#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:34:15 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180790 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/21/2012174.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012174_Fobs loop_ _publ_author_name 'Vasiliev, Alexander D.' 'Astachov, Alexander M.' 'Golubtsova, Oksana A.' 'Pekhotin, Konstantin V.' 'Rogozin, Mark V.' 'Kruglyakova, Ludmila A.' 'Stepanov, Rudolf S.' _publ_section_title ; 5-Nitro-2-nitromethyl-2H-1,2,3,4-tetrazole ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1101 _journal_page_last 1102 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 118.040 _cell_angle_gamma 90.000 _cell_length_a 9.2130 _cell_length_b 7.7610 _cell_length_c 10.1800 _exptl_crystal_F_000 352.00 _reflns_d_resolution_high 0.8201 _cod_data_source_file av1078Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Nitro3 (C2N6O4H2) in P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 106.91 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 209.96 220.71 1.62 o 2 0 0 11430.73 12848.42 66.89 o 3 0 0 3924.96 4034.04 14.59 o 4 0 0 119.45 143.72 2.87 o 5 0 0 276.62 298.58 4.81 o 6 0 0 19.33 23.75 0.99 o 7 0 0 55.06 60.30 2.42 o 1 1 0 39.89 47.72 0.99 o 2 1 0 793.57 896.86 4.88 o 3 1 0 1352.57 1670.78 8.18 o 4 1 0 771.07 865.43 7.05 o 5 1 0 67.67 76.89 2.59 o 6 1 0 258.34 268.46 5.36 o 7 1 0 69.64 78.14 3.14 o 8 1 0 15.34 15.01 0.60 o 9 1 0 22.00 16.94 0.77 o 0 2 0 76.57 61.11 1.32 o 1 2 0 411.94 361.35 3.19 o 2 2 0 337.74 313.58 3.33 o 3 2 0 683.36 721.36 5.88 o 4 2 0 13.25 13.03 0.49 o 5 2 0 38.54 44.44 1.87 o 6 2 0 141.34 150.10 4.19 o 7 2 0 158.26 154.71 4.52 o 8 2 0 207.00 179.13 4.69 o 1 3 0 1367.03 1183.67 7.09 o 2 3 0 93.58 85.24 2.09 o 3 3 0 76.46 78.08 2.26 o 4 3 0 15.16 21.61 0.93 o 5 3 0 46.68 48.79 1.76 o 6 3 0 25.56 30.52 1.15 o 7 3 0 138.19 128.21 4.08 o 8 3 0 22.46 17.76 0.60 o 0 4 0 29.52 32.40 1.32 o 1 4 0 62.35 57.52 1.93 o 2 4 0 70.20 62.81 2.20 o 3 4 0 49.77 48.75 1.87 o 4 4 0 27.09 26.51 1.04 o 5 4 0 12.52 12.31 0.49 o 6 4 0 3.29 4.07 0.38 o 7 4 0 23.50 24.85 1.10 o 8 4 0 13.38 12.42 0.49 o 1 5 0 96.87 90.37 2.81 o 2 5 0 426.78 418.59 6.21 o 3 5 0 231.21 226.65 4.86 o 4 5 0 310.18 317.14 6.13 o 5 5 0 30.68 31.68 1.37 o 6 5 0 190.74 179.18 4.85 o 7 5 0 8.21 9.78 0.44 o 8 5 0 68.89 63.69 2.26 o 0 6 0 5.34 4.73 0.33 o 1 6 0 104.46 106.83 3.52 o 2 6 0 23.43 22.60 0.93 o 3 6 0 32.17 32.01 1.26 o 4 6 0 116.61 123.15 4.08 o 5 6 0 78.47 72.38 2.92 o 6 6 0 43.66 45.16 1.87 o 7 6 0 50.57 41.98 1.60 o 1 7 0 29.72 29.59 1.10 o 2 7 0 10.50 12.09 0.49 o 3 7 0 33.33 33.82 1.32 o 4 7 0 2.42 2.25 1.21 o 5 7 0 42.71 42.58 1.65 o 6 7 0 31.91 31.79 1.21 o 0 8 0 36.56 32.50 1.48 o 1 8 0 16.17 18.09 0.71 o 2 8 0 43.81 44.94 1.82 o 3 8 0 11.35 11.10 0.44 o 4 8 0 7.53 8.74 0.38 o 5 8 0 0.08 0.82 0.66 o 1 9 0 0.06 0.00 0.66 o 2 9 0 12.17 13.96 0.60 o 3 9 0 41.42 41.65 1.65 o -8 1 1 97.61 97.06 3.69 o -7 1 1 132.30 130.18 4.08 o -6 1 1 942.69 1043.07 9.96 o -4 1 1 71.86 74.23 2.04 o -3 1 1 2055.56 2242.91 9.09 o -2 1 1 2137.55 2207.75 7.46 o -1 1 1 336.64 284.61 2.19 o 0 1 1 26.25 25.42 0.56 o 1 1 1 1601.22 1658.51 6.21 o 2 1 1 732.30 801.43 5.18 o 3 1 1 328.16 369.12 4.21 o 4 1 1 156.97 163.81 3.36 o 5 1 1 408.46 481.77 6.65 o 6 1 1 101.76 99.17 3.52 o 7 1 1 153.34 146.06 4.13 o 8 1 1 0.00 0.00 1.10 o -9 2 1 3.64 2.80 1.15 o -8 2 1 71.16 62.41 2.53 o -7 2 1 75.82 83.43 3.19 o -6 2 1 38.96 45.21 1.82 o -5 2 1 1131.96 1199.49 9.79 o -4 2 1 1108.45 1117.76 8.12 o -3 2 1 623.71 635.72 5.26 o -2 2 1 1882.47 1782.72 7.84 o -1 2 1 508.60 468.12 3.59 o 0 2 1 742.16 658.23 2.98 o 1 2 1 466.92 421.92 3.69 o 2 2 1 145.60 164.60 2.65 o 3 2 1 37.81 37.46 1.43 o 4 2 1 3.60 6.49 0.33 o 5 2 1 19.06 21.06 0.77 o 6 2 1 371.72 393.65 6.92 o 8 2 1 63.10 57.34 2.31 o -8 3 1 124.93 118.93 3.91 o -7 3 1 1.51 2.36 1.21 o -6 3 1 5.59 6.05 0.38 o -5 3 1 1.67 1.81 0.27 o -4 3 1 43.09 50.17 1.98 o -3 3 1 40.46 42.20 1.65 o -2 3 1 379.37 355.68 4.11 o -1 3 1 2123.13 1921.32 9.10 o 0 3 1 931.05 847.72 11.46 o 1 3 1 1319.27 1264.22 7.69 o 2 3 1 378.55 367.82 4.49 o 3 3 1 30.72 30.74 1.15 o 4 3 1 1095.64 1267.43 10.61 o 5 3 1 14.57 13.96 0.49 o 6 3 1 0.26 0.00 1.15 o 7 3 1 0.06 0.00 1.21 o 8 3 1 8.04 6.27 0.38 o -8 4 1 16.35 15.34 0.55 o -7 4 1 64.51 63.72 2.48 o -6 4 1 7.68 8.25 0.44 o -5 4 1 11.06 12.53 0.55 o -4 4 1 6.55 6.21 0.33 o -3 4 1 3.46 4.34 0.27 o -2 4 1 316.06 299.30 4.48 o -1 4 1 324.64 275.25 4.10 o 0 4 1 116.60 104.02 1.81 o 1 4 1 20.96 20.68 0.88 o 2 4 1 524.05 525.47 6.28 o 3 4 1 424.17 456.58 6.37 o 4 4 1 188.58 190.89 4.58 o 5 4 1 5.01 3.46 1.15 o 6 4 1 65.99 70.16 2.70 o 7 4 1 7.57 8.47 0.44 o 8 4 1 0.06 0.00 0.82 o -7 5 1 11.82 12.75 0.55 o -6 5 1 42.23 38.89 1.43 o -5 5 1 3.60 5.66 0.38 o -4 5 1 24.43 23.86 0.99 o -3 5 1 42.85 38.83 1.43 o -2 5 1 3.03 1.70 0.82 o -1 5 1 250.90 252.23 4.64 o 0 5 1 220.85 215.68 3.28 o 1 5 1 23.95 26.78 0.93 o 2 5 1 13.84 15.12 0.49 o 3 5 1 65.32 65.37 2.48 o 4 5 1 41.36 43.12 1.65 o 5 5 1 18.16 18.91 0.77 o 6 5 1 194.62 194.26 4.85 o 7 5 1 20.62 20.23 0.88 o -8 6 1 8.57 8.03 0.38 o -7 6 1 15.32 14.73 0.66 o -6 6 1 78.02 78.05 3.14 o -5 6 1 161.40 154.33 4.52 o -4 6 1 23.12 19.41 0.82 o -3 6 1 62.95 56.62 2.20 o -2 6 1 32.89 33.11 1.32 o -1 6 1 0.09 1.65 0.88 o 0 6 1 523.46 495.50 5.24 o 1 6 1 0.00 3.24 0.33 o 2 6 1 161.52 169.66 4.58 o 3 6 1 23.16 19.63 0.82 o 4 6 1 3.30 2.80 1.15 o 5 6 1 0.31 1.54 1.04 o 6 6 1 9.78 8.47 0.38 o 7 6 1 24.96 23.37 1.04 o -7 7 1 18.21 19.08 0.71 o -6 7 1 4.93 6.32 0.33 o -5 7 1 55.59 50.89 2.04 o -4 7 1 70.92 72.86 2.92 o -3 7 1 28.73 26.89 1.21 o -2 7 1 195.57 186.80 4.91 o -1 7 1 136.48 133.93 4.19 o 0 7 1 158.03 149.76 3.16 o 1 7 1 2.15 3.02 0.33 o 2 7 1 80.01 74.41 2.86 o 3 7 1 14.23 14.68 0.55 o 4 7 1 161.84 160.86 4.30 o 5 7 1 2.91 2.86 0.93 o 6 7 1 0.16 0.55 0.66 o -5 8 1 16.25 16.16 0.66 o -4 8 1 27.26 27.72 1.04 o -3 8 1 8.38 9.95 0.44 o -2 8 1 64.38 70.99 2.81 o -1 8 1 0.26 0.00 0.93 o 0 8 1 14.93 14.55 0.44 o 1 8 1 90.01 87.43 3.30 o 2 8 1 10.02 10.33 0.44 o 3 8 1 4.15 4.29 0.33 o 4 8 1 11.91 11.60 0.44 o -3 9 1 0.57 1.32 0.66 o -2 9 1 6.73 7.48 0.33 o -1 9 1 20.47 21.28 0.82 o 0 9 1 9.64 11.32 0.33 o 1 9 1 22.29 25.52 0.99 o 2 9 1 8.82 9.35 0.38 o -8 0 2 118.20 114.78 4.02 o -7 0 2 7.84 11.38 0.49 o -6 0 2 1668.18 1860.89 12.77 o -5 0 2 419.89 471.91 5.49 o -4 0 2 2428.96 2846.24 11.66 o -3 0 2 1852.70 2029.25 8.25 o -2 0 2 176.78 189.84 2.11 o -1 0 2 1797.03 1468.21 5.32 o 0 0 2 880.31 833.55 26.99 o 1 0 2 5.12 8.03 0.33 o 2 0 2 1263.36 1489.77 7.87 o 3 0 2 1494.36 1793.67 10.25 o 4 0 2 0.16 1.65 0.88 o 5 0 2 346.89 368.53 6.20 o 6 0 2 27.55 27.55 1.10 o 7 0 2 342.66 328.30 6.36 o 8 0 2 23.30 22.93 0.99 o -9 1 2 26.73 21.83 0.88 o -8 1 2 20.62 22.38 0.82 o -7 1 2 0.03 0.99 1.26 o -6 1 2 3.54 4.84 0.38 o -5 1 2 18.79 21.72 0.88 o -4 1 2 67.57 73.29 1.98 o -3 1 2 21.96 18.87 0.83 o -2 1 2 7026.00 7320.85 43.95 o -1 1 2 934.88 769.13 4.14 o 0 1 2 7904.60 7943.75 135.41 o 1 1 2 421.92 364.00 3.40 o 2 1 2 0.12 1.59 0.66 o 3 1 2 233.91 271.02 4.03 o 4 1 2 101.96 113.46 3.14 o 5 1 2 0.09 0.11 1.10 o 6 1 2 147.00 146.52 4.41 o 7 1 2 6.22 3.41 1.43 o 8 1 2 1.33 2.47 0.93 o -9 2 2 27.56 28.21 1.15 o -8 2 2 166.18 173.91 4.85 o -7 2 2 16.93 15.67 0.60 o -6 2 2 5.24 6.76 0.38 o -5 2 2 168.06 177.01 3.64 o -4 2 2 7.34 6.71 0.27 o -3 2 2 878.88 811.38 5.97 o -2 2 2 2.39 3.46 0.22 o -1 2 2 8000.08 7841.67 50.14 o 0 2 2 346.32 280.52 4.31 o 1 2 2 0.25 0.16 0.55 o 2 2 2 178.58 189.00 3.15 o 3 2 2 31.07 32.56 1.37 o 4 2 2 263.36 295.96 5.14 o 5 2 2 95.97 117.77 3.74 o 6 2 2 62.80 60.69 2.42 o 7 2 2 38.78 38.39 1.60 o 8 2 2 0.00 1.65 0.88 o -9 3 2 4.89 4.84 0.38 o -8 3 2 96.42 89.63 3.47 o -7 3 2 8.68 10.44 0.49 o -6 3 2 0.84 0.00 0.93 o -5 3 2 69.25 65.33 2.53 o -4 3 2 83.32 84.14 2.48 o -3 3 2 39.62 43.24 1.65 o -2 3 2 69.76 78.96 2.04 o -1 3 2 408.18 403.45 4.28 o 0 3 2 53.06 46.39 1.32 o 1 3 2 561.77 539.41 5.41 o 2 3 2 33.51 36.36 1.43 o 3 3 2 27.53 34.48 1.48 o 4 3 2 49.16 48.36 1.87 o 5 3 2 136.94 143.97 4.30 o 6 3 2 0.44 1.15 1.10 o 7 3 2 88.22 85.66 3.19 o 8 3 2 2.26 2.31 0.88 o -8 4 2 0.00 0.77 0.82 o -7 4 2 67.47 63.39 2.53 o -6 4 2 0.18 1.04 0.99 o -5 4 2 65.14 72.64 2.86 o -4 4 2 83.33 80.43 2.70 o -3 4 2 113.74 118.18 3.03 o -2 4 2 669.48 589.25 6.30 o -1 4 2 141.36 143.86 3.09 o 0 4 2 156.38 147.37 2.24 o 1 4 2 274.41 241.05 4.26 o 2 4 2 6.25 4.23 0.33 o 3 4 2 165.57 163.53 4.08 o 4 4 2 0.29 1.76 0.93 o 5 4 2 7.54 9.29 0.49 o 6 4 2 34.52 33.60 1.37 o 7 4 2 0.05 0.05 0.88 o -8 5 2 33.51 29.20 1.15 o -7 5 2 96.01 90.51 3.41 o -6 5 2 332.78 339.22 6.63 o -5 5 2 68.09 67.47 2.64 o -4 5 2 225.92 218.11 4.97 o -3 5 2 158.46 152.92 3.91 o -2 5 2 0.64 1.10 0.71 o -1 5 2 292.03 276.29 4.98 o 0 5 2 9.39 8.87 0.44 o 1 5 2 34.63 37.45 1.43 o 2 5 2 168.18 170.25 4.36 o 3 5 2 99.32 93.00 3.41 o 4 5 2 24.03 24.47 0.88 o 5 5 2 316.78 324.56 6.41 o 6 5 2 11.27 12.81 0.49 o 7 5 2 43.13 37.41 1.49 o -8 6 2 26.33 22.44 0.82 o -7 6 2 1.84 2.09 0.33 o -6 6 2 0.46 0.33 1.04 o -5 6 2 125.26 129.94 4.19 o -4 6 2 42.82 43.07 1.71 o -3 6 2 31.72 32.61 1.26 o -2 6 2 2.13 2.03 1.15 o -1 6 2 6.97 8.74 0.38 o 0 6 2 274.43 269.08 3.94 o 1 6 2 69.57 70.66 2.92 o 2 6 2 22.02 23.37 0.99 o 3 6 2 1.99 2.03 1.21 o 4 6 2 44.94 48.35 1.71 o 5 6 2 0.10 1.15 0.99 o 6 6 2 0.94 0.77 0.82 o -7 7 2 0.73 1.26 0.71 o -6 7 2 13.44 12.04 0.49 o -5 7 2 0.44 0.00 0.93 o -4 7 2 0.89 0.00 1.10 o -3 7 2 38.52 36.68 1.54 o -2 7 2 53.90 55.73 2.09 o -1 7 2 25.19 29.31 1.21 o 0 7 2 14.86 14.95 0.63 o 1 7 2 2.65 3.08 0.38 o 2 7 2 300.04 318.99 6.35 o 3 7 2 3.25 3.68 0.38 o 4 7 2 45.85 51.11 1.87 o 5 7 2 17.07 18.20 0.71 o -5 8 2 3.96 3.96 0.27 o -4 8 2 65.19 69.95 2.64 o -3 8 2 3.18 0.00 0.99 o -2 8 2 87.28 88.80 3.19 o -1 8 2 17.29 14.24 0.55 o 0 8 2 0.00 0.28 0.60 o 1 8 2 15.95 13.47 0.60 o 2 8 2 12.05 11.82 0.49 o 3 8 2 138.76 130.87 3.36 o 4 8 2 4.66 4.45 0.27 o -3 9 2 6.93 5.72 0.27 o -2 9 2 6.19 6.43 0.27 o -1 9 2 0.65 1.76 0.71 o 0 9 2 0.00 0.46 0.45 o 1 9 2 1.42 1.37 0.22 o -9 1 3 199.36 193.61 4.96 o -8 1 3 11.58 11.60 0.55 o -7 1 3 310.02 337.23 6.14 o -6 1 3 90.96 87.11 2.86 o -5 1 3 6.68 6.93 0.33 o -4 1 3 605.52 615.63 5.58 o -3 1 3 4.05 4.51 0.22 o -2 1 3 2396.93 2186.28 8.68 o -1 1 3 1870.37 1638.41 7.33 o 0 1 3 277.43 253.25 2.14 o 1 1 3 468.89 498.15 4.73 o 2 1 3 26.56 28.10 1.04 o 3 1 3 550.27 610.29 6.84 o 4 1 3 7.37 9.18 0.44 o 5 1 3 3.89 5.11 0.44 o 6 1 3 43.93 46.42 1.87 o 7 1 3 0.18 0.55 1.04 o 8 1 3 0.02 0.00 0.82 o -9 2 3 6.34 5.94 0.44 o -8 2 3 166.77 173.03 4.80 o -7 2 3 27.62 29.58 1.15 o -6 2 3 305.93 330.56 5.64 o -5 2 3 4.50 4.51 0.27 o -4 2 3 489.38 503.54 5.45 o -3 2 3 1707.57 1669.47 8.97 o -2 2 3 5284.71 5255.51 44.78 o -1 2 3 181.67 151.98 2.54 o 0 2 3 190.26 166.42 3.29 o 1 2 3 5.15 5.77 0.27 o 2 2 3 242.04 265.48 4.20 o 3 2 3 14.23 22.21 0.93 o 4 2 3 17.41 18.91 0.77 o 5 2 3 63.83 60.42 2.48 o 6 2 3 108.21 100.88 3.74 o 7 2 3 2.58 1.70 0.33 o 8 2 3 1.35 1.59 0.77 o -9 3 3 3.90 4.07 0.38 o -8 3 3 109.06 102.87 3.69 o -7 3 3 54.29 56.56 2.09 o -6 3 3 22.76 22.93 0.93 o -5 3 3 881.74 892.42 8.84 o -4 3 3 27.42 29.64 1.21 o -3 3 3 1.14 1.15 0.82 o -2 3 3 588.82 520.70 5.35 o -1 3 3 126.56 124.67 2.59 o 0 3 3 1769.58 1718.77 23.03 o 1 3 3 21.59 23.54 0.88 o 2 3 3 959.51 1001.71 8.97 o 3 3 3 83.30 79.27 2.92 o 4 3 3 48.92 48.85 2.09 o 5 3 3 28.21 24.64 0.99 o 6 3 3 36.22 38.06 1.32 o 7 3 3 0.04 0.33 0.82 o -9 4 3 0.00 0.55 0.88 o -8 4 3 0.25 0.11 0.93 o -7 4 3 1.76 2.42 0.38 o -6 4 3 231.77 228.98 5.30 o -5 4 3 22.16 23.37 0.93 o -4 4 3 7.78 7.48 0.33 o -3 4 3 7.92 9.07 0.33 o -2 4 3 1.62 1.32 0.71 o -1 4 3 1241.35 1227.15 9.48 o 0 4 3 13.21 16.52 5.06 o 1 4 3 8.25 9.35 0.38 o 2 4 3 138.24 150.99 3.86 o 3 4 3 0.18 2.91 1.10 o 4 4 3 0.00 0.00 0.99 o 5 4 3 228.43 214.17 5.30 o 6 4 3 196.40 197.99 4.58 o 7 4 3 3.63 1.98 0.93 o -8 5 3 0.05 0.00 0.88 o -7 5 3 14.75 14.24 0.66 o -6 5 3 20.12 21.94 0.71 o -5 5 3 18.84 15.06 0.66 o -4 5 3 21.12 22.43 0.93 o -3 5 3 227.90 212.23 4.69 o -2 5 3 11.33 9.51 0.38 o -1 5 3 26.58 21.61 0.88 o 0 5 3 158.30 148.14 4.63 o 1 5 3 71.28 68.08 2.75 o 2 5 3 12.36 14.07 0.60 o 3 5 3 70.83 76.60 2.92 o 4 5 3 3.39 2.09 1.21 o 5 5 3 9.75 10.22 0.44 o 6 5 3 0.31 0.00 0.82 o -8 6 3 13.25 9.57 0.44 o -7 6 3 8.41 6.60 0.38 o -6 6 3 1.31 0.99 1.04 o -5 6 3 45.65 46.76 1.82 o -4 6 3 2.71 1.59 1.04 o -3 6 3 0.05 0.55 0.88 o -2 6 3 138.12 134.27 4.08 o -1 6 3 4.78 5.72 0.38 o 0 6 3 19.66 20.65 2.01 o 1 6 3 56.60 52.05 2.04 o 2 6 3 2.67 3.46 1.15 o 3 6 3 28.36 30.35 1.21 o 4 6 3 5.60 6.05 0.38 o 5 6 3 3.11 2.86 0.27 o 6 6 3 15.35 15.67 0.60 o -7 7 3 0.18 0.00 0.60 o -6 7 3 6.24 6.32 0.33 o -5 7 3 0.89 0.00 0.77 o -4 7 3 0.77 0.49 1.04 o -3 7 3 38.30 34.10 1.48 o -2 7 3 138.88 141.49 4.30 o -1 7 3 4.57 2.31 1.21 o 0 7 3 43.40 46.33 3.14 o 1 7 3 91.60 86.38 3.36 o 2 7 3 35.03 38.28 1.48 o 3 7 3 0.03 0.00 0.88 o 4 7 3 13.29 12.59 0.49 o -6 8 3 1.11 1.26 0.66 o -5 8 3 3.99 3.79 0.27 o -4 8 3 0.05 2.03 0.77 o -3 8 3 4.81 5.88 0.33 o -2 8 3 1.51 0.00 0.88 o -1 8 3 8.29 7.70 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