#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:33:14 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180789 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/20/2012064.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012064_Fobs loop_ _publ_author_name 'Steinberger, Hans-Uwe' 'Ziemer, Burkhard' 'Meisel, Manfred' _publ_section_title ; Tris(tert-butyl)phosphine sulfide, a phosphine sulfide with three bulky substituents ; _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 835 _journal_page_last 837 _journal_volume 57 _journal_year 2001 _space_group_IT_number 205 _symmetry_space_group_name_Hall '-P 2ac 2ab 3' _symmetry_space_group_name_H-M 'P a -3' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.2320 _cell_length_b 14.2320 _cell_length_c 14.2320 _exptl_crystal_F_000 1040.00 _reflns_d_resolution_high 0.8258 _cod_data_source_file bj1020Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' UST70FS' _shelx_refln_list_code 4 _shelx_f_calc_maximum 182.99 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' 'y, z, x' '-y+1/2, -z, x+1/2' 'y+1/2, -z+1/2, -x' '-y, z+1/2, -x+1/2' 'z, x, y' '-z, x+1/2, -y+1/2' '-z+1/2, -x, y+1/2' 'z+1/2, -x+1/2, -y' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' '-y, -z, -x' 'y-1/2, z, -x-1/2' '-y-1/2, z-1/2, x' 'y, -z-1/2, x-1/2' '-z, -x, -y' 'z, -x-1/2, y-1/2' 'z-1/2, x, -y-1/2' '-z-1/2, x-1/2, y' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 1 7427.32 7148.53 52.57 o 0 0 2 29005.73 29397.73 152.32 o 1 0 2 33485.91 33828.21 54.99 o 1 1 2 13032.07 12523.54 22.54 o 0 2 2 75.07 38.25 3.83 o 1 2 2 10.45 32.69 2.64 o 2 2 2 1602.17 1560.77 9.25 o 1 1 3 1389.09 1354.17 8.56 o 2 1 3 1431.88 1556.89 6.76 o 0 2 3 1415.32 1364.93 8.88 o 1 2 3 24.02 37.07 4.32 o 2 2 3 0.73 69.00 4.74 o 1 3 3 1365.64 1373.99 18.78 o 2 3 3 1.89 31.22 4.38 o 3 3 3 11763.35 10975.15 28.47 o 0 0 4 8669.22 8602.00 36.44 o 1 0 4 10911.03 11053.17 18.30 o 2 0 4 16973.32 17515.65 92.36 o 3 0 4 587.05 572.33 10.80 o 1 1 4 3875.32 3473.15 14.49 o 2 1 4 1018.51 1024.07 9.70 o 3 1 4 1973.13 1965.22 32.34 o 0 2 4 23502.27 23203.46 41.96 o 1 2 4 226.88 328.42 6.08 o 2 2 4 12982.20 12747.77 30.01 o 3 2 4 54.74 200.08 5.75 o 1 3 4 86.87 215.38 5.75 o 3 3 4 2942.72 3093.20 16.02 o 0 4 4 11621.06 11548.29 40.66 o 1 4 4 115.32 148.10 13.01 o 2 4 4 5188.81 4888.41 20.19 o 3 4 4 2755.40 2978.06 16.52 o 4 4 4 717.10 705.01 9.28 o 1 1 5 1110.74 1334.86 10.45 o 2 1 5 4993.74 5090.63 36.60 o 3 1 5 98.70 389.02 4.95 o 4 1 5 412.06 566.02 5.86 o 0 2 5 4320.72 4473.17 18.38 o 1 2 5 3886.94 4083.14 17.76 o 2 2 5 26.06 68.02 5.04 o 4 2 5 5627.01 5727.80 23.19 o 1 3 5 237.19 337.36 6.80 o 2 3 5 4065.96 4096.82 18.86 o 3 3 5 1484.58 1332.17 11.68 o 4 3 5 1775.83 1562.42 12.90 o 1 4 5 444.90 664.60 8.82 o 2 4 5 639.86 1080.40 10.85 o 3 4 5 228.33 276.45 7.00 o 4 4 5 4450.86 4280.17 21.49 o 1 5 5 106.67 169.43 4.43 o 2 5 5 38.35 63.14 5.63 o 3 5 5 247.91 272.96 7.12 o 4 5 5 726.38 791.66 10.53 o 5 5 5 74.29 97.05 6.38 o 0 0 6 15221.44 15541.94 26.24 o 1 0 6 160.90 306.83 6.32 o 2 0 6 20.91 16.28 6.20 o 3 0 6 2897.40 2878.17 11.76 o 4 0 6 8996.23 8732.10 54.74 o 5 0 6 6032.66 6000.47 27.39 o 1 1 6 815.99 831.01 9.43 o 2 1 6 4862.97 5013.99 15.04 o 4 1 6 93.19 115.81 4.29 o 5 1 6 157.42 219.79 14.33 o 0 2 6 508.93 603.64 8.38 o 1 2 6 6508.65 6589.12 24.34 o 2 2 6 5174.77 5064.05 21.71 o 3 2 6 1026.71 907.60 10.38 o 4 2 6 4195.42 3747.39 20.01 o 5 2 6 879.62 885.94 11.12 o 1 3 6 977.63 1191.58 11.28 o 2 3 6 10.64 19.96 5.15 o 3 3 6 9.81 80.20 5.54 o 4 3 6 1054.79 1031.70 11.55 o 5 3 6 490.31 576.06 9.54 o 0 4 6 3873.32 3667.73 19.53 o 1 4 6 1177.17 1361.65 12.53 o 2 4 6 4991.86 4689.03 22.28 o 3 4 6 630.26 762.46 10.14 o 4 4 6 261.26 293.02 7.66 o 5 4 6 7.60 32.50 5.81 o 1 5 6 1907.81 1957.21 15.26 o 2 5 6 2399.25 2403.46 17.03 o 3 5 6 514.51 555.48 9.57 o 4 5 6 741.28 667.04 10.29 o 5 5 6 78.27 93.38 6.70 o 0 6 6 13156.49 12617.68 120.88 o 1 6 6 1005.22 905.84 8.16 o 2 6 6 5895.85 5369.92 25.94 o 3 6 6 546.69 718.99 10.88 o 4 6 6 376.71 400.05 9.42 o 5 6 6 56.37 58.34 6.38 o 6 6 6 124.00 90.46 7.45 o 1 1 7 1893.65 1834.80 14.07 o 2 1 7 647.88 772.53 6.98 o 3 1 7 511.53 531.85 6.19 o 4 1 7 246.24 267.22 5.16 o 5 1 7 1.96 44.30 4.05 o 6 1 7 271.23 380.19 6.45 o 0 2 7 1031.05 1163.51 11.64 o 1 2 7 1406.23 1454.82 12.81 o 2 2 7 756.02 732.03 9.75 o 3 2 7 110.68 271.99 7.18 o 4 2 7 413.03 625.16 9.84 o 5 2 7 1593.56 1676.78 15.25 o 6 2 7 1965.89 1884.51 16.69 o 1 3 7 894.43 854.39 10.56 o 2 3 7 795.44 890.25 10.95 o 3 3 7 235.17 211.68 6.91 o 4 3 7 1.62 30.90 5.90 o 5 3 7 352.91 376.05 8.82 o 6 3 7 1.75 109.10 7.24 o 0 4 7 608.50 616.08 9.60 o 1 4 7 844.05 875.22 10.98 o 2 4 7 48.03 200.88 6.97 o 3 4 7 157.01 183.35 7.06 o 4 4 7 593.59 546.20 9.78 o 5 4 7 1314.12 1474.19 14.95 o 6 4 7 1384.81 1276.77 14.83 o 1 5 7 19.56 96.38 6.32 o 2 5 7 794.89 903.10 11.75 o 3 5 7 68.44 158.21 7.18 o 4 5 7 93.28 193.77 7.66 o 5 5 7 15.08 74.48 7.24 o 6 5 7 20.38 43.86 6.76 o 0 6 7 68.18 158.24 7.66 o 1 6 7 1002.37 1015.71 12.88 o 2 6 7 403.27 569.00 10.43 o 3 6 7 11.82 60.72 6.82 o 4 6 7 332.57 469.04 10.31 o 5 6 7 161.62 217.38 8.43 o 6 6 7 568.04 581.01 11.45 o 1 7 7 964.34 1050.22 9.57 o 2 7 7 1055.67 958.42 13.27 o 3 7 7 1917.63 1994.93 18.36 o 4 7 7 637.36 550.32 11.30 o 5 7 7 268.03 230.78 9.06 o 6 7 7 125.22 124.37 8.07 o 7 7 7 637.18 658.01 13.15 o 0 0 8 1220.84 1035.30 24.59 o 1 0 8 3491.14 3615.06 14.54 o 2 0 8 3604.45 3281.50 14.03 o 3 0 8 864.49 746.15 7.52 o 4 0 8 1068.95 1189.86 9.31 o 5 0 8 6396.55 6284.30 77.49 o 6 0 8 3205.35 3237.22 26.78 o 7 0 8 6514.62 6253.73 58.61 o 1 1 8 1450.57 1546.25 13.94 o 2 1 8 1.67 72.19 16.25 o 3 1 8 980.45 982.86 8.39 o 4 1 8 765.11 827.64 8.09 o 5 1 8 458.76 507.30 15.66 o 6 1 8 6.40 50.55 5.14 o 7 1 8 3373.24 3047.58 53.35 o 0 2 8 4683.88 4255.80 22.47 o 1 2 8 306.60 277.18 7.57 o 2 2 8 6644.33 6375.66 27.77 o 3 2 8 1401.18 1294.94 13.46 o 4 2 8 744.84 753.37 11.12 o 5 2 8 2760.05 2519.66 19.21 o 6 2 8 613.59 586.51 11.09 o 7 2 8 2701.75 2488.95 20.52 o 1 3 8 34.78 119.98 6.61 o 2 3 8 1388.30 1438.46 14.23 o 3 3 8 8.75 17.91 5.75 o 4 3 8 1044.59 1035.22 12.89 o 5 3 8 394.94 443.56 9.72 o 6 3 8 142.11 169.67 7.96 o 7 3 8 185.86 209.57 8.97 o 0 4 8 1000.77 1059.11 12.94 o 1 4 8 1940.89 1802.62 15.88 o 2 4 8 1774.13 1802.62 16.03 o 3 4 8 778.66 798.79 11.72 o 4 4 8 372.95 371.93 9.57 o 5 4 8 2.71 102.91 7.15 o 6 4 8 1302.74 1292.64 15.36 o 7 4 8 7.95 28.87 7.39 o 1 5 8 1469.03 1482.46 15.28 o 2 5 8 108.93 155.57 7.72 o 3 5 8 2785.92 2789.82 20.53 o 4 5 8 0.35 122.27 7.57 o 5 5 8 689.98 600.67 11.72 o 6 5 8 521.75 562.59 11.60 o 7 5 8 808.68 913.69 14.58 o 0 6 8 2479.19 2473.88 19.95 o 1 6 8 10165.26 9969.59 38.61 o 2 6 8 760.85 799.75 12.49 o 3 6 8 579.69 559.89 11.15 o 4 6 8 699.77 742.76 12.73 o 5 6 8 460.86 441.75 10.94 o 6 6 8 188.08 200.48 9.09 o 7 6 8 583.72 435.70 11.54 o 1 7 8 765.96 802.35 12.97 o 2 7 8 653.71 685.40 12.37 o 3 7 8 2366.87 2211.20 20.03 o 4 7 8 398.48 421.28 10.67 o 5 7 8 887.51 893.77 14.43 o 6 7 8 539.17 500.01 12.19 o 7 7 8 267.35 198.67 10.01 o 0 8 8 1178.77 1269.37 11.65 o 1 8 8 1024.09 1087.30 10.68 o 2 8 8 93.40 119.48 7.87 o 3 8 8 283.68 295.29 9.98 o 4 8 8 1544.00 1539.65 17.72 o 5 8 8 194.05 258.20 10.16 o 6 8 8 353.59 463.27 12.16 o 7 8 8 84.82 129.73 10.28 o 8 8 8 311.47 356.08 12.16 o 1 1 9 1340.76 1365.89 14.23 o 2 1 9 59.33 146.30 5.20 o 3 1 9 1359.17 1316.87 10.16 o 4 1 9 23.18 53.99 10.59 o 5 1 9 326.87 386.92 12.55 o 6 1 9 321.58 524.62 29.34 o 7 1 9 479.25 458.20 24.90 o 8 1 9 24.25 45.96 10.52 o 0 2 9 531.91 574.03 10.25 o 1 2 9 1477.85 1387.60 14.53 o 2 2 9 1044.43 944.99 12.56 o 3 2 9 894.25 889.32 12.44 o 4 2 9 0.26 10.93 6.17 o 5 2 9 2161.04 2067.15 18.54 o 6 2 9 262.42 237.18 9.03 o 7 2 9 1530.49 1481.83 17.18 o 8 2 9 99.50 124.52 8.43 o 1 3 9 1469.48 1400.99 14.92 o 2 3 9 969.80 800.81 11.87 o 3 3 9 1012.77 950.10 13.15 o 4 3 9 2632.38 2630.15 20.64 o 5 3 9 234.04 225.50 8.97 o 6 3 9 32.11 48.80 7.21 o 7 3 9 2005.78 1952.61 19.58 o 8 3 9 329.66 338.63 11.03 o 0 4 9 3513.16 3486.95 22.66 o 1 4 9 209.67 255.71 8.55 o 2 4 9 2387.19 2259.31 18.78 o 3 4 9 990.85 943.64 13.12 o 4 4 9 139.12 145.68 8.16 o 5 4 9 878.80 801.73 12.94 o 6 4 9 312.11 349.27 10.28 o 7 4 9 719.60 703.19 13.30 o 8 4 9 21.53 62.36 8.49 o 1 5 9 442.18 577.43 11.18 o 2 5 9 58.91 96.95 7.54 o 3 5 9 132.59 164.54 8.07 o 4 5 9 19.00 24.37 7.21 o 5 5 9 136.76 119.28 8.07 o 6 5 9 48.71 61.29 7.72 o 7 5 9 68.69 68.44 8.25 o 8 5 9 4.82 36.32 8.49 o 0 6 9 1.23 -1.52 6.49 o 1 6 9 310.96 354.26 9.78 o 2 6 9 242.06 282.00 9.39 o 3 6 9 58.34 106.93 7.87 o 4 6 9 539.66 659.43 12.61 o 5 6 9 41.60 65.61 7.72 o 6 6 9 460.23 546.65 12.28 o 7 6 9 150.26 124.34 9.33 o 8 6 9 243.29 233.00 10.49 o 1 7 9 251.23 261.64 9.92 o 2 7 9 54.43 37.96 7.72 o 3 7 9 1443.96 1459.52 17.33 o 4 7 9 29.03 114.26 8.82 o 5 7 9 208.87 169.97 9.42 o 6 7 9 192.73 225.60 10.10 o 7 7 9 337.61 358.63 11.74 o 8 7 9 644.58 619.64 14.22 o 0 8 9 99.81 123.59 8.67 o 1 8 9 2254.63 2216.82 21.10 o 2 8 9 62.01 93.26 8.22 o 3 8 9 92.82 119.90 9.39 o 4 8 9 1180.42 1134.33 16.55 o 5 8 9 188.44 214.78 10.37 o 6 8 9 1034.79 944.90 15.98 o 7 8 9 191.21 129.68 9.65 o 8 8 9 134.54 132.15 10.16 o 1 9 9 108.31 81.15 17.52 o 2 9 9 724.08 750.42 13.98 o 3 9 9 264.68 279.67 11.00 o 4 9 9 291.00 295.11 11.00 o 5 9 9 113.96 128.63 9.65 o 6 9 9 211.10 187.52 10.43 o 7 9 9 67.24 90.81 10.13 o 8 9 9 495.90 481.90 13.86 o 9 9 9 33.63 33.67 9.80 o 0 0 10 3175.42 3244.06 16.77 o 1 0 10 549.33 544.28 7.56 o 2 0 10 2794.64 2759.22 29.98 o 3 0 10 3964.89 3848.09 28.71 o 4 0 10 353.78 415.39 7.44 o 5 0 10 1807.92 1853.83 23.41 o 6 0 10 23.74 113.16 5.78 o 7 0 10 2350.57 2348.27 19.78 o 8 0 10 597.64 655.59 9.45 o 9 0 10 52.34 31.43 5.75 o 1 1 10 508.38 585.29 10.94 o 2 1 10 1512.18 1465.92 11.27 o 3 1 10 70.19 94.47 6.73 o 4 1 10 1697.20 1743.52 12.43 o 5 1 10 0.44 89.13 5.67 o 6 1 10 42.38 74.85 5.53 o 7 1 10 1496.51 1526.01 27.68 o 8 1 10 15.35 58.54 5.61 o 9 1 10 235.18 224.21 7.70 o 0 2 10 1540.76 1425.48 15.55 o 1 2 10 3074.84 3000.62 21.73 o 2 2 10 2578.46 2559.68 20.40 o 3 2 10 2475.57 2535.44 20.58 o 4 2 10 169.41 186.42 8.64 o 5 2 10 467.12 548.07 11.51 o 6 2 10 11.07 32.18 7.36 o 7 2 10 374.51 469.72 11.77 o 8 2 10 17.07 30.45 7.93 o 9 2 10 13.02 23.66 8.01 o 1 3 10 137.58 127.17 7.84 o 2 3 10 90.70 98.59 7.75 o 3 3 10 1006.48 1053.32 14.37 o 4 3 10 14.12 24.07 6.85 o 5 3 10 270.48 337.97 10.22 o 6 3 10 411.35 383.78 10.82 o 7 3 10 52.00 87.69 8.52 o 8 3 10 1055.74 996.85 15.95 o 9 3 10 155.36 155.06 9.98 o 0 4 10 409.28 462.51 10.64 o 1 4 10 1797.65 1872.65 18.35 o 2 4 10 96.19 155.80 8.25 o 3 4 10 395.43 445.84 11.00 o 4 4 10 3967.63 3841.22 26.22 o 5 4 10 363.55 338.95 10.76 o 6 4 10 3797.64 3859.91 27.47 o 7 4 10 566.28 598.10 13.53 o 8 4 10 421.12 380.32 12.13 o 9 4 10 1232.14 1182.30 17.83 o 1 5 10 244.66 268.94 9.45 o 2 5 10 3069.29 3139.87 23.69 o 3 5 10 100.18 206.55 9.21 o 4 5 10 729.06 760.24 13.68 o 5 5 10 176.99 149.20 9.18 o 6 5 10 556.48 561.83 12.91 o 7 5 10 57.01 95.02 9.21 o 8 5 10 2135.48 2222.05 23.04 o 9 5 10 195.42 228.73 11.14 o 0 6 10 11.60 36.08 7.87 o 1 6 10 1581.25 1558.64 17.57 o 2 6 10 23.11 53.54 8.13 o 3 6 10 206.55 240.56 9.92 o 4 6 10 2618.74 2519.79 22.51 o 5 6 10 232.79 197.89 9.86 o 6 6 10 1796.61 1797.97 20.17 o 7 6 10 89.52 185.60 10.49 o 8 6 10 117.47 95.20 9.71 o 9 6 10 1095.97 931.32 17.38 o 1 7 10 290.44 398.82 10.94 o 2 7 10 77.04 114.68 8.70 o 3 7 10 57.35 65.49 8.37 o 4 7 10 32.21 51.01 8.10 o 5 7 10 393.75 352.09 11.47 o 6 7 10 198.92 216.30 10.49 o 7 7 10 13.53 21.06 8.76 o 8 7 10 755.53 716.11 15.44 o 9 7 10 120.97 147.76 10.91 o 0 8 10 455.59 453.50 12.13 o 1 8 10 43.23 51.04 8.76 o 2 8 10 237.80 231.51 10.13 o 3 8 10 302.06 361.36 11.71 o 4 8 10 536.78 548.60 13.38 o 5 8 10 1009.75 960.37 16.31 o 6 8 10 265.75 274.54 11.26 o 7 8 10 398.21 407.03 13.32 o 8 8 10 237.60 226.53 11.86 o 9 8 10 542.44 538.32 15.32 o 1 9 10 7.52 35.84 8.43 o 2 9 10 174.02 182.54 10.07 o 3 9 10 487.57 574.83 13.77 o 4 9 10 34.83 36.38 9.00 o 5 9 10 0.59 26.93 9.15 o 6 9 10 16.75 -13.14 8.76 o 7 9 10 267.85 282.20 12.40 o 8 9 10 106.29 110.63 10.58 o 9 9 10 280.68 287.38 13.05 o 0 10 10 1852.63 1925.11 18.21 o 1 10 10 17.62 23.19 9.61 o 2 10 10 467.24 488.33 13.41 o 3 10 10 170.67 169.57 10.31 o 4 10 10 107.23 112.09 9.53 o 5 10 10 704.12 655.09 14.87 o 6 10 10 172.09 176.37 11.38 o 7 10 10 345.01 317.07 13.08 o 8 10 10 94.35 92.60 11.11 o 9 10 10 175.79 182.68 12.66 o 1 1 11 5.09 60.27 6.97 o 2 1 11 505.57 554.06 16.69 o 3 1 11 126.46 117.55 7.93 o 4 1 11 31.19 86.94 14.57 o 5 1 11 282.47 302.22 9.54 o 6 1 11 119.21 158.12 6.56 o 7 1 11 4.40 15.86 5.43 o 8 1 11 267.08 272.45 7.74 o 9 1 11 2.64 23.51 6.04 o 10 1 11 0.33 11.73 6.11 o 0 2 11 1028.55 1142.00 15.00 o 1 2 11 195.49 190.59 8.82 o 2 2 11 309.47 312.38 9.83 o 3 2 11 1.16 6.38 7.18 o 4 2 11 1085.80 1175.91 15.75 o 5 2 11 226.64 222.48 9.74 o 6 2 11 720.84 738.56 13.86 o 7 2 11 29.77 51.42 8.07 o 8 2 11 126.64 323.97 11.32 o 9 2 11 21.56 32.15 8.88 o 10 2 11 1393.03 1326.89 19.71 o 1 3 11 11.14 72.43 7.36 o 2 3 11 2716.41 2764.44 22.58 o 3 3 11 2011.61 1781.19 18.86 o 4 3 11 1364.55 1278.18 16.82 o 5 3 11 87.34 102.70 8.55 o 6 3 11 17.03 85.00 8.67 o 7 3 11 116.97 158.75 9.39 o 8 3 11 1129.87 1081.19 17.41 o 9 3 11 23.23 56.13 9.24 o 10 3 11 3.42 18.83 9.24 o 0 4 11 943.00 915.56 14.22 o 1 4 11 573.17 548.56 11.95 o 2 4 11 225.64 202.96 9.39 o 3 4 11 90.03 92.34 8.25 o 4 4 11 256.21 286.67 10.52 o 5 4 11 86.87 109.26 8.85 o 6 4 11 156.31 170.95 9.77 o 7 4 11 34.61 43.77 8.52 o 8 4 11 181.52 246.48 10.91 o 9 4 11 6.78 0.18 8.97 o 10 4 11 607.09 597.75 15.17 o 1 5 11 94.78 120.73 8.37 o 2 5 11 3.89 85.27 8.34 o 3 5 11 27.65 49.55 7.66 o 4 5 11 0.02 40.61 8.25 o 5 5 11 8.76 14.99 7.95 o 6 5 11 7.91 -8.31 7.93 o 7 5 11 30.59 25.92 8.49 o 8 5 11 7.88 23.21 9.30 o 9 5 11 59.98 44.69 9.33 o 10 5 11 108.09 98.06 10.70 o 0 6 11 77.20 49.37 8.10 o 1 6 11 48.56 21.21 7.96 o 2 6 11 21.74 42.93 8.01 o 3 6 11 329.12 354.48 11.21 o 4 6 11 694.79 673.49 13.95 o 5 6 11 238.73 243.13 10.55 o 6 6 11 425.83 484.50 13.11 o 7 6 11 180.76 152.56 10.22 o 8 6 11 225.94 204.15 11.56 o 9 6 11 62.72 28.13 9.53 o 10 6 11 7.86 10.87 9.30 o 1 7 11 44.50 43.35 8.22 o 2 7 11 511.06 611.57 13.35 o 3 7 11 62.84 104.94 9.42 o 4 7 11 86.72 93.74 9.18 o 5 7 11 183.33 155.45 9.92 o 6 7 11 275.45 328.33 12.31 o 7 7 11 25.47 3.07 9.36 o 8 7 11 1270.98 1145.30 19.02 o 9 7 11 135.82 114.12 11.02 o 10 7 11 348.30 328.16 13.35 o 0 8 11 2.31 -12.20 8.13 o 1 8 11 735.96 713.80 14.46 o 2 8 11 0.11 47.19 8.64 o 3 8 11 244.95 168.42 10.49 o 4 8 11 1549.77 1532.67 19.89 o 5 8 11 56.78 41.12 10.07 o 6 8 11 1290.77 1187.27 18.79 o 7 8 11 105.47 96.15 10.91 o 8 8 11 23.46 16.71 9.65 o 9 8 11 68.88 39.57 10.40 o 10 8 11 421.46 379.07 14.27 o 1 9 11 43.33 50.98 9.44 o 2 9 11 461.40 538.93 13.59 o 3 9 11 22.16 28.84 9.56 o 4 9 11 79.98 81.52 9.89 o 5 9 11 25.22 3.28 9.39 o 6 9 11 277.53 269.05 12.16 o 7 9 11 0.87 0.15 10.19 o 8 9 11 831.86 776.84 17.35 o 9 9 11 22.35 4.17 10.43 o 0 10 11 13.74 35.90 9.53 o 1 10 11 160.39 137.96 10.91 o 2 10 11 139.62 131.70 10.58 o 3 10 11 121.45 108.40 10.79 o 4 10 11 493.55 601.55 15.83 o 5 10 11 327.09 281.64 12.69 o 6 10 11 381.13 350.64 13.41 o 7 10 11 293.81 326.69 13.65 o 8 10 11 59.10 87.83 11.53 o 1 11 11 61.97 84.35 24.60 o 2 11 11 192.32 138.68 11.35 o 3 11 11 24.62 16.27 9.30 o 4 11 11 89.11 93.74 10.19 o 5 11 11 1.16 17.49 9.30 o 6 11 11 99.46 117.33 11.23 o 7 11 11 40.32 23.66 10.10 o 0 0 12 1399.81 1258.43 11.63 o 1 0 12 1500.75 1499.54 25.57 o 2 0 12 1327.00 1403.26 12.36 o 3 0 12 447.04 440.29 8.34 o 4 0 12 0.01 3.95 5.14 o 5 0 12 67.61 57.88 5.56 o 6 0 12 1.43 -6.39 5.33 o 7 0 12 1380.62 1404.03 13.28 o 8 0 12 130.10 146.72 9.62 o 9 0 12 1275.40 1328.87 36.48 o 10 0 12 1282.22 1192.93 26.57 o 11 0 12 1828.37 1964.28 56.76 o 1 1 12 11.26 34.05 7.84 o 2 1 12 734.13 782.32 13.77 o 3 1 12 1486.80 1386.94 34.44 o 4 1 12 358.09 394.59 7.94 o 5 1 12 12.94 55.10 14.48 o 6 1 12 0.02 26.17 5.53 o 7 1 12 78.43 111.74 17.46 o 8 1 12 247.21 249.54 21.93 o 9 1 12 4.67 37.79 10.53 o 10 1 12 27.93 32.55 22.72 o 11 1 12 603.78 601.89 11.34 o 0 2 12 2112.23 2081.69 20.65 o 1 2 12 1069.39 979.83 15.27 o 2 2 12 1302.01 1254.55 16.82 o 3 2 12 888.48 858.97 14.61 o 4 2 12 16.09 43.38 7.93 o 5 2 12 126.85 139.98 9.18 o 6 2 12 12.93 85.18 8.55 o 7 2 12 327.69 372.42 11.74 o 8 2 12 170.06 211.53 10.64 o 9 2 12 449.66 430.65 13.29 o 10 2 12 461.02 438.25 14.07 o 11 2 12 1057.93 1008.48 19.08 o 1 3 12 4.87 118.43 8.79 o 2 3 12 128.46 151.04 9.36 o 3 3 12 13.77 16.12 8.13 o 4 3 12 56.43 33.10 8.37 o 5 3 12 70.76 91.41 8.55 o 6 3 12 29.63 85.03 8.94 o 7 3 12 405.54 424.23 12.61 o 8 3 12 141.98 156.07 10.43 o 9 3 12 476.80 434.92 13.32 o 10 3 12 227.02 221.55 11.74 o 11 3 12 150.40 131.82 11.53 o 0 4 12 40.86 25.50 7.51 o 1 4 12 135.26 152.14 9.12 o 2 4 12 30.61 74.01 8.52 o 3 4 12 1260.67 1319.94 17.54 o 4 4 12 457.41 420.56 12.46 o 5 4 12 2359.32 2250.69 23.01 o 6 4 12 800.39 836.32 16.04 o 7 4 12 1602.71 1529.96 20.40 o 8 4 12 251.51 190.35 11.17 o 9 4 12 91.50 89.30 10.22 o 10 4 12 0.14 29.50 9.47 o 11 4 12 0.65 -2.23 10.37 o 1 5 12 50.53 84.74 8.64 o 2 5 12 208.71 209.63 9.92 o 3 5 12 988.70 1002.30 16.16 o 4 5 12 15.42 28.57 8.61 o 5 5 12 124.28 109.95 9.42 o 6 5 12 193.54 239.48 10.94 o 7 5 12 617.20 632.76 14.96 o 8 5 12 1286.05 1239.13 19.56 o 9 5 12 861.72 793.08 17.23 o 10 5 12 451.71 421.55 14.45 o 11 5 12 216.81 189.66 12.01 o 0 6 12 0.01 -9.50 7.95 o 1 6 12 329.41 328.38 11.18 o 2 6 12 115.70 253.41 10.64 o 3 6 12 978.00 1011.16 16.70 o 4 6 12 845.86 897.97 16.28 o 5 6 12 1459.31 1373.47 19.77 o 6 6 12 920.00 873.07 16.70 o 7 6 12 399.50 468.33 13.86 o 8 6 12 27.27 35.75 10.13 o 9 6 12 2.26 18.14 9.98 o 10 6 12 256.76 238.62 12.87 o 1 7 12 104.36 121.69 9.24 o 2 7 12 129.38 153.48 9.92 o 3 7 12 32.43 67.45 9.33 o 4 7 12 0.13 71.98 9.77 o 5 7 12 231.47 221.73 11.86 o 6 7 12 304.75 294.36 12.75 o 7 7 12 353.61 351.11 13.23 o 8 7 12 661.34 562.95 15.65 o 9 7 12 298.92 269.20 13.05 o 10 7 12 63.20 57.59 11.08 o 0 8 12 8.40 8.58 8.82 o 1 8 12 938.21 976.07 17.17 o 2 8 12 216.56 273.78 11.71 o 3 8 12 610.57 607.27 14.84 o 4 8 12 117.68 117.69 10.94 o 5 8 12 648.98 583.53 15.08 o 6 8 12 97.68 83.64 10.22 o 7 8 12 29.52 97.37 10.87 o 8 8 12 8.43 75.35 10.76 o 9 8 12 138.79 174.31 12.60 o 1 9 12 45.14 87.62 9.89 o 2 9 12 197.68 253.99 11.95 o 3 9 12 108.84 106.28 10.40 o 4 9 12 271.24 370.55 13.47 o 5 9 12 108.69 90.73 10.88 o 6 9 12 14.92 27.68 10.16 o 7 9 12 0.62 20.91 10.37 o 8 9 12 27.62 69.06 11.17 o 0 10 12 1095.13 989.43 20.66 o 1 10 12 1367.31 1383.96 21.35 o 2 10 12 462.87 413.63 14.96 o 3 10 12 44.34 27.08 10.25 o 4 10 12 60.04 44.30 10.73 o 5 10 12 4.49 -7.90 10.07 o 6 10 12 241.30 207.96 12.60 o 7 10 12 19.95 27.05 10.25 o 1 11 12 178.55 193.47 13.11 o 2 11 12 539.02 492.87 15.86 o 3 11 12 684.89 655.65 17.79 o 4 11 12 354.81 305.48 13.83 o 5 11 12 133.25 167.04 12.78 o 0 12 12 278.82 254.40 9.89 o 1 12 12 714.11 717.02 32.94 o 2 12 12 10.54 17.67 11.23 o 3 12 12 163.65 189.42 12.34 o 1 1 13 0.78 26.31 7.51 o 2 1 13 19.21 28.59 5.71 o 3 1 13 87.39 133.39 6.50 o 4 1 13 25.53 46.14 5.91 o 5 1 13 45.15 42.92 5.87 o 6 1 13 5.98 19.04 5.79 o 7 1 13 86.19 136.04 6.90 o 8 1 13 43.25 57.32 13.75 o 9 1 13 86.19 109.14 7.60 o 10 1 13 7.51 32.37 6.98 o 11 1 13 1.77 9.87 7.43 o 0 2 13 617.17 683.46 14.07 o 1 2 13 455.17 502.73 12.67 o 2 2 13 161.09 199.34 9.98 o 3 2 13 30.42 47.79 8.34 o 4 2 13 7.22 -4.26 7.93 o 5 2 13 230.23 263.81 10.76 o 6 2 13 58.12 92.81 9.12 o 7 2 13 96.67 104.19 9.92 o 8 2 13 19.67 43.20 9.09 o 9 2 13 268.07 260.74 12.31 o 10 2 13 46.51 63.49 10.70 o 11 2 13 686.93 660.65 17.11 o 1 3 13 31.88 27.44 8.43 o 2 3 13 195.82 232.01 10.58 o 3 3 13 1247.28 1264.10 18.04 o 4 3 13 18.87 50.05 8.04 o 5 3 13 43.22 78.03 8.82 o 6 3 13 26.82 35.99 9.15 o 7 3 13 468.39 553.14 14.51 o 8 3 13 160.71 163.67 11.05 o 9 3 13 613.13 540.73 14.99 o 10 3 13 3.60 -11.56 9.80 o 0 4 13 676.42 651.41 14.07 o 1 4 13 893.96 884.30 15.53 o 2 4 13 124.77 134.74 9.65 o 3 4 13 21.52 73.95 9.27 o 4 4 13 72.23 109.53 9.44 o 5 4 13 146.47 165.85 10.22 o 6 4 13 22.44 27.83 8.97 o 7 4 13 3.11 25.77 9.36 o 8 4 13 10.71 13.65 9.41 o 9 4 13 248.27 234.15 12.55 o 10 4 13 45.37 36.77 10.07 o 1 5 13 1.55 26.96 8.46 o 2 5 13 4.18 21.21 8.37 o 3 5 13 6.64 36.88 8.64 o 4 5 13 2.61 11.92 8.49 o 5 5 13 11.30 6.29 8.94 o 6 5 13 54.58 51.93 9.89 o 7 5 13 36.85 33.40 9.83 o 8 5 13 3.01 29.11 9.71 o 9 5 13 9.94 27.59 9.62 o 10 5 13 7.05 15.85 10.22 o 0 6 13 173.64 212.48 10.85 o 1 6 13 28.10 13.85 8.16 o 2 6 13 12.01 25.89 8.25 o 3 6 13 172.72 196.06 10.49 o 4 6 13 220.85 178.52 11.11 o 5 6 13 487.80 512.86 14.28 o 6 6 13 37.48 58.34 10.40 o 7 6 13 498.45 475.27 14.84 o 8 6 13 17.28 22.79 10.19 o 9 6 13 84.78 95.49 10.82 o 1 7 13 51.14 110.12 9.65 o 2 7 13 50.66 93.38 9.65 o 3 7 13 876.97 876.31 17.11 o 4 7 13 35.52 41.47 9.89 o 5 7 13 6.26 15.34 9.30 o 6 7 13 52.73 47.94 10.55 o 7 7 13 569.25 599.75 16.42 o 8 7 13 28.86 6.41 10.84 o 0 8 13 13.73 6.35 8.58 o 1 8 13 125.98 148.50 10.40 o 2 8 13 25.06 32.45 9.74 o 3 8 13 492.60 474.38 14.13 o 4 8 13 344.83 328.19 16.03 o 5 8 13 1902.28 1876.87 24.28 o 6 8 13 241.60 144.67 14.09 o 7 8 13 723.55 636.77 16.75 o 8 8 13 77.29 47.11 10.93 o 1 9 13 135.02 168.56 11.20 o 2 9 13 69.16 58.70 11.62 o 3 9 13 931.60 920.88 18.16 o 4 9 13 30.89 37.18 10.22 o 5 9 13 45.68 74.84 10.70 o 6 9 13 41.67 14.03 11.17 o 0 10 13 5.95 18.62 10.49 o 1 10 13 1.20 0.42 9.86 o 2 10 13 49.50 60.93 11.02 o 3 10 13 364.93 370.78 14.66 o 4 10 13 47.58 -21.18 14.12 o 5 10 13 985.79 944.91 19.35 o 1 11 13 6.61 -14.24 9.92 o 2 11 13 0.08 9.92 10.73 o 0 0 14 37.01 -11.42 7.61 o 1 0 14 5446.55 5542.47 25.44 o 2 0 14 20.33 -24.71 16.48 o 3 0 14 756.86 881.82 11.69 o 4 0 14 212.79 193.02 12.11 o 5 0 14 86.99 103.09 12.99 o 6 0 14 95.68 127.93 12.35 o 7 0 14 32.65 21.27 6.38 o 8 0 14 23.99 40.55 7.24 o 9 0 14 538.17 537.71 28.16 o 10 0 14 11.27 10.95 7.14 o 1 1 14 208.68 246.94 11.59 o 2 1 14 1.57 -10.08 6.72 o 3 1 14 2103.95 2295.94 17.03 o 4 1 14 2.31 -9.61 6.41 o 5 1 14 102.86 119.49 10.26 o 6 1 14 277.75 292.16 10.91 o 7 1 14 39.73 49.05 13.66 o 8 1 14 267.07 268.94 8.71 o 9 1 14 102.03 122.41 9.01 o 10 1 14 152.16 197.41 8.96 o 0 2 14 160.60 208.07 11.41 o 1 2 14 2763.51 2904.03 26.66 o 2 2 14 82.60 104.43 10.46 o 3 2 14 1010.27 1017.50 17.50 o 4 2 14 369.67 424.34 12.93 o 5 2 14 69.83 111.88 10.16 o 6 2 14 326.47 380.40 12.87 o 7 2 14 125.47 153.06 10.76 o 8 2 14 16.80 46.42 10.22 o 9 2 14 255.39 294.32 13.23 o 1 3 14 1.86 8.49 8.64 o 2 3 14 50.01 56.85 9.24 o 3 3 14 24.11 10.70 8.85 o 4 3 14 0.42 19.81 9.03 o 5 3 14 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26.79 38.64 10.96 o 6 7 14 25.42 -15.42 10.28 o 7 7 14 437.62 451.97 15.14 o 0 8 14 35.88 11.53 10.22 o 1 8 14 195.07 195.35 12.46 o 2 8 14 22.66 11.65 9.65 o 3 8 14 187.62 209.06 12.04 o 4 8 14 14.33 -15.51 10.34 o 5 8 14 344.64 310.07 13.47 o 6 8 14 105.68 62.24 11.23 o 1 9 14 67.68 76.07 10.85 o 2 9 14 11.18 -11.11 10.61 o 3 9 14 255.93 279.75 13.05 o 4 9 14 2.96 -0.27 10.34 o 0 10 14 0.83 -28.02 18.68 o 1 10 14 880.17 799.80 18.06 o 1 1 15 174.69 221.81 11.50 o 2 1 15 213.49 206.72 19.49 o 3 1 15 412.77 460.92 9.60 o 4 1 15 20.78 20.89 6.86 o 5 1 15 83.74 118.14 8.18 o 6 1 15 165.07 192.02 8.39 o 7 1 15 23.90 20.96 7.11 o 8 1 15 143.95 178.76 14.63 o 0 2 15 765.81 822.70 16.81 o 1 2 15 836.88 894.59 17.20 o 2 2 15 128.02 117.60 10.85 o 3 2 15 7.04 7.27 9.03 o 4 2 15 280.13 254.72 12.43 o 5 2 15 465.54 493.05 14.34 o 6 2 15 662.97 734.37 16.93 o 7 2 15 84.79 87.63 10.76 o 8 2 15 0.62 -4.71 9.77 o 1 3 15 412.73 463.98 14.30 o 2 3 15 523.91 530.99 15.50 o 3 3 15 659.02 654.52 15.92 o 4 3 15 354.33 400.31 13.74 o 5 3 15 76.76 116.08 11.17 o 6 3 15 131.84 136.70 11.71 o 7 3 15 192.64 168.71 12.60 o 0 4 15 387.99 354.10 13.86 o 1 4 15 730.18 679.18 15.95 o 2 4 15 111.70 80.89 10.43 o 3 4 15 40.23 47.37 10.16 o 4 4 15 245.73 225.63 11.98 o 5 4 15 70.41 41.68 10.34 o 6 4 15 396.40 475.83 15.02 o 7 4 15 48.51 62.63 10.73 o 1 5 15 99.44 134.79 11.17 o 2 5 15 0.60 -4.23 8.97 o 3 5 15 68.97 61.79 10.52 o 4 5 15 3.52 -15.86 10.58 o 5 5 15 223.32 224.91 13.11 o 6 5 15 78.40 61.56 10.76 o 0 6 15 515.68 532.83 15.29 o 1 6 15 107.77 75.20 11.77 o 2 6 15 51.92 92.06 10.90 o 3 6 15 155.78 193.23 11.68 o 4 6 15 22.19 8.43 11.41 o 5 6 15 257.78 231.44 12.75 o 6 6 15 36.38 0.83 10.13 o 1 7 15 8.98 -10.79 10.90 o 2 7 15 529.12 529.88 15.62 o 3 7 15 170.22 149.73 13.65 o 4 7 15 217.82 228.04 12.99 o 0 8 15 549.11 575.57 16.27 o 1 8 15 16.59 -14.54 10.82 o 2 8 15 245.77 250.09 13.02 o 0 0 16 666.65 661.40 11.38 o 1 0 16 230.52 227.15 8.64 o 2 0 16 53.75 64.51 17.06 o 3 0 16 509.07 462.88 11.16 o 4 0 16 744.05 765.12 17.65 o 5 0 16 475.39 464.95 27.45 o 6 0 16 861.75 920.74 13.64 o 1 1 16 5.09 5.06 9.12 o 2 1 16 444.45 511.56 17.33 o 3 1 16 8.45 -12.47 8.31 o 4 1 16 433.36 427.49 10.65 o 5 1 16 157.18 152.31 21.78 o 6 1 16 112.42 153.12 13.21 o 0 2 16 1.38 -15.11 10.07 o 1 2 16 377.95 357.22 13.26 o 2 2 16 14.49 -16.45 10.96 o 3 2 16 439.05 441.87 14.30 o 4 2 16 129.12 89.39 12.78 o 5 2 16 600.10 645.12 17.17 o 6 2 16 253.51 272.77 13.74 o 1 3 16 2.12 9.65 10.58 o 2 3 16 107.15 97.16 10.85 o 3 3 16 23.52 31.25 10.04 o 4 3 16 31.06 4.08 10.79 o 5 3 16 56.89 73.47 10.67 o 0 4 16 1176.52 1288.59 22.06 o 1 4 16 592.21 558.48 18.33 o 2 4 16 123.74 63.76 15.29 o 3 4 16 369.85 426.50 14.60 o 4 4 16 124.96 139.35 12.96 o 5 4 16 281.65 212.85 13.23 o 1 5 16 0.06 -21.36 14.24 o 2 5 16 1169.05 1161.94 20.54 o 3 5 16 67.87 -29.09 19.40 o 4 5 16 779.53 807.32 18.45 o 0 6 16 1107.46 1237.26 22.00 o 1 6 16 434.20 396.75 20.44 o 2 6 16 302.85 222.72 15.38 o 1 1 17 10.63 -14.75 9.83 o 2 1 17 65.65 62.16 7.50 o 0 2 17 224.91 222.32 12.28 o 1 2 17 109.06 61.83 12.81 o 2 2 17 0.87 -14.97 9.98 o