#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/19/2011962.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011962_Fobs loop_ _publ_author_name 'Kelson, Eric P.' 'Phengsy, Proma P.' 'Arif, Atta M.' _publ_section_title ; A chloro(2-pyridinecarboxaldehyde)(2,2':6',2''-terpyridine)ruthenium(II) complex ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 517 _journal_page_last 519 _journal_volume 57 _journal_year 2001 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 68.791 _cell_angle_beta 83.824 _cell_angle_gamma 87.065 _cell_length_a 10.8871 _cell_length_b 13.4187 _cell_length_c 17.9641 _exptl_crystal_F_000 1291.04 _reflns_d_resolution_high 0.6596 _[local]_cod_data_source_file fg1610Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 'FG1610 EK @200K Dark Red Prism Triclinic P-1 SHELXL97' _shelx_refln_list_code 4 _shelx_f_calc_maximum 246.87 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h 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o 2 1 0 185.30 232.24 10.75 o 3 1 0 4156.05 3355.91 65.76 o 4 1 0 2154.31 1984.83 44.12 o 5 1 0 7358.37 7501.96 152.63 o 6 1 0 4819.21 5396.35 107.83 o 7 1 0 4220.36 4564.61 97.44 o 8 1 0 1096.75 1162.44 34.88 o 9 1 0 4253.58 4424.17 104.59 o 10 1 0 531.65 533.96 35.70 o 11 1 0 1054.52 1035.35 104.30 o 12 1 0 97.66 72.16 25.79 o 13 1 0 0.22 69.44 27.34 o 14 1 0 738.19 779.34 63.37 o 15 1 0 51.68 -2.50 27.84 o 16 1 0 40.41 -36.69 55.33 o -16 2 0 33.18 -25.79 45.14 o -15 2 0 480.64 569.28 53.16 o -14 2 0 25.94 -34.07 34.07 o -13 2 0 29.87 -21.05 25.31 o -12 2 0 180.34 155.70 26.87 o -11 2 0 1243.87 1386.45 63.10 o -10 2 0 847.15 903.41 36.40 o -9 2 0 5182.87 5350.21 134.75 o -8 2 0 321.55 322.32 18.96 o -7 2 0 2843.90 2974.33 64.61 o -6 2 0 3119.46 3093.53 60.06 o -5 2 0 560.69 629.71 20.43 o -4 2 0 26313.69 25302.14 481.57 o -3 2 0 1817.32 1888.05 39.62 o -2 2 0 6262.29 6498.33 155.36 o 1 2 0 7136.81 6664.18 247.39 o 2 2 0 1903.26 1858.20 40.41 o 3 2 0 8542.64 8581.85 177.61 o 4 2 0 2386.27 2128.97 49.38 o 5 2 0 573.52 573.29 34.41 o 6 2 0 353.80 208.91 13.68 o 7 2 0 1307.33 1251.70 35.73 o 8 2 0 5380.38 5698.07 115.06 o 9 2 0 2101.86 2361.12 104.38 o 10 2 0 2163.84 2331.67 134.50 o 11 2 0 152.78 154.79 26.31 o 12 2 0 621.73 682.17 50.51 o 13 2 0 751.46 729.00 55.48 o 14 2 0 18.75 86.02 36.66 o 15 2 0 545.51 645.88 72.02 o 16 2 0 33.79 8.93 48.96 o -16 3 0 299.71 221.41 90.28 o -15 3 0 35.56 45.14 49.44 o -14 3 0 547.15 489.58 47.73 o -13 3 0 137.76 186.00 48.36 o -12 3 0 7.82 22.45 22.57 o -11 3 0 53.79 38.69 25.79 o -10 3 0 297.89 334.15 22.66 o -9 3 0 274.04 265.69 18.59 o -8 3 0 6376.27 6650.39 149.55 o -7 3 0 2.15 7.27 9.79 o -6 3 0 5772.03 5679.04 109.17 o -5 3 0 72.28 109.67 7.60 o -4 3 0 102.34 78.55 5.16 o -3 3 0 2460.02 2049.03 51.46 o -2 3 0 2491.76 2384.46 66.89 o -1 3 0 1494.14 1425.24 43.85 o 0 3 0 133.76 173.13 9.12 o 1 3 0 264.32 222.44 11.33 o 2 3 0 2406.57 2403.25 56.19 o 3 3 0 4616.51 4811.54 92.51 o 4 3 0 3.40 -8.26 8.26 o 5 3 0 21576.09 20880.00 407.25 o 6 3 0 875.21 889.35 26.58 o 7 3 0 3285.82 3461.33 79.04 o 8 3 0 27.19 73.42 13.43 o 9 3 0 604.76 555.86 34.18 o 10 3 0 324.80 348.30 35.50 o 11 3 0 1941.37 2092.46 95.09 o 12 3 0 735.58 717.21 47.73 o 13 3 0 1277.52 1310.47 194.63 o 14 3 0 770.40 738.01 59.23 o 15 3 0 52.19 73.19 42.35 o 16 3 0 239.94 244.53 56.96 o -15 4 0 398.36 429.95 70.94 o -14 4 0 100.70 199.83 40.26 o -13 4 0 1565.90 1625.43 83.48 o -12 4 0 750.13 829.17 52.04 o -11 4 0 171.44 185.51 30.09 o -10 4 0 1127.58 1196.20 73.12 o -9 4 0 51.94 66.96 24.72 o -8 4 0 771.51 657.14 26.32 o -7 4 0 1787.78 1809.38 46.39 o -6 4 0 147.39 127.56 8.75 o -5 4 0 1170.73 1203.12 32.55 o -4 4 0 605.63 821.56 20.65 o -3 4 0 2751.58 2632.64 62.53 o -2 4 0 8272.45 8057.77 232.46 o -1 4 0 2583.13 2475.28 75.68 o 0 4 0 10289.79 9673.06 389.60 o 1 4 0 69.46 90.33 10.64 o 2 4 0 9312.47 8558.58 187.77 o 3 4 0 9036.88 8457.78 183.51 o 4 4 0 9772.90 9845.52 188.30 o 5 4 0 295.41 338.07 24.72 o 6 4 0 7215.99 7113.12 173.42 o 7 4 0 20.66 -11.32 11.32 o 8 4 0 1621.62 1582.51 51.46 o 9 4 0 1146.77 1212.74 57.25 o 10 4 0 1737.68 1982.68 79.77 o 11 4 0 14.36 25.03 25.70 o 12 4 0 464.37 407.01 35.51 o 13 4 0 45.18 95.57 56.96 o 14 4 0 426.48 415.00 47.00 o 15 4 0 263.33 252.69 54.15 o 16 4 0 0.64 -6.02 50.08 o -15 5 0 221.41 176.27 83.83 o -14 5 0 135.14 148.32 49.44 o -13 5 0 0.16 12.11 25.79 o -12 5 0 772.69 670.70 49.72 o -11 5 0 720.69 734.31 47.44 o -10 5 0 532.55 564.90 26.57 o -9 5 0 2281.82 2400.10 69.21 o -8 5 0 1339.61 1373.71 43.65 o -7 5 0 7.67 1.95 20.42 o -6 5 0 4307.44 4348.85 96.36 o -5 5 0 439.08 425.73 12.90 o -4 5 0 11755.88 11628.25 258.45 o -3 5 0 2015.64 2181.71 58.15 o -2 5 0 7864.45 7586.65 226.39 o -1 5 0 5422.72 5652.79 160.96 o 0 5 0 729.28 803.53 59.16 o 1 5 0 2402.14 2159.16 61.60 o 2 5 0 3734.14 3501.27 78.30 o 3 5 0 63.90 96.61 13.43 o 4 5 0 9905.49 10452.81 357.82 o 5 5 0 10631.90 11336.90 313.26 o 6 5 0 1064.51 1073.38 33.36 o 7 5 0 1766.42 1852.42 56.81 o 8 5 0 327.22 330.19 29.38 o 9 5 0 715.82 755.64 93.54 o 10 5 0 110.49 90.28 27.36 o 11 5 0 112.19 95.94 53.74 o 12 5 0 193.14 177.69 35.50 o 13 5 0 833.35 983.46 76.33 o 14 5 0 62.48 20.59 41.72 o 15 5 0 567.95 546.85 62.96 o -15 6 0 70.06 109.62 47.29 o -14 6 0 602.37 490.18 88.15 o -13 6 0 67.30 60.18 58.04 o -12 6 0 517.44 577.54 43.30 o -11 6 0 1200.22 1197.39 98.93 o -10 6 0 10.49 16.30 18.05 o -9 6 0 634.79 521.40 49.45 o -8 6 0 1227.75 1212.58 31.42 o -7 6 0 311.61 242.93 10.75 o -6 6 0 163.66 178.42 8.60 o -5 6 0 9989.88 9955.56 212.19 o -4 6 0 2043.77 2021.61 43.06 o -3 6 0 30584.62 32276.91 803.17 o -2 6 0 175.47 211.59 9.79 o -1 6 0 2054.66 1934.63 122.77 o 0 6 0 487.01 493.12 68.81 o 1 6 0 97.47 149.33 30.09 o 2 6 0 5147.93 5049.60 139.89 o 3 6 0 11715.58 12101.34 499.49 o 4 6 0 1255.45 1247.92 43.03 o 5 6 0 19336.65 19690.81 892.81 o 6 6 0 2923.11 2885.57 127.07 o 7 6 0 731.73 713.67 34.41 o 8 6 0 738.69 765.52 40.10 o 9 6 0 469.67 442.29 35.51 o 10 6 0 178.52 155.26 46.22 o 11 6 0 32.11 45.14 42.99 o 12 6 0 14.86 -25.58 26.49 o 13 6 0 104.59 81.26 50.16 o 14 6 0 385.95 349.03 64.48 o 15 6 0 33.09 20.17 59.11 o -15 7 0 285.73 223.56 77.39 o -14 7 0 32.50 -2.15 55.88 o -13 7 0 904.82 1049.29 96.76 o -12 7 0 22.74 4.30 38.69 o -11 7 0 621.25 640.70 66.65 o -10 7 0 1405.27 1333.52 60.22 o -9 7 0 27.95 23.64 8.60 o -8 7 0 2630.71 2492.57 62.42 o -7 7 0 273.95 225.72 8.60 o -6 7 0 564.21 481.64 40.85 o -5 7 0 844.99 853.80 49.46 o -4 7 0 5211.50 5376.74 230.86 o -3 7 0 1166.56 1202.61 32.27 o -2 7 0 7828.50 7570.05 209.44 o -1 7 0 0.08 5.37 7.60 o 0 7 0 2626.72 2363.87 147.57 o 1 7 0 1093.61 1312.68 91.44 o 2 7 0 3159.52 3106.50 213.35 o 3 7 0 604.16 660.99 27.96 o 4 7 0 2013.31 2024.36 60.52 o 5 7 0 786.85 833.79 36.14 o 6 7 0 2303.86 2113.81 77.49 o 7 7 0 134.16 206.36 32.24 o 8 7 0 82.62 96.73 38.69 o 9 7 0 1271.79 1116.27 66.67 o 10 7 0 17.30 42.99 32.24 o 11 7 0 1045.41 944.03 83.87 o 12 7 0 52.53 27.94 38.69 o 13 7 0 48.15 122.52 70.93 o 14 7 0 39.48 4.30 53.74 o 15 7 0 359.28 522.37 118.23 o -14 8 0 97.46 161.21 79.53 o -13 8 0 15.94 2.15 40.84 o -12 8 0 825.25 989.06 92.46 o -11 8 0 379.39 434.25 70.94 o -10 8 0 1078.90 1094.59 92.47 o -9 8 0 2347.04 2257.31 124.81 o -8 8 0 727.71 780.53 68.81 o -7 8 0 981.07 1116.14 77.42 o -6 8 0 2871.07 2652.55 127.03 o -5 8 0 12.30 15.05 32.24 o -4 8 0 5313.79 5278.29 224.33 o -3 8 0 573.36 531.12 15.05 o -2 8 0 135.96 173.35 18.27 o -1 8 0 1566.76 1564.04 57.03 o 0 8 0 85.21 109.80 26.87 o 1 8 0 2205.11 2112.97 99.04 o 2 8 0 145.84 103.21 16.51 o 3 8 0 615.50 666.77 28.98 o 4 8 0 1853.50 1659.52 55.21 o 5 8 0 936.21 900.95 47.45 o 6 8 0 609.09 716.01 55.90 o 7 8 0 5212.90 5550.88 260.84 o 8 8 0 672.92 716.00 60.20 o 9 8 0 646.65 610.62 58.05 o 10 8 0 1679.00 2011.26 148.42 o 11 8 0 1.56 27.94 60.18 o 12 8 0 227.96 156.92 55.89 o 13 8 0 166.44 331.03 90.28 o 14 8 0 34.32 -38.69 62.33 o -14 9 0 11.49 58.03 81.68 o -13 9 0 424.43 363.31 88.14 o -12 9 0 15.82 49.44 40.84 o -11 9 0 603.02 610.59 75.25 o -10 9 0 16.71 70.93 45.14 o -9 9 0 195.99 133.27 36.54 o -8 9 0 192.98 202.06 38.69 o -7 9 0 1127.94 1234.48 77.42 o -6 9 0 661.13 625.70 51.60 o -5 9 0 674.33 683.78 53.76 o -3 9 0 3288.41 3291.78 102.31 o -2 9 0 0.38 -3.22 7.60 o -1 9 0 0.31 10.09 9.79 o 0 9 0 4327.89 4741.81 182.17 o 1 9 0 343.24 298.41 19.59 o 2 9 0 6301.88 6300.78 256.86 o 3 9 0 61.60 101.71 45.14 o 4 9 0 141.56 163.61 23.76 o 5 9 0 51.72 60.18 32.24 o 6 9 0 1567.35 1516.66 77.45 o 7 9 0 22.47 47.29 40.84 o 8 9 0 2993.90 3330.12 161.45 o 9 9 0 43.80 58.03 51.59 o 10 9 0 845.93 920.29 94.61 o 11 9 0 1014.08 830.03 101.07 o 12 9 0 27.31 101.02 47.29 o 13 9 0 197.08 253.65 85.98 o 14 9 0 114.67 223.55 64.48 o -13 10 0 32.57 94.57 73.08 o -12 10 0 164.70 223.55 60.19 o -11 10 0 6.93 -53.73 135.41 o -10 10 0 1052.01 1075.19 94.62 o -9 10 0 0.46 40.84 42.99 o -8 10 0 1248.99 1169.97 92.48 o -7 10 0 26.89 -12.90 38.69 o -6 10 0 34.93 58.03 34.39 o -5 10 0 125.37 141.87 30.09 o -3 10 0 72.05 95.02 7.60 o -2 10 0 2022.34 1990.23 57.86 o -1 10 0 316.14 326.95 21.12 o 0 10 0 0.53 -8.94 14.38 o 1 10 0 5280.17 5703.57 356.90 o 2 10 0 4.44 39.81 16.27 o 3 10 0 10732.46 11147.24 383.96 o 4 10 0 162.01 238.60 38.69 o 5 10 0 1867.33 1766.48 94.67 o 6 10 0 22.64 75.23 42.99 o 7 10 0 1497.13 1675.64 111.85 o 8 10 0 951.73 1027.88 68.81 o 9 10 0 466.43 509.52 75.24 o 10 10 0 40.83 105.32 38.69 o 11 10 0 612.06 653.58 101.05 o 12 10 0 247.31 292.35 111.78 o 13 10 0 4.96 111.77 60.18 o 14 10 0 18.20 103.17 85.98 o -13 11 0 105.59 -60.19 60.19 o -12 11 0 320.64 419.18 83.84 o -11 11 0 82.24 103.17 60.19 o -10 11 0 17.00 36.54 58.03 o -9 11 0 1126.92 959.10 105.37 o -8 11 0 18.93 105.32 47.29 o -7 11 0 1804.56 1705.93 114.02 o -6 11 0 15.66 8.60 25.79 o -5 11 0 48.45 -15.05 25.79 o -3 11 0 0.63 6.14 5.16 o -2 11 0 122.95 93.52 12.16 o -1 11 0 1083.01 1089.30 43.32 o 0 11 0 69.81 49.24 16.51 o 1 11 0 2508.58 2806.37 98.77 o 2 11 0 8205.63 8929.48 407.04 o 3 11 0 783.32 818.49 47.22 o 4 11 0 1526.90 1656.39 94.65 o 5 11 0 370.67 451.46 51.60 o 6 11 0 340.11 339.66 43.00 o 7 11 0 86.08 141.87 49.44 o 8 11 0 1010.11 873.06 86.02 o 9 11 0 177.85 148.32 47.29 o 10 11 0 417.52 333.21 66.64 o 11 11 0 10.40 -23.64 53.74 o 12 11 0 464.51 414.91 98.89 o 13 11 0 16.46 53.74 96.72 o -12 12 0 92.31 -55.89 64.48 o -11 12 0 54.32 -23.64 62.33 o -10 12 0 0.60 -51.59 51.59 o -9 12 0 81.91 103.17 60.19 o -8 12 0 1081.05 1098.86 81.72 o -7 12 0 138.36 141.87 53.74 o -6 12 0 2920.63 2914.27 206.62 o -5 12 0 284.96 270.86 47.29 o -3 12 0 237.45 187.02 10.75 o -2 12 0 2960.66 3173.34 102.97 o -1 12 0 89.84 103.12 24.72 o 0 12 0 4028.09 4231.84 200.32 o 1 12 0 47.15 48.32 19.35 o 2 12 0 819.04 857.07 48.12 o 3 12 0 2.00 -17.20 34.39 o 4 12 0 42.15 38.69 27.94 o 5 12 0 91.64 174.11 38.69 o 6 12 0 148.86 51.59 47.29 o 7 12 0 469.32 483.72 64.50 o 8 12 0 2.94 0.00 55.88 o 9 12 0 88.45 150.46 45.14 o 10 12 0 64.94 66.63 45.14 o 11 12 0 994.49 1004.16 118.26 o 12 12 0 0.22 32.24 62.33 o -11 13 0 14.53 81.68 55.88 o -10 13 0 188.68 279.44 75.23 o -9 13 0 153.28 88.13 70.93 o -8 13 0 226.75 133.28 49.44 o -7 13 0 837.74 821.37 83.86 o -6 13 0 29.05 -6.45 32.24 o -5 13 0 1477.52 1423.87 111.84 o -2 13 0 15.28 38.06 20.42 o -1 13 0 181.71 199.26 42.99 o 0 13 0 349.84 319.85 28.92 o 1 13 0 1324.46 1227.79 144.10 o 2 13 0 228.33 266.55 42.99 o 3 13 0 25.15 -6.45 34.39 o 4 13 0 183.30 219.26 40.84 o 5 13 0 13.50 42.99 36.54 o 6 13 0 547.96 543.93 58.05 o 7 13 0 46.31 55.89 51.59 o 8 13 0 613.49 569.74 77.40 o 9 13 0 15.88 -60.18 60.18 o 10 13 0 27.51 -34.39 49.44 o 11 13 0 63.64 15.05 60.18 o 12 13 0 218.56 268.70 81.68 o -10 14 0 31.84 -60.18 60.18 o -9 14 0 243.35 148.32 58.04 o -7 14 0 273.29 257.96 70.94 o -6 14 0 456.09 380.52 60.19 o -5 14 0 21.77 -36.54 36.54 o -1 14 0 222.21 275.15 30.09 o 0 14 0 20.33 47.29 30.09 o 1 14 0 0.48 -12.90 30.09 o 2 14 0 368.57 369.76 45.14 o 3 14 0 108.98 159.06 38.69 o 4 14 0 236.00 197.77 51.59 o 5 14 0 484.73 565.41 66.65 o 6 14 0 48.30 21.49 40.84 o 7 14 0 1235.35 1279.55 152.69 o 8 14 0 1.66 42.99 62.33 o 9 14 0 348.44 234.32 60.19 o 10 14 0 79.16 189.15 88.13 o 11 14 0 5.89 0.00 70.93 o -9 15 0 36.84 68.78 70.93 o -8 15 0 491.06 505.20 105.34 o -7 15 0 52.23 30.09 62.33 o -6 15 0 503.35 543.91 85.99 o -5 15 0 90.46 45.14 64.48 o -4 15 0 10.02 85.98 40.84 o 0 15 0 1.34 -23.64 25.79 o 1 15 0 42.84 60.18 36.54 o 2 15 0 68.18 27.94 38.69 o 3 15 0 509.40 509.52 66.65 o 4 15 0 36.28 -32.24 32.24 o 5 15 0 1158.98 1410.69 118.27 o 6 15 0 150.82 141.87 40.84 o 7 15 0 425.01 288.07 64.49 o 8 15 0 270.03 163.37 55.89 o 9 15 0 0.03 -68.78 79.53 o 10 15 0 9.73 -4.30 66.63 o -8 16 0 63.93 262.23 94.58 o -7 16 0 104.87 79.53 58.04 o -6 16 0 54.39 6.45 66.63 o -5 16 0 360.16 440.69 75.24 o -4 16 0 363.48 376.20 75.24 o 2 16 0 10.82 -23.64 42.99 o 3 16 0 151.97 202.06 53.74 o 4 16 0 465.92 382.67 64.49 o 5 16 0 2.10 30.09 64.48 o 6 16 0 617.19 677.23 98.90 o 7 16 0 51.56 -30.09 55.89 o 8 16 0 175.04 262.24 68.79 o -7 17 0 21.25 85.98 79.53 o -6 17 0 160.29 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