#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:32:32 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180788 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/19/2011905.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011905_Fobs loop_ _publ_author_name 'N\"ather, Christian' 'Greve, Jan' _publ_section_title ; Poly[copper(I)-\m-bromo-\m-2,3-dimethylpyrazine-N:N'] ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 377 _journal_page_last 378 _journal_volume 57 _journal_year 2001 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.4588 _cell_length_b 9.7078 _cell_length_c 13.4681 _exptl_crystal_F_000 976.00 _reflns_d_resolution_high 0.7100 _cod_data_source_file sk1444Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' CuBr-2,3-Dimethylpyrazin in Pbca (JG267)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 362.69 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 112694.68 121008.42 446.85 o 4 0 0 131542.78 130656.58 522.68 o 6 0 0 46273.45 45375.31 258.13 o 8 0 0 6399.01 6131.02 101.06 o 10 0 0 12631.88 11719.83 157.92 o 12 0 0 1319.16 1368.56 40.86 o 14 0 0 81.36 27.64 85.74 o 16 0 0 138.10 65.03 93.48 o 2 1 0 40.14 62.52 7.39 o 4 1 0 0.47 28.58 12.56 o 6 1 0 2576.77 2446.09 82.53 o 8 1 0 421.75 442.37 18.31 o 10 1 0 15.68 48.53 20.18 o 12 1 0 206.86 245.89 24.84 o 14 1 0 448.03 464.94 59.92 o 16 1 0 97.33 126.48 33.51 o 0 2 0 8140.14 7837.39 59.21 o 2 2 0 1307.82 1568.54 33.01 o 4 2 0 2657.08 2918.00 49.95 o 6 2 0 6632.45 6653.07 92.66 o 8 2 0 3518.11 3422.59 82.28 o 10 2 0 2453.54 2302.67 59.15 o 12 2 0 4597.45 4314.55 120.11 o 14 2 0 1863.53 1790.91 54.66 o 2 3 0 2054.19 1906.37 41.02 o 4 3 0 8335.92 8433.15 87.23 o 6 3 0 31986.31 32259.51 216.63 o 8 3 0 17950.85 18104.85 177.38 o 10 3 0 4703.24 4702.26 110.19 o 12 3 0 1641.54 1765.78 56.37 o 14 3 0 148.81 -32.47 91.87 o 0 4 0 5004.38 5734.56 70.12 o 2 4 0 2396.93 2784.26 53.93 o 4 4 0 1007.45 1050.58 30.20 o 6 4 0 550.27 669.48 23.34 o 8 4 0 158.91 187.48 26.74 o 10 4 0 2.47 8.24 30.05 o 12 4 0 60.90 -4.02 74.48 o 14 4 0 232.25 352.74 45.44 o 2 5 0 407.50 296.60 17.80 o 4 5 0 6616.52 6866.55 95.20 o 6 5 0 7357.21 7820.70 111.70 o 8 5 0 8057.36 8285.25 126.54 o 10 5 0 2388.38 2342.11 66.38 o 12 5 0 680.42 673.88 42.84 o 14 5 0 451.14 409.70 46.25 o 0 6 0 674.05 756.57 26.16 o 2 6 0 140.65 144.76 20.51 o 4 6 0 3129.36 3621.74 78.42 o 6 6 0 4358.44 4611.14 96.37 o 8 6 0 3281.47 3538.07 96.41 o 10 6 0 6212.43 6493.83 137.16 o 12 6 0 2540.36 2448.02 73.32 o 14 6 0 2986.96 3116.39 97.01 o 2 7 0 826.63 874.01 29.98 o 4 7 0 65.30 59.81 25.23 o 6 7 0 2006.47 2047.28 55.30 o 8 7 0 684.37 754.09 34.80 o 10 7 0 601.66 656.75 39.12 o 12 7 0 601.72 653.30 45.95 o 0 8 0 39058.83 37991.94 277.24 o 2 8 0 30261.64 29033.34 241.12 o 4 8 0 23564.58 25124.62 229.51 o 6 8 0 11639.16 12319.55 164.28 o 8 8 0 3959.61 4126.59 115.49 o 10 8 0 1459.48 1517.07 54.74 o 12 8 0 75.67 56.29 88.85 o 2 9 0 292.85 243.60 32.17 o 4 9 0 233.26 204.47 30.96 o 6 9 0 534.48 491.11 36.00 o 8 9 0 92.13 68.25 75.69 o 10 9 0 68.31 51.76 81.41 o 12 9 0 6.49 25.93 98.80 o 0 10 0 1901.76 1586.01 53.57 o 2 10 0 1492.26 1271.06 42.57 o 4 10 0 626.37 564.05 38.72 o 6 10 0 526.40 587.22 37.71 o 8 10 0 335.01 366.94 43.63 o 10 10 0 265.32 322.99 44.23 o 2 11 0 408.63 383.06 40.92 o 4 11 0 1516.65 1575.03 54.44 o 6 11 0 374.85 497.85 45.84 o 8 11 0 767.75 940.99 52.80 o 0 12 0 1281.52 1126.14 49.90 o 2 12 0 860.85 799.07 45.96 o 4 12 0 571.95 521.96 44.75 o 6 12 0 244.45 339.17 47.35 o 2 13 0 118.39 85.74 102.63 o 4 13 0 234.11 271.11 49.56 o 1 1 1 44426.80 44255.38 1028.20 o 2 1 1 385.84 435.16 18.45 o 3 1 1 40018.15 40398.43 836.91 o 4 1 1 3364.92 3174.71 85.18 o 5 1 1 8933.91 8239.79 131.74 o 6 1 1 12096.12 11470.33 164.85 o 7 1 1 4404.11 4043.83 80.88 o 8 1 1 9148.49 8691.71 126.77 o 9 1 1 20.41 15.65 20.69 o 10 1 1 713.18 695.46 23.08 o 11 1 1 26.30 55.30 15.90 o 12 1 1 141.58 139.88 16.84 o 13 1 1 529.79 634.08 27.23 o 14 1 1 4.91 -44.25 44.25 o 15 1 1 452.35 452.06 24.44 o 16 1 1 18.11 24.75 36.65 o 0 2 1 35196.25 35185.20 1441.38 o 1 2 1 224.68 264.08 10.16 o 2 2 1 3719.72 4141.23 96.68 o 3 2 1 1673.33 1656.20 26.48 o 4 2 1 388.87 494.50 46.17 o 5 2 1 2937.17 2848.09 41.51 o 6 2 1 585.92 695.22 15.88 o 7 2 1 2880.95 2743.79 50.77 o 8 2 1 3552.17 3477.44 60.74 o 9 2 1 674.87 685.01 32.24 o 10 2 1 17.18 43.14 19.36 o 11 2 1 67.60 87.91 20.75 o 12 2 1 3558.59 3532.39 79.42 o 13 2 1 64.32 41.93 35.24 o 14 2 1 1261.35 1302.77 39.29 o 15 2 1 224.77 216.96 33.44 o 1 3 1 43014.70 44202.04 554.95 o 2 3 1 1093.64 1270.75 32.80 o 3 3 1 14743.48 15483.60 80.23 o 4 3 1 783.95 863.16 18.64 o 5 3 1 26277.38 28240.79 380.03 o 6 3 1 99.42 120.09 16.69 o 7 3 1 7480.73 7109.84 74.09 o 8 3 1 287.14 306.18 18.59 o 9 3 1 9135.11 9055.59 334.35 o 10 3 1 136.81 137.92 20.64 o 11 3 1 3516.75 3223.81 136.59 o 12 3 1 123.45 125.51 24.68 o 13 3 1 1093.09 1109.16 80.78 o 14 3 1 2.99 25.48 36.33 o 15 3 1 973.78 947.16 45.56 o 0 4 1 23933.01 23483.85 703.81 o 1 4 1 3040.89 3071.25 71.93 o 2 4 1 22254.88 22476.31 106.15 o 3 4 1 5802.52 5766.26 114.54 o 4 4 1 3897.14 3673.26 109.77 o 5 4 1 12810.24 13362.58 90.61 o 6 4 1 1027.02 1055.75 27.48 o 7 4 1 13905.19 14181.96 232.35 o 8 4 1 1166.95 1242.26 29.17 o 9 4 1 6638.50 6729.97 87.07 o 10 4 1 4.16 13.88 44.34 o 11 4 1 4457.45 4397.56 168.59 o 12 4 1 232.73 246.97 26.87 o 13 4 1 924.34 974.71 31.47 o 14 4 1 738.73 828.68 35.02 o 15 4 1 198.56 174.40 77.40 o 1 5 1 3629.65 3816.12 60.37 o 2 5 1 467.28 510.75 20.92 o 3 5 1 9578.25 9829.12 76.04 o 4 5 1 12.26 17.56 16.33 o 5 5 1 5997.36 6397.45 131.89 o 6 5 1 2813.34 3152.04 55.36 o 7 5 1 8726.85 9561.45 92.22 o 8 5 1 565.66 584.23 21.97 o 9 5 1 4489.93 4794.04 77.22 o 10 5 1 75.53 5.36 45.91 o 11 5 1 3768.59 3949.18 85.69 o 12 5 1 31.48 29.44 53.90 o 13 5 1 2687.32 2706.73 60.36 o 14 5 1 163.24 76.02 69.19 o 0 6 1 19.35 73.00 30.66 o 1 6 1 0.33 16.70 12.31 o 2 6 1 430.31 476.08 20.21 o 3 6 1 104.87 95.22 39.45 o 4 6 1 425.63 475.95 18.51 o 5 6 1 12.19 22.27 20.66 o 6 6 1 665.88 674.06 22.53 o 7 6 1 69.82 91.14 18.55 o 8 6 1 252.71 301.09 20.58 o 9 6 1 2.35 17.15 31.21 o 10 6 1 290.76 337.40 23.71 o 11 6 1 32.52 28.05 53.87 o 12 6 1 570.38 596.00 31.42 o 13 6 1 58.63 61.03 63.07 o 14 6 1 127.33 13.98 54.83 o 1 7 1 10814.18 10248.49 125.60 o 2 7 1 439.18 418.76 24.59 o 3 7 1 6079.21 6235.16 88.19 o 4 7 1 1524.10 1559.88 34.77 o 5 7 1 2532.27 2766.09 117.17 o 6 7 1 2199.33 2178.76 40.02 o 7 7 1 372.50 450.67 27.95 o 8 7 1 1631.12 1747.98 45.95 o 9 7 1 0.56 20.65 46.05 o 10 7 1 656.48 740.42 27.66 o 11 7 1 207.24 227.15 39.00 o 12 7 1 122.11 211.72 52.52 o 13 7 1 354.37 332.93 43.78 o 0 8 1 823.78 812.19 23.05 o 1 8 1 79.15 106.48 24.88 o 2 8 1 1892.56 1874.38 80.22 o 3 8 1 94.55 117.92 19.56 o 4 8 1 328.44 337.89 20.79 o 5 8 1 642.77 617.21 23.14 o 6 8 1 117.99 105.30 30.10 o 7 8 1 1012.85 990.13 26.46 o 8 8 1 48.43 40.25 45.75 o 9 8 1 190.03 208.92 24.52 o 10 8 1 70.64 73.98 26.37 o 11 8 1 86.37 72.95 29.10 o 12 8 1 8.31 -65.49 65.49 o 13 8 1 0.56 -32.98 82.82 o 1 9 1 5063.01 5088.52 74.09 o 2 9 1 22.02 63.00 20.82 o 3 9 1 4700.99 4982.33 81.07 o 4 9 1 754.35 827.56 26.53 o 5 9 1 2535.11 2713.66 49.43 o 6 9 1 12.70 8.99 46.47 o 7 9 1 1418.61 1412.68 34.23 o 8 9 1 224.79 255.48 30.26 o 9 9 1 356.67 337.06 39.91 o 10 9 1 119.62 180.57 80.31 o 11 9 1 88.77 60.51 31.41 o 12 9 1 28.92 -8.63 66.38 o 0 10 1 35.19 68.08 29.80 o 1 10 1 1.94 25.31 31.73 o 2 10 1 36.65 61.70 29.81 o 3 10 1 146.50 115.18 42.52 o 4 10 1 13.11 49.17 29.20 o 5 10 1 287.83 306.53 26.19 o 6 10 1 54.51 51.59 45.68 o 7 10 1 168.13 157.79 26.97 o 8 10 1 611.82 623.58 30.93 o 9 10 1 138.52 109.27 85.89 o 10 10 1 291.88 310.60 65.29 o 1 11 1 7420.87 6794.91 73.87 o 2 11 1 55.46 16.68 34.54 o 3 11 1 4694.47 4542.50 93.39 o 4 11 1 4.72 11.53 54.81 o 5 11 1 4024.24 4040.85 75.90 o 6 11 1 474.53 432.56 30.78 o 7 11 1 1730.80 1696.03 40.27 o 8 11 1 72.90 -11.97 65.77 o 9 11 1 1259.78 1233.10 38.59 o 0 12 1 74.75 133.69 43.57 o 1 12 1 26.28 -20.80 41.53 o 2 12 1 891.24 863.03 32.47 o 3 12 1 213.00 216.32 30.63 o 4 12 1 729.47 787.57 34.41 o 5 12 1 483.72 590.91 92.70 o 6 12 1 301.16 271.24 34.63 o 7 12 1 469.62 571.60 37.25 o 1 13 1 445.99 406.95 24.87 o 2 13 1 57.09 -10.42 94.23 o 3 13 1 612.28 603.17 36.79 o 4 13 1 82.27 -3.51 70.85 o 0 0 2 6479.48 7211.49 45.95 o 1 0 2 12109.09 12494.36 252.24 o 2 0 2 51316.11 53115.85 226.39 o 3 0 2 9016.49 9021.00 76.18 o 4 0 2 43046.39 47027.42 234.53 o 5 0 2 30739.45 31618.86 190.64 o 6 0 2 15147.49 16086.55 138.42 o 7 0 2 27899.65 28504.29 207.28 o 8 0 2 7295.51 7159.75 110.80 o 9 0 2 11679.61 11871.38 149.27 o 10 0 2 125.28 174.40 28.85 o 11 0 2 8009.16 7631.39 141.83 o 12 0 2 1462.46 1361.88 42.97 o 13 0 2 838.88 787.23 44.25 o 14 0 2 564.38 567.21 43.74 o 15 0 2 252.57 280.97 44.53 o 16 0 2 4.69 100.20 100.20 o 1 1 2 133.73 188.78 6.65 o 2 1 2 4.07 71.01 8.85 o 3 1 2 5781.18 6209.28 89.70 o 4 1 2 132.61 200.71 12.01 o 5 1 2 1070.77 1051.76 21.29 o 6 1 2 1434.58 1507.75 29.96 o 7 1 2 5893.44 5972.33 68.63 o 8 1 2 703.01 641.11 20.41 o 9 1 2 3561.92 3687.56 140.29 o 10 1 2 326.07 363.29 43.03 o 11 1 2 2139.53 2055.14 64.91 o 12 1 2 285.83 341.52 38.60 o 13 1 2 2489.84 2474.07 54.34 o 14 1 2 132.06 147.92 85.64 o 15 1 2 578.29 575.80 37.10 o 0 2 2 10102.26 9527.79 75.88 o 1 2 2 10340.49 9749.80 444.25 o 2 2 2 28672.38 26154.48 149.60 o 3 2 2 229.73 185.04 13.17 o 4 2 2 3638.98 3285.88 57.53 o 5 2 2 4099.58 3882.28 67.84 o 6 2 2 4196.12 4081.56 75.07 o 7 2 2 3990.31 3919.93 82.17 o 8 2 2 6621.50 6491.52 108.74 o 9 2 2 411.83 410.56 31.98 o 10 2 2 2249.38 2118.24 59.44 o 11 2 2 1495.59 1453.42 51.74 o 12 2 2 1678.15 1627.86 49.83 o 13 2 2 45.10 88.55 36.48 o 14 2 2 100.16 84.63 40.21 o 15 2 2 6.62 17.79 93.27 o 1 3 2 61650.27 60442.27 988.00 o 2 3 2 3833.32 4175.26 57.91 o 3 3 2 29151.04 30190.42 177.33 o 4 3 2 2468.11 2805.01 55.64 o 5 3 2 11924.01 11354.75 115.50 o 6 3 2 224.78 126.18 20.11 o 7 3 2 1476.28 1714.79 44.61 o 8 3 2 139.67 156.61 27.34 o 9 3 2 32.13 32.97 27.24 o 10 3 2 1086.80 938.26 35.72 o 11 3 2 436.51 393.64 33.99 o 12 3 2 351.06 307.14 37.90 o 13 3 2 1447.34 1401.35 48.70 o 14 3 2 82.29 -12.36 90.66 o 15 3 2 689.49 723.42 48.97 o 0 4 2 762.04 737.58 25.67 o 1 4 2 24.35 42.68 10.02 o 2 4 2 2706.49 2950.25 57.19 o 3 4 2 310.39 333.66 17.80 o 4 4 2 66.83 76.39 16.59 o 5 4 2 972.59 973.61 32.01 o 6 4 2 65.85 78.50 21.31 o 7 4 2 2058.77 1978.92 50.89 o 8 4 2 474.87 408.17 30.87 o 9 4 2 504.78 508.63 30.87 o 10 4 2 148.11 184.66 32.17 o 11 4 2 2.03 -70.96 70.96 o 12 4 2 94.29 66.24 70.46 o 13 4 2 19.60 15.08 80.81 o 14 4 2 2.08 37.99 42.11 o 15 4 2 21.49 41.71 100.91 o 1 5 2 21503.72 21171.85 196.23 o 2 5 2 1303.44 1350.16 37.37 o 3 5 2 23668.99 24449.39 181.63 o 4 5 2 167.39 173.62 21.41 o 5 5 2 5737.47 5819.21 92.57 o 6 5 2 739.30 787.49 27.77 o 7 5 2 3571.96 3829.26 90.93 o 8 5 2 40.69 6.63 54.28 o 9 5 2 32.26 -32.36 59.30 o 10 5 2 527.90 569.35 35.50 o 11 5 2 27.83 55.98 69.65 o 12 5 2 293.83 218.75 39.41 o 13 5 2 20.48 63.42 83.72 o 14 5 2 2.79 4.02 91.16 o 0 6 2 7062.15 6712.53 97.18 o 1 6 2 790.68 815.10 19.07 o 2 6 2 7726.35 7985.52 108.20 o 3 6 2 990.53 922.07 28.58 o 4 6 2 3946.82 4016.40 85.87 o 5 6 2 4133.70 4212.46 90.31 o 6 6 2 3265.34 3374.86 85.35 o 7 6 2 5633.65 5993.18 111.74 o 8 6 2 4046.50 4283.35 103.54 o 9 6 2 1067.92 1111.63 38.84 o 10 6 2 1664.01 1698.90 59.09 o 11 6 2 515.23 503.56 41.13 o 12 6 2 1253.24 1272.91 49.50 o 13 6 2 1.02 11.96 41.21 o 14 6 2 323.54 331.65 48.86 o 1 7 2 9471.32 9218.56 100.33 o 2 7 2 9.45 -28.64 53.17 o 3 7 2 3248.87 3020.64 84.05 o 4 7 2 892.53 951.77 33.70 o 5 7 2 3387.01 3398.49 92.91 o 6 7 2 195.33 203.36 28.15 o 7 7 2 1141.41 1278.09 39.85 o 8 7 2 623.66 642.31 34.80 o 9 7 2 1543.84 1660.88 54.15 o 10 7 2 319.67 343.12 35.59 o 11 7 2 411.10 341.33 43.63 o 12 7 2 175.59 240.95 42.72 o 13 7 2 6.35 -39.10 95.18 o 0 8 2 7747.25 7830.21 127.14 o 1 8 2 55.98 -7.51 41.65 o 2 8 2 11475.25 11794.59 154.61 o 3 8 2 2378.72 2406.19 57.84 o 4 8 2 5753.57 6073.41 116.18 o 5 8 2 3695.14 3650.39 100.18 o 6 8 2 3939.55 4399.37 107.65 o 7 8 2 2886.67 3022.15 99.97 o 8 8 2 2564.38 2710.06 71.93 o 9 8 2 3258.33 3589.70 83.05 o 10 8 2 575.82 643.84 42.33 o 11 8 2 1025.94 1129.20 48.89 o 12 8 2 562.50 578.76 49.17 o 1 9 2 49.97 31.18 43.10 o 2 9 2 63.32 104.53 29.45 o 3 9 2 384.75 434.45 33.28 o 4 9 2 6.57 45.23 31.96 o 5 9 2 576.80 640.87 36.00 o 6 9 2 178.09 163.45 33.98 o 7 9 2 1176.80 1275.43 44.97 o 8 9 2 11.51 -80.00 80.00 o 9 9 2 715.14 788.02 41.94 o 10 9 2 217.34 232.51 40.61 o 11 9 2 931.04 966.55 51.90 o 12 9 2 108.09 142.43 47.04 o 0 10 2 1352.22 1099.92 42.97 o 1 10 2 1.74 110.21 75.38 o 2 10 2 1434.52 1368.80 45.19 o 3 10 2 7.00 64.83 31.76 o 4 10 2 1590.64 1468.77 47.61 o 5 10 2 8.16 -76.89 76.89 o 6 10 2 1021.85 1050.80 44.56 o 7 10 2 150.34 0.00 86.55 o 8 10 2 481.28 506.14 44.24 o 9 10 2 2.23 -89.35 89.35 o 10 10 2 161.60 133.79 44.23 o 1 11 2 1715.30 1587.77 35.13 o 2 11 2 7.12 44.73 38.09 o 3 11 2 1080.67 1044.41 45.97 o 4 11 2 13.55 -82.72 82.72 o 5 11 2 308.61 392.07 40.82 o 6 11 2 212.75 292.22 42.12 o 7 11 2 78.03 -59.40 95.49 o 8 11 2 195.01 244.06 49.86 o 9 11 2 0.16 -26.23 98.80 o 0 12 2 154.32 118.01 41.92 o 1 12 2 100.95 123.19 67.19 o 2 12 2 422.87 423.78 46.95 o 3 12 2 223.81 50.76 89.77 o 4 12 2 146.28 115.80 44.23 o 5 12 2 241.33 260.86 45.64 o 6 12 2 93.84 129.86 47.24 o 7 12 2 226.50 164.15 52.98 o 1 13 2 630.19 679.43 35.84 o 2 13 2 27.62 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3 6562.33 5762.25 241.02 o 2 3 3 80.82 82.23 13.17 o 3 3 3 17250.34 16366.54 130.82 o 4 3 3 17.65 -25.93 34.57 o 5 3 3 4105.38 3987.92 73.34 o 6 3 3 232.57 308.15 21.92 o 7 3 3 5225.69 4974.55 98.46 o 8 3 3 164.15 192.40 27.74 o 9 3 3 712.85 720.58 33.49 o 10 3 3 234.64 315.46 31.97 o 11 3 3 226.09 182.76 34.58 o 12 3 3 78.92 31.26 73.88 o 13 3 3 675.81 643.50 42.14 o 14 3 3 252.58 327.41 41.62 o 15 3 3 8.06 -45.23 95.88 o 0 4 3 86963.91 80082.95 376.34 o 1 4 3 4237.82 4456.46 209.85 o 2 4 3 60711.26 58676.30 302.05 o 3 4 3 125.18 179.54 18.20 o 4 4 3 52762.27 54615.09 297.82 o 5 4 3 769.51 767.82 26.06 o 6 4 3 21478.13 20755.42 184.48 o 7 4 3 1413.30 1393.10 44.40 o 8 4 3 2955.47 2907.46 87.83 o 9 4 3 96.07 114.59 27.24 o 10 4 3 728.27 677.89 35.60 o 11 4 3 354.28 392.60 36.70 o 12 4 3 24.88 29.35 75.58 o 13 4 3 407.64 410.20 42.93 o 14 4 3 0.52 76.79 90.56 o 15 4 3 101.77 78.70 46.14 o 1 5 3 20914.34 20790.16 259.19 o 2 5 3 1396.87 1465.78 37.87 o 3 5 3 7569.17 7448.04 100.63 o 4 5 3 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