#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/19/2011912.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011912_Fobs loop_ _publ_author_name 'Bolte, Michael' 'Degen, Alexander' 'R\"uhl, Stephan' _publ_section_title ; Two diastereomers of 9-(2,6-dichlorophenyl)-4a-hydroxy-3,3,6,6-tetramethyl-1,2,3,4,4a,5,6,7,8,9a-decahydroxanthene-1,8-dione in the same crystal ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 444 _journal_page_last 445 _journal_volume 57 _journal_year 2001 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 74.500 _cell_angle_beta 90.160 _cell_angle_gamma 65.500 _cell_length_a 11.9360 _cell_length_b 12.9690 _cell_length_c 16.2040 _exptl_crystal_F_000 920.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file sk1447IIsup2.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' rd5 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 182.07 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 33003.78 26575.97 607.37 o 2 0 0 12829.24 11061.90 283.49 o 3 0 0 1737.19 1575.75 45.48 o 4 0 0 4343.33 3753.04 139.95 o 5 0 0 2550.04 2705.72 77.11 o 6 0 0 1100.07 1181.03 39.51 o 7 0 0 8.17 -11.72 11.72 o 8 0 0 353.36 349.67 21.46 o 9 0 0 113.74 130.67 25.72 o 10 0 0 121.41 160.72 27.76 o 11 0 0 112.51 138.65 36.56 o 12 0 0 4.63 41.32 32.42 o 13 0 0 0.19 81.29 43.30 o -13 1 0 12.18 -2.52 49.93 o -12 1 0 74.57 44.21 33.90 o -11 1 0 0.15 -3.67 28.68 o -10 1 0 530.76 595.41 38.71 o -9 1 0 101.95 74.03 23.00 o -8 1 0 43.47 16.92 22.05 o -7 1 0 55.49 32.31 13.69 o -6 1 0 58.81 57.85 19.64 o -5 1 0 254.42 183.40 16.41 o -4 1 0 832.07 795.17 29.90 o -3 1 0 517.87 383.18 20.48 o -2 1 0 2038.97 2058.52 80.19 o -1 1 0 34.67 28.56 4.68 o 0 1 0 4398.90 4687.46 127.12 o 1 1 0 1091.05 1104.54 40.55 o 2 1 0 2.42 0.03 4.06 o 3 1 0 2182.32 1739.66 49.00 o 4 1 0 2852.63 2527.93 82.97 o 5 1 0 685.82 699.15 28.88 o 6 1 0 2457.95 2459.80 86.10 o 7 1 0 53.66 60.24 12.20 o 8 1 0 157.31 166.51 16.56 o 9 1 0 9.58 38.96 20.07 o 10 1 0 981.81 1000.81 63.20 o 11 1 0 97.58 95.61 33.58 o 12 1 0 112.27 185.98 37.63 o 13 1 0 30.95 110.89 39.95 o 14 1 0 45.70 94.96 56.01 o -13 2 0 139.56 114.87 59.44 o -12 2 0 0.02 40.03 47.58 o -11 2 0 89.31 82.51 34.35 o -10 2 0 20.79 -3.28 26.58 o -9 2 0 80.35 59.54 25.71 o -8 2 0 357.05 374.45 24.78 o -7 2 0 961.18 1061.26 39.28 o -6 2 0 4.62 14.49 14.65 o -5 2 0 145.34 137.26 12.55 o -4 2 0 4631.78 4830.65 131.19 o -3 2 0 2570.53 2607.27 73.44 o -2 2 0 16.59 15.40 6.68 o -1 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67.23 11.65 o 7 3 0 123.72 108.07 11.90 o 8 3 0 298.44 265.90 17.41 o 9 3 0 0.12 -18.11 23.50 o 10 3 0 189.30 222.56 70.75 o 11 3 0 83.37 90.17 27.36 o 12 3 0 0.01 43.01 27.08 o 13 3 0 85.73 71.20 32.47 o 14 3 0 0.22 -16.15 34.36 o -11 4 0 206.89 214.89 50.02 o -10 4 0 165.34 251.06 31.56 o -9 4 0 5.60 12.83 25.74 o -8 4 0 113.02 85.51 25.07 o -7 4 0 31.94 53.57 16.15 o -6 4 0 131.38 149.90 16.55 o -5 4 0 122.13 112.86 14.36 o -4 4 0 68.67 42.35 10.88 o -3 4 0 188.69 177.00 11.25 o -2 4 0 373.02 447.41 19.27 o -1 4 0 2068.35 2483.11 70.71 o 0 4 0 5818.90 7119.82 187.33 o 1 4 0 6759.26 8237.57 215.11 o 2 4 0 1346.80 1765.44 51.73 o 3 4 0 470.63 417.48 28.93 o 4 4 0 83.81 57.76 8.76 o 5 4 0 535.11 444.70 37.66 o 6 4 0 14.22 40.33 10.72 o 7 4 0 1329.72 1328.51 48.37 o 8 4 0 23.50 8.48 12.00 o 9 4 0 78.03 108.24 18.76 o 10 4 0 153.35 119.47 22.42 o 11 4 0 119.31 108.58 27.29 o 12 4 0 92.30 56.34 28.11 o 13 4 0 143.49 234.10 38.37 o 14 4 0 113.17 101.67 40.55 o 15 4 0 38.98 30.10 41.48 o 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