#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/15/2011572.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011572_Fobs loop_ _publ_author_name 'Bolte, Michael' 'Degen, Alexander' 'Egert, Ernst' _publ_section_title ; Diels--Alder adducts of maleic anhydride and dienes: new compounds by crystallization ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1338 _journal_page_last 1342 _journal_volume 56 _journal_year 2000 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.650 _cell_angle_gamma 90.000 _cell_length_a 7.4990 _cell_length_b 7.9240 _cell_length_c 11.8730 _exptl_crystal_F_000 384.00 _reflns_d_resolution_high 0.7500 _[local]_cod_data_source_file sk1412IVasup5.hkl _[local]_cod_data_source_block IVa #BEGIN Tags that were not found in dictionaries: _shelx_title ' ad4 in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 93.65 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 -10 0 193.39 196.80 8.24 o 1 -10 0 310.20 308.78 8.34 o 2 -10 0 36.59 42.58 5.19 o 3 -10 0 105.72 113.59 9.55 o 1 -9 0 255.79 257.81 7.37 o 2 -9 0 444.81 469.45 10.73 o 3 -9 0 170.12 175.36 15.32 o 4 -9 0 43.23 40.49 5.75 o 5 -9 0 149.30 140.54 5.91 o 0 -8 0 118.37 123.49 5.92 o 1 -8 0 735.61 757.50 11.14 o 2 -8 0 219.75 216.23 5.29 o 3 -8 0 60.04 66.09 4.72 o 4 -8 0 392.90 398.53 7.61 o 5 -8 0 71.52 69.61 4.59 o 6 -8 0 80.73 86.14 5.90 o 1 -7 0 259.85 255.52 5.36 o 2 -7 0 427.85 427.13 6.46 o 3 -7 0 53.96 51.48 3.97 o 4 -7 0 219.15 222.40 5.46 o 5 -7 0 121.22 118.74 4.12 o 6 -7 0 674.40 675.30 10.76 o 7 -7 0 3.30 3.32 7.92 o 0 -6 0 871.76 846.79 16.47 o 1 -6 0 628.32 646.80 7.69 o 2 -6 0 204.91 192.49 4.16 o 3 -6 0 364.96 363.15 5.81 o 4 -6 0 103.69 99.84 3.50 o 5 -6 0 433.88 444.43 6.95 o 6 -6 0 32.96 29.94 3.34 o 7 -6 0 13.78 15.13 5.21 o 8 -6 0 138.14 131.33 5.92 o 1 -5 0 868.47 915.75 10.05 o 2 -5 0 1998.54 2003.74 20.26 o 3 -5 0 818.03 829.68 11.49 o 4 -5 0 269.15 293.36 4.67 o 5 -5 0 396.22 405.20 5.79 o 6 -5 0 93.71 104.95 3.80 o 7 -5 0 85.01 78.73 4.35 o 8 -5 0 229.48 239.74 8.27 o 0 -4 0 172.92 157.62 3.50 o 1 -4 0 342.40 386.68 4.99 o 2 -4 0 591.16 639.04 7.38 o 3 -4 0 447.23 446.67 5.26 o 4 -4 0 59.76 59.30 2.33 o 5 -4 0 658.83 651.53 7.93 o 6 -4 0 1294.27 1298.52 14.89 o 7 -4 0 271.95 269.73 4.95 o 8 -4 0 4.68 6.98 5.34 o 9 -4 0 83.81 81.62 4.77 o 1 -3 0 4557.55 4761.69 42.86 o 2 -3 0 254.19 274.81 3.22 o 3 -3 0 1356.64 1448.87 13.28 o 4 -3 0 570.42 588.19 6.18 o 5 -3 0 99.52 101.06 2.36 o 6 -3 0 105.27 112.25 2.63 o 7 -3 0 55.48 53.89 3.09 o 8 -3 0 16.42 8.11 3.27 o 9 -3 0 215.88 221.51 7.12 o 0 -2 0 537.46 567.17 7.87 o 1 -2 0 624.50 619.20 5.75 o 2 -2 0 1065.33 1080.09 10.80 o 3 -2 0 223.34 247.18 2.90 o 4 -2 0 1152.75 1221.62 10.15 o 5 -2 0 122.32 136.86 2.53 o 6 -2 0 107.87 107.94 3.11 o 7 -2 0 820.34 823.32 14.35 o 8 -2 0 47.95 48.35 3.32 o 9 -2 0 69.05 91.69 10.08 o 1 -1 0 352.43 370.16 3.21 o 2 -1 0 732.36 736.94 6.35 o 3 -1 0 2506.44 2588.56 20.14 o 4 -1 0 1105.96 1068.27 8.97 o 5 -1 0 394.92 405.38 4.43 o 6 -1 0 180.47 181.72 4.10 o 7 -1 0 1204.58 1233.41 12.73 o 8 -1 0 409.93 391.64 5.73 o 9 -1 0 178.97 181.49 5.30 o 1 0 0 19.31 27.14 0.87 o 2 0 0 49.10 64.93 1.43 o 3 0 0 7158.19 7581.91 66.64 o 4 0 0 485.36 490.72 5.35 o 5 0 0 187.31 190.28 2.98 o 6 0 0 98.22 93.16 3.09 o 7 0 0 22.08 19.47 2.45 o 8 0 0 27.66 34.73 3.09 o 9 0 0 0.38 0.01 3.31 o 1 1 0 357.73 366.28 3.95 o 2 1 0 723.67 734.88 7.13 o 3 1 0 2482.25 2545.92 21.09 o 4 1 0 1135.08 1096.72 9.61 o 5 1 0 393.09 403.78 4.64 o 6 1 0 183.99 194.37 5.11 o 7 1 0 1210.00 1231.34 13.91 o 8 1 0 408.09 400.81 6.31 o 9 1 0 174.68 173.57 5.42 o 0 2 0 499.27 521.20 6.14 o 1 2 0 609.16 619.03 8.42 o 2 2 0 1080.46 1084.38 12.12 o 3 2 0 228.86 245.85 3.93 o 4 2 0 1148.06 1214.01 12.33 o 5 2 0 120.30 130.85 2.84 o 6 2 0 110.32 107.77 2.66 o 7 2 0 825.08 814.03 9.93 o 8 2 0 49.27 50.60 4.12 o 9 2 0 70.01 72.17 4.04 o 1 3 0 4550.31 4811.92 40.33 o 2 3 0 260.66 279.61 3.23 o 3 3 0 1325.39 1388.47 11.16 o 4 3 0 586.94 600.62 6.23 o 5 3 0 96.53 98.61 2.52 o 6 3 0 93.37 95.39 2.94 o 7 3 0 53.00 46.27 2.83 o 8 3 0 17.33 16.21 3.16 o 9 3 0 216.74 213.11 7.31 o 0 4 0 173.26 162.27 3.55 o 1 4 0 333.03 387.00 4.29 o 2 4 0 556.02 594.43 5.39 o 3 4 0 449.67 456.09 4.72 o 4 4 0 62.46 62.67 2.01 o 5 4 0 636.66 629.66 7.09 o 6 4 0 1294.74 1288.57 13.56 o 7 4 0 276.19 281.28 5.61 o 8 4 0 3.72 3.95 3.35 o 9 4 0 83.31 82.18 5.57 o 1 5 0 856.01 906.88 8.53 o 2 5 0 1984.86 2035.04 17.65 o 3 5 0 830.67 854.11 8.84 o 4 5 0 263.84 280.46 4.14 o 5 5 0 405.19 402.40 5.79 o 6 5 0 97.51 96.24 3.58 o 7 5 0 85.41 82.68 3.73 o 8 5 0 225.12 221.39 5.81 o 0 6 0 894.09 870.94 13.65 o 1 6 0 622.69 641.60 7.00 o 2 6 0 204.32 203.17 3.47 o 3 6 0 370.94 366.25 4.84 o 4 6 0 99.13 94.25 3.26 o 5 6 0 450.33 457.90 7.09 o 6 6 0 33.95 36.02 3.52 o 7 6 0 14.48 13.45 3.60 o 8 6 0 135.44 126.85 4.84 o 1 7 0 255.66 254.41 4.40 o 2 7 0 426.72 424.30 5.90 o 3 7 0 52.07 57.31 3.42 o 4 7 0 222.84 230.13 7.96 o 5 7 0 118.85 121.04 4.26 o 6 7 0 672.89 669.40 8.70 o 7 7 0 3.23 5.37 6.07 o 0 8 0 124.46 120.74 5.07 o 1 8 0 741.78 721.30 8.68 o 2 8 0 225.22 226.38 4.51 o 3 8 0 62.20 66.88 3.69 o 4 8 0 395.79 379.93 6.60 o 5 8 0 68.19 72.79 4.30 o 6 8 0 81.04 74.31 4.56 o 1 9 0 253.92 248.08 4.91 o 2 9 0 443.24 447.59 7.32 o 3 9 0 171.91 167.98 4.97 o 4 9 0 41.23 49.24 4.15 o 5 9 0 150.50 154.68 5.37 o 0 10 0 199.01 194.89 6.88 o 1 10 0 310.37 311.41 6.41 o 2 10 0 36.72 31.79 3.94 o 3 10 0 108.00 112.32 5.57 o -3 -10 1 211.16 209.62 7.54 o -2 -10 1 195.88 191.08 7.12 o -1 -10 1 130.02 128.67 12.21 o 0 -10 1 115.56 117.59 5.28 o 1 -10 1 357.61 374.35 10.20 o 2 -10 1 151.37 149.04 8.15 o -5 -9 1 45.87 42.81 4.67 o -4 -9 1 31.44 27.44 6.09 o -3 -9 1 1.11 -4.04 4.04 o -2 -9 1 51.80 42.62 4.75 o -1 -9 1 44.64 38.46 3.88 o 0 -9 1 27.13 19.06 4.91 o 1 -9 1 317.05 328.41 6.98 o 2 -9 1 86.00 84.81 5.38 o 3 -9 1 23.42 32.77 4.12 o 4 -9 1 366.18 384.31 10.42 o -6 -8 1 198.35 213.52 8.39 o -5 -8 1 122.58 125.71 5.06 o -4 -8 1 216.83 234.68 5.96 o -3 -8 1 143.30 161.36 8.32 o -2 -8 1 128.75 135.29 4.58 o -1 -8 1 30.08 30.88 3.44 o 0 -8 1 65.89 61.80 4.41 o 1 -8 1 97.46 92.37 6.55 o 2 -8 1 303.35 309.81 6.41 o 3 -8 1 87.04 84.83 4.22 o 4 -8 1 18.37 19.92 3.71 o 5 -8 1 200.66 201.93 5.88 o 6 -8 1 64.29 58.61 10.12 o -7 -7 1 160.03 167.63 6.78 o -6 -7 1 285.63 283.97 8.23 o -5 -7 1 65.46 62.64 3.66 o -4 -7 1 63.16 64.65 3.49 o -3 -7 1 397.43 398.05 7.94 o -2 -7 1 167.18 170.41 4.50 o -1 -7 1 63.00 69.82 3.45 o 0 -7 1 1094.66 1077.16 14.48 o 1 -7 1 521.57 541.86 7.52 o 2 -7 1 84.26 91.13 3.33 o 3 -7 1 1469.20 1473.32 17.32 o 4 -7 1 14.79 16.54 4.10 o 5 -7 1 66.67 70.38 3.86 o 6 -7 1 352.80 350.64 8.99 o 7 -7 1 99.17 84.08 5.83 o -8 -6 1 116.33 116.53 5.06 o -7 -6 1 83.55 85.05 4.52 o -6 -6 1 191.23 203.38 4.90 o -5 -6 1 619.78 628.55 8.76 o -4 -6 1 335.26 339.02 5.72 o -3 -6 1 61.18 63.48 2.70 o -2 -6 1 860.85 887.96 9.97 o -1 -6 1 310.39 308.45 5.07 o 0 -6 1 727.39 743.38 9.78 o 1 -6 1 555.69 557.61 6.87 o 2 -6 1 6.21 4.73 2.07 o 3 -6 1 758.19 761.00 9.86 o 4 -6 1 119.91 122.48 3.41 o 5 -6 1 501.50 520.69 7.08 o 6 -6 1 198.23 191.61 5.25 o 7 -6 1 294.77 303.61 6.84 o -8 -5 1 201.95 211.91 5.50 o -7 -5 1 100.46 108.92 4.59 o -6 -5 1 54.88 51.25 3.00 o -5 -5 1 109.00 112.24 3.67 o -4 -5 1 997.38 1006.73 11.35 o -3 -5 1 326.01 328.38 4.09 o -2 -5 1 1632.75 1628.15 15.60 o -1 -5 1 1580.43 1594.36 16.63 o 0 -5 1 1560.51 1606.88 13.58 o 1 -5 1 577.87 590.12 7.02 o 2 -5 1 65.21 65.16 3.68 o 3 -5 1 24.22 25.43 2.15 o 4 -5 1 815.84 794.62 9.30 o 5 -5 1 96.52 99.10 2.95 o 6 -5 1 62.28 55.20 3.13 o 7 -5 1 527.13 514.75 8.08 o 8 -5 1 12.13 3.25 3.59 o -9 -4 1 83.31 75.91 4.66 o -8 -4 1 18.42 23.68 3.51 o -7 -4 1 279.68 279.61 5.04 o -6 -4 1 144.88 143.49 3.15 o -5 -4 1 16.20 15.19 2.02 o -4 -4 1 208.83 227.36 3.43 o -3 -4 1 181.62 186.65 2.89 o -2 -4 1 494.49 531.19 5.58 o -1 -4 1 702.68 767.85 7.92 o 0 -4 1 919.05 973.44 8.58 o 1 -4 1 93.85 106.65 2.50 o 2 -4 1 3168.94 3171.14 31.10 o 3 -4 1 818.77 853.56 9.63 o 4 -4 1 834.03 815.03 9.35 o 5 -4 1 515.74 502.04 6.09 o 6 -4 1 320.51 326.80 7.66 o 7 -4 1 253.51 258.29 4.93 o 8 -4 1 282.62 281.45 6.05 o -9 -3 1 196.58 190.10 7.10 o -8 -3 1 317.59 319.23 5.69 o -7 -3 1 362.84 368.87 10.10 o -6 -3 1 796.33 811.51 7.39 o -5 -3 1 1115.28 1128.81 9.61 o -4 -3 1 1602.88 1651.01 13.36 o -3 -3 1 4337.86 4433.48 33.88 o -2 -3 1 284.45 340.93 3.94 o -1 -3 1 996.45 994.73 9.47 o 0 -3 1 4894.38 5054.74 40.37 o 1 -3 1 364.04 383.91 4.87 o 2 -3 1 843.39 921.25 9.23 o 3 -3 1 660.60 678.61 7.87 o 4 -3 1 310.99 297.42 4.08 o 5 -3 1 320.46 324.39 4.57 o 6 -3 1 72.06 61.78 2.89 o 7 -3 1 63.31 69.60 4.24 o 8 -3 1 43.02 41.34 3.77 o 9 -3 1 38.33 32.08 4.11 o -9 -2 1 0.40 2.14 3.46 o -8 -2 1 274.46 280.14 4.79 o -7 -2 1 702.65 702.50 7.97 o -6 -2 1 201.95 209.80 3.06 o -5 -2 1 1217.65 1257.14 10.50 o -4 -2 1 128.53 140.63 2.25 o -3 -2 1 1466.88 1521.23 12.27 o -2 -2 1 3216.97 3372.82 24.56 o -1 -2 1 3360.48 3439.92 29.40 o 0 -2 1 552.01 562.77 5.57 o 1 -2 1 7509.83 7363.87 63.54 o 2 -2 1 1181.17 1236.75 11.92 o 3 -2 1 952.93 1044.79 10.33 o 4 -2 1 1341.91 1345.29 12.29 o 5 -2 1 850.14 809.16 7.54 o 6 -2 1 351.29 341.62 4.78 o 7 -2 1 55.12 52.82 4.62 o 8 -2 1 32.00 31.50 3.56 o 9 -2 1 28.29 27.54 6.94 o -9 -1 1 6.19 6.86 3.22 o -8 -1 1 124.39 128.40 4.07 o -7 -1 1 168.45 158.64 3.73 o -6 -1 1 319.25 310.34 5.72 o -5 -1 1 604.18 595.63 5.27 o -4 -1 1 66.04 59.91 1.57 o -3 -1 1 581.12 621.44 5.27 o -2 -1 1 960.56 960.49 7.81 o -1 -1 1 9.97 14.31 1.05 o 0 -1 1 5552.85 5561.78 43.66 o 1 -1 1 1055.41 1021.28 8.39 o 2 -1 1 6160.70 6175.70 48.69 o 3 -1 1 1004.59 1006.95 8.42 o 4 -1 1 4345.74 4424.55 33.71 o 5 -1 1 1311.70 1318.89 10.91 o 6 -1 1 54.81 58.25 2.50 o 7 -1 1 585.09 587.54 7.67 o 8 -1 1 78.35 74.77 3.53 o 9 -1 1 97.15 93.12 5.22 o -9 0 1 615.01 600.78 8.46 o -8 0 1 46.59 46.42 4.10 o -7 0 1 33.12 37.72 2.54 o -6 0 1 2176.40 2159.12 18.14 o -5 0 1 710.13 717.79 6.81 o -4 0 1 2166.49 2117.19 17.59 o -3 0 1 125.91 122.84 5.56 o -2 0 1 21.10 25.52 1.30 o -1 0 1 3895.18 3735.75 26.42 o 0 0 1 95.07 80.55 4.12 o 1 0 1 4223.13 4130.49 39.74 o 2 0 1 5275.56 5110.92 38.58 o 3 0 1 1.13 5.76 1.86 o 4 0 1 26.73 44.90 1.68 o 5 0 1 457.44 450.27 4.77 o 6 0 1 68.30 66.47 2.58 o 7 0 1 69.49 72.95 3.08 o 8 0 1 584.07 560.61 8.54 o 9 0 1 538.74 547.79 9.54 o -9 1 1 6.71 3.37 3.14 o -8 1 1 124.94 127.36 3.98 o -7 1 1 157.45 157.78 3.83 o -6 1 1 322.28 320.24 4.26 o -5 1 1 615.33 609.01 6.50 o -4 1 1 65.92 57.33 1.86 o -3 1 1 581.12 626.84 7.86 o -2 1 1 965.22 964.21 11.21 o -1 1 1 11.82 16.71 1.00 o 0 1 1 5471.03 5394.83 42.35 o 1 1 1 1050.60 1022.95 8.71 o 2 1 1 6131.42 6069.79 48.04 o 3 1 1 985.08 993.91 9.26 o 4 1 1 4386.84 4411.98 35.35 o 5 1 1 1341.70 1348.85 11.68 o 6 1 1 52.17 52.42 2.44 o 7 1 1 589.59 592.49 7.67 o 8 1 1 75.40 76.85 3.92 o 9 1 1 100.15 101.02 5.34 o -9 2 1 0.30 -2.05 3.83 o -8 2 1 270.18 268.69 5.18 o -7 2 1 705.01 694.69 8.07 o -6 2 1 198.10 198.59 3.68 o -5 2 1 1192.88 1226.25 11.56 o -4 2 1 138.15 147.49 2.75 o -3 2 1 1445.72 1497.02 15.29 o -2 2 1 3294.08 3425.93 30.93 o -1 2 1 3381.72 3446.51 27.30 o 0 2 1 575.32 591.71 6.59 o 1 2 1 7480.21 7457.62 58.79 o 2 2 1 1162.83 1212.03 10.85 o 3 2 1 961.14 1063.50 9.23 o 4 2 1 1335.49 1351.96 12.36 o 5 2 1 852.58 818.11 8.13 o 6 2 1 351.08 342.72 5.18 o 7 2 1 52.85 59.17 3.13 o 8 2 1 29.88 34.95 3.58 o 9 2 1 29.52 27.02 5.10 o -9 3 1 191.06 194.22 5.10 o -8 3 1 319.54 320.08 5.25 o -7 3 1 353.35 356.44 4.89 o -6 3 1 804.45 799.70 8.88 o -5 3 1 1136.42 1137.50 10.80 o -4 3 1 1612.93 1652.42 13.34 o -3 3 1 4320.35 4373.78 36.89 o -2 3 1 304.97 360.99 3.83 o -1 3 1 1040.16 1047.50 8.99 o 0 3 1 4945.61 5144.29 45.63 o 1 3 1 373.01 396.41 4.60 o 2 3 1 855.31 944.19 8.27 o 3 3 1 664.52 705.38 6.72 o 4 3 1 302.63 289.91 4.05 o 5 3 1 317.79 319.56 4.45 o 6 3 1 71.24 60.78 2.66 o 7 3 1 67.80 68.81 3.29 o 8 3 1 45.23 45.25 3.50 o 9 3 1 37.20 36.80 5.08 o -9 4 1 85.13 84.86 4.46 o -8 4 1 16.83 18.81 3.33 o -7 4 1 280.21 292.58 4.53 o -6 4 1 147.29 146.64 3.28 o -5 4 1 16.00 19.77 2.24 o -4 4 1 210.05 232.51 3.17 o -3 4 1 180.99 181.15 2.82 o -2 4 1 480.82 520.30 5.38 o -1 4 1 706.11 798.93 8.10 o 0 4 1 917.43 1015.89 9.30 o 1 4 1 93.87 103.79 2.28 o 2 4 1 3163.00 3176.39 25.70 o 3 4 1 800.73 820.93 7.46 o 4 4 1 820.68 805.03 7.99 o 5 4 1 521.06 508.63 7.01 o 6 4 1 320.34 313.51 5.14 o 7 4 1 253.04 267.89 5.64 o 8 4 1 282.65 259.73 5.91 o -8 5 1 193.78 195.68 5.00 o -7 5 1 98.25 107.31 4.82 o -6 5 1 55.92 55.25 3.07 o -5 5 1 103.95 114.01 3.31 o -4 5 1 987.02 992.02 9.42 o -3 5 1 320.18 322.30 3.57 o -2 5 1 1624.51 1643.95 14.48 o -1 5 1 1605.20 1613.69 15.17 o 0 5 1 1548.50 1615.69 15.17 o 1 5 1 597.15 626.14 6.30 o 2 5 1 61.45 64.11 2.25 o 3 5 1 22.16 23.96 2.44 o 4 5 1 825.84 798.71 8.52 o 5 5 1 96.96 96.06 3.25 o 6 5 1 56.77 52.64 3.18 o 7 5 1 526.37 516.73 7.76 o 8 5 1 10.95 4.34 3.70 o -8 6 1 123.29 125.16 4.67 o -7 6 1 81.43 84.95 3.94 o -6 6 1 193.50 197.46 4.48 o -5 6 1 620.47 627.42 7.93 o -4 6 1 333.04 347.36 5.26 o -3 6 1 63.35 71.42 3.57 o -2 6 1 861.09 862.38 8.91 o -1 6 1 301.29 300.20 4.17 o 0 6 1 736.19 757.58 7.97 o 1 6 1 556.15 558.63 8.67 o 2 6 1 7.21 7.12 2.01 o 3 6 1 752.74 763.51 8.87 o 4 6 1 111.49 115.71 4.38 o 5 6 1 507.31 505.72 7.59 o 6 6 1 193.68 179.12 4.85 o 7 6 1 294.64 298.77 6.31 o -7 7 1 160.07 163.59 5.78 o -6 7 1 286.19 295.57 5.47 o -5 7 1 68.77 70.96 3.40 o -4 7 1 62.46 63.73 3.98 o -3 7 1 395.89 392.14 6.93 o -2 7 1 170.50 175.45 3.77 o -1 7 1 61.18 75.93 3.57 o 0 7 1 1091.99 1081.43 11.75 o 1 7 1 515.70 536.24 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