#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:31:24 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180787 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/18/2011877.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011877_Fobs loop_ _publ_author_name 'Creaven, Bernadette S.' 'Howie, R. Alan' 'Long, Conor' _publ_section_title ; Pentacarbonyl(4-phenylpyridine)tungsten(0) and pentacarbonyl(2-phenylpyridine)chromium(0) ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 385 _journal_page_last 387 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.600 _cell_angle_gamma 90.000 _cell_length_a 6.2230 _cell_length_b 13.6350 _cell_length_c 18.1700 _exptl_crystal_F_000 704.00 _reflns_d_resolution_high 0.7094 _cod_data_source_file gd1123IIsup3.hkl _cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' 2-PhPy Cr(CO)5 (Z=4, P21/c)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 171.05 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y+1/2, z+1/2' '-x, -y, -z' '-x, y-1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2659.37 3193.41 74.67 o 2 0 0 3045.27 3307.95 74.52 o 3 0 0 670.31 672.26 37.59 o 4 0 0 26.22 26.90 36.13 o 5 0 0 981.49 1120.46 78.16 o 6 0 0 345.85 292.44 72.62 o 7 0 0 90.77 148.50 75.04 o 8 0 0 114.13 185.64 105.40 o 1 1 0 14276.75 14615.59 229.54 o 2 1 0 473.24 518.13 26.86 o 3 1 0 35.03 17.41 24.95 o 4 1 0 993.89 1039.20 59.97 o 5 1 0 1124.04 1065.58 78.73 o 6 1 0 81.39 113.45 62.45 o 7 1 0 561.57 565.81 99.79 o 8 1 0 5.82 93.67 88.90 o 0 2 0 15276.17 14268.09 196.15 o 1 2 0 1559.36 1522.65 38.55 o 2 2 0 1332.10 1293.78 38.30 o 3 2 0 490.61 423.49 34.32 o 4 2 0 312.84 244.44 44.33 o 5 2 0 652.70 726.53 70.20 o 6 2 0 517.48 527.22 83.66 o 7 2 0 17.70 26.69 75.49 o 8 2 0 146.30 277.29 101.05 o 1 3 0 2415.33 2416.00 56.75 o 2 3 0 813.49 792.92 32.88 o 3 3 0 302.16 263.53 32.07 o 4 3 0 839.40 767.27 58.28 o 5 3 0 1283.99 1373.75 85.11 o 6 3 0 1.97 29.70 63.41 o 7 3 0 118.96 129.59 86.02 o 8 3 0 0.38 20.49 17.80 o 0 4 0 310.26 300.97 19.14 o 1 4 0 7026.78 6875.40 156.37 o 2 4 0 1145.66 1119.90 38.21 o 3 4 0 125.49 143.44 29.34 o 4 4 0 483.82 530.70 54.09 o 5 4 0 10.71 66.99 50.93 o 6 4 0 84.55 10.48 67.06 o 7 4 0 0.12 55.94 75.99 o 8 4 0 30.67 100.03 100.85 o 1 5 0 1423.21 1399.83 37.92 o 2 5 0 56.50 9.74 20.90 o 3 5 0 669.53 727.74 43.61 o 4 5 0 474.80 536.96 59.75 o 5 5 0 16.00 62.76 48.28 o 6 5 0 110.86 4.62 26.11 o 7 5 0 12.81 1.56 18.62 o 8 5 0 0.76 46.78 94.94 o 0 6 0 231.68 217.04 19.66 o 1 6 0 12.15 20.69 16.75 o 2 6 0 79.29 133.10 23.54 o 3 6 0 82.19 74.32 31.41 o 4 6 0 1.27 22.73 24.54 o 5 6 0 80.96 61.95 53.92 o 6 6 0 116.30 128.54 69.09 o 7 6 0 4.44 22.17 78.59 o 8 6 0 1.17 38.59 93.56 o 1 7 0 1178.97 1181.39 40.13 o 2 7 0 997.35 919.84 44.35 o 3 7 0 544.30 530.14 47.56 o 4 7 0 46.15 4.14 18.98 o 5 7 0 0.48 5.66 12.54 o 6 7 0 71.80 99.35 76.85 o 7 7 0 1.00 78.27 83.53 o 0 8 0 38.83 7.28 17.77 o 1 8 0 347.58 326.16 28.73 o 2 8 0 20.45 57.52 25.59 o 3 8 0 67.16 110.68 34.55 o 4 8 0 12.75 4.18 19.40 o 5 8 0 139.66 129.82 62.13 o 6 8 0 3.50 50.65 71.67 o 7 8 0 2.07 5.30 16.87 o 1 9 0 136.45 168.86 27.84 o 2 9 0 97.87 89.97 33.34 o 3 9 0 0.27 22.91 22.44 o 4 9 0 2.22 13.37 21.14 o 5 9 0 51.68 147.52 59.68 o 6 9 0 2.41 20.05 65.15 o 7 9 0 18.91 170.98 88.91 o 0 10 0 771.85 752.91 39.43 o 1 10 0 173.03 209.65 30.65 o 2 10 0 113.22 111.10 33.27 o 3 10 0 1.26 40.02 22.10 o 4 10 0 0.07 7.65 8.50 o 5 10 0 47.08 65.19 61.22 o 6 10 0 59.94 90.65 84.53 o 7 10 0 0.01 71.28 95.10 o 1 11 0 437.45 349.50 38.62 o 2 11 0 28.52 46.93 31.20 o 3 11 0 191.25 156.28 43.78 o 4 11 0 261.88 328.30 64.85 o 5 11 0 55.16 58.44 60.32 o 6 11 0 76.01 44.05 86.25 o 7 11 0 29.04 1.87 19.86 o 0 12 0 2723.26 2633.05 77.02 o 1 12 0 350.74 295.66 39.71 o 2 12 0 1.33 22.24 32.67 o 3 12 0 72.78 151.68 45.66 o 4 12 0 38.94 37.86 58.73 o 5 12 0 94.50 201.16 67.69 o 6 12 0 3.06 61.99 82.72 o 1 13 0 405.05 410.19 44.69 o 2 13 0 103.46 190.53 39.49 o 3 13 0 24.96 6.77 18.84 o 4 13 0 146.13 179.42 68.56 o 5 13 0 43.52 12.56 69.39 o 6 13 0 5.94 3.03 19.31 o 0 14 0 233.29 298.51 36.35 o 1 14 0 40.48 10.97 19.68 o 2 14 0 22.91 63.95 40.01 o 3 14 0 119.16 144.95 52.82 o 4 14 0 26.52 8.46 11.94 o 5 14 0 63.52 13.46 68.63 o 6 14 0 49.60 43.87 88.20 o 1 15 0 92.01 92.24 37.21 o 2 15 0 21.75 6.78 41.53 o 3 15 0 3.58 12.70 25.23 o 4 15 0 92.75 152.07 65.66 o 5 15 0 64.93 100.16 68.56 o 0 16 0 585.72 626.47 53.30 o 1 16 0 41.33 106.36 39.82 o 2 16 0 2.55 16.33 22.26 o 3 16 0 57.85 100.59 53.53 o 4 16 0 1.97 75.71 67.31 o 1 17 0 150.63 154.55 43.86 o 2 17 0 21.19 27.79 41.87 o 3 17 0 0.68 7.64 21.62 o 4 17 0 19.09 81.31 67.10 o 0 18 0 75.97 83.02 38.34 o 1 18 0 9.56 45.59 41.92 o 2 18 0 41.86 59.27 47.11 o 3 18 0 18.76 56.28 60.63 o 1 19 0 51.84 121.51 43.70 o -8 1 1 3.55 76.51 89.54 o -7 1 1 1.36 39.41 72.56 o -6 1 1 79.87 72.48 57.99 o -5 1 1 2.27 38.95 47.08 o -4 1 1 8.95 25.34 33.78 o -3 1 1 134.99 196.87 27.54 o -2 1 1 1288.13 1522.35 41.54 o -1 1 1 454.12 485.43 17.81 o 0 1 1 136.16 200.23 7.99 o 1 1 1 451.92 440.83 17.78 o 2 1 1 7045.68 7563.46 145.04 o 3 1 1 1.58 7.55 23.40 o 4 1 1 327.95 302.51 43.51 o 5 1 1 0.05 5.43 18.55 o 6 1 1 77.49 50.22 60.73 o 7 1 1 0.28 99.17 81.76 o 8 1 1 5.14 51.32 92.91 o -8 2 1 0.37 2.94 15.55 o -7 2 1 55.47 23.87 21.05 o -6 2 1 37.92 12.05 12.86 o -5 2 1 17.48 98.09 48.28 o -4 2 1 1293.20 1402.48 66.78 o -3 2 1 151.29 181.40 27.82 o -2 2 1 4351.46 4718.68 103.99 o -1 2 1 337.75 351.83 18.29 o 0 2 1 69.63 65.82 11.76 o 1 2 1 4488.32 4477.04 105.58 o 2 2 1 370.55 381.13 25.55 o 3 2 1 16.83 3.62 19.70 o 4 2 1 33.11 92.47 36.76 o 5 2 1 0.33 32.33 21.66 o 6 2 1 116.69 52.09 65.09 o 7 2 1 7.82 35.83 21.18 o 8 2 1 0.22 3.10 17.94 o -8 3 1 5.39 6.83 22.65 o -7 3 1 6.61 16.82 15.00 o -6 3 1 56.66 172.86 64.27 o -5 3 1 65.59 144.30 52.24 o -4 3 1 150.62 161.18 44.79 o -3 3 1 192.67 135.44 28.07 o -2 3 1 394.53 398.19 26.37 o -1 3 1 198.39 205.40 18.75 o 0 3 1 2812.93 2866.78 66.63 o 1 3 1 214.80 199.05 19.01 o 2 3 1 1711.59 1868.81 46.58 o 3 3 1 2239.37 2256.72 65.21 o 4 3 1 39.74 97.58 41.19 o 5 3 1 108.00 131.82 52.29 o 6 3 1 147.72 29.88 68.66 o 7 3 1 12.93 157.63 80.21 o 8 3 1 0.13 2.95 16.16 o -8 4 1 34.84 117.99 103.12 o -7 4 1 87.91 111.75 85.03 o -6 4 1 356.71 308.66 74.83 o -5 4 1 37.03 17.61 48.18 o -4 4 1 732.72 751.36 60.48 o -3 4 1 605.80 570.92 40.46 o -2 4 1 204.17 207.95 23.68 o -1 4 1 493.13 465.40 23.25 o 0 4 1 319.53 320.14 19.97 o 1 4 1 12733.29 12764.65 300.03 o 2 4 1 2616.63 2726.82 64.98 o 3 4 1 250.11 262.33 32.83 o 4 4 1 887.02 839.36 63.18 o 5 4 1 25.23 53.23 48.77 o 6 4 1 139.79 205.33 70.04 o 7 4 1 12.16 154.50 77.50 o 8 4 1 0.65 5.55 21.01 o -8 5 1 22.88 6.96 25.74 o -7 5 1 13.70 15.23 17.89 o -6 5 1 37.87 18.46 19.06 o -5 5 1 988.37 914.79 81.48 o -4 5 1 180.35 88.09 50.93 o -3 5 1 326.36 380.15 36.77 o -2 5 1 3863.95 4090.23 96.00 o -1 5 1 765.56 730.79 28.09 o 0 5 1 2691.08 2633.58 64.52 o 1 5 1 3945.08 3833.72 83.41 o 2 5 1 112.60 161.80 25.29 o 3 5 1 924.54 987.18 50.38 o 4 5 1 219.02 199.62 48.03 o 5 5 1 556.32 538.26 67.86 o 6 5 1 374.88 347.97 78.73 o 7 5 1 8.47 15.26 21.92 o 8 5 1 18.23 37.59 107.13 o -8 6 1 6.51 38.52 98.18 o -7 6 1 73.29 1.93 19.41 o -6 6 1 142.09 189.84 76.89 o -5 6 1 57.60 166.31 53.44 o -4 6 1 1473.08 1592.11 84.97 o -3 6 1 123.62 99.72 33.95 o -2 6 1 449.26 451.20 32.16 o -1 6 1 4991.15 4647.04 97.95 o 0 6 1 7.99 3.72 11.17 o 1 6 1 241.22 159.18 21.20 o 2 6 1 1402.26 1323.25 46.20 o 3 6 1 55.76 80.40 31.41 o 4 6 1 1260.80 1380.65 77.70 o 5 6 1 741.13 883.75 80.47 o 6 6 1 6.81 8.45 20.91 o 7 6 1 135.85 156.02 89.42 o 8 6 1 25.65 18.43 20.35 o -7 7 1 0.02 7.81 88.02 o -6 7 1 51.24 116.63 72.32 o -5 7 1 551.01 509.14 71.79 o -4 7 1 7.75 47.15 40.87 o -3 7 1 1557.33 1520.60 66.54 o -2 7 1 1934.43 1880.86 56.75 o -1 7 1 899.77 869.96 35.57 o 0 7 1 4152.08 4159.52 94.32 o 1 7 1 1361.90 1262.55 41.48 o 2 7 1 136.68 142.42 28.02 o 3 7 1 1428.40 1506.53 66.73 o 4 7 1 0.44 31.55 21.96 o 5 7 1 122.77 107.54 56.67 o 6 7 1 639.62 810.98 100.10 o 7 7 1 0.08 11.43 22.28 o -7 8 1 202.20 238.22 99.60 o -6 8 1 59.97 94.77 77.18 o -5 8 1 0.39 17.64 23.55 o -4 8 1 170.79 252.59 53.62 o -3 8 1 96.39 50.95 36.99 o -2 8 1 2.99 31.11 24.69 o -1 8 1 1005.98 985.53 40.27 o 0 8 1 117.32 137.84 21.84 o 1 8 1 1666.84 1682.21 51.04 o 2 8 1 4118.79 4074.82 103.18 o 3 8 1 27.33 4.34 20.81 o 4 8 1 4.11 65.24 46.73 o 5 8 1 140.51 144.04 60.66 o 6 8 1 83.26 57.29 77.20 o 7 8 1 168.37 82.56 92.67 o -7 9 1 1.95 102.48 91.17 o -6 9 1 174.59 253.88 87.08 o -5 9 1 283.39 318.72 68.02 o -4 9 1 16.25 106.48 47.13 o -3 9 1 340.07 284.58 47.61 o -2 9 1 900.55 912.70 51.55 o -1 9 1 392.07 401.40 32.13 o 0 9 1 3728.69 3633.14 89.70 o 1 9 1 946.90 923.90 44.45 o 2 9 1 292.75 272.97 39.00 o 3 9 1 430.43 534.67 49.54 o 4 9 1 17.04 18.44 44.13 o 5 9 1 17.34 47.78 56.58 o 6 9 1 173.74 33.55 79.66 o 7 9 1 7.30 265.98 98.13 o -7 10 1 91.79 71.21 92.45 o -6 10 1 16.90 76.66 76.72 o -5 10 1 222.06 290.74 68.68 o -4 10 1 239.31 240.88 57.34 o -3 10 1 11.09 60.72 33.79 o -2 10 1 199.16 224.64 35.96 o -1 10 1 655.45 656.75 42.41 o 0 10 1 59.41 18.02 22.71 o 1 10 1 930.02 852.79 47.58 o 2 10 1 200.60 217.07 37.24 o 3 10 1 1.67 22.16 35.69 o 4 10 1 30.18 35.73 51.00 o 5 10 1 308.76 538.68 74.14 o 6 10 1 9.26 8.13 22.07 o 7 10 1 68.35 26.82 94.22 o -7 11 1 27.88 65.30 98.28 o -6 11 1 53.01 36.67 78.00 o -5 11 1 164.74 239.00 72.19 o -4 11 1 165.03 51.81 56.97 o -3 11 1 42.30 36.08 42.07 o -2 11 1 269.82 322.01 41.44 o -1 11 1 24.52 29.46 27.02 o 0 11 1 787.93 703.89 42.21 o 1 11 1 5.14 3.47 25.78 o 2 11 1 132.34 94.28 35.25 o 3 11 1 89.82 102.60 43.27 o 4 11 1 122.05 186.55 60.63 o 5 11 1 18.67 5.33 61.03 o 6 11 1 79.56 7.37 79.00 o 7 11 1 11.73 4.02 18.45 o -6 12 1 47.75 20.30 19.89 o -5 12 1 60.67 40.17 64.15 o -4 12 1 199.37 151.35 66.92 o -3 12 1 5.70 36.26 38.86 o -2 12 1 5.98 2.47 33.66 o -1 12 1 475.81 384.79 41.27 o 0 12 1 185.89 182.91 29.84 o 1 12 1 488.55 496.46 44.31 o 2 12 1 5.97 22.31 32.42 o 3 12 1 2.49 19.87 39.74 o 4 12 1 145.51 114.05 65.49 o 5 12 1 69.29 69.28 73.04 o 6 12 1 0.01 62.19 76.99 o -6 13 1 5.95 7.01 23.49 o -5 13 1 8.93 138.03 66.92 o -4 13 1 7.05 7.67 14.74 o -3 13 1 45.35 76.93 44.67 o -2 13 1 75.00 49.01 34.04 o -1 13 1 220.11 158.16 36.30 o 0 13 1 358.09 423.99 36.98 o 1 13 1 66.45 103.39 34.05 o 2 13 1 39.13 90.15 34.23 o 3 13 1 200.32 228.04 48.43 o 4 13 1 72.90 118.24 61.52 o 5 13 1 0.21 44.16 66.50 o 6 13 1 15.23 12.26 18.64 o -5 14 1 3.91 47.10 67.62 o -4 14 1 27.63 43.62 60.24 o -3 14 1 0.01 68.45 47.12 o -2 14 1 1.14 25.27 17.27 o -1 14 1 101.09 75.91 34.76 o 0 14 1 38.23 30.33 27.98 o 1 14 1 75.85 31.89 32.46 o 2 14 1 75.13 30.55 41.20 o 3 14 1 15.96 48.47 47.79 o 4 14 1 35.66 27.15 13.85 o 5 14 1 0.53 5.84 11.78 o -5 15 1 1.22 35.76 73.96 o -4 15 1 2.13 17.54 61.04 o -3 15 1 3.21 70.43 50.17 o -2 15 1 94.40 122.12 41.54 o -1 15 1 0.03 11.12 12.06 o 0 15 1 0.25 5.90 18.29 o 1 15 1 43.83 10.87 36.89 o 2 15 1 8.24 17.01 40.11 o 3 15 1 0.17 20.27 24.37 o 4 15 1 0.01 105.60 63.15 o 5 15 1 13.11 22.44 18.19 o -4 16 1 10.51 50.46 59.87 o -3 16 1 8.40 6.83 22.65 o -2 16 1 6.04 31.25 23.41 o -1 16 1 0.43 22.56 15.25 o 0 16 1 1.60 4.44 21.72 o 1 16 1 55.37 53.28 36.05 o 2 16 1 0.40 9.11 20.21 o 3 16 1 28.42 14.41 56.64 o 4 16 1 19.59 24.84 19.53 o -4 17 1 19.79 6.78 63.92 o -3 17 1 0.76 5.30 20.51 o -2 17 1 6.50 59.65 41.91 o -1 17 1 1.30 22.56 36.62 o 0 17 1 54.30 103.30 33.38 o 1 17 1 0.03 25.81 38.19 o 2 17 1 32.32 15.90 47.37 o 3 17 1 10.01 41.64 51.00 o 4 17 1 0.01 135.87 71.93 o -3 18 1 10.58 44.99 60.06 o -2 18 1 22.79 46.63 48.88 o -1 18 1 24.80 59.67 41.72 o 0 18 1 0.12 25.79 30.49 o 1 18 1 3.10 17.24 20.00 o 2 18 1 8.66 4.24 44.66 o 3 18 1 19.89 28.22 57.85 o -1 19 1 9.41 72.19 38.15 o 0 19 1 10.19 14.60 16.77 o 1 19 1 6.77 3.90 20.43 o -8 0 2 24.21 33.72 96.85 o -7 0 2 216.82 141.89 88.02 o -6 0 2 463.20 438.97 74.45 o -5 0 2 1613.85 1781.40 92.59 o -4 0 2 105.83 141.57 38.31 o -3 0 2 537.00 534.61 34.11 o -2 0 2 2107.94 2314.44 54.93 o -1 0 2 287.25 288.51 16.34 o 0 0 2 6988.39 6637.09 114.97 o 1 0 2 13340.79 12811.65 225.07 o 2 0 2 507.65 505.50 27.11 o 3 0 2 2777.42 2938.45 73.02 o 4 0 2 163.61 150.87 42.70 o 5 0 2 5.14 52.37 46.79 o 6 0 2 224.31 274.71 69.53 o 7 0 2 14.49 85.15 72.69 o 8 0 2 63.11 153.64 92.71 o -8 1 2 31.48 221.19 92.35 o -7 1 2 0.80 49.29 22.63 o -6 1 2 333.61 186.18 72.30 o -5 1 2 74.72 156.60 50.89 o -4 1 2 1554.95 1624.11 69.28 o -3 1 2 71.94 34.17 24.90 o -2 1 2 2321.93 2537.62 58.81 o -1 1 2 3617.25 3635.77 74.26 o 0 1 2 7813.92 7363.85 134.31 o 1 1 2 5278.63 5544.94 111.77 o 2 1 2 3557.85 3677.04 83.24 o 3 1 2 553.84 577.71 36.69 o 4 1 2 1366.99 1331.94 65.55 o 5 1 2 1055.63 1055.56 77.94 o 6 1 2 44.43 13.84 59.94 o 7 1 2 259.85 466.59 92.00 o 8 1 2 172.50 60.29 111.27 o -8 2 2 22.39 43.27 88.69 o -7 2 2 139.58 133.47 92.04 o -6 2 2 65.79 117.72 63.75 o -5 2 2 826.66 929.75 77.84 o -4 2 2 75.93 18.84 20.64 o -3 2 2 3942.66 3935.26 95.77 o -2 2 2 2614.60 2736.34 68.45 o -1 2 2 7012.97 6936.91 133.56 o 0 2 2 6154.40 5915.38 143.07 o 1 2 2 21852.16 21737.03 329.11 o 2 2 2 2103.04 2216.56 53.76 o 3 2 2 191.26 208.30 28.33 o 4 2 2 26.33 67.13 35.63 o 5 2 2 0.42 10.90 19.06 o 6 2 2 301.23 397.12 74.65 o 7 2 2 72.71 67.59 75.31 o 8 2 2 57.00 96.44 96.51 o -8 3 2 2.36 6.52 22.28 o -7 3 2 84.88 1.10 13.60 o -6 3 2 333.08 410.73 75.14 o -5 3 2 113.15 33.71 49.53 o -4 3 2 2688.03 2891.35 93.82 o -3 3 2 2114.79 2080.99 60.86 o -2 3 2 2864.32 2839.16 66.99 o -1 3 2 11.89 14.29 16.73 o 0 3 2 235.70 239.61 16.88 o 1 3 2 4147.77 4221.64 97.53 o 2 3 2 8501.58 8656.09 171.88 o 3 3 2 164.92 184.30 30.65 o 4 3 2 21.49 66.07 35.98 o 5 3 2 79.75 112.83 47.29 o 6 3 2 18.58 65.42 62.26 o 7 3 2 252.75 428.34 85.76 o 8 3 2 40.14 26.88 90.93 o -8 4 2 15.87 45.41 91.30 o -7 4 2 25.90 38.81 25.11 o -6 4 2 125.53 236.07 68.20 o -5 4 2 1132.12 1127.73 83.58 o -4 4 2 449.42 427.86 54.67 o -3 4 2 380.33 401.58 35.73 o -2 4 2 2.00 35.44 22.36 o -1 4 2 487.45 481.54 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