#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:31:24 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180787 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/18/2011815.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011815_Fobs loop_ _publ_author_name 'Steinberger, Hans-Uwe' 'Ziemer, Burkhard' 'Meisel, Manfred' _publ_section_title ; Tris(tert-butyl)phosphine selenide, the missing link in tris(tert-butyl)phosphine chalcogenide structures ^t^Bu~3~P=X (X = O, S, Se, Te) ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 323 _journal_page_last 324 _journal_volume 57 _journal_year 2001 _space_group_IT_number 205 _symmetry_space_group_name_Hall '-P 2ac 2ab 3' _symmetry_space_group_name_H-M 'P a -3' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.4773 _cell_length_b 14.4773 _cell_length_c 14.4773 _exptl_crystal_F_000 1184.00 _reflns_d_resolution_high 0.8118 _cod_data_source_file jz1439Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' UST87' _shelx_refln_list_code 4 _shelx_f_calc_maximum 237.04 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' 'y, z, x' '-y+1/2, -z, x+1/2' 'y+1/2, -z+1/2, -x' '-y, z+1/2, -x+1/2' 'z, x, y' '-z, x+1/2, -y+1/2' '-z+1/2, -x, y+1/2' 'z+1/2, -x+1/2, -y' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' '-y, -z, -x' 'y-1/2, z, -x-1/2' '-y-1/2, z-1/2, x' 'y, -z-1/2, x-1/2' '-z, -x, -y' 'z, -x-1/2, y-1/2' 'z-1/2, x, -y-1/2' '-z-1/2, x-1/2, y' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 2 14150.56 13125.08 146.73 o 0 2 2 15420.06 15947.50 215.34 o 1 2 2 10.16 38.23 13.91 o 2 2 2 8996.79 9470.50 174.77 o 1 1 3 1586.02 1565.54 17.90 o 2 1 3 1437.55 1560.06 18.10 o 0 2 3 2389.25 2348.15 46.87 o 1 2 3 27.53 30.76 14.65 o 2 2 3 116.69 107.77 15.16 o 1 3 3 1320.99 1210.48 16.78 o 2 3 3 12.01 46.71 14.30 o 3 3 3 10369.27 11495.93 236.15 o 0 0 4 45866.71 50804.84 232.50 o 1 0 4 15897.15 15987.68 126.58 o 3 0 4 16.58 71.31 21.56 o 1 1 4 3848.13 3542.50 31.67 o 2 1 4 1985.12 1826.18 18.05 o 3 1 4 1508.35 1636.38 16.62 o 1 2 4 1404.06 1468.51 17.71 o 2 2 4 56190.32 57451.91 224.29 o 3 2 4 419.10 486.79 13.89 o 1 3 4 101.41 94.30 14.26 o 2 3 4 451.20 410.81 14.02 o 3 3 4 3407.53 3614.52 37.51 o 0 4 4 48485.13 51887.73 1061.17 o 1 4 4 131.34 167.27 13.31 o 2 4 4 33287.43 34557.48 375.85 o 3 4 4 6272.30 6434.25 57.68 o 4 4 4 13344.80 13251.54 237.39 o 1 1 5 1353.88 1341.87 17.00 o 2 1 5 4991.49 5317.59 44.63 o 3 1 5 77.25 131.32 13.02 o 4 1 5 247.01 264.84 13.92 o 0 2 5 3347.43 3428.03 42.81 o 1 2 5 3900.23 3857.77 30.46 o 2 2 5 24.99 36.03 14.40 o 3 2 5 2.97 5.02 13.11 o 4 2 5 8487.52 8712.92 91.72 o 1 3 5 321.11 310.62 13.43 o 2 3 5 4561.08 4659.86 46.61 o 3 3 5 1156.46 1008.11 15.70 o 4 3 5 1423.99 1317.95 15.27 o 0 4 5 345.42 406.64 19.30 o 1 4 5 462.08 396.20 14.31 o 2 4 5 2479.46 2615.66 24.39 o 3 4 5 508.84 568.45 14.42 o 4 4 5 7414.84 7478.22 66.05 o 1 5 5 104.42 134.09 13.56 o 2 5 5 169.90 156.85 13.57 o 3 5 5 323.55 285.58 12.98 o 4 5 5 1088.75 1126.69 15.25 o 5 5 5 74.08 101.74 26.95 o 0 0 6 314.29 407.30 38.26 o 1 0 6 1255.66 1352.92 26.80 o 2 0 6 12990.91 13574.35 141.25 o 3 0 6 7420.91 7431.71 93.88 o 4 0 6 37161.84 38601.76 551.89 o 5 0 6 12501.84 12482.16 151.42 o 1 1 6 847.16 848.17 16.73 o 2 1 6 3569.84 3726.06 34.80 o 3 1 6 34.03 62.26 14.00 o 4 1 6 295.00 309.85 13.94 o 5 1 6 289.02 284.70 14.64 o 0 2 6 15768.80 16518.96 181.94 o 1 2 6 14129.69 14662.27 149.27 o 2 2 6 32313.36 32445.79 330.30 o 3 2 6 4426.82 4544.18 39.57 o 4 2 6 26048.55 26043.98 260.39 o 5 2 6 3640.94 3430.32 35.07 o 1 3 6 1364.68 1315.07 16.67 o 2 3 6 346.81 346.45 14.57 o 3 3 6 59.47 56.34 13.56 o 4 3 6 3040.32 3031.21 22.59 o 5 3 6 731.32 706.75 13.84 o 0 4 6 26090.36 27199.83 330.21 o 1 4 6 4568.96 4425.23 39.64 o 2 4 6 29248.54 29786.43 258.03 o 3 4 6 2759.81 2756.37 21.42 o 4 4 6 10244.56 9871.87 90.77 o 5 4 6 451.59 396.84 13.14 o 1 5 6 2305.35 2304.09 20.51 o 2 5 6 3495.79 3490.51 25.20 o 3 5 6 788.39 792.77 13.58 o 4 5 6 1802.66 1639.62 14.78 o 5 5 6 96.77 100.05 13.11 o 0 6 6 38871.05 41271.02 545.87 o 1 6 6 4317.60 4262.15 41.15 o 2 6 6 25383.70 25120.21 234.33 o 3 6 6 2801.11 2792.53 23.68 o 4 6 6 9954.79 9978.45 89.50 o 5 6 6 1110.79 1022.90 13.64 o 6 6 6 3831.03 4051.05 89.33 o 1 1 7 2405.11 2267.53 23.59 o 2 1 7 413.91 438.69 14.35 o 3 1 7 836.06 893.10 16.51 o 4 1 7 145.86 157.79 14.13 o 5 1 7 6.83 9.43 12.69 o 6 1 7 327.84 346.34 14.50 o 0 2 7 173.09 224.23 21.60 o 1 2 7 1790.99 1712.68 17.44 o 2 2 7 233.06 258.10 13.91 o 3 2 7 45.52 47.78 13.00 o 4 2 7 962.43 919.36 14.36 o 5 2 7 2076.22 2055.09 18.07 o 6 2 7 2445.62 2452.12 26.37 o 1 3 7 1038.29 1052.04 15.10 o 2 3 7 715.78 721.62 15.68 o 3 3 7 336.52 270.08 13.19 o 4 3 7 36.53 26.59 13.43 o 5 3 7 238.28 239.73 14.16 o 6 3 7 5.00 4.07 13.52 o 0 4 7 18.90 5.66 21.58 o 1 4 7 746.06 777.02 14.37 o 2 4 7 932.98 879.04 15.26 o 3 4 7 322.97 300.30 13.90 o 4 4 7 1736.49 1702.45 15.88 o 5 4 7 1531.44 1468.44 14.23 o 6 4 7 2590.48 2535.95 27.20 o 1 5 7 12.13 9.29 13.71 o 2 5 7 465.67 459.18 13.84 o 3 5 7 99.74 140.21 12.79 o 4 5 7 21.87 31.59 13.16 o 5 5 7 8.40 18.95 12.30 o 6 5 7 99.09 99.13 13.39 o 0 6 7 468.92 520.24 17.12 o 1 6 7 1475.27 1451.10 13.93 o 2 6 7 2303.23 2251.23 21.79 o 3 6 7 29.27 8.80 13.65 o 4 6 7 1997.98 1861.85 18.90 o 5 6 7 109.09 137.60 12.75 o 6 6 7 2131.93 2160.41 24.23 o 1 7 7 1195.22 1208.16 14.93 o 2 7 7 1186.14 1184.07 16.34 o 3 7 7 2263.55 2368.75 19.36 o 4 7 7 621.64 543.72 14.48 o 5 7 7 166.21 150.97 13.89 o 6 7 7 293.46 265.69 12.89 o 7 7 7 1152.89 1140.56 23.23 o 0 0 8 20032.84 20057.51 123.65 o 1 0 8 672.92 708.70 21.60 o 2 0 8 24076.22 23817.39 210.94 o 3 0 8 5117.42 4868.98 50.39 o 4 0 8 12190.40 12543.79 110.31 o 5 0 8 14446.89 14705.46 205.60 o 6 0 8 15932.29 15926.02 183.34 o 7 0 8 13336.08 13225.35 182.21 o 1 1 8 1671.54 1798.61 17.70 o 2 1 8 198.53 189.00 14.50 o 3 1 8 886.56 840.02 15.57 o 4 1 8 2649.96 2562.78 24.17 o 5 1 8 213.56 237.03 13.51 o 6 1 8 424.16 401.29 13.35 o 7 1 8 4844.65 4917.51 38.70 o 0 2 8 23812.01 24032.19 245.75 o 1 2 8 3887.39 3762.27 32.98 o 2 2 8 28305.11 29362.85 235.39 o 3 2 8 6424.77 6274.04 56.12 o 4 2 8 11074.50 11116.23 91.95 o 5 2 8 7624.03 7659.00 62.00 o 6 2 8 8805.35 9006.16 78.18 o 7 2 8 6105.77 5865.11 50.58 o 1 3 8 12.90 24.68 13.59 o 2 3 8 2244.85 2250.78 23.03 o 3 3 8 94.66 67.60 13.37 o 4 3 8 2170.89 2190.46 16.34 o 5 3 8 727.00 703.69 14.23 o 6 3 8 1360.08 1430.71 16.51 o 7 3 8 324.44 323.07 13.13 o 0 4 8 12709.89 13307.42 138.91 o 1 4 8 6499.08 6381.31 42.92 o 2 4 8 14748.13 14812.93 140.49 o 3 4 8 3654.79 3579.06 25.62 o 4 4 8 8971.32 8913.14 59.96 o 5 4 8 1209.84 1213.69 15.20 o 6 4 8 11294.16 11119.08 84.48 o 7 4 8 889.04 889.54 14.58 o 1 5 8 1661.15 1780.90 16.21 o 2 5 8 231.15 250.68 14.39 o 3 5 8 3173.46 3147.19 20.17 o 4 5 8 183.52 176.56 12.93 o 5 5 8 727.38 659.66 14.43 o 6 5 8 2530.24 2424.98 24.33 o 7 5 8 752.47 753.63 14.10 o 0 6 8 13276.96 13207.86 154.98 o 1 6 8 18656.69 18869.83 188.50 o 2 6 8 8450.48 8621.60 74.68 o 3 6 8 2965.89 2872.38 25.52 o 4 6 8 9058.87 8795.24 73.79 o 5 6 8 70.24 90.13 12.30 o 6 6 8 5523.76 5568.10 50.11 o 7 6 8 46.95 74.05 14.23 o 1 7 8 880.67 862.70 15.52 o 2 7 8 970.12 926.33 14.07 o 3 7 8 2574.44 2350.07 27.06 o 4 7 8 1076.39 1071.84 14.16 o 5 7 8 1017.32 937.95 14.78 o 6 7 8 2009.89 1930.61 20.08 o 7 7 8 129.89 121.44 13.25 o 0 8 8 9540.68 9728.76 94.77 o 1 8 8 3367.20 3230.37 26.19 o 2 8 8 4673.32 4647.78 47.24 o 3 8 8 2192.58 2175.44 16.36 o 4 8 8 8711.05 8607.60 87.64 o 5 8 8 1993.85 2049.11 20.71 o 6 8 8 4249.44 4087.58 28.48 o 7 8 8 1375.01 1450.88 18.42 o 8 8 8 3472.12 3472.50 41.20 o 1 1 9 1460.16 1512.76 18.78 o 2 1 9 0.18 5.05 13.88 o 3 1 9 1504.73 1392.48 15.91 o 4 1 9 0.56 9.54 13.81 o 5 1 9 399.40 436.93 13.74 o 6 1 9 388.64 397.53 14.37 o 7 1 9 508.17 506.85 13.30 o 8 1 9 44.79 52.92 13.20 o 0 2 9 1477.13 1380.42 25.42 o 1 2 9 1112.30 1086.31 16.50 o 2 2 9 1869.48 1711.74 19.51 o 3 2 9 1323.13 1256.32 16.77 o 4 2 9 12.91 25.29 12.85 o 5 2 9 2230.74 2230.41 18.23 o 6 2 9 212.20 209.50 13.80 o 7 2 9 1543.31 1459.58 16.28 o 8 2 9 1.82 1.11 12.65 o 1 3 9 1246.50 1173.98 16.83 o 2 3 9 1225.38 1102.42 16.51 o 3 3 9 602.79 602.96 15.22 o 4 3 9 3127.66 3018.07 22.74 o 5 3 9 82.33 73.92 13.43 o 6 3 9 6.51 4.80 13.13 o 7 3 9 1821.45 1778.21 19.31 o 8 3 9 455.89 469.16 13.09 o 0 4 9 6285.12 6311.46 86.14 o 1 4 9 7.84 2.52 13.78 o 2 4 9 4312.97 4275.17 45.15 o 3 4 9 1369.08 1359.72 17.13 o 4 4 9 9.20 11.70 13.86 o 5 4 9 945.62 933.71 14.18 o 6 4 9 19.65 18.72 12.32 o 7 4 9 723.91 685.58 13.39 o 8 4 9 166.56 201.84 12.12 o 1 5 9 338.49 329.37 13.23 o 2 5 9 116.52 109.99 13.85 o 3 5 9 134.45 98.73 13.80 o 4 5 9 49.53 41.50 12.80 o 5 5 9 146.99 156.60 12.82 o 6 5 9 12.92 0.06 13.04 o 7 5 9 4.78 3.05 12.69 o 8 5 9 6.24 -0.20 13.44 o 0 6 9 441.41 423.31 19.64 o 1 6 9 611.37 648.62 14.21 o 2 6 9 1420.61 1417.05 15.70 o 3 6 9 127.86 124.89 13.49 o 4 6 9 2558.68 2540.40 16.17 o 5 6 9 148.60 128.62 13.05 o 6 6 9 1957.59 1992.00 18.14 o 7 6 9 296.59 289.92 12.88 o 8 6 9 992.67 1024.15 16.48 o 1 7 9 370.64 408.91 13.24 o 2 7 9 195.80 208.83 12.81 o 3 7 9 1328.60 1276.86 14.62 o 4 7 9 59.16 59.56 12.70 o 5 7 9 189.12 165.05 12.69 o 6 7 9 603.78 577.76 13.84 o 7 7 9 534.69 557.07 16.28 o 8 7 9 1270.67 1302.00 16.56 o 0 8 9 1022.92 1002.07 21.54 o 1 8 9 2958.54 2815.84 21.95 o 2 8 9 914.79 965.29 13.24 o 3 8 9 257.76 240.31 12.92 o 4 8 9 4716.49 4556.72 46.52 o 5 8 9 35.93 32.41 14.75 o 6 8 9 3717.73 3756.29 29.29 o 7 8 9 50.93 50.11 14.97 o 8 8 9 962.85 991.03 14.57 o 1 9 9 94.83 78.48 12.57 o 2 9 9 732.58 729.32 14.14 o 3 9 9 70.15 74.97 14.30 o 4 9 9 202.23 186.52 14.95 o 5 9 9 80.77 73.72 15.00 o 6 9 9 656.50 629.59 14.99 o 7 9 9 75.39 51.73 14.12 o 8 9 9 930.88 907.91 15.32 o 9 9 9 32.19 30.75 23.28 o 0 0 10 18974.34 19485.08 187.32 o 1 0 10 4629.92 4523.75 36.38 o 2 0 10 15572.61 16072.95 140.98 o 3 0 10 10148.03 9971.12 100.78 o 4 0 10 1715.50 1717.93 23.70 o 5 0 10 5543.06 5652.75 66.77 o 6 0 10 3164.86 3245.45 35.90 o 7 0 10 6814.71 6769.74 103.38 o 8 0 10 5777.70 5984.89 76.55 o 9 0 10 660.21 701.48 21.40 o 1 1 10 375.43 399.63 15.73 o 2 1 10 2661.29 2529.74 24.00 o 3 1 10 428.06 398.96 13.62 o 4 1 10 3528.89 3482.08 19.25 o 5 1 10 46.01 47.34 13.86 o 6 1 10 619.36 558.98 13.11 o 7 1 10 1738.32 1700.91 16.09 o 8 1 10 393.99 439.45 13.44 o 9 1 10 242.26 253.53 15.68 o 0 2 10 11268.00 11298.88 102.05 o 1 2 10 10589.76 10835.89 69.52 o 2 2 10 13717.08 13687.99 119.80 o 3 2 10 7830.30 8053.08 55.03 o 4 2 10 5963.00 6236.87 37.48 o 5 2 10 2728.72 2864.52 26.15 o 6 2 10 3569.65 3504.09 28.59 o 7 2 10 2189.49 2194.10 23.31 o 8 2 10 2855.94 2868.85 29.69 o 9 2 10 647.31 686.14 17.02 o 1 3 10 216.90 199.92 14.65 o 2 3 10 30.43 53.58 13.59 o 3 3 10 1256.18 1291.25 16.88 o 4 3 10 319.86 312.24 14.02 o 5 3 10 429.60 434.66 15.20 o 6 3 10 1941.87 1839.41 15.09 o 7 3 10 165.23 161.79 12.63 o 8 3 10 3479.33 3526.89 35.14 o 9 3 10 414.86 408.94 16.72 o 0 4 10 2113.61 1969.71 29.62 o 1 4 10 5850.53 5988.50 42.95 o 2 4 10 5587.67 5768.31 37.84 o 3 4 10 3104.18 3145.45 28.46 o 4 4 10 16211.58 15968.04 103.12 o 5 4 10 3646.20 3526.79 26.75 o 6 4 10 13321.59 13159.17 97.03 o 7 4 10 3610.79 3586.70 31.52 o 8 4 10 3455.37 3519.96 26.44 o 9 4 10 4099.17 4186.43 37.74 o 1 5 10 200.02 207.25 13.58 o 2 5 10 2631.61 2587.18 21.71 o 3 5 10 20.87 39.47 13.64 o 4 5 10 149.52 134.42 13.44 o 5 5 10 293.06 267.67 13.88 o 6 5 10 2447.26 2417.40 20.56 o 7 5 10 11.18 3.24 15.95 o 8 5 10 5159.97 5332.78 41.92 o 9 5 10 716.17 720.45 14.66 o 0 6 10 2654.28 2593.65 34.10 o 1 6 10 5080.35 5146.61 40.29 o 2 6 10 3748.60 3828.52 32.98 o 3 6 10 2494.14 2404.12 19.65 o 4 6 10 11676.66 11643.64 110.92 o 5 6 10 2731.30 2582.04 20.12 o 6 6 10 8001.98 8148.17 70.00 o 7 6 10 1554.10 1524.17 17.35 o 8 6 10 2041.94 2109.53 23.09 o 9 6 10 2954.70 2954.62 27.47 o 1 7 10 283.93 275.92 12.74 o 2 7 10 7.56 18.59 11.97 o 3 7 10 35.78 58.41 13.09 o 4 7 10 48.60 66.17 12.05 o 5 7 10 614.70 620.91 16.09 o 6 7 10 1081.51 1104.02 17.30 o 7 7 10 258.35 267.51 15.18 o 8 7 10 2180.62 2175.24 22.89 o 9 7 10 496.83 476.92 13.61 o 0 8 10 5478.21 5362.93 54.12 o 1 8 10 1166.54 1146.00 13.94 o 2 8 10 4208.66 4296.71 37.62 o 3 8 10 2424.60 2556.64 25.91 o 4 8 10 3959.62 3991.85 38.39 o 5 8 10 4053.57 4091.77 34.33 o 6 8 10 2521.41 2544.66 24.78 o 7 8 10 2228.77 2202.70 19.68 o 8 8 10 2259.15 2248.34 19.88 o 9 8 10 2015.39 2034.92 15.97 o 1 9 10 8.37 -0.84 13.90 o 2 9 10 628.07 606.83 15.84 o 3 9 10 374.52 392.98 14.34 o 4 9 10 480.11 480.42 14.43 o 5 9 10 46.69 47.14 14.89 o 6 9 10 265.86 270.28 12.93 o 7 9 10 548.79 537.72 15.21 o 8 9 10 16.87 25.31 14.10 o 9 9 10 650.54 622.96 14.82 o 0 10 10 7020.98 7144.36 121.03 o 1 10 10 1174.13 1202.39 16.71 o 2 10 10 3671.67 3650.89 30.67 o 3 10 10 1493.76 1474.77 16.82 o 4 10 10 431.19 464.55 15.70 o 5 10 10 2241.74 2149.89 19.85 o 6 10 10 190.24 188.22 14.13 o 7 10 10 1412.12 1382.10 17.08 o 8 10 10 1226.93 1223.58 17.40 o 9 10 10 907.55 932.55 16.69 o 10 10 10 1394.32 1323.26 32.40 o 1 1 11 1.24 -12.92 15.48 o 2 1 11 693.53 750.97 15.66 o 3 1 11 183.12 151.32 13.40 o 4 1 11 58.39 69.84 14.31 o 5 1 11 398.40 382.81 15.43 o 6 1 11 136.32 142.81 13.57 o 7 1 11 22.68 34.26 15.48 o 8 1 11 248.23 246.79 15.31 o 9 1 11 0.01 -0.22 14.41 o 10 1 11 5.37 9.03 14.78 o 0 2 11 1791.08 1979.28 24.13 o 1 2 11 409.12 370.40 13.97 o 2 2 11 650.81 653.95 15.24 o 3 2 11 0.65 7.52 13.44 o 4 2 11 783.17 793.66 14.62 o 5 2 11 437.56 390.27 14.56 o 6 2 11 397.17 398.89 13.95 o 7 2 11 20.90 30.26 14.74 o 8 2 11 441.36 476.28 15.17 o 9 2 11 113.44 94.63 14.41 o 10 2 11 1752.68 1753.40 16.97 o 1 3 11 57.27 42.47 13.59 o 2 3 11 2513.09 2481.97 16.79 o 3 3 11 2790.24 2534.62 18.83 o 4 3 11 1113.63 1018.81 15.84 o 5 3 11 85.96 88.88 14.94 o 6 3 11 42.33 27.67 13.68 o 7 3 11 11.07 13.07 16.06 o 8 3 11 807.10 837.90 17.19 o 9 3 11 131.22 137.83 15.47 o 10 3 11 32.28 33.76 12.68 o 0 4 11 1724.34 1682.52 26.93 o 1 4 11 956.24 845.35 14.04 o 2 4 11 740.30 669.41 14.64 o 3 4 11 119.51 141.02 14.27 o 4 4 11 8.50 12.80 14.38 o 5 4 11 86.99 92.73 13.36 o 6 4 11 18.73 32.58 16.22 o 7 4 11 55.57 45.84 16.51 o 8 4 11 747.43 734.04 15.46 o 9 4 11 15.42 10.76 14.32 o 10 4 11 1194.01 1174.86 17.75 o 1 5 11 80.16 90.72 12.71 o 2 5 11 6.32 5.06 12.94 o 3 5 11 0.14 -2.48 12.97 o 4 5 11 7.15 -9.27 12.50 o 5 5 11 12.17 11.94 14.48 o 6 5 11 51.71 33.35 15.07 o 7 5 11 8.00 9.83 14.52 o 8 5 11 121.32 94.11 14.38 o 9 5 11 44.11 66.45 15.13 o 10 5 11 309.97 311.64 15.97 o 0 6 11 153.50 163.74 18.44 o 1 6 11 70.93 66.33 12.51 o 2 6 11 264.58 245.63 12.79 o 3 6 11 597.95 594.57 13.94 o 4 6 11 2192.30 2238.42 19.22 o 5 6 11 666.55 628.40 16.25 o 6 6 11 1555.50 1564.23 17.23 o 7 6 11 403.45 421.84 15.73 o 8 6 11 681.76 663.95 15.17 o 9 6 11 202.10 210.80 14.28 o 10 6 11 143.22 141.48 14.43 o 1 7 11 41.28 31.62 14.25 o 2 7 11 566.72 588.08 15.89 o 3 7 11 2.59 -15.81 14.09 o 4 7 11 42.31 42.54 13.57 o 5 7 11 158.56 161.37 15.81 o 6 7 11 604.89 609.42 16.03 o 7 7 11 31.96 41.59 14.47 o 8 7 11 1767.75 1817.78 17.71 o 9 7 11 167.72 193.15 13.69 o 10 7 11 482.84 510.13 16.33 o 0 8 11 404.01 421.97 20.77 o 1 8 11 947.33 976.12 14.98 o 2 8 11 545.79 571.72 16.20 o 3 8 11 548.20 583.80 17.33 o 4 8 11 3810.70 3840.38 50.26 o 5 8 11 501.51 485.98 14.55 o 6 8 11 2987.96 3027.70 24.66 o 7 8 11 381.06 383.90 14.84 o 8 8 11 405.58 428.77 13.28 o 9 8 11 167.99 162.12 13.81 o 10 8 11 45.80 49.47 16.00 o 1 9 11 24.29 18.64 14.68 o 2 9 11 234.97 248.61 14.93 o 3 9 11 155.29 145.92 13.72 o 4 9 11 10.70 24.28 15.40 o 5 9 11 6.86 17.07 13.47 o 6 9 11 506.56 503.70 14.17 o 7 9 11 0.46 6.54 13.23 o 8 9 11 1005.69 993.36 16.01 o 9 9 11 34.45 25.67 15.04 o 10 9 11 385.01 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