#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2012026.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012026_Fobs loop_ _publ_author_name 'Goeta, Andr\`es E.' 'Hughes, Andrew K.' 'Malget, John M.' _publ_section_title ; \m-Oxo-bis[(\h^5^-1,2-dicarbaundecaborato)bis(N,N-dimethylacetamidinato)tantalum] dichloromethane hemisolvate ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 702 _journal_page_last 703 _journal_volume 57 _journal_year 2001 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.303 _cell_angle_gamma 90.000 _cell_length_a 11.4141 _cell_length_b 10.7689 _cell_length_c 17.8633 _exptl_crystal_F_000 998.00 _reflns_d_resolution_high 0.7019 _[local]_cod_data_source_file gd1146IIIsup2.hkl _[local]_cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' 00srv012 in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 323.77 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 -15 0 80.53 -40.94 213.63 o 0 -14 0 23.81 70.99 245.65 o 1 -14 0 25.28 319.94 219.57 o 2 -14 0 350.54 312.26 139.78 o 3 -14 0 271.68 18.73 144.70 o 4 -14 0 358.74 675.92 155.74 o 5 -14 0 1611.24 1675.39 289.57 o 6 -14 0 639.47 431.54 282.96 o 1 -13 0 3312.26 3702.36 196.76 o 2 -13 0 2644.44 2596.60 162.55 o 3 -13 0 135.20 99.63 128.60 o 4 -13 0 1028.66 1268.30 150.57 o 5 -13 0 1625.79 1761.95 174.17 o 6 -13 0 118.35 197.12 234.43 o 7 -13 0 389.61 291.61 163.09 o 8 -13 0 85.30 2.01 179.52 o 0 -12 0 1086.81 1144.78 270.58 o 1 -12 0 309.67 363.77 105.97 o 2 -12 0 546.27 431.41 95.52 o 3 -12 0 478.02 479.39 93.01 o 4 -12 0 522.41 304.05 216.43 o 5 -12 0 1985.37 2199.63 167.15 o 6 -12 0 1211.81 1347.53 152.68 o 7 -12 0 496.67 394.79 408.60 o 8 -12 0 2595.00 2638.82 191.97 o 9 -12 0 1010.55 810.94 162.26 o 1 -11 0 4507.32 4803.69 103.14 o 2 -11 0 4729.95 5181.32 172.62 o 3 -11 0 814.46 1075.35 136.20 o 4 -11 0 1616.39 1641.08 178.46 o 5 -11 0 1898.57 2088.23 149.65 o 6 -11 0 698.87 708.94 126.96 o 7 -11 0 963.10 1042.34 147.77 o 8 -11 0 323.64 523.10 139.12 o 9 -11 0 318.38 -55.09 142.64 o 10 -11 0 461.77 494.59 169.85 o 0 -10 0 3043.32 3232.80 146.77 o 1 -10 0 1417.06 1449.99 88.93 o 2 -10 0 1577.29 1499.25 87.68 o 3 -10 0 3209.75 3642.23 152.85 o 4 -10 0 954.06 1089.00 120.33 o 5 -10 0 4335.39 4106.94 165.79 o 6 -10 0 2561.20 2836.05 157.33 o 7 -10 0 630.00 806.70 157.33 o 8 -10 0 3581.10 4089.39 208.01 o 9 -10 0 1752.57 1964.77 149.38 o 10 -10 0 37.77 15.72 145.18 o 11 -10 0 1436.62 1597.33 177.79 o 1 -9 0 8254.94 7864.13 141.06 o 2 -9 0 6696.07 6383.92 304.04 o 3 -9 0 2010.79 1842.35 136.01 o 4 -9 0 3199.19 3352.97 256.38 o 5 -9 0 3065.80 3253.83 204.05 o 6 -9 0 2619.29 2706.50 139.36 o 7 -9 0 2750.84 2841.33 153.68 o 8 -9 0 469.86 256.62 122.77 o 9 -9 0 1316.37 1296.22 203.72 o 10 -9 0 2344.28 2265.65 176.04 o 11 -9 0 360.97 521.53 151.28 o 12 -9 0 886.73 928.70 389.12 o 1 -8 0 3121.43 3056.48 134.33 o 2 -8 0 2299.23 2307.21 92.13 o 3 -8 0 8532.05 8053.43 110.56 o 4 -8 0 6797.95 6293.53 268.93 o 5 -8 0 5632.89 5597.43 232.28 o 6 -8 0 4028.63 3949.58 150.68 o 7 -8 0 1082.12 927.96 108.96 o 8 -8 0 4808.85 5102.90 189.28 o 9 -8 0 2442.09 2506.73 160.96 o 10 -8 0 211.98 216.28 122.52 o 11 -8 0 2243.27 2297.69 176.03 o 12 -8 0 1139.47 1356.48 310.37 o 13 -8 0 644.54 538.19 203.06 o 1 -7 0 6243.84 5842.42 143.61 o 2 -7 0 5938.22 5704.95 110.01 o 3 -7 0 2478.80 2383.20 94.55 o 4 -7 0 7574.11 7534.97 116.77 o 5 -7 0 4664.36 4290.00 148.36 o 6 -7 0 7439.98 7395.39 379.21 o 7 -7 0 6706.96 6620.00 184.01 o 8 -7 0 581.67 537.03 103.88 o 9 -7 0 1938.89 2000.97 148.32 o 10 -7 0 3992.69 3939.36 178.90 o 11 -7 0 1553.07 1403.63 148.17 o 12 -7 0 824.90 643.16 259.36 o 13 -7 0 1341.87 1469.57 171.23 o 1 -6 0 12429.32 12025.37 171.79 o 2 -6 0 2226.06 2440.30 74.14 o 3 -6 0 11199.33 11030.95 105.13 o 4 -6 0 4606.37 4616.58 123.10 o 5 -6 0 6825.57 6638.25 330.51 o 6 -6 0 3646.03 3612.76 141.06 o 7 -6 0 831.93 967.41 111.05 o 8 -6 0 4262.86 4576.63 160.54 o 9 -6 0 2003.93 2152.93 138.54 o 10 -6 0 373.44 328.56 116.07 o 11 -6 0 2353.83 2642.01 166.00 o 12 -6 0 1447.47 1583.91 180.44 o 13 -6 0 1304.60 1059.01 165.70 o 14 -6 0 877.46 968.39 162.65 o 1 -5 0 3964.79 3487.22 101.54 o 2 -5 0 8824.21 8782.55 118.26 o 3 -5 0 10990.00 10889.32 92.90 o 4 -5 0 14101.71 14056.58 160.33 o 5 -5 0 2306.59 2426.51 51.98 o 6 -5 0 12309.55 12415.92 210.82 o 7 -5 0 13200.79 13072.88 227.86 o 8 -5 0 1691.47 1794.71 202.07 o 9 -5 0 4661.20 4928.65 174.30 o 10 -5 0 8070.02 7839.82 443.76 o 11 -5 0 1120.74 1085.19 127.83 o 12 -5 0 1163.04 872.53 141.04 o 13 -5 0 1891.71 2064.93 164.75 o 14 -5 0 604.95 505.32 166.09 o 1 -4 0 15259.03 15644.58 338.93 o 2 -4 0 3083.68 2965.09 65.53 o 3 -4 0 28107.35 28590.56 234.59 o 4 -4 0 15670.74 15515.49 97.26 o 5 -4 0 3123.46 3174.30 126.77 o 6 -4 0 6007.88 5793.07 182.24 o 7 -4 0 2236.00 2189.10 239.05 o 8 -4 0 2402.14 2435.78 130.89 o 9 -4 0 1953.70 1766.87 128.44 o 10 -4 0 407.92 385.53 108.68 o 11 -4 0 1520.22 1788.14 138.80 o 12 -4 0 817.87 740.08 131.90 o 13 -4 0 2034.38 2059.34 172.88 o 14 -4 0 1777.90 1820.79 177.15 o 1 -3 0 4327.75 4834.55 94.27 o 2 -3 0 12158.09 12808.67 88.71 o 3 -3 0 10456.79 12222.45 160.22 o 4 -3 0 6745.00 5900.79 60.05 o 5 -3 0 4107.96 4397.54 72.64 o 6 -3 0 16978.56 15798.74 176.20 o 7 -3 0 20848.78 20623.04 182.40 o 8 -3 0 1370.82 1395.78 111.55 o 9 -3 0 6536.15 7129.37 194.20 o 10 -3 0 14096.13 13351.95 270.28 o 11 -3 0 2652.93 2781.85 156.67 o 12 -3 0 1765.27 1744.92 237.40 o 13 -3 0 3377.58 3695.82 194.60 o 14 -3 0 898.12 830.42 150.94 o 15 -3 0 127.18 82.20 162.88 o 1 -2 0 14673.87 12242.74 374.50 o 2 -2 0 4559.55 4482.55 62.53 o 3 -2 0 28449.63 29474.92 336.55 o 4 -2 0 15821.23 17314.21 490.21 o 5 -2 0 4596.14 5611.58 58.65 o 6 -2 0 7357.79 6958.54 108.90 o 7 -2 0 2442.24 2381.60 61.86 o 8 -2 0 499.62 485.44 65.73 o 9 -2 0 318.14 208.69 104.67 o 10 -2 0 1218.85 1431.06 167.24 o 11 -2 0 600.92 575.37 126.54 o 12 -2 0 731.72 891.78 158.32 o 13 -2 0 3531.47 3974.42 197.79 o 14 -2 0 2173.47 2311.09 181.49 o 15 -2 0 162.34 146.24 142.46 o 1 -1 0 1279.60 599.68 19.95 o 2 -1 0 1501.52 1951.97 57.62 o 3 -1 0 20135.89 22565.38 397.41 o 4 -1 0 14960.29 14678.50 264.50 o 5 -1 0 706.33 760.76 44.73 o 6 -1 0 23697.77 23905.50 309.79 o 7 -1 0 28509.60 28546.43 244.10 o 8 -1 0 916.68 1084.76 110.28 o 9 -1 0 8569.25 8448.97 139.30 o 10 -1 0 14249.59 14603.97 274.39 o 11 -1 0 2866.56 2746.57 175.16 o 12 -1 0 1248.57 1283.11 145.78 o 13 -1 0 4745.01 4719.46 200.84 o 14 -1 0 1080.53 1075.98 263.48 o 15 -1 0 86.91 139.41 153.74 o 1 0 0 45659.95 38588.26 463.08 o 2 0 0 30031.05 33474.34 192.87 o 3 0 0 30050.70 29154.10 317.16 o 4 0 0 17316.10 17343.31 129.25 o 5 0 0 848.39 864.95 57.28 o 6 0 0 3885.53 3920.11 92.28 o 7 0 0 6080.65 6184.74 142.59 o 8 0 0 13.99 5.46 51.27 o 9 0 0 12.84 -54.53 54.53 o 10 0 0 656.66 651.28 89.43 o 11 0 0 868.74 793.70 116.73 o 12 0 0 536.29 506.99 145.44 o 13 0 0 3201.49 3385.96 301.45 o 14 0 0 1407.18 1736.88 205.21 o 15 0 0 132.76 -28.26 143.71 o 1 1 0 1352.35 589.21 27.03 o 2 1 0 1407.32 1879.13 44.48 o 3 1 0 19899.53 22429.64 237.33 o 4 1 0 14777.26 14603.00 107.43 o 5 1 0 687.04 727.47 50.82 o 6 1 0 23504.94 24245.93 218.43 o 7 1 0 28425.89 27992.38 185.62 o 8 1 0 949.53 1048.35 60.68 o 9 1 0 8443.60 7865.51 184.29 o 10 1 0 14234.19 13967.92 160.03 o 11 1 0 2883.06 2850.63 114.38 o 12 1 0 1260.25 1220.73 130.51 o 13 1 0 4747.62 4658.44 200.43 o 14 1 0 1064.95 1054.64 153.85 o 15 1 0 86.79 -71.53 161.07 o 0 2 0 54021.05 54641.87 467.70 o 1 2 0 14358.94 12554.24 179.42 o 2 2 0 4767.58 4849.86 144.69 o 3 2 0 28281.69 29830.18 279.99 o 4 2 0 15956.93 17553.86 166.11 o 5 2 0 4641.32 5557.00 104.42 o 6 2 0 7355.30 7152.22 99.90 o 7 2 0 2415.59 2390.40 90.79 o 8 2 0 509.72 547.96 59.30 o 9 2 0 312.55 265.44 59.22 o 10 2 0 1223.23 1329.90 75.93 o 11 2 0 600.89 701.17 73.25 o 12 2 0 727.39 655.92 124.07 o 13 2 0 3514.25 3759.63 194.41 o 14 2 0 2176.19 2380.37 179.36 o 15 2 0 159.13 -35.73 159.47 o 1 3 0 4513.13 5245.81 177.22 o 2 3 0 12380.36 12719.83 499.92 o 3 3 0 10283.77 12155.28 448.45 o 4 3 0 6514.97 5998.92 120.24 o 5 3 0 4141.84 4371.95 85.69 o 6 3 0 16821.01 15990.03 182.86 o 7 3 0 20892.20 21141.96 178.55 o 8 3 0 1345.02 1269.11 72.30 o 9 3 0 6581.04 6490.94 119.45 o 10 3 0 14076.87 13947.79 197.25 o 11 3 0 2689.24 2673.58 98.24 o 12 3 0 1774.25 1652.40 120.33 o 13 3 0 3406.52 3706.79 198.35 o 14 3 0 887.80 619.19 368.64 o 15 3 0 124.79 87.46 179.15 o 0 4 0 59159.32 56658.97 367.16 o 1 4 0 15084.22 15690.41 130.59 o 2 4 0 3166.86 3094.05 188.01 o 3 4 0 28131.94 28798.60 453.34 o 4 4 0 15794.93 15744.64 229.99 o 5 4 0 3180.45 3143.41 79.30 o 6 4 0 6067.51 6013.61 134.68 o 7 4 0 2212.70 2103.70 78.67 o 8 4 0 2422.81 2346.76 105.51 o 9 4 0 1945.37 1841.07 84.22 o 10 4 0 416.47 315.77 74.17 o 11 4 0 1497.23 1651.64 89.73 o 12 4 0 826.28 710.56 82.71 o 13 4 0 2013.63 1865.75 133.24 o 14 4 0 1782.61 1895.66 184.80 o 15 4 0 276.92 465.92 170.23 o 1 5 0 4069.19 3478.23 71.82 o 2 5 0 9013.61 9244.54 240.35 o 3 5 0 11051.42 10868.58 166.71 o 4 5 0 14064.81 14195.20 533.33 o 5 5 0 2230.12 2346.47 119.21 o 6 5 0 12136.86 12067.54 362.67 o 7 5 0 13120.61 13063.65 220.90 o 8 5 0 1703.83 1742.04 81.80 o 9 5 0 4656.62 4609.53 118.11 o 10 5 0 8092.18 7812.85 173.80 o 11 5 0 1142.09 1085.44 121.61 o 12 5 0 1177.12 1172.95 96.22 o 13 5 0 1855.87 1766.09 115.31 o 14 5 0 594.64 501.42 179.44 o 15 5 0 625.00 675.25 488.33 o 0 6 0 24332.44 24018.62 290.89 o 1 6 0 12321.55 12321.68 206.21 o 2 6 0 2323.10 2820.48 120.68 o 3 6 0 11046.49 10979.60 514.91 o 4 6 0 4646.31 4720.26 158.16 o 5 6 0 6824.41 6734.17 130.72 o 6 6 0 3587.76 3488.04 95.27 o 7 6 0 853.52 910.64 75.59 o 8 6 0 4219.67 4274.07 154.12 o 9 6 0 2013.70 2161.78 142.49 o 10 6 0 381.89 298.69 77.08 o 11 6 0 2370.56 2378.42 171.71 o 12 6 0 1458.59 1435.92 108.53 o 13 6 0 1304.33 1347.49 145.54 o 14 6 0 884.96 1039.51 130.36 o 1 7 0 6223.40 6218.80 310.08 o 2 7 0 6074.00 6273.46 128.37 o 3 7 0 2461.51 2449.49 111.11 o 4 7 0 7611.63 7372.98 207.35 o 5 7 0 4657.78 4480.91 145.70 o 6 7 0 7441.45 7257.98 182.91 o 7 7 0 6710.57 6572.10 135.42 o 8 7 0 574.51 558.12 73.35 o 9 7 0 1942.86 1820.92 98.31 o 10 7 0 4032.68 3860.08 123.76 o 11 7 0 1579.48 1594.05 105.18 o 12 7 0 820.90 767.74 117.86 o 13 7 0 1348.27 1268.81 248.16 o 14 7 0 530.97 587.95 160.14 o 0 8 0 4500.82 4466.53 155.51 o 1 8 0 3136.88 3303.55 210.02 o 2 8 0 2230.18 2287.27 160.81 o 3 8 0 8567.02 7930.57 174.22 o 4 8 0 6878.99 6680.10 315.16 o 5 8 0 5613.71 5330.99 279.00 o 6 8 0 4038.34 4142.87 152.10 o 7 8 0 1057.38 1036.02 106.87 o 8 8 0 4835.62 4835.86 173.12 o 9 8 0 2452.16 2357.56 123.01 o 10 8 0 204.01 -37.55 101.73 o 11 8 0 2244.79 2437.66 169.18 o 12 8 0 1128.19 1053.76 137.44 o 13 8 0 637.17 714.03 144.21 o 1 9 0 8185.15 8060.58 312.40 o 2 9 0 6582.27 6630.60 277.06 o 3 9 0 2060.37 2105.90 140.99 o 4 9 0 3247.60 3200.62 193.15 o 5 9 0 3005.10 2880.33 293.53 o 6 9 0 2614.35 2574.73 191.50 o 7 9 0 2700.59 2710.20 145.33 o 8 9 0 472.85 333.06 111.39 o 9 9 0 1318.59 1359.80 167.40 o 10 9 0 2355.85 2463.45 161.31 o 11 9 0 367.47 446.46 125.54 o 12 9 0 897.85 799.96 144.17 o 0 10 0 3032.60 3183.58 192.49 o 1 10 0 1414.92 1248.15 86.07 o 2 10 0 1605.71 1457.20 106.92 o 3 10 0 3208.51 3226.84 215.77 o 4 10 0 953.54 872.07 108.16 o 5 10 0 4378.01 4153.13 164.20 o 6 10 0 2561.85 2609.59 144.97 o 7 10 0 631.78 599.98 116.45 o 8 10 0 3551.62 3645.59 174.49 o 9 10 0 1758.21 1712.14 146.04 o 10 10 0 35.99 111.07 119.17 o 11 10 0 1436.08 1662.34 160.11 o 1 11 0 4518.69 5009.47 244.33 o 2 11 0 4686.50 5280.45 448.55 o 3 11 0 795.85 732.85 104.19 o 4 11 0 1622.42 1402.81 121.85 o 5 11 0 1898.46 1803.09 133.16 o 6 11 0 710.37 620.41 130.26 o 7 11 0 967.12 1143.43 138.51 o 8 11 0 324.50 360.54 119.92 o 9 11 0 322.33 272.14 355.77 o 10 11 0 473.96 530.56 149.26 o 1 12 0 296.36 123.16 157.50 o 2 12 0 538.86 344.05 171.03 o 3 12 0 485.42 503.22 125.72 o 4 12 0 518.51 496.01 117.44 o 5 12 0 1973.38 2086.77 145.59 o 6 12 0 1205.71 1239.21 134.01 o 7 12 0 505.59 531.91 130.84 o 8 12 0 2593.23 2506.56 172.50 o 2 13 0 2626.40 3000.99 229.14 o 3 13 0 140.82 72.64 169.38 o 4 13 0 1017.28 839.97 203.06 o 5 13 0 1632.30 2014.75 244.66 o 6 13 0 124.91 92.82 143.36 o 7 13 0 377.35 391.55 151.03 o 3 14 0 270.27 489.98 227.16 o 4 14 0 353.04 42.26 209.66 o 5 14 0 1604.06 2009.14 244.33 o -3 -15 1 97.91 45.32 168.49 o 2 -15 1 477.51 250.28 270.09 o 3 -15 1 15.66 279.06 311.03 o -6 -14 1 279.48 756.77 301.78 o -5 -14 1 1374.92 1336.58 223.04 o -4 -14 1 272.90 271.60 147.05 o -3 -14 1 829.55 926.57 159.60 o -2 -14 1 2769.14 3147.77 254.83 o -1 -14 1 1052.16 837.99 286.60 o 0 -14 1 354.89 703.28 238.06 o 1 -14 1 2433.69 3261.17 296.50 o 2 -14 1 1336.42 1295.06 203.22 o 3 -14 1 122.92 173.25 149.98 o 4 -14 1 800.89 987.36 175.96 o 5 -14 1 237.55 252.44 158.04 o -8 -13 1 1076.36 1315.10 283.95 o -7 -13 1 34.91 95.26 148.99 o -6 -13 1 1159.02 1168.00 167.87 o -5 -13 1 904.80 1124.20 159.24 o -4 -13 1 101.79 26.54 128.83 o -3 -13 1 458.74 173.61 129.83 o -2 -13 1 62.93 233.72 118.24 o -1 -13 1 267.67 252.09 108.39 o 0 -13 1 244.98 177.28 149.75 o 1 -13 1 686.96 913.25 141.93 o 2 -13 1 1042.06 1057.44 199.92 o 3 -13 1 128.92 80.59 102.56 o 4 -13 1 1410.30 1164.04 162.95 o 5 -13 1 2701.27 2804.81 235.09 o 6 -13 1 350.44 346.74 159.87 o 7 -13 1 913.29 907.59 184.54 o 8 -13 1 1914.57 2070.88 270.09 o -10 -12 1 405.69 364.85 249.95 o -9 -12 1 146.65 1.09 159.41 o -8 -12 1 670.46 538.78 263.15 o -7 -12 1 702.24 718.07 147.00 o -6 -12 1 858.87 1217.94 180.94 o -5 -12 1 2361.77 2321.39 125.21 o -4 -12 1 730.45 884.99 130.33 o -3 -12 1 1050.04 1048.62 125.18 o -2 -12 1 4948.05 4987.81 272.56 o -1 -12 1 2021.79 2124.19 125.96 o 0 -12 1 386.72 378.90 68.54 o 1 -12 1 3750.88 3906.66 119.89 o 2 -12 1 1664.54 1908.72 193.48 o 3 -12 1 244.89 244.80 123.45 o 4 -12 1 1026.69 1326.75 145.08 o 5 -12 1 732.54 829.23 139.40 o 6 -12 1 465.48 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