#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/15/2011580.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011580_Fobs loop_ _publ_author_name 'Batten, Stuart R.' 'Harris, Alexander R.' 'Murray, Keith S.' _publ_section_title ; Phase change in tetraphenylphosphonium perchlorate ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1394 _journal_page_last 1395 _journal_volume 56 _journal_year 2000 _space_group_IT_number 82 _symmetry_space_group_name_Hall 'I -4' _symmetry_space_group_name_H-M 'I -4' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 17.0481 _cell_length_b 17.0481 _cell_length_c 13.7568 _exptl_crystal_F_000 1824.00 _reflns_d_resolution_high 0.7001 _[local]_cod_data_source_file ta1294Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Ph4PClO4 in I-4' _shelx_refln_list_code 4 _shelx_f_calc_maximum 275.37 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' 'y, -x, -z' '-y, x, -z' 'x+1/2, y+1/2, z+1/2' '-x+1/2, -y+1/2, z+1/2' 'y+1/2, -x+1/2, -z+1/2' '-y+1/2, x+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 2.25 0.94 0.70 o 2 2 0 53779.93 26594.06 1882.39 o -1 3 0 0.00 17.52 5.16 o 1 3 0 8.81 11.57 3.17 o 3 3 0 5.71 24.74 3.69 o 0 4 0 41270.64 41202.41 1284.93 o 2 4 0 2854.10 2922.44 59.97 o 4 4 0 25263.77 23504.71 435.37 o -3 5 0 2.53 4.77 3.41 o -1 5 0 1.58 7.20 4.47 o 1 5 0 0.31 2.92 4.27 o 3 5 0 45.28 39.89 3.53 o 5 5 0 86.61 86.52 8.43 o -4 6 0 185.67 211.23 11.99 o -2 6 0 75830.57 71866.41 3605.74 o 0 6 0 5765.97 5319.73 112.04 o 2 6 0 3052.18 2842.75 60.54 o 4 6 0 36.84 70.75 4.43 o 6 6 0 50.13 18.27 5.48 o -5 7 0 154.45 180.85 7.02 o -3 7 0 9.64 15.21 3.88 o -1 7 0 20.75 29.80 4.46 o 1 7 0 0.04 11.24 3.77 o 3 7 0 34.07 21.25 3.99 o 5 7 0 281.59 285.49 8.61 o 7 7 0 219.89 234.57 11.88 o -6 8 0 15613.28 18547.90 357.45 o -4 8 0 1423.88 1001.28 30.78 o -2 8 0 1533.31 1889.83 37.71 o 0 8 0 2175.38 1812.48 35.10 o 2 8 0 676.39 736.94 16.68 o 4 8 0 24868.88 24953.46 457.70 o 6 8 0 6258.41 7054.61 134.60 o 8 8 0 3848.09 3590.44 70.98 o -7 9 0 201.92 203.79 8.27 o -5 9 0 53.65 47.25 5.71 o -3 9 0 19.81 14.49 4.70 o -1 9 0 1.20 5.21 5.38 o 1 9 0 30.52 49.45 5.84 o 3 9 0 63.97 41.91 4.91 o 5 9 0 28.32 7.63 4.67 o 7 9 0 341.37 324.21 13.81 o 9 9 0 160.21 199.44 10.51 o -8 10 0 36.45 13.03 9.21 o -6 10 0 10763.65 11567.91 232.26 o -4 10 0 136.94 117.60 12.49 o -2 10 0 59505.29 61545.99 2158.24 o 0 10 0 12220.27 13667.45 262.10 o 2 10 0 10734.57 10113.54 187.10 o 4 10 0 779.03 1039.75 23.01 o 6 10 0 14535.96 15113.01 308.47 o 8 10 0 4455.92 5106.56 119.85 o 10 10 0 10833.21 10206.49 343.48 o -9 11 0 116.02 131.32 10.85 o -7 11 0 83.86 97.60 11.06 o -5 11 0 38.34 36.00 6.90 o -3 11 0 6.13 11.86 6.50 o -1 11 0 157.41 170.13 10.00 o 1 11 0 2.36 5.20 5.21 o 3 11 0 84.82 102.49 7.38 o 5 11 0 334.96 332.47 12.04 o 7 11 0 2.12 -9.62 9.62 o 9 11 0 140.94 148.90 14.02 o 11 11 0 13.08 16.87 11.91 o -10 12 0 814.06 945.24 37.30 o -8 12 0 16713.66 16606.10 354.06 o -6 12 0 93.34 129.43 15.75 o -4 12 0 19125.50 20659.84 440.76 o -2 12 0 6.12 7.17 8.32 o 0 12 0 9874.65 9899.36 296.45 o 2 12 0 4051.34 3562.35 76.01 o 4 12 0 19434.29 19687.66 474.12 o 6 12 0 9670.30 9320.29 219.80 o 8 12 0 14376.84 14795.74 360.59 o 10 12 0 838.08 914.95 30.24 o 12 12 0 3792.55 4045.78 101.71 o -11 13 0 54.80 52.92 9.62 o -9 13 0 16.20 13.91 12.51 o -7 13 0 42.88 39.09 12.31 o -5 13 0 2.11 8.02 21.00 o -3 13 0 69.65 68.48 7.94 o -1 13 0 139.77 163.34 9.89 o 1 13 0 321.42 317.37 13.58 o 3 13 0 83.76 55.82 9.85 o 5 13 0 66.28 91.18 18.65 o 7 13 0 65.97 49.29 10.23 o 9 13 0 0.01 2.16 11.61 o 11 13 0 5.04 14.90 13.18 o 13 13 0 51.91 54.47 14.17 o -12 14 0 450.26 428.99 22.66 o -10 14 0 9273.75 9213.19 240.97 o -8 14 0 2805.28 2147.96 56.97 o -6 14 0 9631.97 9662.77 243.90 o -4 14 0 3365.29 3737.69 92.73 o -2 14 0 107.35 133.81 10.81 o 0 14 0 1587.04 1822.66 43.83 o 2 14 0 46384.90 46539.17 1135.12 o 4 14 0 4433.69 4517.78 185.07 o 6 14 0 9359.61 9187.05 224.74 o 8 14 0 291.61 268.32 32.37 o 10 14 0 2799.87 2802.00 78.81 o 12 14 0 293.77 320.98 19.23 o 14 14 0 5523.54 5356.46 159.96 o -13 15 0 71.61 87.70 17.41 o -11 15 0 84.58 99.04 16.79 o -9 15 0 39.64 32.18 26.74 o -7 15 0 26.60 35.23 11.91 o -5 15 0 17.47 14.07 9.95 o -3 15 0 12.75 6.22 9.59 o -1 15 0 43.01 36.17 8.86 o 1 15 0 0.03 10.30 10.91 o 3 15 0 313.57 295.08 17.91 o 5 15 0 3.09 -12.44 12.44 o 7 15 0 0.50 5.82 16.54 o 9 15 0 1.12 2.74 15.83 o 11 15 0 102.35 110.48 15.35 o 13 15 0 19.41 23.74 20.41 o 15 15 0 136.83 115.97 24.98 o -14 16 0 310.04 343.91 67.55 o -12 16 0 13942.84 14020.19 463.38 o -10 16 0 2138.53 2292.27 78.54 o -8 16 0 14750.32 14026.22 382.61 o -6 16 0 32.05 17.53 15.13 o -4 16 0 5013.25 4955.84 162.55 o -2 16 0 231.31 250.18 18.87 o 0 16 0 1992.26 1915.27 57.12 o 2 16 0 36.60 45.03 17.24 o 4 16 0 20.18 31.03 26.39 o 6 16 0 16825.31 17000.30 469.19 o 8 16 0 454.38 458.44 22.44 o 10 16 0 70.58 41.15 13.41 o 12 16 0 6787.44 6628.62 197.73 o 14 16 0 52.39 100.34 22.33 o 16 16 0 979.55 921.71 43.78 o -15 17 0 3.20 12.81 21.74 o -13 17 0 40.99 78.64 20.42 o -11 17 0 4.05 20.72 16.57 o -9 17 0 0.25 -13.72 13.72 o -7 17 0 2.18 1.34 10.13 o -5 17 0 1.00 19.64 11.41 o -3 17 0 46.26 35.51 13.83 o -1 17 0 51.22 52.60 14.33 o 1 17 0 140.99 152.75 34.13 o 3 17 0 181.53 227.67 48.20 o 5 17 0 1.35 -9.69 9.69 o 7 17 0 3.21 14.78 16.89 o 9 17 0 6.58 16.51 23.57 o 11 17 0 3.47 -3.31 16.83 o 13 17 0 186.69 156.00 23.87 o 15 17 0 4.69 -4.66 21.21 o 17 17 0 6.11 -17.22 20.54 o -16 18 0 19.42 34.48 30.26 o -14 18 0 392.89 342.65 31.02 o -12 18 0 747.50 635.44 50.67 o -10 18 0 28.75 30.77 18.42 o -8 18 0 781.25 877.79 38.54 o -6 18 0 4112.51 3798.81 135.23 o -4 18 0 315.69 377.14 41.87 o -2 18 0 6233.01 6292.24 170.42 o 0 18 0 2036.16 2092.74 64.22 o 2 18 0 5654.67 5894.80 245.59 o 4 18 0 259.26 253.20 34.83 o 6 18 0 3374.17 3703.73 110.61 o 8 18 0 53.82 47.61 14.71 o 10 18 0 500.55 527.37 30.61 o 12 18 0 136.80 195.35 27.09 o 14 18 0 1611.20 1336.92 56.31 o 16 18 0 126.26 97.09 26.95 o -15 19 0 5.75 -27.44 27.44 o -13 19 0 4.61 -18.65 18.65 o -11 19 0 32.54 27.99 18.65 o -9 19 0 5.21 7.34 15.20 o -7 19 0 6.59 7.74 14.43 o -5 19 0 4.00 -16.22 16.22 o -3 19 0 1.55 -13.18 24.28 o -1 19 0 13.26 21.70 12.17 o 1 19 0 41.81 74.10 16.40 o 3 19 0 131.77 168.92 21.47 o 5 19 0 111.97 140.56 17.44 o 7 19 0 10.21 -14.78 23.22 o 9 19 0 0.22 -15.55 15.55 o 11 19 0 65.13 96.88 36.59 o 13 19 0 99.75 121.93 31.31 o 15 19 0 121.03 110.11 26.95 o -12 20 0 56.18 49.96 38.00 o -10 20 0 12.18 32.39 21.47 o -8 20 0 2015.38 1943.84 70.28 o -6 20 0 5.62 24.52 22.04 o -4 20 0 337.48 327.58 24.54 o -2 20 0 838.99 803.51 33.95 o 0 20 0 3352.60 3500.29 103.40 o 2 20 0 157.60 156.70 20.62 o 4 20 0 10266.65 10150.57 332.31 o 6 20 0 8.08 47.63 24.63 o 8 20 0 698.45 783.00 37.35 o 10 20 0 674.52 687.25 62.63 o 12 20 0 1386.44 1370.48 65.92 o -11 21 0 60.02 63.33 42.93 o -9 21 0 8.73 3.65 22.77 o -7 21 0 15.80 31.67 20.04 o -5 21 0 0.70 0.32 16.22 o -3 21 0 0.20 -1.88 14.48 o -1 21 0 41.11 38.21 14.02 o 1 21 0 84.72 107.76 19.74 o 3 21 0 273.88 296.62 25.33 o 5 21 0 98.51 110.49 24.32 o 7 21 0 254.54 260.89 22.13 o 9 21 0 23.38 32.37 33.78 o 11 21 0 15.87 4.44 27.89 o -10 22 0 3041.82 2740.90 250.52 o -8 22 0 4.15 -31.67 38.00 o -6 22 0 85.79 64.04 26.74 o -4 22 0 1532.72 1521.90 55.63 o -2 22 0 1002.42 1076.99 46.43 o 0 22 0 1.59 18.10 20.15 o 2 22 0 2409.37 2408.54 97.81 o 4 22 0 33.78 39.30 19.09 o 6 22 0 4380.65 4448.57 148.11 o 8 22 0 265.55 264.38 27.15 o 10 22 0 1896.14 1786.80 84.03 o -7 23 0 5.88 -16.19 64.04 o -5 23 0 9.31 43.63 45.04 o -3 23 0 0.01 -17.59 41.52 o -1 23 0 111.28 128.47 21.54 o 1 23 0 281.19 274.98 28.35 o 3 23 0 32.11 75.53 56.65 o 5 23 0 139.08 158.37 28.07 o 7 23 0 225.61 261.05 37.65 o -2 24 0 235.16 167.48 38.00 o 0 24 0 4815.22 5014.54 258.96 o 2 24 0 333.15 425.03 63.33 o 4 24 0 2884.31 2886.74 125.03 o 1 0 1 41.43 -0.57 0.57 o 3 0 1 448.97 483.44 22.52 o 5 0 1 497.56 472.68 11.31 o 7 0 1 457.75 419.51 10.36 o 9 0 1 3651.73 3681.94 71.78 o 11 0 1 138.71 137.16 9.55 o 13 0 1 2307.64 2385.58 52.21 o 15 0 1 1291.83 1184.72 34.95 o 17 0 1 718.17 692.21 51.72 o 19 0 1 219.94 234.45 22.94 o 21 0 1 499.89 544.78 27.59 o 23 0 1 836.76 841.02 38.31 o -24 1 1 1280.01 1196.43 153.05 o -22 1 1 663.22 705.08 62.28 o -20 1 1 231.36 222.92 21.64 o -18 1 1 127.30 113.26 16.53 o -16 1 1 192.41 168.71 15.17 o -14 1 1 1170.50 1229.10 36.55 o -12 1 1 1025.94 944.59 24.87 o -10 1 1 3233.53 3137.45 66.70 o -8 1 1 1489.95 1399.78 28.60 o -6 1 1 722.04 685.43 13.64 o -4 1 1 477.27 479.77 10.75 o -2 1 1 53.83 0.14 1.96 o 0 1 1 41.04 -0.25 0.78 o 2 1 1 54.38 1.17 3.66 o 4 1 1 911.58 940.23 19.77 o 6 1 1 814.00 798.66 19.61 o 8 1 1 4172.10 4198.29 79.94 o 10 1 1 554.03 541.56 16.25 o 12 1 1 1913.42 1873.05 50.44 o 14 1 1 63.08 60.43 9.64 o 16 1 1 513.86 456.96 21.11 o 18 1 1 142.53 176.41 36.94 o 20 1 1 155.53 146.33 35.18 o 22 1 1 470.67 431.60 30.42 o 24 1 1 241.91 160.21 85.15 o -23 2 1 222.57 229.39 28.85 o -21 2 1 656.26 727.27 35.37 o -19 2 1 127.41 116.30 63.68 o -17 2 1 2144.60 2326.05 69.91 o -15 2 1 3131.16 3155.12 86.28 o -13 2 1 785.12 769.24 22.99 o -11 2 1 2415.07 2305.83 44.48 o -9 2 1 591.22 630.58 13.73 o -7 2 1 891.57 854.78 19.22 o -5 2 1 173.19 171.51 10.26 o -3 2 1 453.62 494.03 12.59 o -1 2 1 53.90 -0.49 2.03 o 1 2 1 53.67 0.31 2.03 o 3 2 1 92.80 102.18 5.24 o 5 2 1 144.32 138.81 5.94 o 7 2 1 3436.13 3581.48 75.03 o 9 2 1 584.52 690.52 17.68 o 11 2 1 915.35 960.39 20.92 o 13 2 1 119.31 148.21 14.33 o 15 2 1 19.75 20.47 17.59 o 17 2 1 85.93 89.41 15.39 o 19 2 1 61.44 68.52 15.87 o 21 2 1 168.20 128.88 19.70 o 23 2 1 213.98 264.60 28.74 o -24 3 1 189.12 178.49 41.87 o -22 3 1 237.39 246.65 28.86 o -20 3 1 1234.21 1183.53 48.07 o -18 3 1 2850.60 2730.38 87.01 o -16 3 1 2309.62 2392.97 71.68 o -14 3 1 4376.52 4386.40 123.07 o -12 3 1 1612.06 1550.01 37.77 o -10 3 1 931.54 858.56 18.96 o -8 3 1 992.02 976.78 23.67 o -6 3 1 18.72 22.45 4.14 o -4 3 1 63.17 65.54 4.49 o -2 3 1 91.83 107.26 4.10 o 0 3 1 445.19 464.55 13.46 o 2 3 1 449.52 504.72 12.78 o 4 3 1 181.46 173.57 5.59 o 6 3 1 3451.24 3449.64 73.09 o 8 3 1 314.54 376.96 10.54 o 10 3 1 973.55 1071.61 22.17 o 12 3 1 236.62 184.30 28.85 o 14 3 1 101.70 129.65 10.39 o 16 3 1 461.00 453.86 19.15 o 18 3 1 103.24 127.04 16.57 o 20 3 1 72.45 38.70 15.40 o 22 3 1 101.81 131.63 21.54 o 24 3 1 123.53 334.26 97.11 o -23 4 1 602.72 591.58 49.96 o -21 4 1 432.19 360.01 23.54 o -19 4 1 681.32 771.69 31.11 o -17 4 1 3146.53 3090.43 158.33 o -15 4 1 546.45 624.32 24.32 o -13 4 1 1443.78 1398.58 30.84 o -11 4 1 262.76 281.11 10.56 o -9 4 1 870.36 829.83 18.88 o -7 4 1 1756.41 1792.55 36.99 o -5 4 1 303.20 280.64 8.63 o -3 4 1 180.06 180.74 7.82 o -1 4 1 905.85 945.76 22.14 o 1 4 1 474.50 484.52 12.93 o 3 4 1 63.13 74.20 3.89 o 5 4 1 1040.33 968.61 20.33 o 7 4 1 728.34 696.22 19.91 o 9 4 1 7.71 7.89 5.48 o 11 4 1 482.57 516.92 18.48 o 13 4 1 65.56 51.46 8.96 o 15 4 1 320.35 335.58 19.35 o 17 4 1 232.91 218.28 17.83 o 19 4 1 246.99 256.39 26.39 o 21 4 1 42.45 34.78 28.15 o 23 4 1 56.82 43.63 37.30 o -22 5 1 488.97 499.62 53.13 o -20 5 1 1367.44 1432.52 55.38 o -18 5 1 244.46 266.28 26.04 o -16 5 1 1285.65 1326.48 46.02 o -14 5 1 276.26 247.33 20.64 o -12 5 1 1497.59 1471.57 120.33 o -10 5 1 1459.79 1623.48 36.47 o -8 5 1 1499.64 1560.17 47.76 o -6 5 1 1206.34 1248.09 30.65 o -4 5 1 1034.61 964.30 21.89 o -2 5 1 143.59 125.24 5.97 o 0 5 1 489.88 485.91 11.01 o 2 5 1 174.63 160.58 5.48 o 4 5 1 307.52 298.53 8.62 o 6 5 1 3101.81 3189.46 59.92 o 8 5 1 16.38 17.98 4.74 o 10 5 1 1460.96 1532.37 34.05 o 12 5 1 71.32 85.73 9.30 o 14 5 1 865.64 829.46 29.86 o 16 5 1 122.62 125.04 14.07 o 18 5 1 394.54 336.31 27.09 o 20 5 1 100.43 146.74 41.52 o 22 5 1 99.77 89.08 21.38 o -23 6 1 269.57 227.82 29.84 o -21 6 1 1469.05 1541.89 61.71 o -19 6 1 627.95 572.36 26.59 o -17 6 1 477.92 514.59 22.74 o -15 6 1 62.76 76.89 24.76 o -13 6 1 1283.43 1286.14 42.28 o -11 6 1 1387.57 1342.27 52.49 o -9 6 1 889.55 871.32 17.77 o -7 6 1 499.32 526.53 13.55 o -5 6 1 3134.64 3226.10 65.37 o -3 6 1 3429.11 3447.70 64.18 o -1 6 1 809.99 814.57 15.81 o 1 6 1 733.16 687.29 15.06 o 3 6 1 16.84 7.04 3.66 o 5 6 1 1188.47 1207.07 27.83 o 7 6 1 996.08 1080.28 22.14 o 9 6 1 1165.53 1117.64 28.39 o 11 6 1 75.02 69.60 8.15 o 13 6 1 1053.21 1113.21 29.56 o 15 6 1 325.94 293.82 17.62 o 17 6 1 896.68 881.44 34.29 o 19 6 1 324.61 327.49 65.09 o 21 6 1 223.84 251.99 23.04 o 23 6 1 108.06 138.63 35.89 o -22 7 1 755.04 801.93 53.48 o -20 7 1 37.23 46.40 16.62 o -18 7 1 44.53 41.73 17.03 o -16 7 1 825.31 893.12 33.56 o -14 7 1 443.83 429.24 53.83 o -12 7 1 2852.42 2880.75 83.98 o -10 7 1 4.46 1.56 5.65 o -8 7 1 451.06 423.02 11.55 o -6 7 1 985.03 1075.77 24.93 o -4 7 1 743.87 707.30 16.84 o -2 7 1 3416.42 3544.27 82.90 o 0 7 1 466.27 433.32 10.80 o 2 7 1 896.25 847.07 19.14 o 4 7 1 1733.32 1818.56 33.83 o 6 7 1 506.56 534.94 12.65 o 8 7 1 978.12 908.54 20.04 o 10 7 1 768.33 777.83 23.49 o 12 7 1 1993.70 1865.41 45.06 o 14 7 1 969.81 912.17 24.13 o 16 7 1 1250.20 1106.92 43.68 o 18 7 1 872.06 850.84 35.29 o 20 7 1 151.56 152.84 21.12 o 22 7 1 245.52 269.46 71.78 o -21 8 1 55.76 43.78 24.63 o -19 8 1 26.37 31.31 16.53 o -17 8 1 67.21 57.19 10.81 o -15 8 1 243.65 211.41 24.28 o -13 8 1 645.04 652.26 24.88 o -11 8 1 2225.93 1994.14 52.13 o -9 8 1 869.95 984.12 25.67 o -7 8 1 985.41 931.43 25.11 o -5 8 1 14.56 25.60 7.31 o -3 8 1 305.95 395.96 11.48 o -1 8 1 4184.07 4247.66 90.48 o 1 8 1 1474.58 1412.29 33.16 o 3 8 1 1006.80 979.07 19.74 o 5 8 1 1498.26 1529.95 28.41 o 7 8 1 448.82 438.56 11.51 o 9 8 1 879.67 812.55 19.58 o 11 8 1 2079.73 1985.50 47.92 o 13 8 1 1134.94 922.87 42.38 o 15 8 1 3441.38 3344.28 138.98 o 17 8 1 446.26 401.11 23.74 o 19 8 1 194.02 218.65 20.61 o 21 8 1 269.44 231.43 26.71 o -22 9 1 525.34 515.63 36.33 o -20 9 1 3.97 -13.40 19.15 o -18 9 1 248.15 236.85 18.05 o -16 9 1 40.06 55.60 12.88 o -14 9 1 12.63 10.91 13.43 o -12 9 1 227.72 206.79 18.30 o -10 9 1 609.31 526.86 19.95 o -8 9 1 861.00 814.16 21.06 o -6 9 1 1188.79 1155.82 25.08 o -4 9 1 6.16 5.93 4.61 o -2 9 1 572.34 711.88 14.14 o 0 9 1 3660.84 3767.50 73.28 o 2 9 1 601.32 623.41 19.80 o 4 9 1 868.12 824.96 18.26 o 6 9 1 867.56 859.11 20.11 o 8 9 1 884.75 1008.70 21.98 o 10 9 1 875.64 739.95 21.68 o 12 9 1 775.90 740.94 39.13 o 14 9 1 2446.63 2354.32 68.81 o 16 9 1 16.72 -7.04 23.22 o 18 9 1 439.67 457.22 25.59 o 20 9 1 597.99 564.71 37.30 o 22 9 1 1075.31 1192.77 90.07 o -21 10 1 194.11 165.92 22.47 o -19 10 1 139.86 143.80 16.56 o -17 10 1 361.99 347.38 26.39 o -15 10 1 411.98 437.34 23.63 o -13 10 1 512.24 547.12 22.10 o -11 10 1 162.29 213.53 22.87 o -9 10 1 878.84 714.04 21.59 o -7 10 1 752.76 783.67 20.03 o -5 10 1 1490.23 1575.42 53.22 o -3 10 1 968.88 1027.85 22.42 o -1 10 1 542.65 559.77 13.92 o 1 10 1 3260.74 3113.88 63.79 o 3 10 1 911.72 841.18 22.04 o 5 10 1 1461.33 1585.99 34.02 o 7 10 1 4.85 -5.24 5.24 o 9 10 1 592.11 533.36 19.56 o 11 10 1 404.99 370.47 15.92 o 13 10 1 481.88 446.43 68.26 o 15 10 1 688.37 773.33 31.75 o 17 10 1 353.47 419.90 69.67 o 19 10 1 223.19 322.62 40.81 o 21 10 1 2356.56 2402.52 104.22 o -20 11 1 0.69 40.07 35.54 o -18 11 1 113.21 106.12 22.52 o -16 11 1 379.28 372.65 23.88 o -14 11 1 478.86 474.16 27.80 o -12 11 1 309.67 286.47 15.48 o -10 11 1 404.29 365.95 34.48 o -8 11 1 2074.26 1956.33 45.55 o -6 11 1 70.87 73.71 9.16 o -4 11 1 485.98 520.15 16.25 o -2 11 1 917.19 945.23 22.65 o 0 11 1 146.81 146.67 8.55 o 2 11 1 2417.38 2419.30 52.64 o 4 11 1 260.18 279.60 10.39 o 6 11 1 1376.54 1323.18 31.36 o 8 11 1 2241.78 2124.61 53.62 o 10 11 1 164.84 216.93 22.17 o 12 11 1 641.84 546.30 47.85 o 14 11 1 865.01 852.98 32.36 o 16 11 1 947.37 991.14 44.52 o 18 11 1 1186.29 1430.74 51.72 o 20 11 1 1309.82 1316.02 57.50 o -21 12 1 311.88 287.46 31.52 o -19 12 1 635.82 614.38 38.54 o -17 12 1 373.14 384.14 26.95 o -15 12 1 520.51 495.85 26.53 o -13 12 1 95.32 133.34 16.19 o -11 12 1 655.04 571.64 45.74 o -9 12 1 763.64 748.07 29.03 o -7 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