#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2012113.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012113_Fobs loop_ _publ_author_name 'Cambie, Richard C.' 'Rickard, Clifton E. F.' 'Rutledge, P. Stewart' 'Wellington, Keri D.' _publ_section_title ; Hamigerin A and a hamigerin D decomposition product ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 958 _journal_page_last 960 _journal_volume 57 _journal_year 2001 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.0958 _cell_length_b 16.0501 _cell_length_c 16.8559 _exptl_crystal_F_000 880.00 _reflns_d_resolution_high 0.8110 _[local]_cod_data_source_file bk1599Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' kdw1 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 143.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 12000.18 12482.33 312.53 o 4 0 0 364.80 367.58 10.33 o 1 1 0 72.84 105.84 2.25 o 2 1 0 7555.00 6836.29 124.58 o 3 1 0 101.11 118.50 14.82 o 4 1 0 410.50 365.83 7.24 o 0 2 0 578.14 585.01 15.07 o 1 2 0 22.81 18.82 2.00 o 2 2 0 585.04 561.27 23.15 o 3 2 0 6734.54 6669.49 118.42 o 4 2 0 30.19 31.39 8.41 o 1 3 0 3469.50 2928.61 103.68 o 2 3 0 3817.35 3944.82 220.93 o 3 3 0 72.53 119.75 20.15 o 4 3 0 1591.71 1584.72 28.81 o 0 4 0 886.55 607.74 16.24 o 1 4 0 4567.43 4434.47 79.03 o 2 4 0 2653.73 2475.51 66.37 o 3 4 0 221.00 211.93 4.83 o 4 4 0 2.96 3.83 2.75 o 5 4 0 444.29 419.46 12.99 o 1 5 0 1896.17 1887.59 34.23 o 2 5 0 2780.24 2701.02 48.63 o 3 5 0 629.44 580.34 20.90 o 4 5 0 1229.39 1265.20 33.64 o 5 5 0 0.32 2.50 3.83 o 0 6 0 36.43 16.99 2.66 o 1 6 0 400.15 387.64 8.08 o 2 6 0 770.70 736.23 39.06 o 3 6 0 2207.17 2206.20 43.14 o 4 6 0 56.51 67.87 5.41 o 5 6 0 14.68 18.90 4.58 o 1 7 0 13946.71 13207.07 234.67 o 2 7 0 569.22 631.64 12.49 o 3 7 0 4.82 5.00 2.17 o 4 7 0 278.69 251.66 9.74 o 5 7 0 970.34 964.82 27.15 o 0 8 0 538.80 376.07 11.66 o 1 8 0 1617.31 1919.07 35.31 o 2 8 0 1249.77 1239.71 23.32 o 3 8 0 54.00 53.96 4.25 o 4 8 0 164.49 172.13 8.66 o 5 8 0 0.78 -3.41 4.25 o 1 9 0 739.86 834.08 16.99 o 2 9 0 1278.39 1287.68 30.73 o 3 9 0 403.12 380.23 8.83 o 4 9 0 1348.82 1330.15 36.39 o 5 9 0 72.37 58.38 7.24 o 0 10 0 2216.25 2075.30 54.38 o 1 10 0 297.97 296.54 8.49 o 2 10 0 10.30 6.91 2.66 o 3 10 0 812.27 804.19 22.57 o 4 10 0 332.29 345.76 12.99 o 5 10 0 634.55 592.00 19.24 o 1 11 0 105.36 89.10 5.00 o 2 11 0 28.90 19.82 3.33 o 3 11 0 0.24 3.50 6.91 o 4 11 0 27.24 30.23 7.00 o 5 11 0 59.14 77.70 7.33 o 0 12 0 1527.87 1619.86 43.72 o 1 12 0 99.37 88.85 5.25 o 2 12 0 3.91 7.66 3.91 o 3 12 0 14.28 20.49 3.66 o 4 12 0 0.34 7.99 5.16 o 6 12 0 50.90 34.23 7.24 o 1 13 0 204.56 181.12 6.50 o 2 13 0 299.79 344.76 22.23 o 3 13 0 50.91 37.64 4.50 o 4 13 0 12.42 14.91 6.75 o 5 13 0 13.06 15.16 6.75 o 6 13 0 0.25 0.50 4.50 o 0 14 0 96.19 157.14 9.83 o 1 14 0 100.74 86.61 10.74 o 2 14 0 301.57 293.29 10.24 o 3 14 0 353.47 367.99 14.66 o 4 14 0 40.25 22.32 7.33 o 5 14 0 62.93 63.96 10.91 o 6 14 0 13.05 29.40 8.49 o 1 15 0 1061.82 1123.21 22.98 o 2 15 0 38.12 34.89 13.32 o 3 15 0 5.23 -4.33 5.58 o 4 15 0 87.26 94.93 10.24 o 5 15 0 150.97 181.54 11.49 o 0 16 0 83.89 68.95 7.91 o 1 16 0 57.84 72.37 10.24 o 2 16 0 88.38 80.69 6.16 o 3 16 0 168.56 201.03 12.74 o 4 16 0 3.76 10.08 7.24 o 5 16 0 1.40 -7.83 7.83 o 1 17 0 81.81 65.70 6.08 o 2 17 0 0.84 0.42 7.74 o 3 17 0 63.11 60.87 9.08 o 4 17 0 15.09 26.73 9.24 o 0 18 0 0.52 -1.33 6.75 o 1 18 0 60.64 57.38 6.66 o 2 18 0 28.40 35.81 6.25 o 3 18 0 14.38 15.57 8.16 o 1 19 0 2.13 -4.33 4.58 o 2 19 0 1.36 -2.00 7.41 o 1 0 1 12195.99 12026.90 219.76 o 2 0 1 1341.01 1107.81 47.05 o 3 0 1 3240.85 3138.30 55.96 o 4 0 1 254.75 209.94 4.58 o -4 1 1 25.29 31.56 6.33 o -3 1 1 2916.19 2699.27 50.13 o -2 1 1 1963.08 1919.15 48.72 o -1 1 1 7758.44 7176.72 179.96 o 0 1 1 1159.67 912.86 27.31 o 1 1 1 8152.17 7702.85 408.71 o 2 1 1 1884.15 1875.02 111.42 o 3 1 1 2817.33 2735.92 48.88 o 4 1 1 51.03 60.46 8.41 o -4 2 1 1498.22 1659.92 42.89 o -3 2 1 75.87 96.02 2.66 o -2 2 1 558.03 540.62 9.99 o -1 2 1 5278.81 5096.76 128.08 o 0 2 1 6135.90 6258.45 111.01 o 1 2 1 3665.00 3380.71 113.84 o 2 2 1 609.78 594.75 60.21 o 3 2 1 92.39 104.93 3.16 o 4 2 1 1504.28 1672.58 55.54 o -5 3 1 308.43 384.40 11.99 o -4 3 1 39.63 44.47 4.16 o -3 3 1 2325.01 2043.07 36.72 o -2 3 1 876.10 812.93 14.91 o -1 3 1 990.02 886.13 23.07 o 0 3 1 14767.66 14260.25 433.28 o 1 3 1 1450.77 1308.50 19.65 o 2 3 1 791.14 756.72 13.99 o 3 3 1 2385.03 2079.79 37.47 o 4 3 1 47.52 50.38 2.41 o -5 4 1 212.96 216.60 8.24 o -4 4 1 1869.78 1634.60 42.72 o -3 4 1 348.82 342.34 10.24 o -2 4 1 5498.84 4897.82 87.27 o -1 4 1 99.95 101.18 4.16 o 0 4 1 1497.90 1698.73 125.91 o 1 4 1 78.58 102.84 5.33 o 2 4 1 5182.36 4723.11 117.75 o 3 4 1 261.56 260.73 14.91 o 4 4 1 2078.21 1946.30 46.05 o -5 5 1 598.98 575.01 17.24 o -4 5 1 493.09 480.08 14.32 o -3 5 1 2117.65 1957.21 80.86 o -2 5 1 713.48 664.78 18.90 o -1 5 1 4564.17 4675.47 118.17 o 0 5 1 9899.73 9299.90 165.30 o 1 5 1 4245.28 4412.24 112.25 o 2 5 1 856.00 837.91 22.73 o 3 5 1 1996.92 1857.53 98.85 o 4 5 1 540.24 538.21 10.74 o 5 5 1 573.61 528.71 15.66 o -5 6 1 194.53 167.13 7.91 o -4 6 1 1.27 11.66 4.41 o -3 6 1 442.70 509.48 11.16 o -2 6 1 2918.34 2713.60 48.97 o -1 6 1 7057.69 6440.82 162.55 o 0 6 1 44.35 52.30 3.33 o 1 6 1 6895.39 6486.87 94.43 o 2 6 1 2721.40 2511.57 65.29 o 3 6 1 366.30 409.80 8.58 o 4 6 1 1.13 13.91 4.25 o 5 6 1 166.45 134.57 7.49 o -5 7 1 80.81 88.94 6.91 o -4 7 1 314.79 273.23 10.33 o -3 7 1 2731.44 2566.87 57.54 o -2 7 1 870.10 786.28 34.31 o -1 7 1 311.71 285.72 9.49 o 0 7 1 1868.33 1815.14 33.31 o 1 7 1 289.10 227.01 5.50 o 2 7 1 894.72 821.34 15.82 o 3 7 1 2270.05 2128.51 38.97 o 4 7 1 376.68 362.91 12.24 o 5 7 1 50.95 56.96 6.00 o -5 8 1 369.84 347.01 12.49 o -4 8 1 799.98 776.12 22.48 o -3 8 1 1142.54 1135.45 21.57 o -2 8 1 2278.75 2252.59 41.22 o -1 8 1 1092.09 1176.43 19.15 o 0 8 1 762.71 883.38 28.56 o 1 8 1 1120.99 1190.17 18.32 o 2 8 1 2452.62 2347.02 42.89 o 3 8 1 1087.41 1063.84 20.32 o 4 8 1 844.75 808.43 23.32 o 5 8 1 451.06 424.12 14.24 o -5 9 1 376.25 344.09 12.91 o -4 9 1 310.36 322.94 11.83 o -3 9 1 973.47 957.08 18.65 o -2 9 1 344.87 280.30 7.08 o -1 9 1 102.96 106.93 3.83 o 0 9 1 2475.43 2389.74 67.12 o 1 9 1 89.35 97.27 5.50 o 2 9 1 401.35 338.85 8.08 o 3 9 1 913.47 915.03 17.90 o 4 9 1 221.37 246.24 10.16 o 5 9 1 255.63 214.02 9.91 o -6 10 1 129.37 110.01 9.08 o -5 10 1 338.89 360.25 13.66 o -4 10 1 331.24 344.26 12.82 o -3 10 1 102.18 91.94 5.16 o -2 10 1 511.20 518.89 11.24 o -1 10 1 1175.62 1149.28 18.15 o 0 10 1 64.55 56.54 3.91 o 1 10 1 1143.83 1116.55 30.56 o 2 10 1 556.25 587.42 12.57 o 3 10 1 92.69 79.36 4.41 o 4 10 1 319.19 304.87 11.74 o 5 10 1 346.46 353.50 13.66 o -6 11 1 1.07 -1.17 4.08 o -5 11 1 92.33 89.77 8.74 o -4 11 1 187.50 205.52 10.24 o -3 11 1 745.52 710.25 14.74 o -2 11 1 229.18 222.51 9.24 o -1 11 1 254.04 290.05 15.32 o 0 11 1 6.12 2.41 2.83 o 1 11 1 206.39 237.00 10.08 o 2 11 1 275.86 278.55 10.33 o 3 11 1 805.11 784.95 16.16 o 4 11 1 161.25 152.14 8.83 o 5 11 1 78.99 46.05 7.83 o -6 12 1 17.45 12.82 5.08 o -5 12 1 282.58 311.20 9.74 o -4 12 1 264.26 268.23 8.99 o -3 12 1 224.79 220.76 7.58 o -2 12 1 484.30 500.48 9.41 o -1 12 1 87.01 104.01 4.16 o 0 12 1 3.43 11.99 3.08 o 1 12 1 97.95 128.83 7.58 o 2 12 1 425.03 411.96 13.66 o 3 12 1 295.37 294.04 11.08 o 4 12 1 274.45 305.04 12.57 o -6 13 1 77.38 89.19 20.57 o -5 13 1 168.62 166.72 18.90 o -4 13 1 118.85 133.82 11.41 o -3 13 1 5.09 -1.42 4.50 o -2 13 1 57.89 62.12 14.82 o -1 13 1 41.74 56.71 6.58 o 0 13 1 306.50 342.59 17.99 o 1 13 1 43.74 65.62 6.75 o 2 13 1 56.11 53.55 6.66 o 3 13 1 0.68 -4.16 4.16 o -6 14 1 23.62 44.22 13.49 o -5 14 1 17.64 32.31 10.58 o -4 14 1 35.84 31.14 11.16 o -3 14 1 180.82 196.61 10.74 o -2 14 1 446.73 425.20 9.91 o -1 14 1 567.48 570.85 10.99 o 0 14 1 19.96 27.15 10.99 o 1 14 1 492.87 493.15 34.98 o 2 14 1 376.79 327.02 12.91 o 3 14 1 204.87 206.19 10.33 o -5 15 1 1.23 -1.25 9.16 o -4 15 1 48.93 66.37 6.66 o -3 15 1 19.45 35.31 5.83 o -2 15 1 182.18 168.47 12.24 o -1 15 1 72.95 80.53 6.75 o 0 15 1 28.64 18.57 4.83 o 1 15 1 69.82 88.94 11.83 o 2 15 1 144.44 132.41 8.58 o -5 16 1 23.40 18.82 8.33 o -4 16 1 79.57 87.52 7.24 o -3 16 1 8.53 5.41 6.66 o -2 16 1 166.29 149.98 7.16 o -1 16 1 4.53 4.08 10.99 o 0 16 1 5.25 12.82 8.41 o 1 16 1 5.81 12.16 4.75 o 2 16 1 184.13 150.81 9.49 o 3 16 1 9.36 -1.33 6.58 o 4 16 1 72.28 92.02 10.58 o 5 16 1 11.60 26.81 8.83 o -4 17 1 19.79 11.49 7.24 o -3 17 1 8.06 -1.42 6.75 o -2 17 1 5.95 6.75 4.58 o -1 17 1 23.77 24.32 5.33 o 0 17 1 44.93 54.13 6.50 o 1 17 1 26.52 22.73 5.66 o 2 17 1 6.64 5.41 4.41 o 3 17 1 10.46 17.82 8.49 o 4 17 1 23.02 29.73 8.91 o -3 18 1 18.91 17.24 8.49 o -2 18 1 0.19 -1.00 4.66 o -1 18 1 31.21 36.56 6.08 o 0 18 1 1.03 -1.58 5.75 o 1 18 1 34.40 40.97 5.91 o 2 18 1 2.47 13.66 7.99 o 3 18 1 18.80 25.82 9.66 o -2 19 1 1.72 29.06 9.83 o -1 19 1 2.70 -4.08 4.33 o 0 19 1 0.68 1.17 12.99 o 1 19 1 2.96 4.50 7.00 o 2 19 1 3.37 -4.25 4.25 o 0 0 2 209.87 345.76 9.08 o 1 0 2 1988.40 2209.03 39.39 o 2 0 2 3205.65 2853.67 50.80 o 3 0 2 259.57 286.63 5.75 o 4 0 2 518.48 461.93 13.07 o -5 1 2 299.56 281.47 9.33 o -4 1 2 959.61 975.82 25.90 o -3 1 2 1105.43 1207.74 31.39 o -2 1 2 12472.53 12620.82 223.59 o -1 1 2 13666.99 13759.60 243.66 o 0 1 2 3445.39 3758.45 135.99 o 1 1 2 13842.26 13628.53 482.00 o 2 1 2 11690.23 11864.68 297.46 o 3 1 2 1073.11 1139.87 29.56 o 4 1 2 673.88 692.26 13.07 o -5 2 2 174.25 180.04 7.33 o -4 2 2 534.50 516.14 14.74 o -3 2 2 5672.61 5381.81 135.82 o -2 2 2 1489.32 1558.16 43.14 o -1 2 2 17179.37 16948.95 557.03 o 0 2 2 8.76 30.98 5.08 o 1 2 2 16094.14 16153.84 736.98 o 2 2 2 1487.20 1558.91 39.81 o 3 2 2 6455.75 6459.64 114.84 o 4 2 2 496.13 478.41 21.98 o -5 3 2 510.82 579.68 16.90 o -4 3 2 757.24 761.47 20.90 o -3 3 2 1553.29 1678.57 43.39 o -2 3 2 2139.81 2162.98 38.14 o -1 3 2 8669.47 8297.10 147.31 o 0 3 2 12.40 11.83 1.33 o 1 3 2 10600.63 10518.21 358.33 o 2 3 2 2571.18 2704.69 68.54 o 3 3 2 1598.85 1821.39 40.31 o 4 3 2 772.37 771.63 14.66 o -5 4 2 79.85 83.36 5.66 o -4 4 2 360.23 378.57 11.83 o -3 4 2 367.31 353.09 7.08 o -2 4 2 1567.03 1565.57 32.98 o -1 4 2 493.78 501.65 14.91 o 0 4 2 18264.98 17643.46 425.53 o 1 4 2 416.54 415.38 11.66 o 2 4 2 1605.94 1629.94 41.80 o 3 4 2 411.81 412.04 9.24 o 4 4 2 318.37 348.76 7.49 o -5 5 2 609.64 527.30 16.07 o -4 5 2 695.64 693.68 19.74 o -3 5 2 1835.30 1861.86 47.13 o -2 5 2 1908.95 1844.04 32.98 o -1 5 2 346.61 382.15 9.49 o 0 5 2 1028.18 995.05 18.49 o 1 5 2 350.86 341.68 7.00 o 2 5 2 2638.14 2538.89 64.70 o 3 5 2 1953.16 2004.59 64.29 o 4 5 2 708.54 722.99 33.48 o -5 6 2 394.77 414.21 13.66 o -4 6 2 213.45 219.85 8.83 o -3 6 2 1975.64 1930.31 35.23 o -2 6 2 39.17 53.80 8.16 o -1 6 2 337.80 310.45 9.83 o 0 6 2 1229.12 1126.29 29.40 o 1 6 2 528.19 523.38 10.41 o 2 6 2 47.34 75.86 4.33 o 3 6 2 1898.10 1920.15 87.94 o 4 6 2 274.84 277.31 8.58 o 5 6 2 351.72 391.73 12.66 o -5 7 2 1139.11 1197.49 33.14 o -4 7 2 778.55 783.45 22.65 o -3 7 2 21.36 26.40 2.50 o -2 7 2 1385.06 1446.07 21.90 o -1 7 2 509.56 406.13 16.90 o 0 7 2 436.56 457.51 9.49 o 1 7 2 348.22 245.16 8.41 o 2 7 2 1486.29 1544.50 40.31 o 3 7 2 31.49 34.06 2.91 o 4 7 2 694.12 641.55 18.74 o 5 7 2 1087.03 1090.82 30.06 o -5 8 2 76.60 70.78 7.41 o -4 8 2 274.31 260.65 10.66 o -3 8 2 693.97 695.76 22.15 o -2 8 2 1502.29 1371.70 33.64 o -1 8 2 1618.41 1616.87 30.06 o 0 8 2 3350.27 3051.86 142.82 o 1 8 2 1618.28 1541.25 28.65 o 2 8 2 1350.67 1226.47 32.64 o 3 8 2 695.54 702.09 14.16 o 4 8 2 324.66 290.21 10.91 o -5 9 2 247.24 250.07 19.07 o -4 9 2 589.80 577.76 29.90 o -3 9 2 310.24 324.77 6.91 o -2 9 2 1632.12 1611.70 48.47 o -1 9 2 1114.78 1139.28 25.07 o 0 9 2 23.65 23.57 4.83 o 1 9 2 1126.70 1104.64 81.78 o 2 9 2 1511.90 1471.72 39.06 o 3 9 2 435.45 440.27 13.57 o -6 10 2 23.93 41.47 7.66 o -5 10 2 152.60 146.73 13.74 o -4 10 2 496.80 478.16 13.66 o -3 10 2 977.02 1018.62 26.98 o -2 10 2 363.23 383.65 19.99 o -1 10 2 252.95 253.57 7.16 o 0 10 2 158.76 216.18 8.58 o 1 10 2 345.49 336.68 7.99 o 2 10 2 339.78 359.41 12.07 o 3 10 2 882.06 926.68 25.73 o -6 11 2 98.74 81.69 8.41 o -5 11 2 257.42 268.56 12.74 o -4 11 2 461.71 429.45 26.56 o -3 11 2 66.10 64.37 10.41 o -2 11 2 108.85 110.01 6.91 o -1 11 2 1028.30 1060.01 51.80 o 0 11 2 32.80 47.05 7.24 o 1 11 2 936.29 962.83 19.07 o 2 11 2 124.87 112.50 6.41 o 3 11 2 66.19 62.21 5.75 o -6 12 2 56.51 62.04 6.25 o -5 12 2 68.93 78.61 6.16 o -4 12 2 36.52 34.98 7.58 o -3 12 2 10.03 23.07 5.50 o -2 12 2 655.89 603.74 10.91 o -1 12 2 73.30 68.70 4.58 o 0 12 2 170.06 152.81 8.58 o 1 12 2 90.31 83.86 7.00 o 2 12 2 664.60 588.59 18.15 o 3 12 2 19.00 26.81 5.33 o -6 13 2 2.84 4.41 5.16 o -5 13 2 0.41 -5.41 5.41 o -4 13 2 199.86 201.86 10.91 o -3 13 2 232.85 218.85 8.24 o -2 13 2 287.12 331.52 7.66 o -1 13 2 118.54 120.17 4.66 o 0 13 2 106.57 118.00 8.74 o 1 13 2 124.19 106.01 8.41 o 2 13 2 292.07 317.44 11.83 o 3 13 2 227.75 207.19 9.83 o -6 14 2 44.07 53.13 9.74 o -5 14 2 56.53 62.54 6.50 o -4 14 2 152.94 162.47 7.49 o -3 14 2 115.91 126.74 7.08 o -2 14 2 16.06 9.74 6.25 o -1 14 2 317.01 308.95 7.24 o 0 14 2 97.94 123.08 4.83 o 1 14 2 315.38 315.03 12.57 o 2 14 2 17.91 13.07 5.75 o 3 14 2 111.93 116.92 8.41 o -5 15 2 50.08 34.73 5.75 o -4 15 2 21.79 19.40 5.41 o -3 15 2 8.30 3.00 10.08 o -2 15 2 32.15 35.81 4.08 o -1 15 2 0.83 1.92 7.16 o 0 15 2 30.09 28.48 4.33 o 1 15 2 11.79 -2.33 5.25 o 2 15 2 32.38 7.49 5.33 o 3 15 2 10.16 12.32 5.58 o -5 16 2 6.12 4.00 5.41 o -4 16 2 11.23 2.75 12.91 o -3 16 2 6.88 13.99 4.91 o -2 16 2 141.77 138.65 9.83 o -1 16 2 67.73 85.19 12.91 o 0 16 2 294.54 303.79 9.41 o 1 16 2 58.86 79.53 20.15 o 2 16 2 164.04 161.55 10.41 o -4 17 2 74.56 75.11 15.99 o -3 17 2 0.88 -6.41 6.41 o -2 17 2 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