#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:28:50 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180785 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/16/2011611.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011611_Fobs loop_ _publ_author_name 'Sun, Ming' 'Macculloch, Alasdair C.' 'Hamor, Thomas A.' 'Walker, Richard T.' _publ_section_title ; 5-Methyl-2'-deoxy-4'-thio-\a-uridine (R)-S-oxide ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1492 _journal_page_last 1493 _journal_volume 56 _journal_year 2000 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _exptl_crystal_F_000 576.00 _cod_data_source_file gs1102Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' als31rnn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 48.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 578.36 374.50 1.94 o 4 0 0 432.91 445.84 12.83 o 6 0 0 387.19 404.44 3.73 o 8 0 0 13.24 16.69 0.92 o 2 1 0 37.53 49.20 0.68 o 4 1 0 870.37 922.29 17.89 o 5 1 0 846.46 811.56 12.15 o 6 1 0 0.99 2.66 0.44 o 7 1 0 3.69 4.18 0.27 o 8 1 0 255.52 249.62 3.75 o 9 1 0 11.59 31.24 20.63 o 2 2 0 732.10 611.80 10.23 o 4 2 0 1450.47 1388.05 10.31 o 5 2 0 223.91 236.75 1.25 o 6 2 0 59.42 57.92 1.08 o 7 2 0 1.12 1.89 0.38 o 8 2 0 58.81 55.52 1.68 o 9 2 0 53.74 47.15 1.23 o 2 3 0 542.13 458.38 5.44 o 3 3 0 252.64 209.16 1.44 o 4 3 0 194.56 173.94 3.50 o 5 3 0 381.39 436.09 7.87 o 6 3 0 17.21 21.79 1.44 o 7 3 0 280.49 276.57 2.42 o 8 3 0 13.89 8.69 0.67 o 2 4 0 221.48 224.80 3.10 o 3 4 0 590.99 553.75 2.33 o 4 4 0 1477.99 1516.96 6.97 o 5 4 0 147.29 161.48 1.21 o 6 4 0 45.62 53.61 1.07 o 7 4 0 33.54 34.07 0.98 o 8 4 0 26.52 28.68 1.21 o 9 4 0 2.14 1.97 0.68 o 5 5 0 298.46 314.19 3.08 o 6 5 0 2.46 1.76 0.76 o 7 5 0 23.82 27.78 0.76 o 8 5 0 284.61 275.87 5.84 o 9 5 0 19.67 19.19 2.61 o 2 6 0 397.14 341.29 2.90 o 3 6 0 152.21 165.40 1.01 o 4 6 0 413.70 494.11 2.41 o 5 6 0 353.66 363.72 4.83 o 6 6 0 5.57 11.35 0.41 o 7 6 0 379.77 331.67 4.95 o 8 6 0 22.50 17.63 1.02 o 9 6 0 150.84 136.15 5.60 o 2 7 0 641.36 627.02 6.56 o 3 7 0 536.80 545.59 5.38 o 4 7 0 24.96 24.06 0.45 o 5 7 0 5.37 6.56 0.49 o 6 7 0 77.15 87.11 0.88 o 7 7 0 1.11 0.63 0.31 o 8 7 0 107.74 116.62 1.73 o 9 7 0 30.80 26.72 2.38 o 1 8 0 173.08 201.99 1.25 o 2 8 0 1148.40 1210.08 6.87 o 3 8 0 1476.77 1608.24 8.29 o 4 8 0 49.29 43.41 0.54 o 5 8 0 340.76 333.37 1.91 o 6 8 0 43.11 39.46 0.63 o 7 8 0 20.62 24.15 0.99 o 8 8 0 5.17 4.86 0.57 o 9 8 0 1.48 0.69 0.31 o 1 9 0 792.42 792.33 10.07 o 2 9 0 71.23 60.67 0.62 o 4 9 0 326.50 348.12 4.11 o 5 9 0 23.16 21.67 0.55 o 6 9 0 341.10 364.90 4.85 o 7 9 0 5.08 6.31 0.44 o 8 9 0 21.30 24.55 1.44 o 1 10 0 3.73 3.22 0.24 o 2 10 0 1062.69 1180.54 5.79 o 3 10 0 347.42 360.32 2.35 o 4 10 0 587.99 597.68 2.44 o 5 10 0 0.20 1.40 0.28 o 6 10 0 484.64 485.83 5.03 o 7 10 0 2.84 1.58 0.38 o 8 10 0 4.91 4.15 0.62 o 1 11 0 1235.39 1210.75 10.65 o 2 11 0 1651.20 1620.62 13.37 o 3 11 0 91.61 67.15 0.66 o 4 11 0 1.38 1.42 0.39 o 5 11 0 36.70 34.83 0.71 o 6 11 0 67.29 59.99 2.64 o 7 11 0 415.21 396.80 5.16 o 8 11 0 6.70 5.80 0.44 o 0 12 0 1325.85 1353.51 16.92 o 1 12 0 113.56 114.50 0.81 o 2 12 0 1992.37 2024.33 9.49 o 3 12 0 71.26 72.00 0.71 o 4 12 0 243.00 217.68 2.14 o 5 12 0 153.41 175.56 1.32 o 6 12 0 89.09 94.47 1.01 o 7 12 0 10.18 13.95 0.66 o 8 12 0 19.51 21.78 0.92 o 1 13 0 184.57 166.22 1.31 o 2 13 0 35.43 42.20 0.60 o 3 13 0 318.85 316.35 4.31 o 4 13 0 11.11 9.27 0.30 o 5 13 0 110.43 118.43 2.71 o 6 13 0 96.88 87.52 1.01 o 7 13 0 131.24 134.93 2.23 o 8 13 0 13.35 11.33 1.33 o 0 14 0 1104.36 1064.02 19.04 o 1 14 0 248.38 220.40 1.97 o 2 14 0 301.27 302.91 1.83 o 3 14 0 1.11 3.05 0.23 o 4 14 0 83.79 81.48 0.98 o 5 14 0 87.29 83.95 1.37 o 6 14 0 2.83 0.87 0.23 o 7 14 0 29.10 32.13 0.78 o 1 15 0 21.35 30.73 2.45 o 2 15 0 1099.06 1087.93 4.82 o 3 15 0 415.73 417.63 2.22 o 4 15 0 324.79 339.28 3.32 o 5 15 0 7.22 6.34 0.32 o 6 15 0 49.35 47.52 0.95 o 7 15 0 0.81 1.19 0.33 o 0 16 0 268.43 256.55 3.89 o 1 16 0 150.44 139.26 1.42 o 2 16 0 198.45 205.19 1.59 o 3 16 0 7.16 6.31 0.29 o 4 16 0 171.55 188.86 1.39 o 5 16 0 76.16 75.27 1.32 o 6 16 0 1.50 0.82 0.16 o 7 16 0 37.86 34.93 0.90 o 1 17 0 93.75 92.16 1.03 o 2 17 0 270.23 269.34 1.92 o 3 17 0 3.02 3.67 0.54 o 4 17 0 32.62 36.43 0.83 o 5 17 0 13.24 11.70 0.44 o 6 17 0 50.69 47.37 0.99 o 0 18 0 83.69 74.55 1.16 o 1 18 0 30.62 30.88 0.66 o 2 18 0 67.15 66.67 1.01 o 3 18 0 26.44 24.49 0.78 o 4 18 0 0.55 1.37 0.20 o 5 18 0 78.09 95.58 1.33 o 6 18 0 5.40 5.90 0.46 o 1 19 0 95.06 80.88 1.26 o 2 19 0 88.83 91.18 1.88 o 3 19 0 20.65 21.46 0.68 o 4 19 0 7.30 8.96 0.35 o 5 19 0 3.04 4.60 0.66 o 0 20 0 14.77 13.72 0.55 o 1 20 0 275.14 255.62 1.74 o 2 20 0 49.19 50.24 0.81 o 3 20 0 0.00 1.35 0.36 o 4 20 0 153.82 132.61 2.48 o 5 20 0 8.69 8.40 0.36 o 1 21 0 10.23 10.47 0.41 o 2 21 0 103.64 107.02 1.34 o 3 21 0 224.38 225.30 3.14 o 4 21 0 75.03 64.57 1.58 o 0 22 0 213.73 219.03 3.42 o 1 22 0 17.58 19.23 0.57 o 2 22 0 39.24 41.78 0.79 o 3 22 0 0.88 1.13 0.30 o 1 23 0 61.67 58.18 1.01 o 2 23 0 6.03 6.65 0.48 o 1 0 1 78.74 71.09 0.50 o 2 0 1 275.86 280.71 2.74 o 4 0 1 716.01 680.61 10.97 o 5 0 1 15.10 19.37 0.50 o 6 0 1 0.47 2.57 0.21 o 7 0 1 11.65 16.07 0.81 o 8 0 1 167.61 165.45 2.08 o -9 1 1 106.38 110.45 8.50 o -8 1 1 20.15 20.88 1.04 o -7 1 1 131.11 129.56 1.30 o -6 1 1 412.69 420.79 2.96 o -5 1 1 676.77 684.37 12.89 o -4 1 1 104.70 108.94 2.20 o -3 1 1 1234.08 1346.26 15.98 o -2 1 1 784.35 783.74 1.81 o 2 1 1 788.81 780.21 9.83 o 3 1 1 1232.15 1377.06 30.71 o 4 1 1 104.82 110.07 2.31 o 5 1 1 688.81 700.20 9.84 o 6 1 1 408.37 415.85 4.77 o 7 1 1 127.53 126.56 2.23 o 8 1 1 20.42 18.66 0.97 o 9 1 1 106.44 126.38 2.95 o -9 2 1 25.62 35.33 7.46 o -8 2 1 118.73 110.79 2.39 o -7 2 1 84.84 79.92 1.75 o -6 2 1 167.71 183.56 1.58 o -5 2 1 644.29 682.75 4.64 o -4 2 1 21.51 23.59 2.96 o -3 2 1 662.33 587.15 6.83 o -2 2 1 1045.50 995.73 11.48 o 0 2 1 367.77 309.42 1.27 o 3 2 1 642.37 573.03 6.32 o 4 2 1 21.81 27.37 3.77 o 5 2 1 649.21 690.23 2.40 o 6 2 1 166.37 182.08 2.69 o 7 2 1 82.69 75.88 1.23 o 8 2 1 120.21 116.25 2.49 o 9 2 1 25.69 26.82 1.29 o -7 3 1 80.49 87.93 1.32 o -6 3 1 33.14 27.65 0.85 o -5 3 1 262.42 247.62 6.37 o -3 3 1 534.78 596.39 5.33 o -2 3 1 272.45 301.46 4.12 o 2 3 1 264.35 293.33 1.82 o 3 3 1 531.49 591.50 4.80 o 5 3 1 265.53 251.05 4.15 o 6 3 1 34.34 29.30 1.42 o 7 3 1 82.16 90.19 3.91 o 8 3 1 110.43 110.50 3.43 o -9 4 1 154.16 147.22 4.50 o -8 4 1 6.71 6.32 0.67 o -7 4 1 566.34 546.04 6.26 o -6 4 1 106.32 114.66 1.16 o -5 4 1 564.95 596.69 6.92 o -4 4 1 462.18 467.78 3.65 o -3 4 1 450.18 413.61 1.88 o -2 4 1 666.59 656.13 5.24 o 0 4 1 395.12 448.46 1.03 o 2 4 1 677.99 674.06 3.29 o 3 4 1 427.11 389.85 4.02 o 4 4 1 466.93 474.06 1.60 o 5 4 1 570.71 599.64 3.95 o 6 4 1 105.87 115.13 2.71 o 7 4 1 563.72 547.98 4.84 o 8 4 1 7.18 6.86 0.38 o 9 4 1 156.80 147.13 6.33 o -9 5 1 27.88 37.47 11.19 o -8 5 1 12.82 15.68 1.19 o -7 5 1 58.10 58.27 2.12 o -6 5 1 333.43 318.64 5.18 o -5 5 1 292.29 302.01 2.88 o -4 5 1 529.48 478.55 4.61 o -3 5 1 215.69 222.16 2.84 o -2 5 1 794.27 756.42 8.60 o 2 5 1 783.15 749.64 5.34 o 3 5 1 217.89 224.40 2.39 o 4 5 1 537.82 483.72 3.34 o 5 5 1 295.19 300.56 2.72 o 6 5 1 334.41 319.96 4.14 o 7 5 1 58.68 59.45 1.90 o 8 5 1 13.18 15.61 2.58 o 9 5 1 28.21 22.01 2.90 o -9 6 1 87.26 85.64 4.48 o -8 6 1 102.47 103.85 1.60 o -7 6 1 86.83 89.13 3.06 o -6 6 1 44.66 43.56 1.71 o -5 6 1 16.75 17.89 0.57 o -4 6 1 78.84 90.57 0.73 o -3 6 1 2242.10 2185.08 9.34 o 0 6 1 477.83 539.64 8.56 o 4 6 1 79.93 92.71 0.84 o 5 6 1 16.07 16.54 0.50 o 6 6 1 45.26 44.62 1.01 o 7 6 1 89.74 91.81 1.80 o 8 6 1 102.74 100.53 2.11 o 9 6 1 87.33 83.84 3.54 o -9 7 1 18.03 15.44 1.07 o -8 7 1 6.09 4.34 0.56 o -7 7 1 125.44 118.19 1.93 o -6 7 1 702.77 668.77 6.75 o -5 7 1 268.21 256.99 1.85 o -4 7 1 22.70 23.55 0.52 o -3 7 1 241.11 274.19 2.98 o -2 7 1 82.82 66.66 0.58 o -1 7 1 175.17 205.27 1.68 o 1 7 1 175.18 202.37 1.55 o 2 7 1 80.06 63.78 1.02 o 3 7 1 243.41 279.40 2.58 o 4 7 1 21.38 22.38 0.57 o 5 7 1 262.39 247.42 1.66 o 6 7 1 703.30 657.42 2.68 o 7 7 1 128.10 120.89 1.55 o 8 7 1 5.88 4.64 0.31 o 9 7 1 17.90 16.35 1.69 o -9 8 1 1.38 2.35 0.48 o -8 8 1 43.21 49.33 0.81 o -7 8 1 5.56 3.39 0.41 o -6 8 1 190.52 203.41 1.71 o -5 8 1 64.21 64.60 0.75 o -4 8 1 262.84 272.58 1.60 o -3 8 1 210.21 190.24 1.18 o -2 8 1 34.37 33.68 0.58 o -1 8 1 1294.03 1213.40 9.69 o 0 8 1 1417.23 1314.15 26.92 o 1 8 1 1284.16 1193.01 7.47 o 2 8 1 39.83 38.73 0.58 o 3 8 1 220.79 201.71 1.04 o 4 8 1 260.58 276.24 1.54 o 5 8 1 62.74 61.60 0.98 o 6 8 1 187.60 196.41 4.23 o 7 8 1 6.69 4.93 0.51 o 8 8 1 45.32 51.35 0.87 o -8 9 1 72.37 74.28 1.32 o -7 9 1 78.34 77.92 0.95 o -6 9 1 26.38 19.49 0.55 o -5 9 1 237.41 231.74 2.51 o -4 9 1 315.58 305.66 3.38 o -3 9 1 297.61 299.10 3.60 o -2 9 1 132.21 130.21 1.10 o 0 9 1 582.37 527.28 6.49 o 1 9 1 2368.59 2168.53 7.59 o 2 9 1 136.14 134.08 0.98 o 3 9 1 299.92 301.12 2.86 o 4 9 1 317.25 304.15 3.23 o 5 9 1 240.49 235.60 2.33 o 6 9 1 27.46 20.18 0.47 o 7 9 1 81.91 81.94 1.33 o 8 9 1 72.93 76.58 1.64 o -8 10 1 11.81 14.46 0.54 o -7 10 1 12.54 11.44 0.39 o -6 10 1 37.29 37.02 0.61 o -5 10 1 20.72 23.30 0.57 o -4 10 1 133.00 128.74 0.95 o -3 10 1 353.40 358.70 2.31 o -2 10 1 2223.23 2190.58 7.36 o -1 10 1 784.17 801.48 5.61 o 0 10 1 361.76 352.78 4.40 o 1 10 1 778.30 795.93 5.38 o 2 10 1 2257.53 2195.92 10.02 o 3 10 1 358.16 362.97 1.50 o 4 10 1 130.00 125.23 1.21 o 5 10 1 19.81 21.78 0.46 o 6 10 1 35.89 35.12 0.68 o 7 10 1 11.99 10.04 0.64 o 8 10 1 13.10 13.99 0.52 o -8 11 1 18.05 17.27 1.02 o -7 11 1 200.61 206.88 4.40 o -6 11 1 9.53 6.38 0.46 o -5 11 1 401.60 402.90 5.54 o -4 11 1 85.08 80.37 0.82 o -3 11 1 423.03 456.54 3.51 o -2 11 1 330.12 341.12 1.41 o -1 11 1 1329.70 1183.67 3.89 o 0 11 1 104.50 126.29 1.69 o 1 11 1 1320.25 1179.66 5.75 o 2 11 1 332.06 340.57 2.64 o 3 11 1 425.24 453.35 3.65 o 4 11 1 86.07 81.24 0.78 o 5 11 1 400.93 403.53 3.03 o 6 11 1 9.42 6.30 0.59 o 7 11 1 198.60 199.27 3.48 o 8 11 1 18.10 17.95 0.52 o -8 12 1 90.44 78.84 1.26 o -7 12 1 9.69 9.41 0.61 o -6 12 1 85.02 84.90 0.96 o -5 12 1 173.99 163.19 1.61 o -4 12 1 362.44 371.90 2.44 o -3 12 1 612.27 623.32 3.37 o -2 12 1 1705.58 1662.63 3.45 o -1 12 1 220.01 194.90 1.36 o 0 12 1 2.76 6.26 0.37 o 1 12 1 222.14 196.35 1.10 o 2 12 1 1677.07 1624.54 7.95 o 3 12 1 609.95 619.80 4.06 o 4 12 1 362.31 369.55 2.73 o 5 12 1 174.18 165.28 1.30 o 6 12 1 86.34 86.07 0.96 o 7 12 1 9.68 9.22 0.54 o 8 12 1 88.95 75.07 1.94 o -8 13 1 20.49 15.19 0.94 o -7 13 1 102.15 105.45 3.17 o -6 13 1 1.26 3.19 0.52 o -5 13 1 6.11 6.50 0.28 o -4 13 1 144.33 138.33 1.26 o -3 13 1 142.17 144.35 1.28 o -2 13 1 30.25 38.55 2.78 o -1 13 1 323.31 298.02 4.98 o 0 13 1 255.54 262.18 1.79 o 1 13 1 316.16 287.03 1.41 o 2 13 1 30.18 33.63 2.26 o 3 13 1 140.16 140.15 1.87 o 4 13 1 149.43 143.83 1.10 o 5 13 1 5.14 4.43 0.27 o 6 13 1 1.13 2.13 0.25 o 7 13 1 100.32 104.09 2.76 o 8 13 1 20.48 16.39 1.10 o -7 14 1 2.45 3.38 0.51 o -6 14 1 15.84 17.00 0.52 o -5 14 1 38.47 34.78 0.60 o -4 14 1 295.92 305.16 3.55 o -3 14 1 808.12 773.23 5.67 o -2 14 1 488.00 482.70 3.44 o -1 14 1 320.85 314.81 1.92 o 0 14 1 18.20 10.92 0.28 o 1 14 1 327.45 325.99 1.58 o 2 14 1 481.50 477.22 1.99 o 3 14 1 806.73 767.58 6.93 o 4 14 1 295.50 304.89 1.86 o 5 14 1 39.71 36.15 0.99 o 6 14 1 15.35 16.04 0.44 o 7 14 1 1.85 2.88 0.33 o -7 15 1 15.22 15.02 0.56 o -6 15 1 139.07 133.30 1.65 o -5 15 1 1.50 2.91 0.21 o -4 15 1 19.73 20.12 1.23 o -3 15 1 94.33 96.06 0.98 o -2 15 1 302.28 302.37 2.12 o -1 15 1 121.00 133.62 1.25 o 0 15 1 551.13 541.83 5.19 o 1 15 1 118.79 131.40 1.21 o 2 15 1 298.69 299.81 1.80 o 3 15 1 95.41 96.32 1.37 o 4 15 1 22.61 22.29 0.50 o 5 15 1 1.45 2.61 0.23 o 6 15 1 135.96 128.10 3.66 o 7 15 1 15.83 15.28 0.48 o -7 16 1 86.23 81.51 2.65 o -6 16 1 13.52 15.34 0.49 o -5 16 1 56.52 56.10 0.93 o -4 16 1 50.75 55.44 1.43 o -3 16 1 1409.70 1415.79 10.51 o -2 16 1 218.35 221.74 1.89 o -1 16 1 96.88 90.19 1.22 o 0 16 1 39.13 32.13 0.50 o 1 16 1 101.60 95.64 0.95 o 2 16 1 220.97 225.10 1.39 o 3 16 1 1399.48 1403.28 11.74 o 4 16 1 50.24 53.49 0.77 o 5 16 1 56.17 54.65 0.91 o 6 16 1 13.25 15.96 0.53 o 7 16 1 86.41 77.14 3.64 o -6 17 1 204.57 199.44 3.45 o -5 17 1 40.92 41.46 1.27 o -4 17 1 165.95 172.35 1.42 o -3 17 1 320.72 338.38 5.80 o -2 17 1 256.74 283.68 1.96 o -1 17 1 11.60 12.44 0.73 o 0 17 1 6.28 11.07 0.40 o 1 17 1 11.18 12.05 0.62 o 2 17 1 259.07 291.57 2.61 o 3 17 1 318.23 333.58 2.29 o 4 17 1 162.80 167.00 1.98 o 5 17 1 41.27 42.27 0.90 o 6 17 1 202.98 195.87 2.45 o -6 18 1 5.63 4.33 0.83 o -5 18 1 19.76 18.91 0.53 o -4 18 1 53.44 52.60 0.83 o -3 18 1 221.30 235.55 1.88 o -2 18 1 77.93 75.72 1.00 o -1 18 1 115.38 118.24 1.06 o 0 18 1 80.80 77.47 0.96 o 1 18 1 112.80 114.53 1.13 o 2 18 1 78.44 77.69 0.95 o 3 18 1 210.66 223.54 2.02 o 4 18 1 54.45 53.31 0.80 o 5 18 1 20.83 20.29 0.52 o 6 18 1 5.31 3.64 0.45 o -5 19 1 123.55 125.19 1.53 o -4 19 1 20.05 21.38 0.55 o -3 19 1 48.85 47.63 0.74 o -2 19 1 0.87 2.59 0.68 o -1 19 1 19.45 18.23 0.44 o 0 19 1 205.62 212.57 3.21 o 1 19 1 18.92 17.59 0.50 o 2 19 1 0.62 1.64 0.32 o 3 19 1 48.68 46.93 0.73 o 4 19 1 18.57 19.86 0.53 o 5 19 1 122.94 122.95 1.79 o -5 20 1 2.83 2.80 0.56 o -4 20 1 131.51 131.00 1.76 o -3 20 1 26.16 32.48 0.65 o -2 20 1 63.74 67.19 1.03 o -1 20 1 67.70 67.15 0.88 o 0 20 1 14.53 13.77 0.56 o 1 20 1 67.90 65.06 1.17 o 2 20 1 64.29 66.73 1.04 o 3 20 1 25.52 31.29 0.78 o 4 20 1 129.19 128.32 2.10 o 5 20 1 2.94 2.65 0.53 o -4 21 1 15.57 12.57 0.48 o -3 21 1 17.32 18.76 0.74 o -2 21 1 69.14 70.84 0.98 o -1 21 1 110.58 107.01 1.28 o 0 21 1 287.28 274.85 4.29 o 1 21 1 112.48 108.53 1.13 o 2 21 1 67.80 68.99 1.08 o 3 21 1 17.87 18.35 0.60 o 4 21 1 15.99 13.72 0.45 o -3 22 1 1.58 1.01 0.24 o -2 22 1 303.74 308.77 6.50 o -1 22 1 76.02 73.68 2.02 o 0 22 1 37.80 40.86 0.83 o 1 22 1 75.57 76.91 0.98 o 2 22 1 300.04 311.78 3.97 o 3 22 1 1.59 0.66 0.22 o -2 23 1 1.01 2.02 0.74 o -1 23 1 121.50 115.41 2.38 o 0 23 1 33.91 29.79 0.74 o 1 23 1 120.56 115.58 2.75 o 2 23 1 0.92 1.12 0.21 o 2 0 2 2.42 7.44 0.30 o 3 0 2 124.80 122.56 1.86 o 4 0 2 526.03 534.07 8.37 o 5 0 2 161.41 180.88 3.36 o 6 0 2 363.99 351.39 7.49 o 7 0 2 332.13 370.14 9.25 o 8 0 2 2.64 5.31 0.54 o -7 1 2 126.72 130.73 3.89 o -6 1 2 282.38 261.47 2.57 o -5 1 2 112.62 113.86 1.54 o -4 1 2 89.77 93.36 0.79 o -3 1 2 538.28 483.33 4.46 o -2 1 2 1040.32 1011.30 19.59 o -1 1 2 55.98 48.74 0.62 o 1 1 2 52.67 44.79 0.42 o 2 1 2 1039.91 1004.77 2.50 o 3 1 2 538.78 485.65 6.74 o 4 1 2 88.78 89.99 1.30 o 5 1 2 116.21 115.33 2.21 o 6 1 2 278.46 259.61 3.26 o 7 1 2 119.22 120.95 2.53 o 9 1 2 111.38 109.54 3.14 o -8 2 2 24.50 22.01 1.02 o -7 2 2 69.33 82.87 4.33 o -6 2 2 598.88 624.01 11.64 o -5 2 2 293.44 294.92 3.53 o -4 2 2 384.21 368.89 5.30 o -3 2 2 85.50 74.91 1.76 o 0 2 2 85.13 90.81 7.01 o 3 2 2 83.56 72.94 1.35 o 4 2 2 387.27 366.43 1.91 o 5 2 2 293.88 295.78 3.03 o 6 2 2 590.23 608.91 17.14 o 7 2 2 71.16 90.34 6.07 o 8 2 2 24.24 18.86 0.96 o 9 2 2 30.24 26.28 0.88 o -8 3 2 48.08 48.71 1.53 o -7 3 2 272.11 281.14 3.48 o -6 3 2 74.50 76.83 0.94 o -5 3 2 382.52 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142.88 1.42 o -2 14 2 45.27 39.83 0.61 o -1 14 2 40.45 34.61 0.61 o 0 14 2 418.14 416.20 2.65 o 1 14 2 40.83 34.81 0.52 o 2 14 2 44.00 39.40 0.62 o 3 14 2 146.17 143.95 1.79 o 4 14 2 333.99 336.39 2.02 o 5 14 2 231.85 232.27 1.62 o 6 14 2 85.37 87.40 1.29 o 7 14 2 12.70 12.24 0.45 o -7 15 2 18.89 18.54 0.64 o -6 15 2 121.48 128.95 1.84 o -5 15 2 71.12 71.38 0.93 o -4 15 2 92.41 101.40 1.04 o -3 15 2 55.68 54.93 0.75 o -2 15 2 619.73 610.41 2.48 o -1 15 2 590.71 584.83 4.83 o 0 15 2 336.91 362.41 3.89 o 1 15 2 593.95 586.93 3.99 o 2 15 2 615.26 609.75 2.82 o 3 15 2 59.17 60.67 0.73 o 4 15 2 91.80 100.67 1.49 o 5 15 2 71.18 71.69 1.02 o 6 15 2 120.00 122.14 2.57 o 7 15 2 18.72 19.03 0.58 o -6 16 2 20.29 21.84 0.54 o -5 16 2 267.25 258.65 2.59 o -4 16 2 219.97 222.36 2.27 o -3 16 2 13.03 17.40 0.42 o -2 16 2 7.56 6.73 0.47 o -1 16 2 174.84 171.85 2.00 o 0 16 2 102.13 96.56 1.40 o 1 16 2 170.82 166.68 1.24 o 2 16 2 7.86 8.11 0.43 o 3 16 2 12.47 17.10 0.46 o 4 16 2 220.68 222.26 2.59 o 5 16 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