#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2011942.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011942_Fobs loop_ _publ_author_name 'Mazumder, G.' 'De, M.' 'Mazumder, S. K.' 'Mukhopadhyay, A.' _publ_section_title ; Oxonium 5-aminouracil-6-sulfonate hydrate ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 562 _journal_page_last 563 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.260 _cell_angle_gamma 90.000 _cell_length_a 10.5790 _cell_length_b 12.1040 _cell_length_c 7.0030 _exptl_crystal_F_000 504.00 _reflns_d_resolution_high 0.8218 _[local]_cod_data_source_file bm1438Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sulphaminouracil p21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 116.88 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y+1/2, z+1/2' '-x, -y, -z' '-x, y-1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2161.03 1996.71 10.71 o 2 0 0 609.84 531.99 3.64 o 3 0 0 7691.67 6256.92 33.98 o 4 0 0 13662.04 12840.38 87.13 o 5 0 0 1554.50 1352.62 9.05 o 6 0 0 681.16 757.44 5.22 o 8 0 0 1148.59 1064.87 7.91 o 9 0 0 26.25 31.17 1.52 o 10 0 0 93.80 107.67 2.48 o 12 0 0 57.00 41.12 1.53 o 1 1 0 243.08 255.65 1.66 o 3 1 0 228.46 190.73 1.42 o 4 1 0 7508.88 7358.81 43.95 o 5 1 0 436.70 508.95 3.87 o 6 1 0 42.38 22.01 0.96 o 7 1 0 55.96 41.99 1.43 o 8 1 0 95.42 72.88 2.04 o 9 1 0 59.07 51.03 1.82 o 10 1 0 1.07 6.34 1.33 o 11 1 0 5.17 12.41 1.44 o 12 1 0 4.18 0.89 1.12 o 0 2 0 6980.49 6639.82 65.80 o 2 2 0 1714.95 1424.01 9.55 o 3 2 0 2363.77 2304.31 15.68 o 4 2 0 936.86 844.04 6.07 o 5 2 0 3312.59 3376.10 23.15 o 6 2 0 1181.43 965.58 6.48 o 7 2 0 292.76 326.31 3.40 o 8 2 0 245.11 250.15 3.78 o 9 2 0 1.16 3.38 1.25 o 10 2 0 1.19 3.16 1.36 o 11 2 0 473.18 453.52 4.38 o 1 3 0 521.28 389.97 3.08 o 2 3 0 166.51 113.57 1.28 o 3 3 0 2705.42 2346.13 16.71 o 4 3 0 15.33 5.40 0.55 o 5 3 0 624.42 625.15 4.31 o 6 3 0 158.10 125.28 2.10 o 7 3 0 39.16 54.72 1.64 o 8 3 0 80.26 105.52 2.45 o 9 3 0 312.50 356.20 4.52 o 10 3 0 90.98 83.87 2.34 o 11 3 0 224.91 215.22 3.01 o 12 3 0 132.46 114.98 2.01 o 0 4 0 2713.78 2966.29 32.90 o 1 4 0 746.15 697.82 5.05 o 2 4 0 325.05 285.23 2.03 o 3 4 0 1470.19 1276.91 8.80 o 4 4 0 177.73 141.69 2.03 o 6 4 0 322.03 303.35 3.28 o 7 4 0 661.41 692.11 5.43 o 8 4 0 1908.03 1974.39 14.00 o 9 4 0 49.16 39.05 1.81 o 10 4 0 1.43 1.74 1.32 o 11 4 0 95.99 109.14 2.14 o 12 4 0 19.12 16.83 0.84 o 2 5 0 27.27 13.03 0.68 o 3 5 0 1800.57 1573.00 10.49 o 5 5 0 1453.50 1379.31 9.72 o 7 5 0 591.58 559.55 4.87 o 8 5 0 157.62 156.07 2.98 o 9 5 0 109.71 121.21 2.63 o 10 5 0 3.95 4.42 1.36 o 11 5 0 5.11 8.17 1.26 o 1 6 0 981.49 822.23 5.97 o 2 6 0 137.26 164.40 2.19 o 3 6 0 3263.75 2921.41 20.44 o 5 6 0 42.50 63.90 1.63 o 6 6 0 26.12 35.90 1.53 o 7 6 0 8.57 10.95 1.13 o 8 6 0 270.97 281.47 4.01 o 9 6 0 130.90 142.63 2.85 o 10 6 0 13.81 19.50 1.13 o 11 6 0 133.71 116.98 2.03 o 1 7 0 439.37 401.15 3.44 o 2 7 0 355.33 381.14 3.34 o 3 7 0 12.80 13.64 1.07 o 4 7 0 165.95 174.62 2.71 o 6 7 0 1730.42 1680.78 12.17 o 7 7 0 0.99 1.54 0.99 o 9 7 0 582.10 631.14 6.04 o 10 7 0 76.90 95.97 2.00 o 0 8 0 788.22 899.38 8.79 o 1 8 0 19.43 22.39 1.13 o 2 8 0 31.99 25.05 1.28 o 3 8 0 1143.35 1047.98 7.85 o 4 8 0 0.76 1.59 1.35 o 5 8 0 912.53 877.11 6.64 o 6 8 0 60.35 67.80 2.10 o 7 8 0 233.98 233.81 3.66 o 8 8 0 533.36 585.16 5.81 o 9 8 0 29.11 29.67 1.39 o 10 8 0 209.04 234.32 2.88 o 1 9 0 377.37 426.19 4.24 o 2 9 0 358.91 353.34 3.86 o 3 9 0 36.20 35.81 1.63 o 4 9 0 201.80 207.99 3.45 o 5 9 0 137.81 127.98 2.70 o 6 9 0 509.23 507.61 5.41 o 7 9 0 2.91 1.17 1.47 o 8 9 0 23.08 23.20 1.23 o 9 9 0 89.80 107.54 2.12 o 0 10 0 905.84 931.32 10.00 o 1 10 0 420.43 425.83 4.95 o 2 10 0 466.74 464.36 5.17 o 3 10 0 1195.10 1111.74 8.09 o 4 10 0 31.21 35.19 1.51 o 5 10 0 183.60 183.99 3.24 o 6 10 0 193.23 219.17 3.54 o 7 10 0 60.27 62.31 1.88 o 8 10 0 67.73 59.55 1.71 o 9 10 0 15.05 16.00 0.95 o 1 11 0 28.18 24.79 1.44 o 2 11 0 126.07 126.58 2.88 o 3 11 0 101.94 103.32 2.60 o 4 11 0 237.73 232.81 3.65 o 5 11 0 2.48 3.10 1.20 o 7 11 0 81.79 83.10 1.86 o 8 11 0 24.88 33.89 1.19 o 0 12 0 918.37 980.11 10.26 o 1 12 0 0.58 0.71 1.02 o 2 12 0 1.05 4.10 1.00 o 3 12 0 416.76 381.86 4.69 o 4 12 0 43.80 37.99 1.57 o 5 12 0 264.87 228.78 3.10 o 6 12 0 1.31 1.20 1.06 o 7 12 0 2.08 4.27 0.70 o 1 13 0 22.47 19.43 1.28 o 2 13 0 559.86 517.39 4.69 o 3 13 0 78.42 66.04 1.94 o 4 13 0 9.39 7.84 0.86 o 5 13 0 16.03 10.73 0.89 o 0 14 0 62.94 51.67 2.08 o 1 14 0 5.75 6.96 0.85 o 2 14 0 119.85 90.40 1.95 o 3 14 0 15.41 9.59 0.79 o -12 1 1 168.60 185.95 2.79 o -11 1 1 469.89 482.56 5.27 o -10 1 1 18.49 27.74 1.61 o -9 1 1 10.38 13.26 1.61 o -8 1 1 313.68 310.52 3.62 o -7 1 1 432.34 443.44 3.97 o -6 1 1 760.65 642.47 4.81 o -5 1 1 103.62 77.58 1.35 o -4 1 1 2982.74 2536.06 19.29 o -3 1 1 4493.31 3862.38 26.18 o -2 1 1 309.71 315.97 2.15 o -1 1 1 5478.81 5510.94 35.57 o 0 1 1 574.97 662.90 4.52 o 1 1 1 983.75 1053.56 6.92 o 2 1 1 7942.88 8441.41 56.92 o 4 1 1 4243.24 3839.59 26.39 o 5 1 1 1442.05 1291.11 9.43 o 6 1 1 61.01 56.93 1.41 o 7 1 1 1197.38 1256.06 9.22 o 8 1 1 366.18 401.15 4.80 o 9 1 1 351.76 336.56 4.39 o 10 1 1 334.51 373.52 4.63 o 11 1 1 1.27 2.84 1.35 o 12 1 1 319.48 298.87 2.96 o -12 2 1 28.44 33.20 1.28 o -11 2 1 69.58 80.27 2.14 o -10 2 1 6.56 2.56 1.55 o -9 2 1 1283.68 1307.64 9.41 o -8 2 1 239.89 234.71 3.14 o -7 2 1 448.78 469.60 4.09 o -6 2 1 707.19 561.83 4.09 o -5 2 1 1093.30 859.87 6.12 o -4 2 1 455.31 457.45 3.31 o -3 2 1 653.36 599.37 4.25 o -2 2 1 0.50 4.17 0.56 o -1 2 1 397.39 368.76 2.33 o 0 2 1 1185.69 1159.70 8.52 o 1 2 1 698.98 757.53 5.29 o 4 2 1 430.83 514.58 3.51 o 5 2 1 50.44 63.66 1.36 o 6 2 1 221.24 237.63 2.90 o 7 2 1 41.57 36.02 1.43 o 8 2 1 403.14 399.87 4.79 o 9 2 1 34.26 28.66 1.55 o 10 2 1 103.77 109.31 2.49 o 11 2 1 8.80 7.23 0.92 o 12 2 1 116.48 123.91 1.90 o -12 3 1 138.09 140.78 2.23 o -11 3 1 171.39 213.31 3.24 o -10 3 1 26.91 32.13 1.64 o -9 3 1 36.75 34.49 1.70 o -8 3 1 695.37 677.18 5.37 o -7 3 1 177.38 201.09 2.90 o -6 3 1 9.35 4.35 0.99 o -5 3 1 282.60 274.09 2.83 o -4 3 1 1141.19 1059.37 7.38 o -3 3 1 185.72 193.25 1.66 o -2 3 1 8340.31 6924.70 38.97 o -1 3 1 3647.94 2983.87 22.67 o 0 3 1 3564.03 3526.55 23.52 o 1 3 1 5244.62 5717.89 32.28 o 2 3 1 6415.44 6216.08 38.50 o 4 3 1 1623.31 1800.00 12.68 o 5 3 1 470.78 464.79 3.70 o 6 3 1 34.76 55.09 1.52 o 7 3 1 1643.74 1492.07 10.79 o 8 3 1 58.44 47.33 1.76 o 9 3 1 46.14 36.74 1.65 o 10 3 1 690.65 734.80 6.53 o 11 3 1 69.36 98.30 2.03 o -12 4 1 6.11 5.80 0.78 o -11 4 1 58.97 60.84 1.86 o -10 4 1 36.27 51.98 1.84 o -9 4 1 6.46 9.28 1.19 o -8 4 1 5.11 6.73 1.10 o -7 4 1 15.51 22.46 1.21 o -6 4 1 173.51 153.72 2.33 o -5 4 1 381.44 487.25 3.78 o -4 4 1 531.51 546.70 4.02 o -3 4 1 59.17 63.99 1.23 o -2 4 1 86.30 133.48 1.38 o -1 4 1 3.21 4.45 0.50 o 0 4 1 1478.71 1498.83 10.96 o 1 4 1 1563.38 1834.28 13.65 o 3 4 1 721.39 708.79 5.06 o 4 4 1 376.61 413.28 3.48 o 5 4 1 7.81 16.96 1.33 o 6 4 1 178.76 200.61 2.90 o 7 4 1 600.99 594.78 5.03 o 8 4 1 44.18 61.47 2.00 o 9 4 1 205.10 219.73 3.54 o 10 4 1 92.27 101.58 2.40 o 11 4 1 58.16 48.65 1.43 o -12 5 1 199.73 178.87 2.29 o -11 5 1 318.82 296.85 3.54 o -10 5 1 51.44 56.26 1.79 o -9 5 1 426.20 459.69 5.14 o -8 5 1 154.38 128.04 2.70 o -7 5 1 133.33 123.58 2.65 o -6 5 1 92.68 52.08 1.60 o -5 5 1 111.22 145.48 2.26 o -4 5 1 1.84 9.54 0.79 o -3 5 1 24.38 22.72 0.89 o -2 5 1 11.18 9.86 0.59 o -1 5 1 146.25 147.57 1.87 o 0 5 1 1202.23 1381.42 9.75 o 1 5 1 4415.64 4766.78 35.87 o 3 5 1 897.52 772.43 5.78 o 4 5 1 546.71 442.47 3.61 o 5 5 1 1885.31 1853.99 12.84 o 6 5 1 616.79 624.63 5.15 o 7 5 1 852.06 895.93 7.22 o 8 5 1 99.71 122.68 2.83 o 9 5 1 24.40 24.28 1.51 o 10 5 1 226.60 257.18 3.29 o 11 5 1 22.58 16.55 0.97 o -11 6 1 17.81 19.28 1.05 o -10 6 1 204.04 224.65 3.33 o -9 6 1 9.32 11.29 1.72 o -8 6 1 3.44 0.36 2.92 o -7 6 1 137.20 101.03 2.40 o -6 6 1 0.09 1.36 1.31 o -4 6 1 86.83 124.58 2.09 o -3 6 1 27.35 12.90 0.86 o -2 6 1 1487.31 1474.83 10.76 o -1 6 1 691.89 706.67 5.05 o 0 6 1 225.95 197.93 2.40 o 1 6 1 830.84 742.80 5.19 o 2 6 1 83.53 110.56 1.79 o 3 6 1 198.89 152.22 2.32 o 4 6 1 64.89 90.66 1.95 o 5 6 1 82.23 98.49 2.03 o 6 6 1 967.26 975.48 7.01 o 7 6 1 10.34 11.01 1.69 o 8 6 1 71.80 80.27 2.29 o 9 6 1 18.50 26.86 1.41 o 10 6 1 7.58 7.09 1.27 o 11 6 1 11.02 13.89 1.21 o -11 7 1 69.91 90.89 1.79 o -10 7 1 1.18 1.26 1.22 o -9 7 1 10.69 13.01 1.17 o -8 7 1 61.25 61.90 2.01 o -7 7 1 65.32 62.85 2.03 o -6 7 1 698.89 704.28 5.48 o -5 7 1 505.46 545.01 4.81 o -4 7 1 202.47 255.90 3.00 o -3 7 1 38.89 68.04 1.69 o -2 7 1 4.06 5.20 1.16 o -1 7 1 715.18 628.70 4.32 o 0 7 1 111.51 103.43 1.91 o 1 7 1 1001.14 1155.13 8.24 o 2 7 1 742.31 889.29 6.17 o 3 7 1 15.62 21.27 1.10 o 4 7 1 1297.66 1270.42 8.67 o 5 7 1 868.16 785.84 5.80 o 6 7 1 45.02 51.87 1.84 o 7 7 1 114.14 104.40 2.61 o 8 7 1 133.49 126.43 2.68 o 9 7 1 27.91 32.13 1.45 o 10 7 1 247.49 220.18 2.79 o -10 8 1 22.60 27.48 1.25 o -9 8 1 52.46 49.22 1.67 o -7 8 1 1490.06 1460.20 10.63 o -6 8 1 174.82 173.45 3.15 o -5 8 1 205.89 220.77 3.55 o -4 8 1 283.22 209.57 2.97 o -3 8 1 193.98 161.92 2.61 o -2 8 1 150.78 129.25 2.33 o -1 8 1 43.95 51.87 1.59 o 0 8 1 0.54 1.13 1.10 o 2 8 1 277.55 284.33 3.46 o 3 8 1 938.09 971.68 7.54 o 4 8 1 182.98 148.22 2.91 o 5 8 1 488.31 490.51 5.32 o 6 8 1 367.78 355.51 4.52 o 7 8 1 45.94 52.73 1.85 o 8 8 1 9.34 8.62 1.05 o 9 8 1 208.82 193.95 2.85 o -10 9 1 5.56 7.88 0.76 o -9 9 1 54.85 59.65 1.84 o -8 9 1 121.89 131.05 2.73 o -7 9 1 265.03 260.09 3.86 o -6 9 1 26.27 24.20 1.42 o -5 9 1 0.67 3.76 1.39 o -4 9 1 95.20 68.01 1.97 o -3 9 1 1062.88 1097.45 7.45 o -2 9 1 1127.38 1090.90 8.01 o -1 9 1 1089.59 1005.39 7.13 o 0 9 1 443.77 405.39 4.14 o 1 9 1 498.29 518.29 4.69 o 2 9 1 587.60 536.19 4.77 o 3 9 1 168.94 150.86 2.93 o 4 9 1 79.29 89.06 2.41 o 5 9 1 313.20 342.79 4.43 o 6 9 1 10.90 7.32 1.20 o 7 9 1 660.07 711.90 6.42 o 8 9 1 2.35 7.27 0.92 o 9 9 1 92.39 99.60 1.87 o -9 10 1 4.07 6.47 1.04 o -8 10 1 80.43 87.02 1.91 o -7 10 1 147.49 155.43 2.98 o -6 10 1 0.17 0.99 1.30 o -5 10 1 71.59 74.87 2.21 o -4 10 1 3.93 6.96 1.48 o -3 10 1 251.77 265.50 3.90 o -2 10 1 1439.06 1432.80 9.87 o -1 10 1 116.01 127.51 2.69 o 0 10 1 64.71 63.53 2.04 o 1 10 1 96.79 87.03 2.23 o 2 10 1 22.66 31.26 1.62 o 3 10 1 3.99 2.37 1.41 o 4 10 1 38.86 40.76 1.85 o 5 10 1 4.60 3.83 1.63 o 6 10 1 591.26 592.18 5.85 o 7 10 1 100.74 103.87 2.08 o 8 10 1 62.50 59.15 1.70 o -8 11 1 84.10 85.33 1.73 o -7 11 1 22.39 22.79 1.22 o -6 11 1 167.11 160.04 3.02 o -4 11 1 95.05 85.45 2.36 o -3 11 1 398.88 368.89 4.60 o -2 11 1 180.97 184.90 3.25 o -1 11 1 116.06 117.32 2.58 o 0 11 1 60.15 63.93 2.04 o 1 11 1 112.62 127.30 2.69 o 2 11 1 1864.39 1774.24 12.52 o 3 11 1 128.40 138.17 2.81 o 4 11 1 106.11 100.25 2.39 o 5 11 1 45.35 45.81 1.73 o 7 11 1 162.20 164.94 2.41 o -7 12 1 44.22 34.92 1.21 o -6 12 1 142.77 141.17 2.43 o -5 12 1 46.18 36.95 1.45 o -4 12 1 2.19 0.99 0.83 o -3 12 1 310.77 323.23 4.30 o -2 12 1 81.88 89.88 2.26 o -1 12 1 1.48 2.59 0.98 o 0 12 1 53.75 64.60 2.05 o 1 12 1 556.69 567.82 5.73 o 2 12 1 25.83 25.55 1.46 o 3 12 1 11.86 6.87 1.16 o 4 12 1 61.95 64.35 1.91 o 6 12 1 23.27 22.96 1.06 o -6 13 1 10.41 14.21 0.83 o -4 13 1 26.47 30.14 1.31 o -3 13 1 162.07 152.80 2.53 o -2 13 1 112.12 103.04 2.42 o -1 13 1 50.78 39.27 1.60 o 0 13 1 3.85 3.63 1.13 o 1 13 1 62.80 62.05 1.88 o 2 13 1 190.73 159.34 2.59 o 3 13 1 0.08 0.61 1.04 o 4 13 1 94.97 96.56 2.01 o 5 13 1 139.65 113.95 2.00 o -2 14 1 130.77 109.17 1.96 o -1 14 1 5.13 4.82 0.82 o 0 14 1 11.90 8.08 0.87 o 1 14 1 10.49 4.38 0.78 o 2 14 1 9.17 11.70 1.34 o 3 14 1 25.71 21.92 1.04 o -12 0 2 292.93 252.75 3.26 o -10 0 2 154.66 130.17 2.92 o -9 0 2 369.99 361.72 4.56 o -8 0 2 78.99 113.18 2.54 o -7 0 2 827.20 664.38 4.89 o -5 0 2 7.05 2.67 0.58 o -4 0 2 1183.46 1304.21 9.47 o -3 0 2 687.39 402.09 3.13 o -2 0 2 5605.77 5987.19 33.25 o -1 0 2 9295.89 10569.47 64.82 o 0 0 2 7182.50 7931.92 55.94 o 2 0 2 2074.30 2116.34 14.83 o 3 0 2 2310.28 2436.26 17.64 o 4 0 2 8286.43 9671.19 61.00 o 5 0 2 1058.03 1031.53 6.68 o 6 0 2 1355.99 1287.41 8.74 o 7 0 2 47.87 38.62 1.59 o 8 0 2 307.66 318.80 4.27 o 9 0 2 348.98 441.96 5.03 o 10 0 2 565.24 547.33 4.82 o 11 0 2 295.58 212.52 2.74 o -12 1 2 215.70 238.95 3.17 o -11 1 2 9.87 8.57 1.10 o -10 1 2 59.88 56.27 1.92 o -9 1 2 51.82 43.99 1.81 o -8 1 2 16.80 8.87 1.12 o -7 1 2 22.16 19.36 1.12 o -6 1 2 14.08 12.77 0.91 o -4 1 2 96.31 53.65 1.12 o -3 1 2 1.85 12.77 0.55 o -2 1 2 1597.09 1562.96 11.27 o -1 1 2 4620.59 5710.06 31.99 o 0 1 2 5125.80 5902.87 32.82 o 1 1 2 2586.85 3096.32 23.33 o 2 1 2 3532.71 4147.58 30.87 o 3 1 2 66.30 103.66 1.56 o 4 1 2 155.68 182.50 2.31 o 5 1 2 626.16 480.14 4.15 o 6 1 2 696.26 680.75 4.94 o 7 1 2 297.97 337.68 4.08 o 8 1 2 59.06 78.72 2.12 o 9 1 2 140.22 140.03 2.82 o 10 1 2 11.35 3.73 0.99 o 11 1 2 85.69 62.80 1.62 o -12 2 2 78.05 105.21 2.10 o -11 2 2 17.99 13.70 1.13 o -10 2 2 38.73 42.85 1.78 o -9 2 2 2163.05 2192.06 15.62 o -8 2 2 800.01 837.21 5.98 o -7 2 2 490.73 519.36 4.30 o -6 2 2 1031.03 875.61 6.15 o -5 2 2 930.24 824.62 5.97 o -4 2 2 98.01 46.76 1.05 o -3 2 2 1887.52 1663.96 11.62 o -2 2 2 1431.79 1681.72 12.33 o -1 2 2 11078.61 12067.36 76.65 o 0 2 2 7249.16 8401.93 49.41 o 1 2 2 848.16 871.50 6.17 o 3 2 2 1117.45 1195.65 8.43 o 5 2 2 643.46 688.66 4.97 o 6 2 2 616.90 564.55 4.90 o 7 2 2 525.36 566.48 5.31 o 8 2 2 561.35 537.44 5.57 o 9 2 2 391.19 420.51 4.91 o 10 2 2 191.27 209.00 2.96 o 11 2 2 568.33 526.73 4.34 o -12 3 2 40.16 45.23 1.37 o -11 3 2 43.36 35.01 1.51 o -10 3 2 82.59 103.78 2.43 o -9 3 2 52.40 49.93 1.80 o -8 3 2 533.75 511.29 4.66 o -7 3 2 1205.09 1170.15 8.31 o -6 3 2 1395.78 1487.08 10.75 o -5 3 2 3965.85 4022.49 26.56 o -4 3 2 618.38 596.67 4.21 o -3 3 2 1896.13 1551.04 11.18 o -2 3 2 82.29 97.63 1.18 o -1 3 2 2342.11 2129.14 14.14 o 0 3 2 53.71 42.36 1.00 o 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