#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2012227.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012227_Fobs loop_ _publ_author_name 'Linden, Anthony' 'Lee, C. Kuan' 'Muhammad Sofian, A. S.' _publ_section_title ; 3-O-Acetyl-4-deoxy-4-iodo-\b-D-fructofuranosyl 2,3,6-tri-O-acetyl-4-chloro-4-deoxy-\a-D-glucopyranoside ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1098 _journal_page_last 1100 _journal_volume 57 _journal_year 2001 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.8407 _cell_length_b 10.5562 _cell_length_c 28.2974 _exptl_crystal_F_000 1288.00 _reflns_d_resolution_high 0.7110 _[local]_cod_data_source_file sk1489Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' MS64 (L0105)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 183.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5766.50 5621.64 99.82 o 4 0 0 17423.59 17664.44 481.45 o 6 0 0 4264.07 3943.97 89.78 o 8 0 0 198.30 172.45 15.74 o 10 0 0 5276.89 5312.95 137.78 o 12 0 0 179.97 150.99 27.68 o 2 1 0 145.72 140.53 2.92 o 3 1 0 3089.70 2996.60 45.54 o 4 1 0 8687.25 8555.65 118.51 o 5 1 0 31020.04 30339.30 1093.85 o 6 1 0 2.67 20.83 3.78 o 7 1 0 1139.59 1254.89 23.56 o 8 1 0 458.57 463.40 14.31 o 9 1 0 2188.28 2216.50 44.00 o 10 1 0 304.87 317.65 13.80 o 11 1 0 2983.56 2964.06 79.18 o 12 1 0 108.50 90.53 22.18 o 2 2 0 10779.38 10762.73 139.67 o 3 2 0 18.68 48.89 2.49 o 4 2 0 1370.92 1432.21 25.49 o 5 2 0 2614.14 2680.00 39.59 o 6 2 0 13340.47 13438.96 238.03 o 7 2 0 28.58 34.59 4.20 o 8 2 0 20.79 59.20 10.33 o 9 2 0 0.66 6.36 5.44 o 10 2 0 8053.84 8476.54 163.79 o 11 2 0 86.87 66.48 17.23 o 12 2 0 809.78 746.16 53.85 o 1 3 0 18876.34 18351.36 326.56 o 2 3 0 6721.60 7012.40 87.79 o 3 3 0 315.73 341.67 6.94 o 4 3 0 43.57 38.44 3.55 o 5 3 0 14288.19 14329.64 241.21 o 6 3 0 384.85 413.42 13.23 o 7 3 0 6752.27 6527.98 99.04 o 8 3 0 308.33 272.23 10.59 o 9 3 0 1318.21 1406.25 34.26 o 10 3 0 65.03 51.69 8.74 o 11 3 0 2454.37 2596.06 103.71 o 12 3 0 0.00 21.72 19.10 o 0 4 0 1680.46 1599.71 27.52 o 1 4 0 458.48 454.31 6.77 o 2 4 0 319.13 348.71 7.30 o 3 4 0 662.19 713.32 15.18 o 4 4 0 8809.55 9156.82 132.50 o 5 4 0 1343.51 1473.87 26.71 o 6 4 0 10931.63 11387.39 190.73 o 7 4 0 301.98 291.41 10.61 o 8 4 0 458.11 526.68 17.56 o 9 4 0 544.00 548.93 17.67 o 10 4 0 1937.88 2167.35 72.91 o 11 4 0 20.37 17.77 13.78 o 1 5 0 27131.75 27696.92 426.48 o 2 5 0 88.47 116.08 5.18 o 3 5 0 5343.95 5702.57 83.58 o 4 5 0 358.34 326.32 9.07 o 5 5 0 6657.06 6515.08 95.72 o 6 5 0 403.46 455.73 12.88 o 7 5 0 2094.06 2057.81 50.84 o 8 5 0 19.65 36.47 16.86 o 9 5 0 522.37 608.32 21.68 o 10 5 0 6.08 3.11 13.62 o 11 5 0 1407.64 1350.64 52.43 o 0 6 0 7493.45 7624.53 217.40 o 1 6 0 4013.86 4115.69 71.15 o 2 6 0 38.71 71.67 4.94 o 3 6 0 299.16 358.93 9.38 o 4 6 0 11765.89 12152.97 187.21 o 5 6 0 65.86 60.12 5.18 o 6 6 0 5615.98 5783.79 104.01 o 7 6 0 493.67 438.93 15.73 o 8 6 0 1.17 55.91 11.59 o 9 6 0 135.64 117.95 10.02 o 10 6 0 820.94 843.59 36.43 o 11 6 0 43.72 37.62 16.49 o 1 7 0 6472.60 6417.43 127.50 o 2 7 0 15.70 26.25 4.33 o 3 7 0 1610.75 1692.32 29.41 o 4 7 0 886.94 871.54 24.10 o 5 7 0 4724.24 4725.81 124.48 o 6 7 0 54.62 93.08 8.24 o 7 7 0 1387.21 1442.52 32.43 o 8 7 0 88.55 100.78 9.80 o 9 7 0 1411.31 1445.62 39.92 o 10 7 0 275.65 220.56 29.25 o 0 8 0 7929.28 7874.96 286.12 o 1 8 0 498.93 498.59 15.05 o 2 8 0 2463.12 2598.51 46.43 o 3 8 0 809.50 967.37 20.68 o 4 8 0 2207.45 2281.72 47.11 o 5 8 0 1.95 3.26 5.92 o 6 8 0 6248.27 6430.01 121.31 o 7 8 0 138.98 142.29 10.62 o 8 8 0 106.22 112.49 10.70 o 9 8 0 81.30 99.42 16.97 o 10 8 0 1592.35 1426.32 82.64 o 1 9 0 5815.46 5763.30 116.82 o 2 9 0 77.59 102.24 7.67 o 3 9 0 206.90 189.35 8.24 o 4 9 0 146.89 130.42 9.56 o 5 9 0 6885.82 7121.74 124.19 o 6 9 0 9.26 11.74 9.92 o 7 9 0 104.84 125.66 12.63 o 8 9 0 57.56 47.50 17.04 o 9 9 0 1011.33 1052.21 52.08 o 0 10 0 6796.59 6556.79 341.37 o 1 10 0 121.06 69.56 10.27 o 2 10 0 1026.92 1073.10 32.91 o 3 10 0 128.18 174.51 15.33 o 4 10 0 1256.74 1373.96 53.76 o 5 10 0 7.65 9.45 7.69 o 6 10 0 981.58 1002.13 31.47 o 7 10 0 2.59 8.00 14.41 o 8 10 0 35.26 57.40 13.30 o 9 10 0 0.79 7.20 27.59 o 1 11 0 1735.06 1927.33 61.26 o 2 11 0 204.10 218.50 26.42 o 3 11 0 8.37 -0.10 8.20 o 4 11 0 95.22 107.71 15.05 o 5 11 0 1468.06 1448.17 69.81 o 6 11 0 80.39 91.63 22.79 o 7 11 0 106.69 81.79 22.60 o 8 11 0 55.28 56.21 17.94 o 0 12 0 936.99 1066.09 73.07 o 1 12 0 106.88 102.38 13.10 o 2 12 0 483.43 427.36 48.60 o 3 12 0 0.39 13.30 13.88 o 4 12 0 416.62 427.50 24.35 o 5 12 0 0.46 12.42 12.26 o 6 12 0 334.81 316.40 25.64 o 7 12 0 153.78 170.03 28.33 o 1 13 0 464.07 468.51 27.95 o 2 13 0 321.20 478.07 52.50 o 3 13 0 5.89 17.08 29.93 o 4 13 0 15.61 14.30 25.68 o 5 13 0 594.66 523.21 35.45 o 0 14 0 347.57 350.30 47.79 o 1 14 0 12.46 11.10 28.31 o 2 14 0 347.26 355.79 24.86 o 3 14 0 9.67 0.26 20.65 o 4 14 0 601.11 597.22 45.46 o 1 0 1 31.89 7.54 3.34 o 2 0 1 533.13 608.92 7.91 o 4 0 1 12056.45 11984.11 197.72 o 5 0 1 2156.10 2215.30 39.65 o 6 0 1 1016.60 1094.47 23.52 o 7 0 1 7491.94 7808.42 116.79 o 8 0 1 2809.00 2929.49 60.45 o 9 0 1 623.95 663.55 19.29 o 10 0 1 37.16 64.43 12.15 o 11 0 1 8.08 26.90 12.70 o 12 0 1 446.06 382.99 30.78 o -12 1 1 433.78 380.67 31.55 o -11 1 1 231.05 238.07 18.39 o -10 1 1 222.37 220.99 14.93 o -9 1 1 1406.09 1432.13 32.36 o -8 1 1 2869.16 2955.32 55.23 o -7 1 1 5089.96 4984.65 76.60 o -6 1 1 271.82 275.35 8.30 o -5 1 1 301.33 374.97 14.92 o -4 1 1 3060.28 3096.41 47.60 o -3 1 1 19571.22 19546.43 419.32 o -2 1 1 6338.47 6372.65 78.73 o -1 1 1 7147.22 4311.19 625.42 o 1 1 1 6919.62 5057.78 696.27 o 2 1 1 5485.68 5404.74 67.63 o 3 1 1 19356.93 19203.20 417.97 o 4 1 1 2614.92 2639.94 37.51 o 5 1 1 356.19 436.19 9.96 o 6 1 1 280.57 283.02 10.89 o 7 1 1 4981.21 4960.71 79.63 o 8 1 1 2759.98 2772.14 47.16 o 9 1 1 1426.04 1443.39 26.87 o 10 1 1 195.71 176.88 12.03 o 11 1 1 248.24 228.27 20.29 o 12 1 1 504.20 478.43 28.91 o -12 2 1 394.91 296.53 45.60 o -11 2 1 71.24 64.69 12.16 o -10 2 1 31.21 85.07 13.23 o -9 2 1 2023.75 2156.83 60.88 o -8 2 1 3061.69 3077.38 67.52 o -7 2 1 2721.10 2777.98 46.08 o -6 2 1 1826.20 1783.01 30.70 o -5 2 1 1997.11 1977.13 29.20 o -4 2 1 4802.67 4859.64 81.83 o -3 2 1 12494.52 13066.32 205.19 o -2 2 1 19768.93 20287.40 559.92 o 0 2 1 15111.23 15345.25 448.82 o 3 2 1 11990.29 12474.98 209.20 o 4 2 1 4214.46 4153.68 70.49 o 5 2 1 2022.85 1982.62 31.91 o 6 2 1 1852.03 1879.32 32.59 o 7 2 1 2682.50 2705.85 47.39 o 8 2 1 3038.97 3026.36 53.45 o 9 2 1 2065.35 2103.46 47.55 o 10 2 1 15.76 57.32 8.86 o 11 2 1 95.19 97.11 15.78 o 12 2 1 428.93 331.00 51.66 o -12 3 1 483.98 288.75 47.51 o -11 3 1 132.43 116.10 16.21 o -10 3 1 365.09 382.02 25.15 o -9 3 1 1153.49 1183.53 40.75 o -8 3 1 3206.45 3278.35 60.74 o -7 3 1 3878.21 3925.51 70.57 o -6 3 1 588.47 656.08 13.21 o -5 3 1 256.32 242.75 12.56 o -4 3 1 2498.42 2442.83 37.70 o -3 3 1 13480.23 13910.59 265.83 o -2 3 1 23368.93 23631.06 526.47 o -1 3 1 5939.48 6200.57 68.61 o 0 3 1 11571.86 11722.24 159.54 o 1 3 1 6221.28 6493.41 80.55 o 2 3 1 22759.48 22697.19 498.07 o 3 3 1 13399.13 13587.51 196.81 o 4 3 1 2386.53 2348.68 37.15 o 5 3 1 275.19 258.15 7.71 o 6 3 1 627.05 654.67 12.65 o 7 3 1 3913.43 3977.44 71.64 o 8 3 1 3232.39 3272.76 60.75 o 9 3 1 1234.94 1292.01 33.37 o 10 3 1 356.14 369.40 17.98 o 11 3 1 147.30 119.97 15.62 o 12 3 1 534.11 531.05 105.02 o -11 4 1 270.94 301.64 23.96 o -10 4 1 209.24 224.36 17.96 o -9 4 1 1027.91 1041.36 29.62 o -8 4 1 4148.44 4220.89 92.42 o -7 4 1 896.33 991.33 22.94 o -6 4 1 2468.23 2467.69 39.80 o -5 4 1 17.65 31.49 6.25 o -4 4 1 4284.63 4192.94 77.64 o -3 4 1 11223.50 11364.81 170.93 o -2 4 1 5652.17 5795.58 77.70 o -1 4 1 8170.19 8404.44 111.84 o 0 4 1 1522.67 1503.22 17.62 o 1 4 1 8507.54 8772.56 100.78 o 2 4 1 6320.93 6433.96 91.63 o 3 4 1 11675.41 11769.50 163.31 o 4 4 1 4551.25 4481.06 69.65 o 5 4 1 12.43 41.23 4.91 o 6 4 1 2630.70 2678.73 50.12 o 7 4 1 985.49 1071.27 20.87 o 8 4 1 4128.54 4068.12 84.95 o 9 4 1 957.42 977.99 25.13 o 10 4 1 182.16 206.06 13.57 o 11 4 1 301.65 321.67 21.57 o -11 5 1 129.73 153.23 16.63 o -10 5 1 163.73 172.60 28.52 o -9 5 1 1343.80 1417.57 39.07 o -8 5 1 3392.42 3424.20 71.59 o -7 5 1 3077.75 3181.12 64.91 o -6 5 1 3029.52 3008.27 54.85 o -5 5 1 1572.84 1589.47 28.32 o -4 5 1 3665.09 3666.27 70.51 o -3 5 1 7673.08 7625.27 109.89 o -2 5 1 7944.32 7854.82 113.56 o -1 5 1 819.31 809.80 12.78 o 0 5 1 1398.65 1511.02 22.66 o 1 5 1 713.26 706.80 13.45 o 2 5 1 8155.88 8017.65 115.66 o 3 5 1 7607.11 7528.40 116.39 o 4 5 1 3606.32 3603.56 53.37 o 5 5 1 1507.02 1527.01 27.99 o 6 5 1 3137.80 3191.40 83.22 o 7 5 1 3008.54 3203.63 54.47 o 8 5 1 3344.39 3410.30 79.90 o 9 5 1 1248.58 1251.52 50.42 o 10 5 1 186.91 196.42 19.05 o 11 5 1 123.72 127.40 15.87 o -11 6 1 63.15 60.67 28.69 o -10 6 1 214.45 192.08 16.57 o -9 6 1 505.17 553.60 18.25 o -8 6 1 3309.58 3413.68 78.23 o -7 6 1 2465.18 2463.74 47.10 o -6 6 1 1158.96 1247.70 28.34 o -5 6 1 360.23 397.85 10.65 o -4 6 1 2571.58 2516.37 46.24 o -3 6 1 9183.92 9441.61 159.31 o -2 6 1 9551.14 9573.97 142.74 o -1 6 1 3374.31 3532.56 56.39 o 0 6 1 445.67 573.41 12.70 o 1 6 1 3161.23 3303.39 58.83 o 2 6 1 9686.27 9637.99 143.12 o 3 6 1 8867.35 9166.78 155.76 o 4 6 1 2218.32 2121.62 32.03 o 5 6 1 356.06 358.42 12.21 o 6 6 1 1050.87 1110.85 29.66 o 7 6 1 2155.22 2254.62 41.12 o 8 6 1 3150.22 3164.13 76.86 o 9 6 1 491.55 563.49 24.13 o 10 6 1 226.08 199.47 16.64 o 11 6 1 71.00 63.93 47.03 o -10 7 1 140.27 124.30 21.60 o -9 7 1 149.59 139.98 12.92 o -8 7 1 2127.44 2139.14 44.16 o -7 7 1 2581.73 2487.19 53.89 o -6 7 1 793.75 838.93 21.40 o -5 7 1 426.70 424.24 15.50 o -4 7 1 3371.08 3274.56 61.08 o -3 7 1 2663.11 2627.36 45.56 o -2 7 1 2260.62 2358.07 37.67 o -1 7 1 420.00 388.06 10.84 o 0 7 1 3166.30 3555.06 69.65 o 1 7 1 436.65 380.27 10.12 o 2 7 1 1976.43 2016.00 40.43 o 3 7 1 2461.81 2412.85 40.32 o 4 7 1 3471.16 3403.34 55.73 o 5 7 1 442.63 470.91 14.79 o 6 7 1 687.61 698.09 28.07 o 7 7 1 2662.86 2642.26 57.26 o 8 7 1 2340.57 2433.27 56.68 o 9 7 1 173.28 193.22 13.64 o 10 7 1 145.07 127.89 22.14 o -10 8 1 87.86 82.37 22.18 o -9 8 1 1224.21 1206.34 48.92 o -8 8 1 453.42 505.80 19.65 o -7 8 1 1416.26 1471.49 36.70 o -6 8 1 650.00 727.24 26.17 o -5 8 1 402.49 427.65 15.90 o -4 8 1 687.42 658.22 20.47 o -3 8 1 2548.99 2652.98 55.99 o -2 8 1 4035.53 4034.80 67.21 o -1 8 1 539.76 568.53 19.05 o 0 8 1 12.79 27.89 8.87 o 1 8 1 495.32 508.25 13.87 o 2 8 1 4116.25 4186.65 91.75 o 3 8 1 2866.80 2894.70 62.62 o 4 8 1 725.92 705.51 18.38 o 5 8 1 366.11 388.15 14.29 o 6 8 1 614.59 691.90 19.95 o 7 8 1 1412.13 1444.22 34.93 o 8 8 1 525.73 569.49 29.39 o 9 8 1 1326.80 1289.62 42.13 o 10 8 1 107.55 120.54 35.00 o -9 9 1 727.02 729.54 40.32 o -8 9 1 743.05 762.41 34.71 o -7 9 1 225.89 200.03 12.51 o -6 9 1 534.61 574.03 22.98 o -5 9 1 238.69 250.47 12.09 o -4 9 1 583.00 573.68 25.79 o -3 9 1 1250.47 1255.10 32.42 o -2 9 1 4389.50 4524.62 98.34 o -1 9 1 1337.01 1336.12 41.15 o 0 9 1 386.97 436.52 30.60 o 1 9 1 1316.79 1341.76 47.36 o 2 9 1 4322.61 4424.99 95.83 o 3 9 1 1255.98 1270.92 31.36 o 4 9 1 663.71 642.28 17.43 o 5 9 1 248.71 253.79 15.67 o 6 9 1 533.17 555.35 27.90 o 7 9 1 354.38 360.66 16.74 o 8 9 1 837.78 895.83 46.55 o 9 9 1 709.10 682.80 30.69 o -9 10 1 385.45 343.46 37.70 o -8 10 1 573.16 548.22 26.90 o -7 10 1 955.19 951.50 32.80 o -6 10 1 155.53 122.22 13.31 o -5 10 1 136.37 140.04 9.80 o -4 10 1 1634.59 1610.86 42.33 o -3 10 1 1635.16 1741.04 47.13 o -2 10 1 240.38 270.50 29.30 o -1 10 1 1394.31 1396.95 66.81 o 0 10 1 83.02 129.40 12.60 o 1 10 1 1375.51 1394.55 35.43 o 2 10 1 332.68 347.61 17.29 o 3 10 1 1665.42 1784.12 47.73 o 4 10 1 1616.47 1600.58 78.09 o 5 10 1 130.38 131.52 46.69 o 6 10 1 157.40 132.89 30.96 o 7 10 1 944.67 992.17 35.18 o 8 10 1 587.49 596.31 32.34 o 9 10 1 378.89 278.15 24.28 o -8 11 1 599.49 557.56 35.02 o -7 11 1 471.22 469.23 25.15 o -6 11 1 29.88 33.32 12.94 o -5 11 1 104.52 90.98 14.12 o -4 11 1 585.57 565.78 46.46 o -3 11 1 958.82 954.60 41.37 o -2 11 1 1366.80 1338.78 60.77 o -1 11 1 334.93 357.16 16.30 o 0 11 1 23.79 33.36 14.91 o 1 11 1 360.64 381.16 27.55 o 3 11 1 920.18 957.07 44.24 o 4 11 1 524.12 573.83 34.75 o 5 11 1 95.12 66.66 10.99 o 6 11 1 26.14 17.68 11.99 o 7 11 1 410.24 367.39 24.59 o 8 11 1 524.52 538.65 46.10 o -7 12 1 423.89 437.91 37.14 o -6 12 1 405.92 386.26 28.50 o -5 12 1 339.99 296.71 19.28 o -4 12 1 349.70 352.99 25.38 o -3 12 1 712.73 661.51 40.28 o -2 12 1 822.78 820.09 55.50 o -1 12 1 410.81 474.87 31.14 o 0 12 1 42.48 28.54 13.76 o 1 12 1 456.66 477.86 43.76 o 2 12 1 826.08 927.59 55.61 o 3 12 1 659.68 625.73 31.88 o 4 12 1 343.35 343.36 24.06 o 5 12 1 351.81 369.42 24.76 o 6 12 1 397.74 439.73 29.48 o 7 12 1 419.70 338.00 27.11 o -5 13 1 48.78 69.05 17.48 o -4 13 1 436.48 341.04 27.23 o -3 13 1 753.58 761.93 40.58 o -2 13 1 239.80 224.72 24.08 o -1 13 1 626.12 651.68 29.55 o 0 13 1 138.14 105.63 27.45 o 1 13 1 631.06 627.86 42.96 o 2 13 1 245.87 258.34 44.49 o 3 13 1 805.85 742.43 48.20 o 4 13 1 453.79 392.85 66.99 o 5 13 1 54.47 49.71 18.61 o -4 14 1 90.82 55.47 32.00 o -3 14 1 312.94 313.37 38.08 o -2 14 1 612.58 549.94 34.79 o -1 14 1 215.37 210.09 17.82 o 0 14 1 28.38 10.06 22.32 o 1 14 1 195.70 169.02 30.25 o 2 14 1 588.63 557.47 35.46 o 3 14 1 288.23 276.06 25.55 o 4 14 1 102.50 102.20 20.56 o 2 0 2 0.66 3.28 1.21 o 3 0 2 6681.30 6720.86 92.49 o 4 0 2 174.93 123.60 5.72 o 5 0 2 16408.41 15975.78 360.90 o 6 0 2 0.62 12.36 3.68 o 7 0 2 1372.70 1460.84 37.46 o 8 0 2 66.85 66.34 6.06 o 9 0 2 893.05 1038.03 26.81 o 10 0 2 315.96 264.78 15.57 o 11 0 2 3741.44 3844.74 106.77 o 12 0 2 0.34 -8.22 25.07 o -12 1 2 429.14 398.52 39.00 o -11 1 2 63.61 65.74 12.20 o -10 1 2 3179.01 3360.75 82.33 o -9 1 2 688.90 715.73 21.59 o 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25.75 o 4 2 2 239.90 226.90 8.03 o 5 2 2 15420.46 15163.44 226.22 o 6 2 2 986.89 992.32 16.28 o 7 2 2 181.67 209.40 8.43 o 8 2 2 55.63 58.67 7.52 o 9 2 2 775.99 867.92 24.60 o 10 2 2 234.30 218.25 21.33 o 11 2 2 1252.05 1242.09 57.64 o 12 2 2 24.24 19.83 17.18 o -12 3 2 484.64 405.64 25.22 o -11 3 2 81.20 64.11 11.93 o -10 3 2 1795.41 1986.91 73.35 o -9 3 2 10.24 12.33 7.54 o -8 3 2 207.05 291.64 27.81 o -7 3 2 790.73 784.36 18.21 o -6 3 2 5533.37 5486.35 93.18 o -5 3 2 998.93 1014.30 18.13 o -4 3 2 13986.63 14365.70 231.46 o -3 3 2 1193.85 1233.81 22.71 o -2 3 2 4150.61 4165.75 49.61 o -1 3 2 403.00 394.36 5.91 o 1 3 2 373.28 364.39 5.79 o 2 3 2 4436.03 4469.83 52.51 o 3 3 2 1208.62 1239.27 16.75 o 4 3 2 13569.66 13753.13 225.05 o 5 3 2 939.87 927.66 18.70 o 6 3 2 5265.81 5028.93 83.53 o 7 3 2 771.61 761.34 16.63 o 8 3 2 210.83 297.99 18.83 o 9 3 2 11.38 26.18 6.46 o 10 3 2 1852.37 1936.03 51.39 o 11 3 2 83.04 74.04 21.61 o 12 3 2 538.04 427.53 72.75 o -11 4 2 2217.81 2315.61 85.36 o 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