#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/19/2011958.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011958_Fobs loop_ _publ_author_name 'Zukerman-Schpector, J.' 'Caracelli, I.' 'Vega, Mauricio' 'Constantino, Mauricio Gomes' 'Beatriz, Adilson' 'da Silva, Gil Valdo' _publ_section_title ; Two polycyclic compounds derived from a Diels--Alder reaction ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 646 _journal_page_last 648 _journal_volume 57 _journal_year 2001 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.0796 _cell_length_b 10.1970 _cell_length_c 13.7534 _exptl_crystal_F_000 512.00 _reflns_d_resolution_high 0.8269 _[local]_cod_data_source_file da1175Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 'C12 H16 O5' _shelx_refln_list_code 4 _shelx_f_calc_maximum 93.02 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x+1/2, -y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 138.64 141.53 2.42 o 4 0 0 357.66 400.46 5.55 o 6 0 0 7.67 6.57 0.76 o 8 0 0 270.57 273.42 7.41 o 1 1 0 5262.81 5570.96 13.80 o 2 1 0 605.21 570.23 4.83 o 3 1 0 308.27 333.18 4.48 o 4 1 0 8.38 10.10 0.56 o 5 1 0 246.39 242.58 5.07 o 6 1 0 0.97 1.95 0.68 o 7 1 0 60.39 60.15 1.79 o 8 1 0 4.09 5.86 0.94 o 9 1 0 1.31 0.56 2.55 o 0 2 0 1336.53 1278.29 6.32 o 1 2 0 78.24 82.62 1.89 o 2 2 0 6067.62 6252.90 19.71 o 3 2 0 24.52 12.12 0.53 o 4 2 0 46.15 36.96 1.07 o 5 2 0 33.96 31.49 0.95 o 6 2 0 236.89 244.76 5.74 o 7 2 0 96.63 86.34 2.97 o 8 2 0 216.09 215.82 4.70 o 9 2 0 11.89 11.09 1.21 o 1 3 0 13.39 10.73 0.48 o 2 3 0 0.49 -1.11 1.11 o 3 3 0 1332.17 1279.24 9.83 o 4 3 0 1.47 -0.16 1.37 o 5 3 0 0.73 0.69 1.64 o 6 3 0 0.09 0.49 0.75 o 7 3 0 41.91 38.07 1.22 o 8 3 0 0.39 -2.58 2.58 o 9 3 0 4.35 5.61 1.13 o 0 4 0 89.42 87.20 2.48 o 1 4 0 636.75 664.35 6.47 o 2 4 0 102.68 89.51 2.68 o 3 4 0 729.47 743.66 7.93 o 4 4 0 0.71 -0.54 1.62 o 5 4 0 310.74 307.85 6.18 o 6 4 0 195.56 193.99 5.76 o 7 4 0 77.90 71.39 2.05 o 8 4 0 0.24 -0.37 1.00 o 9 4 0 0.28 -2.75 2.75 o 1 5 0 621.98 674.41 7.30 o 2 5 0 11.13 13.75 0.65 o 3 5 0 35.07 33.74 0.87 o 4 5 0 146.26 159.67 4.44 o 5 5 0 325.32 322.97 6.69 o 6 5 0 313.73 308.83 7.21 o 7 5 0 26.14 26.68 1.20 o 8 5 0 0.40 -2.55 2.67 o 0 6 0 566.56 570.31 7.29 o 1 6 0 140.63 153.81 4.00 o 2 6 0 16.93 17.38 0.77 o 3 6 0 5.76 5.46 0.73 o 4 6 0 0.00 -0.45 1.91 o 5 6 0 1.86 1.72 0.81 o 6 6 0 35.66 34.82 1.23 o 7 6 0 10.91 13.37 1.07 o 8 6 0 1.17 1.06 1.12 o 1 7 0 75.61 72.76 2.35 o 2 7 0 7.19 5.71 0.78 o 3 7 0 562.53 550.26 8.65 o 4 7 0 756.79 714.25 10.27 o 5 7 0 202.82 202.16 4.22 o 6 7 0 21.68 18.31 1.10 o 7 7 0 24.69 24.37 1.40 o 8 7 0 6.09 6.95 1.23 o 0 8 0 71.00 75.64 2.07 o 1 8 0 62.60 55.47 1.69 o 2 8 0 6.56 7.28 0.92 o 3 8 0 21.62 24.05 1.11 o 4 8 0 35.15 37.28 1.22 o 5 8 0 72.13 66.27 2.09 o 6 8 0 18.26 20.71 1.28 o 7 8 0 0.00 1.58 2.67 o 1 9 0 194.02 175.89 3.95 o 2 9 0 23.01 22.99 1.12 o 3 9 0 38.90 33.85 1.27 o 4 9 0 6.18 4.34 0.94 o 5 9 0 36.62 46.22 1.57 o 6 9 0 7.34 5.43 1.19 o 0 10 0 0.05 -1.08 2.51 o 1 10 0 52.53 49.94 1.39 o 2 10 0 1.39 -0.16 2.43 o 3 10 0 1.89 1.19 2.57 o 4 10 0 0.78 -0.48 1.07 o 5 10 0 0.76 -0.98 2.49 o 1 11 0 13.12 11.98 1.28 o 2 11 0 4.39 4.60 1.19 o 3 11 0 20.73 25.51 1.42 o 4 11 0 48.75 53.55 1.84 o 0 12 0 1.69 -0.20 3.08 o 1 12 0 8.86 7.51 1.30 o 2 12 0 5.43 5.97 1.28 o 1 0 1 1230.69 1265.79 5.41 o 2 0 1 10.00 10.84 0.44 o 3 0 1 280.03 276.36 4.02 o 4 0 1 99.34 100.08 2.12 o 5 0 1 89.80 104.52 2.45 o 6 0 1 93.56 87.78 2.66 o 7 0 1 8.08 7.80 0.88 o 8 0 1 30.90 31.36 1.25 o 9 0 1 0.26 0.00 1.09 o 0 1 1 3862.72 3855.64 9.98 o 1 1 1 4670.10 4534.54 12.72 o 2 1 1 4846.34 5005.02 16.23 o 3 1 1 252.26 242.17 3.90 o 4 1 1 183.50 186.55 3.90 o 5 1 1 145.00 144.39 4.04 o 6 1 1 23.23 22.14 0.91 o 7 1 1 77.29 77.08 2.27 o 8 1 1 32.99 31.20 1.25 o 9 1 1 3.46 2.26 1.11 o 0 2 1 8652.39 8204.53 73.51 o 1 2 1 284.75 274.92 3.22 o 2 2 1 392.99 384.74 4.36 o 3 2 1 988.04 993.30 8.17 o 4 2 1 71.17 71.23 1.92 o 5 2 1 408.14 393.27 6.49 o 6 2 1 37.71 39.46 1.16 o 7 2 1 29.24 26.07 1.10 o 8 2 1 128.36 118.90 3.69 o 9 2 1 2.02 1.64 1.09 o 0 3 1 879.65 837.12 6.26 o 1 3 1 1872.80 1848.97 9.89 o 2 3 1 962.39 909.87 7.43 o 3 3 1 1519.71 1554.89 10.86 o 4 3 1 123.84 126.37 2.51 o 5 3 1 114.58 121.10 2.77 o 6 3 1 256.30 265.20 6.20 o 7 3 1 31.97 25.12 1.13 o 8 3 1 23.71 20.81 1.14 o 9 3 1 1.13 0.49 1.13 o 0 4 1 7.90 12.11 0.51 o 1 4 1 585.56 606.95 6.24 o 2 4 1 899.62 876.74 8.04 o 3 4 1 201.59 228.88 4.48 o 4 4 1 74.25 73.30 2.17 o 5 4 1 303.25 306.54 6.23 o 6 4 1 50.65 53.71 1.54 o 7 4 1 50.86 50.68 1.47 o 8 4 1 50.28 53.03 1.64 o 9 4 1 3.15 1.00 2.91 o 0 5 1 247.15 252.82 4.45 o 1 5 1 1258.50 1287.40 10.20 o 2 5 1 146.86 155.58 3.87 o 3 5 1 65.13 59.76 1.60 o 4 5 1 110.94 114.82 2.82 o 5 5 1 28.16 25.55 1.03 o 6 5 1 26.35 29.59 1.11 o 7 5 1 26.80 24.95 1.17 o 8 5 1 37.38 36.43 1.52 o 0 6 1 262.08 260.91 5.09 o 1 6 1 115.45 119.25 2.53 o 2 6 1 120.25 121.61 2.68 o 3 6 1 119.94 121.88 2.82 o 4 6 1 54.56 62.74 1.96 o 5 6 1 149.43 146.70 3.57 o 6 6 1 125.24 123.59 3.56 o 7 6 1 4.35 3.83 0.92 o 8 6 1 11.79 11.48 1.28 o 0 7 1 168.05 171.59 4.60 o 1 7 1 55.95 54.30 1.34 o 2 7 1 122.38 123.49 2.98 o 3 7 1 27.83 24.55 1.01 o 4 7 1 108.70 96.35 2.96 o 5 7 1 30.58 28.41 1.15 o 6 7 1 21.19 20.64 1.14 o 7 7 1 19.66 19.71 1.36 o 8 7 1 3.93 3.14 1.16 o 0 8 1 15.82 20.22 0.99 o 1 8 1 184.22 179.38 5.15 o 2 8 1 182.59 195.64 5.45 o 3 8 1 24.14 22.72 1.06 o 4 8 1 79.21 75.24 2.38 o 5 8 1 25.83 19.76 1.15 o 6 8 1 9.99 8.77 1.14 o 7 8 1 49.12 49.08 1.76 o 0 9 1 9.76 10.16 0.96 o 1 9 1 115.06 117.04 3.30 o 2 9 1 116.62 124.50 3.51 o 3 9 1 44.74 40.98 1.31 o 4 9 1 224.53 227.49 6.75 o 5 9 1 24.68 21.27 1.31 o 6 9 1 27.30 24.80 1.44 o 0 10 1 27.41 29.51 1.21 o 1 10 1 59.88 57.97 1.63 o 2 10 1 38.38 37.30 1.31 o 3 10 1 7.24 6.44 1.03 o 4 10 1 3.51 2.36 1.09 o 5 10 1 7.06 7.22 1.18 o 0 11 1 24.95 27.49 1.36 o 1 11 1 4.09 5.09 1.09 o 2 11 1 22.86 25.43 1.44 o 3 11 1 8.31 10.91 1.20 o 4 11 1 1.72 1.82 3.00 o 0 12 1 51.30 46.70 1.76 o 1 12 1 10.03 10.05 1.30 o 2 12 1 2.45 -0.82 3.00 o 0 0 2 272.35 258.00 2.37 o 1 0 2 3120.31 3224.31 10.61 o 2 0 2 4748.87 4904.23 16.32 o 3 0 2 2494.52 2583.62 13.07 o 4 0 2 194.17 198.97 4.07 o 5 0 2 146.23 138.60 4.01 o 6 0 2 425.66 413.10 7.29 o 7 0 2 4.55 5.57 0.85 o 8 0 2 5.07 -1.11 2.58 o 9 0 2 102.07 104.95 3.07 o 0 1 2 2403.21 2379.37 8.53 o 1 1 2 402.16 403.09 3.61 o 2 1 2 5038.59 5004.34 17.00 o 3 1 2 2363.10 2506.63 12.97 o 4 1 2 280.97 308.56 5.04 o 5 1 2 870.37 883.42 9.54 o 6 1 2 287.93 290.75 6.20 o 7 1 2 31.61 32.77 1.11 o 8 1 2 5.71 6.36 0.90 o 9 1 2 8.63 7.35 1.25 o 0 2 2 1283.35 1198.65 6.80 o 1 2 2 2185.27 2088.26 9.74 o 2 2 2 2119.52 2045.94 10.78 o 3 2 2 75.13 85.18 1.82 o 4 2 2 169.27 180.73 4.06 o 5 2 2 88.59 89.64 2.43 o 6 2 2 43.87 41.32 1.10 o 7 2 2 23.34 23.78 1.08 o 8 2 2 25.81 27.26 1.20 o 9 2 2 11.60 13.86 1.30 o 0 3 2 1602.80 1511.48 8.89 o 1 3 2 77.46 78.87 2.25 o 2 3 2 1196.03 1149.48 8.62 o 3 3 2 1406.45 1398.65 10.49 o 4 3 2 600.53 590.71 7.46 o 5 3 2 392.73 406.56 6.93 o 6 3 2 29.08 24.18 1.04 o 7 3 2 66.42 63.89 2.25 o 8 3 2 33.25 33.45 1.27 o 9 3 2 0.66 -2.35 2.75 o 0 4 2 551.29 531.43 5.94 o 1 4 2 1017.48 990.65 8.16 o 2 4 2 1163.88 1207.94 9.60 o 3 4 2 91.80 98.59 2.27 o 4 4 2 459.44 472.12 7.04 o 5 4 2 3.32 3.62 0.72 o 6 4 2 183.66 184.99 5.41 o 7 4 2 79.55 78.11 2.41 o 8 4 2 34.85 36.90 1.47 o 9 4 2 2.26 1.96 1.12 o 0 5 2 30.32 24.24 0.84 o 1 5 2 47.94 57.45 1.79 o 2 5 2 233.94 247.30 4.79 o 3 5 2 523.23 543.83 7.41 o 4 5 2 198.65 189.65 4.99 o 5 5 2 322.73 323.22 6.85 o 6 5 2 100.35 89.35 3.12 o 7 5 2 2.25 -2.24 2.38 o 8 5 2 8.18 10.31 1.20 o 0 6 2 602.88 581.61 7.52 o 1 6 2 64.69 62.69 2.04 o 2 6 2 480.36 473.10 7.13 o 3 6 2 121.37 121.21 2.86 o 4 6 2 155.58 144.75 3.28 o 5 6 2 132.97 112.63 3.21 o 6 6 2 33.73 28.01 1.15 o 7 6 2 2.02 2.38 0.96 o 8 6 2 20.30 23.39 1.39 o 0 7 2 434.25 420.39 7.07 o 1 7 2 33.32 32.54 0.99 o 2 7 2 195.64 205.64 5.36 o 3 7 2 105.27 97.42 2.89 o 4 7 2 60.32 54.83 1.78 o 5 7 2 18.91 15.71 1.03 o 6 7 2 19.74 21.70 1.15 o 7 7 2 17.61 20.44 1.32 o 0 8 2 0.05 0.24 2.20 o 1 8 2 105.06 100.03 2.90 o 2 8 2 410.33 392.36 7.69 o 3 8 2 174.36 156.17 3.68 o 4 8 2 3.10 1.84 0.86 o 5 8 2 94.18 91.18 2.68 o 6 8 2 142.23 142.34 4.20 o 7 8 2 11.56 14.52 1.26 o 0 9 2 5.71 6.82 0.93 o 1 9 2 33.33 32.48 1.21 o 2 9 2 86.28 79.85 2.46 o 3 9 2 57.07 50.25 1.72 o 4 9 2 20.26 21.30 1.16 o 5 9 2 13.17 12.07 1.20 o 6 9 2 1.01 -2.64 2.64 o 0 10 2 341.21 348.24 8.08 o 1 10 2 53.15 49.56 1.48 o 2 10 2 143.12 143.02 3.94 o 3 10 2 17.78 19.05 1.15 o 4 10 2 3.47 4.27 1.10 o 5 10 2 2.12 4.38 1.10 o 0 11 2 39.89 38.60 1.55 o 1 11 2 1.80 -0.36 2.98 o 2 11 2 9.86 9.84 1.21 o 3 11 2 3.52 2.93 1.17 o 4 11 2 10.79 14.50 1.29 o 0 12 2 36.26 37.61 1.63 o 1 12 2 7.91 9.45 1.26 o 1 0 3 36.80 43.95 1.12 o 2 0 3 180.78 185.92 3.15 o 3 0 3 2190.02 2259.23 12.58 o 4 0 3 50.92 59.40 1.74 o 5 0 3 645.96 681.54 8.56 o 6 0 3 1.60 2.48 0.74 o 7 0 3 31.32 28.68 1.12 o 8 0 3 177.04 171.22 4.24 o 9 0 3 18.23 19.96 1.36 o 0 1 3 164.83 169.80 2.58 o 1 1 3 3030.58 2970.11 11.81 o 2 1 3 2419.08 2382.99 11.66 o 3 1 3 1004.05 1037.15 8.45 o 4 1 3 270.11 249.15 4.72 o 5 1 3 64.04 59.64 1.69 o 6 1 3 75.29 70.61 2.51 o 7 1 3 0.69 1.34 0.79 o 8 1 3 74.97 80.67 2.25 o 9 1 3 8.75 8.57 1.20 o 0 2 3 28.36 27.21 0.86 o 1 2 3 1657.47 1646.94 9.15 o 2 2 3 421.86 408.86 4.88 o 3 2 3 35.79 42.19 1.16 o 4 2 3 431.71 414.23 6.15 o 5 2 3 52.04 55.31 1.70 o 6 2 3 354.48 366.17 7.06 o 7 2 3 40.72 38.28 1.30 o 8 2 3 18.41 19.78 1.16 o 9 2 3 38.05 41.37 1.64 o 0 3 3 323.20 300.16 4.14 o 1 3 3 756.83 736.04 6.62 o 2 3 3 727.87 721.08 7.01 o 3 3 3 804.48 828.51 8.22 o 4 3 3 472.87 467.23 6.76 o 5 3 3 215.84 206.40 5.17 o 6 3 3 282.15 273.95 6.26 o 7 3 3 27.14 23.95 1.08 o 8 3 3 10.12 11.86 1.04 o 9 3 3 23.14 25.28 1.40 o 0 4 3 10.75 12.12 0.53 o 1 4 3 469.05 508.09 6.04 o 2 4 3 154.32 149.43 3.62 o 3 4 3 936.74 982.57 9.52 o 4 4 3 11.93 16.70 0.78 o 5 4 3 89.01 83.43 2.63 o 6 4 3 104.23 101.41 3.13 o 7 4 3 3.24 3.08 0.88 o 8 4 3 20.83 20.68 1.32 o 9 4 3 1.17 -2.91 2.91 o 0 5 3 444.74 410.87 5.89 o 1 5 3 214.48 227.97 4.58 o 2 5 3 466.47 465.96 6.64 o 3 5 3 243.17 270.64 5.44 o 4 5 3 51.70 56.94 1.75 o 5 5 3 203.62 218.21 5.67 o 6 5 3 131.65 126.59 3.48 o 7 5 3 8.37 7.31 0.94 o 8 5 3 57.90 59.71 1.76 o 0 6 3 48.17 46.57 1.53 o 1 6 3 75.83 70.89 2.18 o 2 6 3 83.76 90.12 2.42 o 3 6 3 197.54 204.37 5.14 o 4 6 3 14.92 14.54 0.90 o 5 6 3 32.71 33.25 1.15 o 6 6 3 57.91 57.22 1.64 o 7 6 3 5.04 6.42 1.07 o 8 6 3 17.75 20.21 1.37 o 0 7 3 39.64 41.37 1.42 o 1 7 3 468.57 447.85 7.33 o 2 7 3 13.44 16.57 0.87 o 3 7 3 5.56 7.73 0.82 o 4 7 3 24.19 26.19 1.06 o 5 7 3 65.66 63.70 1.74 o 6 7 3 1.31 0.00 2.51 o 7 7 3 14.01 17.06 1.32 o 0 8 3 5.75 8.39 0.88 o 1 8 3 121.27 125.33 3.29 o 2 8 3 207.60 195.28 5.73 o 3 8 3 21.95 24.86 1.07 o 4 8 3 36.80 38.99 1.28 o 5 8 3 23.36 19.08 1.11 o 6 8 3 8.24 9.78 1.18 o 7 8 3 26.80 30.15 1.49 o 0 9 3 24.63 29.35 1.18 o 1 9 3 16.44 17.77 1.06 o 2 9 3 196.30 176.25 4.20 o 3 9 3 21.36 22.76 1.13 o 4 9 3 83.16 84.12 2.59 o 5 9 3 10.25 13.41 1.23 o 6 9 3 0.74 3.08 1.07 o 0 10 3 18.96 20.84 1.20 o 1 10 3 63.67 61.91 1.66 o 2 10 3 6.06 4.11 1.02 o 3 10 3 2.10 1.22 2.50 o 4 10 3 2.51 0.00 2.81 o 5 10 3 6.54 9.45 1.21 o 0 11 3 71.10 72.22 2.05 o 1 11 3 6.92 7.41 1.21 o 2 11 3 74.57 78.72 2.40 o 3 11 3 32.89 31.35 1.54 o 4 11 3 23.75 23.81 1.53 o 0 12 3 15.93 16.22 1.36 o 1 12 3 4.40 8.45 1.21 o 0 0 4 1445.08 1305.02 7.77 o 1 0 4 332.40 366.18 4.21 o 2 0 4 142.94 130.07 2.85 o 3 0 4 99.22 98.31 2.83 o 4 0 4 165.13 194.18 4.28 o 5 0 4 163.87 170.26 4.56 o 6 0 4 100.38 87.42 2.73 o 7 0 4 0.39 -0.99 2.21 o 8 0 4 239.38 251.40 7.18 o 9 0 4 49.94 43.92 1.70 o 0 1 4 535.06 504.37 4.87 o 1 1 4 282.29 284.06 3.82 o 2 1 4 596.12 592.32 6.02 o 3 1 4 442.51 467.87 5.84 o 4 1 4 577.33 595.19 7.40 o 5 1 4 104.30 113.26 2.79 o 6 1 4 65.42 69.68 2.06 o 7 1 4 37.03 32.95 1.14 o 8 1 4 32.91 34.76 1.36 o 9 1 4 19.69 18.95 1.32 o 0 2 4 4498.54 4435.06 16.80 o 1 2 4 10.63 14.19 0.50 o 2 2 4 685.17 693.45 6.77 o 3 2 4 399.60 391.14 5.63 o 4 2 4 449.84 435.78 6.54 o 5 2 4 236.64 250.68 5.42 o 6 2 4 38.20 35.48 1.34 o 7 2 4 14.49 14.92 0.98 o 8 2 4 164.86 161.83 4.31 o 9 2 4 19.48 20.17 1.33 o 0 3 4 251.21 261.06 4.10 o 1 3 4 1468.60 1493.95 10.07 o 2 3 4 218.98 223.51 4.12 o 3 3 4 176.21 176.57 4.04 o 4 3 4 73.38 78.66 2.27 o 5 3 4 358.68 357.84 6.71 o 6 3 4 34.19 29.68 1.08 o 7 3 4 56.65 50.41 1.36 o 8 3 4 0.26 0.87 2.53 o 9 3 4 13.02 15.99 1.36 o 0 4 4 3014.82 3172.18 16.10 o 1 4 4 260.67 313.97 4.99 o 2 4 4 131.12 128.05 3.45 o 3 4 4 267.21 301.71 5.46 o 4 4 4 281.18 294.12 5.90 o 5 4 4 243.35 241.16 5.89 o 6 4 4 37.64 35.32 1.19 o 7 4 4 179.92 176.51 4.30 o 8 4 4 33.38 32.38 1.48 o 0 5 4 134.24 158.20 3.99 o 1 5 4 976.19 1005.92 9.69 o 2 5 4 198.85 186.05 4.40 o 3 5 4 334.42 326.03 6.10 o 4 5 4 140.87 139.36 3.16 o 5 5 4 393.83 384.27 7.75 o 6 5 4 139.46 150.83 3.75 o 7 5 4 94.54 93.72 2.77 o 8 5 4 35.43 36.45 1.54 o 0 6 4 24.62 19.11 0.82 o 1 6 4 605.28 620.79 8.16 o 2 6 4 222.07 218.52 5.13 o 3 6 4 9.36 8.36 0.80 o 4 6 4 85.43 81.87 2.27 o 5 6 4 80.94 80.79 2.33 o 6 6 4 125.49 121.19 3.59 o 7 6 4 6.61 9.44 1.14 o 8 6 4 18.74 18.44 1.41 o 0 7 4 67.93 63.02 1.91 o 1 7 4 10.15 10.14 0.83 o 2 7 4 11.52 11.07 0.90 o 3 7 4 455.50 445.12 8.15 o 4 7 4 35.99 31.87 1.18 o 5 7 4 71.75 65.50 1.99 o 6 7 4 20.09 19.82 1.15 o 7 7 4 17.98 19.78 1.39 o 0 8 4 470.60 460.77 8.26 o 1 8 4 71.35 71.88 2.19 o 2 8 4 204.13 203.92 5.93 o 3 8 4 15.61 13.13 0.98 o 4 8 4 50.58 47.62 1.47 o 5 8 4 1.53 2.47 0.90 o 6 8 4 8.52 8.51 1.18 o 7 8 4 3.23 3.30 1.16 o 0 9 4 411.63 408.24 8.37 o 1 9 4 190.80 172.28 4.07 o 2 9 4 26.46 22.44 1.14 o 3 9 4 42.22 38.08 1.45 o 4 9 4 50.51 51.92 1.63 o 5 9 4 70.11 75.03 1.93 o 6 9 4 0.80 1.62 2.73 o 0 10 4 206.04 189.33 4.52 o 1 10 4 83.14 75.79 2.58 o 2 10 4 13.38 13.76 1.09 o 3 10 4 7.71 5.45 1.13 o 4 10 4 31.06 36.11 1.57 o 5 10 4 13.42 14.43 1.40 o 0 11 4 13.80 12.81 1.27 o 1 11 4 52.56 50.44 1.70 o 2 11 4 32.31 37.46 1.56 o 3 11 4 36.81 41.39 1.69 o 1 0 5 412.41 379.01 4.70 o 2 0 5 29.61 31.37 1.01 o 3 0 5 0.04 0.74 0.50 o 4 0 5 154.94 156.18 4.10 o 5 0 5 447.57 493.38 7.75 o 6 0 5 0.00 0.51 0.80 o 7 0 5 0.97 1.11 0.82 o 8 0 5 1.66 0.00 2.37 o 9 0 5 0.14 -0.60 2.77 o 0 1 5 296.09 293.71 4.13 o 1 1 5 1274.75 1265.37 8.83 o 2 1 5 118.51 125.91 3.04 o 3 1 5 20.04 18.10 0.64 o 4 1 5 316.74 301.44 5.56 o 5 1 5 11.00 8.96 0.75 o 6 1 5 385.97 401.72 7.72 o 7 1 5 89.45 87.69 3.18 o 8 1 5 19.73 16.73 1.16 o 9 1 5 22.28 25.81 1.48 o 0 2 5 174.49 176.51 3.45 o 1 2 5 331.50 318.74 4.64 o 2 2 5 256.82 300.96 4.79 o 3 2 5 459.34 484.30 6.52 o 4 2 5 339.54 341.84 5.95 o 5 2 5 106.81 114.27 2.84 o 6 2 5 84.06 85.25 2.74 o 7 2 5 17.33 22.53 1.11 o 8 2 5 0.89 2.95 1.02 o 9 2 5 4.84 4.48 1.20 o 0 3 5 867.12 928.82 8.18 o 1 3 5 71.55 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6 589.47 577.38 8.63 o 4 5 6 112.26 112.70 3.18 o 5 5 6 146.28 140.55 3.56 o 6 5 6 78.97 77.16 2.12 o 7 5 6 8.69 6.30 1.14 o 8 5 6 20.91 19.22 1.44 o 0 6 6 18.07 18.14 0.88 o 1 6 6 45.41 44.77 1.32 o 2 6 6 412.65 422.60 7.54 o 3 6 6 45.74 51.12 1.49 o 4 6 6 129.51 116.69 3.38 o 5 6 6 184.74 176.24 4.13 o 6 6 6 71.51 74.11 1.93 o 7 6 6 20.57 20.52 1.34 o 0 7 6 95.34 101.04 2.99 o 1 7 6 120.27 110.49 3.11 o 2 7 6 12.67 11.43 0.95 o 3 7 6 135.15 135.06 3.52 o 4 7 6 75.27 78.14 2.12 o 5 7 6 109.87 112.26 3.49 o 6 7 6 0.42 0.73 2.58 o 7 7 6 26.22 23.79 1.49 o 0 8 6 256.16 259.53 6.61 o 1 8 6 191.11 188.60 4.12 o 2 8 6 127.09 119.06 3.41 o 3 8 6 215.25 204.89 4.44 o 4 8 6 40.44 40.35 1.37 o 5 8 6 10.85 11.76 1.21 o 6 8 6 0.83 -3.04 3.04 o 0 9 6 4.05 5.05 0.92 o 1 9 6 52.63 53.32 1.69 o 2 9 6 48.58 45.65 1.41 o 3 9 6 10.36 8.69 1.05 o 4 9 6 25.28 33.90 1.46 o 5 9 6 63.05 69.72 2.14 o 0 10 6 29.12 29.35 1.42 o 1 10 6 4.54 5.39 1.07 o 2 10 6 27.68 29.28 1.48 o 3 10 6 90.20 101.01 3.06 o 4 10 6 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20.10 1.33 o 3 8 10 0.85 1.13 2.74 o 4 8 10 1.20 -0.20 2.93 o 0 9 10 0.18 -0.96 2.53 o 1 9 10 11.21 13.23 1.26 o 2 9 10 7.42 9.66 1.25 o 3 9 10 12.87 15.20 1.39 o 1 0 11 46.57 47.14 1.26 o 2 0 11 130.76 114.70 3.28 o 3 0 11 34.13 30.06 1.18 o 4 0 11 0.13 -0.59 2.47 o 5 0 11 19.99 16.28 1.17 o 6 0 11 5.79 6.27 1.20 o 7 0 11 0.03 -1.40 2.89 o 0 1 11 96.63 96.23 2.93 o 1 1 11 182.78 166.02 3.71 o 2 1 11 223.90 211.65 5.78 o 3 1 11 10.62 7.33 0.93 o 4 1 11 250.33 260.94 6.84 o 5 1 11 53.92 47.90 1.43 o 6 1 11 50.52 51.40 1.75 o 7 1 11 4.77 4.22 1.23 o 0 2 11 45.46 43.83 1.32 o 1 2 11 42.84 42.79 1.34 o 2 2 11 235.18 224.58 6.15 o 3 2 11 93.60 88.60 2.92 o 4 2 11 75.21 72.95 2.06 o 5 2 11 39.27 36.82 1.34 o 6 2 11 28.35 27.14 1.38 o 7 2 11 2.90 2.69 1.15 o 0 3 11 7.07 5.29 0.92 o 1 3 11 8.33 7.56 0.93 o 2 3 11 228.07 232.35 6.20 o 3 3 11 40.90 35.19 1.21 o 4 3 11 129.43 128.85 3.72 o 5 3 11 31.11 33.51 1.31 o 6 3 11 11.44 14.16 1.22 o 0 4 11 12.78 15.70 1.04 o 1 4 11 83.20 78.84 2.42 o 2 4 11 15.60 16.15 1.04 o 3 4 11 24.77 20.97 1.11 o 4 4 11 10.56 11.53 0.99 o 5 4 11 12.48 10.58 1.21 o 6 4 11 17.87 17.49 1.34 o 0 5 11 109.64 114.27 3.43 o 1 5 11 3.68 3.23 0.91 o 2 5 11 144.36 139.18 3.83 o 3 5 11 61.98 63.08 2.06 o 4 5 11 2.25 0.34 2.25 o 5 5 11 13.15 12.58 1.25 o 6 5 11 32.54 35.89 1.58 o 0 6 11 189.09 191.33 4.46 o 1 6 11 75.40 72.12 2.10 o 2 6 11 59.67 56.53 1.77 o 3 6 11 79.85 86.66 2.37 o 4 6 11 9.96 7.89 1.20 o 5 6 11 42.82 45.88 1.63 o 0 7 11 0.92 1.46 0.96 o 1 7 11 47.99 50.30 1.48 o 2 7 11 16.07 13.92 1.32 o 3 7 11 29.08 31.06 1.47 o 4 7 11 3.47 1.77 3.03 o 0 8 11 21.90 17.62 1.34 o 1 8 11 59.31 62.67 2.00 o 2 8 11 0.70 -1.54 3.00 o 3 8 11 6.68 6.55 1.20 o 0 9 11 22.64 20.08 1.40 o 1 9 11 9.77 11.60 1.28 o 0 0 12 27.77 25.36 1.09 o 1 0 12 47.91 45.05 1.27 o 2 0 12 251.17 238.54 6.43 o 3 0 12 88.33 88.30 2.57 o 4 0 12 15.84 16.29 1.12 o 5 0 12 12.48 11.30 1.23 o 6 0 12 4.77 4.64 1.18 o 0 1 12 72.34 72.31 2.27 o 1 1 12 28.24 29.15 1.12 o 2 1 12 150.75 140.75 3.72 o 3 1 12 440.99 447.11 8.99 o 4 1 12 2.16 1.65 0.97 o 5 1 12 77.41 80.84 2.35 o 6 1 12 7.53 10.10 1.23 o 0 2 12 373.98 349.84 7.60 o 1 2 12 20.94 23.48 1.13 o 2 2 12 127.09 124.61 3.51 o 3 2 12 15.46 17.86 1.06 o 4 2 12 12.47 10.27 1.05 o 5 2 12 100.22 104.53 2.90 o 6 2 12 9.73 12.32 1.22 o 0 3 12 214.69 207.92 6.08 o 1 3 12 687.51 655.26 10.53 o 2 3 12 96.69 97.83 2.71 o 3 3 12 25.71 25.79 1.18 o 4 3 12 3.63 3.23 0.95 o 5 3 12 26.58 22.61 1.41 o 6 3 12 4.26 5.53 1.16 o 0 4 12 164.50 157.21 3.93 o 1 4 12 34.71 35.97 1.29 o 2 4 12 32.29 32.63 1.24 o 3 4 12 210.30 202.38 4.63 o 4 4 12 11.88 6.95 1.21 o 5 4 12 40.41 44.81 1.63 o 0 5 12 20.89 23.34 1.19 o 1 5 12 29.49 27.81 1.25 o 2 5 12 58.28 54.85 1.46 o 3 5 12 8.75 11.62 1.22 o 4 5 12 2.06 0.99 1.13 o 5 5 12 19.38 19.99 1.48 o 0 6 12 139.16 140.81 4.06 o 1 6 12 62.18 67.44 1.93 o 2 6 12 28.45 31.95 1.43 o 3 6 12 24.22 23.94 1.38 o 4 6 12 3.00 5.39 1.12 o 0 7 12 28.03 22.60 1.45 o 1 7 12 19.98 22.02 1.37 o 2 7 12 43.26 43.78 1.66 o 3 7 12 0.93 0.40 2.76 o 0 8 12 29.47 30.32 1.56 o 1 8 12 4.40 7.18 1.27 o 2 8 12 47.83 53.10 1.81 o 1 0 13 59.23 62.03 1.80 o 2 0 13 46.93 43.97 1.36 o 3 0 13 2.64 1.86 0.94 o 4 0 13 81.01 81.37 2.33 o 5 0 13 0.05 0.41 1.10 o 6 0 13 5.72 4.84 1.31 o 0 1 13 3.98 3.37 0.92 o 1 1 13 106.90 109.54 3.40 o 2 1 13 67.84 62.35 2.02 o 3 1 13 129.77 126.01 3.87 o 4 1 13 42.09 42.18 1.57 o 5 1 13 14.78 13.03 1.31 o 6 1 13 4.26 6.27 1.25 o 0 2 13 674.98 636.82 10.58 o 1 2 13 122.99 114.40 3.58 o 2 2 13 94.15 89.19 2.62 o 3 2 13 18.71 18.31 1.12 o 4 2 13 25.62 29.65 1.44 o 5 2 13 0.99 0.00 2.79 o 0 3 13 108.47 99.53 3.41 o 1 3 13 2.46 1.36 0.97 o 2 3 13 14.41 15.03 1.13 o 3 3 13 10.95 13.82 1.11 o 4 3 13 2.35 -2.19 2.87 o 5 3 13 75.50 80.52 2.55 o 0 4 13 3.56 -2.78 2.78 o 1 4 13 7.84 8.26 1.01 o 2 4 13 89.74 96.62 2.76 o 3 4 13 7.84 10.07 1.21 o 4 4 13 21.86 22.01 1.44 o 5 4 13 15.67 16.48 1.41 o 0 5 13 44.61 45.43 1.58 o 1 5 13 7.49 9.82 1.20 o 2 5 13 32.25 31.68 1.49 o 3 5 13 33.59 32.54 1.50 o 4 5 13 37.42 42.97 1.65 o 0 6 13 20.64 20.35 1.42 o 1 6 13 42.33 42.79 1.67 o 2 6 13 36.16 41.66 1.61 o 3 6 13 4.89 5.77 1.19 o 0 7 13 12.56 14.58 1.35 o 1 7 13 5.72 5.64 1.21 o 2 7 13 4.87 1.02 2.95 o 0 0 14 62.63 67.25 1.76 o 1 0 14 29.03 28.05 1.28 o 2 0 14 4.70 2.13 0.97 o 3 0 14 5.17 3.13 1.13 o 4 0 14 6.09 3.21 1.21 o 5 0 14 0.01 0.00 3.03 o 0 1 14 42.93 39.46 1.39 o 1 1 14 4.39 4.33 0.99 o 2 1 14 45.91 47.30 1.53 o 3 1 14 12.21 10.53 1.22 o 4 1 14 53.58 57.95 1.79 o 5 1 14 7.92 5.89 1.27 o 0 2 14 35.82 33.49 1.34 o 1 2 14 168.70 161.74 4.27 o 2 2 14 50.27 53.08 1.65 o 3 2 14 22.41 26.46 1.45 o 4 2 14 36.03 38.01 1.62 o 5 2 14 16.21 15.71 1.43 o 0 3 14 19.92 20.14 1.22 o 1 3 14 30.16 27.29 1.47 o 2 3 14 6.02 5.24 1.16 o 3 3 14 7.37 9.46 1.21 o 4 3 14 24.05 29.58 1.49 o 0 4 14 39.41 30.84 1.55 o 1 4 14 80.01 81.07 2.18 o 2 4 14 31.31 33.15 1.53 o 3 4 14 72.44 76.76 2.19 o 4 4 14 11.13 12.19 1.34 o 0 5 14 27.02 28.38 1.49 o 1 5 14 31.53 33.12 1.54 o 2 5 14 67.29 72.59 1.91 o 3 5 14 3.06 2.30 1.18 o 0 6 14 0.00 -2.59 3.12 o 1 6 14 30.59 27.27 1.57 o 2 6 14 29.96 36.49 1.71 o 1 0 15 62.57 66.30 1.86 o 2 0 15 15.65 17.60 1.36 o 3 0 15 7.00 8.55 1.23 o 4 0 15 65.15 73.80 2.04 o 0 1 15 27.43 29.08 1.47 o 1 1 15 46.63 47.91 1.65 o 2 1 15 27.04 28.10 1.45 o 3 1 15 13.16 18.10 1.33 o 4 1 15 3.20 4.25 1.30 o 0 2 15 9.54 6.57 1.25 o 1 2 15 39.91 41.09 1.59 o 2 2 15 21.39 19.85 1.38 o 3 2 15 39.14 39.95 1.68 o 0 3 15 6.24 5.96 1.24 o 1 3 15 8.34 7.56 1.20 o 2 3 15 13.39 13.27 1.30 o 3 3 15 15.46 18.41 1.41 o 0 4 15 40.67 40.52 1.64 o 1 4 15 33.80 36.41 1.63 o 2 4 15 16.21 16.84 1.41 o 0 5 15 122.95 140.90 4.50 o 1 5 15 0.07 -0.62 1.15 o 0 0 16 0.64 1.37 2.77 o 1 0 16 87.61 92.60 2.66 o 2 0 16 1.24 0.61 2.70 o 0 1 16 0.69 -0.59 2.84 o 1 1 16 71.35 67.58 2.46 o 2 1 16 35.71 38.52 1.67 o 0 2 16 12.88 12.76 1.32 o 1 2 16 15.58 18.04 1.46 o 2 2 16 6.52 6.79 1.32 o 0 3 16 92.03 99.68 2.52 o 1 3 16 13.25 11.66 1.38 o