2985.74 2600.98 157.84 o 7 9 0 1005.03 1075.85 151.11 o 8 9 0 6643.93 6537.24 253.54 o 9 9 0 1392.40 1600.75 201.26 o 10 9 0 738.76 375.09 183.20 o 11 9 0 2220.06 2379.16 250.09 o 12 9 0 1145.25 1172.77 226.00 o 0 10 0 1588.90 1618.62 100.33 o 1 10 0 8550.01 8384.01 156.77 o 2 10 0 2485.11 2529.88 113.05 o 3 10 0 42816.47 43918.09 342.89 o 4 10 0 2595.54 2752.93 132.43 o 5 10 0 395.05 327.62 109.65 o 6 10 0 873.80 910.02 132.39 o 7 10 0 7383.98 7565.81 234.17 o 8 10 0 1259.53 1253.05 182.54 o 9 10 0 10297.46 10424.45 321.85 o 10 10 0 18.32 86.25 158.45 o 11 10 0 1840.59 1793.35 238.04 o 12 10 0 99.84 61.51 190.55 o 1 11 0 22399.95 23250.72 237.19 o 2 11 0 2015.49 1942.99 105.68 o 3 11 0 122.76 240.02 92.93 o 4 11 0 9300.45 9838.04 198.84 o 5 11 0 19251.86 19210.52 293.55 o 6 11 0 64.27 -3.34 134.38 o 7 11 0 1407.27 1453.02 158.47 o 8 11 0 2437.26 2460.89 197.27 o 9 11 0 4854.86 4762.12 257.50 o 10 11 0 392.31 314.91 191.89 o 11 11 0 2577.06 2671.43 252.77 o 12 11 0 661.88 701.37 232.01 o 0 12 0 33326.02 33443.18 282.14 o 1 12 0 2880.83 3011.06 127.77 o 2 12 0 16021.16 16527.58 222.63 o 3 12 0 5022.00 5073.28 148.55 o 4 12 0 3448.08 3297.01 145.15 o 5 12 0 40.84 54.15 123.02 o 6 12 0 21958.48 21232.23 339.77 o 7 12 0 1080.66 1032.39 157.13 o 8 12 0 479.53 519.51 177.18 o 9 12 0 175.69 215.95 173.83 o 10 12 0 5581.18 5714.66 275.57 o 11 12 0 53.46 -33.43 204.58 o 12 12 0 1014.86 1227.58 230.67 o 1 13 0 291.92 258.75 88.26 o 2 13 0 22491.77 21415.77 263.79 o 3 13 0 11.30 18.05 90.26 o 4 13 0 8802.94 8916.78 205.50 o 5 13 0 11133.91 11346.81 240.34 o 6 13 0 3082.28 3043.02 191.94 o 7 13 0 461.50 340.32 152.44 o 8 13 0 10266.01 9885.63 311.83 o 9 13 0 211.33 204.59 170.49 o 10 13 0 18.81 0.67 198.57 o 11 13 0 1983.29 1832.81 240.05 o 12 13 0 1828.13 1850.16 258.10 o 0 14 0 31588.50 33945.11 307.33 o 1 14 0 1116.37 920.81 98.30 o 2 14 0 60.77 -318.91 143.08 o 3 14 0 33888.63 34460.94 344.03 o 4 14 0 4706.50 4943.84 173.94 o 5 14 0 82.54 -5.35 128.37 o 6 14 0 38.52 39.45 134.38 o 7 14 0 5383.40 5499.81 222.75 o 8 14 0 21.93 -49.47 187.20 o 9 14 0 7377.97 7843.58 301.03 o 10 14 0 859.67 736.15 192.56 o 11 14 0 449.42 424.56 217.96 o 12 14 0 0.76 132.38 194.56 o 1 15 0 10278.84 10790.79 196.90 o 2 15 0 430.05 225.99 99.62 o 3 15 0 418.08 393.81 124.36 o 4 15 0 6824.69 7310.54 201.42 o 5 15 0 16177.92 15296.35 290.03 o 6 15 0 852.73 903.32 162.48 o 7 15 0 1637.18 1436.32 179.21 o 8 15 0 2750.75 2691.64 214.66 o 9 15 0 2844.69 2628.08 238.07 o 10 15 0 43.37 155.11 191.88 o 11 15 0 2613.53 2450.76 258.78 o 12 15 0 178.44 215.95 212.61 o 0 16 0 30444.87 30377.22 313.77 o 1 16 0 15861.65 17757.24 247.33 o 2 16 0 10565.71 11441.96 212.27 o 3 16 0 838.16 887.97 122.36 o 4 16 0 16627.89 16179.12 282.72 o 5 16 0 3699.52 3665.30 191.29 o 6 16 0 12948.72 12270.19 296.56 o 7 16 0 2347.63 2281.00 197.94 o 8 16 0 891.51 908.66 186.55 o 9 16 0 16.09 -49.47 179.85 o 10 16 0 4923.84 5266.21 286.25 o 11 16 0 58.66 64.85 221.97 o 12 16 0 1097.02 1081.16 257.42 o 1 17 0 685.23 910.03 112.33 o 2 17 0 7228.38 7035.95 192.75 o 3 17 0 22.04 -185.86 125.69 o 4 17 0 2987.34 2923.38 167.20 o 5 17 0 5383.34 5118.91 209.39 o 6 17 0 2134.10 2322.45 185.23 o 7 17 0 348.69 254.07 163.14 o 8 17 0 6768.20 6555.01 284.30 o 9 17 0 562.55 601.74 197.24 o 10 17 0 131.32 157.79 212.61 o 11 17 0 1154.53 1167.42 227.33 o 0 18 0 2186.65 2336.75 134.43 o 1 18 0 88.54 370.40 106.30 o 2 18 0 115.56 -17.38 119.68 o 3 18 0 22482.25 23344.19 321.82 o 4 18 0 283.19 169.82 132.38 o 5 18 0 9.52 66.86 148.42 o 6 18 0 822.93 831.11 170.50 o 7 18 0 5189.19 5381.81 250.16 o 8 18 0 537.91 518.84 186.54 o 9 18 0 4883.71 4907.80 279.57 o 10 18 0 838.75 782.28 204.60 o 11 18 0 291.72 454.64 228.66 o 1 19 0 15687.44 15980.08 263.31 o 2 19 0 64.59 69.53 105.64 o 3 19 0 32.54 -399.14 157.78 o 4 19 0 23.86 -72.87 133.05 o 5 19 0 16339.20 15804.07 329.49 o 6 19 0 2147.24 2293.01 205.96 o 7 19 0 1359.13 1142.06 202.60 o 8 19 0 2250.78 2274.90 234.04 o 9 19 0 2968.19 3011.93 256.79 o 10 19 0 15.91 17.38 211.94 o 11 19 0 2180.35 2377.12 269.47 o 0 20 0 29355.65 29305.57 354.36 o 1 20 0 6182.78 6412.75 194.04 o 2 20 0 4144.64 5004.18 183.28 o 3 20 0 1011.20 790.35 135.07 o 4 20 0 8209.74 8272.93 236.22 o 5 20 0 3858.41 3442.48 258.17 o 6 20 0 10827.59 11077.93 317.89 o 7 20 0 2970.80 3055.49 227.37 o 8 20 0 832.91 885.92 212.62 o 9 20 0 3.34 96.27 211.27 o 10 20 0 4645.70 5051.36 302.96 o 11 20 0 20.31 -30.75 282.81 o 1 21 0 2076.59 2197.50 151.81 o 2 21 0 10258.37 9977.94 245.00 o 3 21 0 235.66 135.72 131.71 o 4 21 0 4672.17 4499.71 220.07 o 5 21 0 2949.12 3061.62 217.35 o 6 21 0 1289.39 1138.72 239.38 o 7 21 0 28.49 -68.86 195.89 o 8 21 0 6302.71 5915.10 292.31 o 9 21 0 1432.29 1362.03 228.01 o 10 21 0 79.24 -26.07 276.12 o 11 21 0 656.66 728.78 217.30 o 0 22 0 189.33 125.70 115.00 o 1 22 0 1676.00 1813.54 150.46 o 2 22 0 3203.62 2992.97 178.58 o 3 22 0 12261.24 12279.97 280.51 o 4 22 0 48.00 -115.00 144.41 o 5 22 0 31.75 -65.52 175.84 o 6 22 0 309.85 300.87 191.22 o 7 22 0 4063.61 4077.66 244.78 o 8 22 0 33.44 16.05 244.03 o 9 22 0 3384.60 3573.73 290.23 o 10 22 0 605.81 793.63 213.28 o 11 22 0 815.17 879.22 271.46 o 1 23 0 18178.37 17725.63 314.21 o 2 23 0 1871.05 1809.54 162.50 o 3 23 0 628.40 497.45 171.17 o 4 23 0 478.89 366.40 147.09 o 5 23 0 6861.43 6453.16 262.25 o 6 23 0 1564.99 1407.54 211.97 o 7 23 0 1229.74 825.10 232.02 o 8 23 0 1657.01 1328.63 207.28 o 9 23 0 2741.60 2268.92 301.59 o 10 23 0 164.89 191.21 243.36 o 11 23 0 2940.02 3269.94 324.32 o 0 24 0 25768.08 24657.26 370.10 o 1 24 0 3002.76 3477.06 187.93 o 2 24 0 139.30 277.46 141.07 o 3 24 0 1634.32 1666.37 171.85 o 4 24 0 4081.50 3693.32 213.36 o 5 24 0 192.27 10.03 183.19 o 6 24 0 12910.51 12839.23 360.75 o 7 24 0 3362.59 3389.91 248.78 o 8 24 0 831.41 847.81 230.00 o 9 24 0 488.88 433.25 246.04 o 10 24 0 2270.53 2197.27 268.81 o 1 25 0 102.35 343.65 139.73 o 2 25 0 8287.31 8259.89 257.62 o 3 25 0 916.73 1089.88 166.49 o 4 25 0 3275.56 2935.27 205.32 o 5 25 0 795.72 684.67 180.53 o 6 25 0 530.84 82.91 233.34 o 7 25 0 12.06 -95.61 204.58 o 8 25 0 4819.19 4555.94 294.28 o 9 25 0 584.79 606.42 220.64 o 10 25 0 337.67 91.60 254.06 o 0 26 0 53.58 167.14 136.39 o 1 26 0 1127.41 1189.53 165.83 o 2 26 0 772.34 1009.63 172.51 o 3 26 0 5415.26 5339.32 236.13 o 4 26 0 1426.71 1491.12 197.26 o 5 26 0 568.00 472.04 189.88 o 6 26 0 201.43 82.90 181.86 o 7 26 0 5028.63 5279.76 284.25 o 8 26 0 271.90 244.03 227.32 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244.09 o 5 33 0 700.30 774.92 206.60 o 6 33 0 803.76 864.52 221.98 o 7 33 0 243.07 253.39 225.31 o 8 33 0 2843.52 3190.36 282.19 o 0 34 0 1988.83 2168.54 226.01 o 1 34 0 1509.37 1620.82 206.61 o 2 34 0 1846.71 1833.50 217.32 o 3 34 0 7214.71 7041.99 311.06 o 4 34 0 1321.94 1428.89 219.98 o 5 34 0 61.10 162.46 201.91 o 6 34 0 119.21 113.66 185.20 o 7 34 0 1874.85 1843.49 252.75 o 8 34 0 20.88 112.99 213.94 o 1 35 0 3917.65 3832.77 250.79 o 2 35 0 70.39 59.50 179.18 o 3 35 0 583.10 619.13 222.65 o 4 35 0 582.12 532.88 203.26 o 5 35 0 5869.00 5833.06 323.06 o 6 35 0 14.92 -12.03 206.59 o 7 35 0 505.18 486.74 220.64 o 8 35 0 83.07 167.14 237.35 o 0 36 0 5352.65 6030.33 286.27 o 1 36 0 182.70 121.68 187.20 o 2 36 0 262.40 591.03 202.58 o 3 36 0 2046.61 2178.55 222.00 o 4 36 0 3447.92 3530.28 271.51 o 5 36 0 0.03 281.47 214.61 o 6 36 0 2375.86 2625.91 268.81 o 7 36 0 1910.72 1915.71 264.79 o 1 37 0 83.95 108.98 180.52 o 2 37 0 6191.86 6017.90 303.67 o 3 37 0 0.39 166.48 181.18 o 4 37 0 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