#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/22/2012243.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012243_Fobs loop_ _publ_author_name 'Creed, Tim' 'Leardini, Rino' 'McNab, Hamish' 'Nanni, Daniele' 'Nicolson, Iain S.' 'Parkin, Andrew' 'Parsons, Simon' _publ_section_title ; Short intramolecular S···O interactions in S-substituted 2-mercaptoacetophenones ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1174 _journal_page_last 1176 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.497 _cell_angle_gamma 90.000 _cell_length_a 9.0151 _cell_length_b 12.7805 _cell_length_c 10.6400 _exptl_crystal_F_000 480.00 _reflns_d_resolution_high 0.8202 _[local]_cod_data_source_file bm1449IIsup2.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' sptc01 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 116.81 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 765.72 748.55 22.95 o 2 0 0 60.48 46.60 3.27 o 3 0 0 1294.16 1363.22 72.52 o 4 0 0 617.43 608.72 46.04 o 5 0 0 10.27 6.67 0.70 o 6 0 0 79.41 96.19 5.10 o 7 0 0 294.61 252.81 26.52 o 8 0 0 2.73 0.51 0.93 o 9 0 0 3.49 1.45 0.88 o 1 1 0 758.78 808.07 18.33 o 2 1 0 2961.37 3099.34 74.36 o 3 1 0 2492.21 2528.36 85.44 o 4 1 0 955.02 980.66 41.39 o 5 1 0 25.73 30.08 1.50 o 6 1 0 1.13 3.49 0.54 o 7 1 0 36.35 30.43 2.57 o 8 1 0 5.78 7.25 0.84 o 9 1 0 77.39 66.19 7.66 o 0 2 0 3990.17 3943.26 18.70 o 1 2 0 0.14 -0.02 0.98 o 2 2 0 4830.19 5278.18 382.49 o 3 2 0 3008.97 3280.01 172.67 o 4 2 0 544.73 567.10 49.43 o 5 2 0 280.90 278.03 19.57 o 6 2 0 70.91 73.66 5.30 o 7 2 0 160.78 143.99 17.41 o 8 2 0 7.19 3.81 1.03 o 9 2 0 0.20 0.12 0.86 o 1 3 0 64.79 82.87 3.23 o 2 3 0 21.12 22.76 2.65 o 3 3 0 824.72 893.73 66.99 o 4 3 0 1515.34 1583.70 159.58 o 5 3 0 332.59 317.15 24.66 o 6 3 0 1501.87 1473.51 117.77 o 7 3 0 5.33 6.52 1.01 o 8 3 0 147.55 140.52 20.39 o 9 3 0 3.48 4.86 1.02 o 10 3 0 74.12 106.47 2.53 o 0 4 0 1045.49 1109.97 6.35 o 1 4 0 775.43 795.01 30.14 o 2 4 0 142.97 174.00 7.89 o 3 4 0 0.16 -0.56 0.73 o 4 4 0 99.33 94.30 11.00 o 5 4 0 1.35 0.68 0.76 o 6 4 0 132.33 138.44 8.31 o 7 4 0 489.67 463.51 48.34 o 8 4 0 28.25 26.43 4.92 o 9 4 0 177.89 162.62 25.89 o 10 4 0 5.66 6.66 1.12 o 1 5 0 1812.38 1907.56 47.36 o 2 5 0 365.85 429.50 24.13 o 3 5 0 9.01 5.50 0.86 o 4 5 0 26.57 32.95 1.79 o 5 5 0 91.27 99.77 8.03 o 6 5 0 372.81 374.37 39.89 o 7 5 0 18.03 16.46 2.61 o 8 5 0 26.09 24.52 3.25 o 9 5 0 65.91 61.35 11.88 o 10 5 0 55.30 39.88 1.13 o 0 6 0 2064.89 2048.03 11.44 o 1 6 0 306.85 346.83 3.69 o 2 6 0 743.98 736.26 39.02 o 3 6 0 30.51 27.56 1.39 o 4 6 0 8.88 7.58 1.02 o 5 6 0 51.44 50.91 2.02 o 6 6 0 107.61 120.55 11.61 o 7 6 0 284.69 299.53 38.83 o 8 6 0 0.02 1.67 0.96 o 9 6 0 182.47 160.14 28.79 o 1 7 0 208.77 201.66 3.61 o 2 7 0 190.28 231.40 7.71 o 3 7 0 571.04 600.84 39.44 o 4 7 0 6.35 4.18 1.07 o 5 7 0 191.91 190.14 11.86 o 6 7 0 0.73 1.89 1.15 o 7 7 0 121.59 120.60 18.05 o 8 7 0 77.33 67.19 10.12 o 9 7 0 15.03 12.38 0.91 o 0 8 0 39.41 35.50 1.92 o 1 8 0 81.73 90.00 1.90 o 2 8 0 0.85 1.33 0.91 o 3 8 0 17.06 22.02 1.48 o 4 8 0 0.23 -0.55 1.16 o 5 8 0 928.77 921.10 66.85 o 6 8 0 49.96 49.83 5.09 o 7 8 0 39.88 39.45 3.76 o 8 8 0 22.27 20.94 2.95 o 9 8 0 42.12 36.43 1.08 o 1 9 0 273.09 271.69 3.45 o 2 9 0 172.06 172.66 2.90 o 3 9 0 255.06 260.24 16.56 o 4 9 0 715.24 743.08 82.90 o 5 9 0 9.83 12.11 1.06 o 6 9 0 25.48 22.30 2.37 o 7 9 0 4.45 4.44 0.85 o 8 9 0 15.88 15.68 1.02 o 0 10 0 101.62 103.28 3.36 o 1 10 0 105.35 112.13 2.56 o 2 10 0 10.62 9.08 1.38 o 3 10 0 3.23 2.36 1.22 o 4 10 0 9.99 10.36 1.36 o 5 10 0 1.16 1.91 0.91 o 6 10 0 6.38 7.38 1.24 o 7 10 0 7.26 6.29 0.86 o 8 10 0 3.42 3.23 0.62 o 1 11 0 494.34 494.30 6.71 o 2 11 0 96.82 94.67 2.58 o 3 11 0 18.51 17.47 1.49 o 4 11 0 15.35 13.20 1.35 o 5 11 0 0.60 1.36 0.81 o 6 11 0 25.66 24.95 2.35 o 7 11 0 8.74 7.04 0.80 o 0 12 0 0.53 1.24 1.71 o 1 12 0 93.29 84.49 2.61 o 2 12 0 278.64 292.65 4.20 o 3 12 0 2.32 3.03 1.14 o 4 12 0 26.51 28.89 2.61 o 5 12 0 20.94 21.97 1.99 o 6 12 0 3.31 2.65 0.80 o 1 13 0 57.51 55.22 1.99 o 2 13 0 1.85 2.08 1.35 o 3 13 0 60.27 61.19 2.26 o 4 13 0 24.48 19.35 1.95 o 5 13 0 5.79 6.06 1.18 o 0 14 0 0.64 0.66 1.37 o 1 14 0 2.81 1.84 1.10 o 2 14 0 22.58 21.07 1.56 o 3 14 0 18.76 16.69 1.69 o 4 14 0 3.55 1.98 1.14 o 1 15 0 1.07 0.82 1.11 o 2 15 0 10.20 9.78 0.84 o -9 1 1 9.92 6.86 0.81 o -8 1 1 21.93 21.74 1.14 o -7 1 1 33.77 24.49 1.07 o -6 1 1 71.80 62.88 1.66 o -5 1 1 676.89 657.43 10.06 o -4 1 1 1203.37 1222.66 24.87 o -3 1 1 427.41 412.93 9.40 o -2 1 1 3525.13 3585.17 24.18 o -1 1 1 106.16 118.00 3.50 o 0 1 1 1793.81 1715.84 41.09 o 1 1 1 8076.45 8384.89 209.97 o 2 1 1 8210.02 8923.06 29.07 o 3 1 1 192.26 220.44 2.42 o 4 1 1 3848.38 4336.13 49.48 o 5 1 1 26.59 35.54 1.35 o 6 1 1 245.40 263.71 6.11 o 7 1 1 227.34 255.31 8.58 o 8 1 1 15.90 17.41 1.42 o 9 1 1 94.27 122.26 2.52 o -9 2 1 112.60 89.54 2.28 o -8 2 1 1.94 0.70 1.21 o -7 2 1 121.21 110.54 4.53 o -6 2 1 120.40 104.98 3.51 o -5 2 1 20.29 13.01 1.22 o -4 2 1 1925.83 1930.93 10.87 o -3 2 1 552.77 570.78 4.47 o -2 2 1 4742.44 4904.62 21.39 o -1 2 1 7557.72 7720.71 33.42 o 0 2 1 5.18 9.55 0.74 o 1 2 1 618.51 616.06 3.83 o 2 2 1 616.99 575.12 4.29 o 3 2 1 316.42 338.74 3.68 o 4 2 1 2.62 1.34 1.03 o 5 2 1 1107.17 1193.72 9.62 o 6 2 1 3.95 4.83 1.50 o 7 2 1 129.40 146.88 4.09 o 8 2 1 7.16 7.76 2.02 o 9 2 1 9.86 11.03 1.82 o -10 3 1 1.24 1.16 0.82 o -9 3 1 7.75 7.13 1.74 o -8 3 1 0.85 0.44 1.20 o -7 3 1 6.99 6.11 1.39 o -6 3 1 25.19 24.82 1.32 o -5 3 1 268.97 258.44 2.89 o -4 3 1 937.09 946.72 7.21 o -3 3 1 5.54 15.42 1.06 o -2 3 1 236.05 233.43 2.60 o -1 3 1 61.62 76.13 1.42 o 0 3 1 95.04 117.86 1.64 o 1 3 1 163.78 171.12 2.09 o 3 3 1 221.37 222.01 3.08 o 4 3 1 1635.81 1868.98 11.57 o 5 3 1 356.15 393.10 5.37 o 6 3 1 0.90 1.50 1.50 o 7 3 1 21.53 26.37 2.34 o 8 3 1 0.75 0.54 1.69 o 9 3 1 11.90 16.33 1.66 o -10 4 1 3.46 4.00 0.84 o -9 4 1 158.54 135.46 2.70 o -8 4 1 4.88 4.05 1.29 o -7 4 1 25.37 18.72 1.53 o -6 4 1 443.57 418.28 4.35 o -5 4 1 927.55 876.04 5.70 o -4 4 1 1920.17 1904.90 11.59 o -3 4 1 596.96 638.26 5.41 o -2 4 1 1671.99 1616.07 8.82 o -1 4 1 277.09 264.01 2.87 o 0 4 1 1099.51 1116.99 6.44 o 1 4 1 1455.78 1531.20 8.23 o 2 4 1 148.80 161.05 2.55 o 3 4 1 2.09 3.53 1.11 o 4 4 1 64.59 65.35 2.21 o 5 4 1 531.76 629.24 7.16 o 6 4 1 22.70 20.97 2.12 o 7 4 1 99.46 112.37 3.65 o 8 4 1 160.81 185.62 4.65 o 9 4 1 4.66 5.86 1.57 o -10 5 1 12.06 9.12 0.76 o -9 5 1 28.16 20.12 1.32 o -8 5 1 129.26 101.10 3.80 o -7 5 1 952.58 848.26 6.91 o -6 5 1 174.64 164.37 2.91 o -5 5 1 389.64 362.12 3.79 o -4 5 1 16.53 16.37 1.53 o -3 5 1 1348.65 1355.82 9.04 o -2 5 1 125.04 134.02 2.50 o -1 5 1 204.69 178.73 2.68 o 0 5 1 738.68 763.00 5.60 o 1 5 1 319.71 336.84 3.73 o 2 5 1 17.86 8.57 1.12 o 3 5 1 89.44 102.44 2.54 o 4 5 1 357.73 389.64 5.35 o 5 5 1 21.50 24.76 2.02 o 6 5 1 139.65 157.58 4.19 o 7 5 1 9.83 11.44 2.23 o 8 5 1 177.45 205.52 4.93 o 9 5 1 59.79 76.67 2.69 o -9 6 1 73.08 56.18 1.67 o -8 6 1 70.67 56.19 1.98 o -7 6 1 25.07 23.22 3.61 o -6 6 1 603.23 544.78 5.32 o -5 6 1 1.14 1.33 0.88 o -4 6 1 2.10 3.37 1.15 o -3 6 1 75.84 64.78 2.09 o -2 6 1 36.80 39.15 1.61 o -1 6 1 360.77 375.85 4.22 o 0 6 1 381.26 415.84 4.42 o 1 6 1 675.79 718.02 6.14 o 2 6 1 540.62 605.44 6.00 o 3 6 1 82.57 110.63 2.90 o 4 6 1 113.01 121.71 3.31 o 5 6 1 30.19 36.94 2.33 o 6 6 1 296.02 345.80 6.46 o 7 6 1 41.81 59.34 2.97 o 8 6 1 6.36 7.62 1.85 o -9 7 1 2.99 2.62 0.82 o -8 7 1 72.77 60.56 3.22 o -7 7 1 2.42 2.33 1.05 o -6 7 1 16.75 15.31 1.45 o -5 7 1 1334.97 1240.36 8.08 o -4 7 1 116.93 110.87 3.54 o -3 7 1 182.96 169.70 3.49 o -2 7 1 384.10 403.25 5.11 o -1 7 1 372.25 367.89 4.64 o 0 7 1 275.43 284.08 4.14 o 1 7 1 481.66 527.86 5.77 o 2 7 1 563.26 539.29 6.05 o 3 7 1 149.99 172.68 3.74 o 4 7 1 88.24 102.75 3.38 o 5 7 1 6.59 9.16 1.93 o 6 7 1 241.00 293.23 5.97 o 7 7 1 3.24 7.74 1.64 o 8 7 1 8.24 8.23 1.61 o -9 8 1 18.01 16.59 0.92 o -8 8 1 12.83 11.48 1.15 o -7 8 1 38.90 34.01 1.54 o -6 8 1 193.25 179.13 8.92 o -5 8 1 10.07 7.90 1.27 o -4 8 1 125.89 109.68 3.32 o -3 8 1 116.10 119.05 3.29 o -2 8 1 97.22 84.41 2.73 o -1 8 1 454.59 452.45 5.71 o 0 8 1 745.19 799.39 7.79 o 1 8 1 54.71 40.20 1.98 o 2 8 1 69.70 72.59 2.64 o 3 8 1 360.57 415.60 6.24 o 4 8 1 0.05 -0.45 1.78 o 5 8 1 298.26 329.92 6.20 o 6 8 1 68.52 76.86 3.60 o 7 8 1 195.53 213.78 4.88 o -8 9 1 1.43 -0.22 0.83 o -7 9 1 1.09 0.18 2.10 o -6 9 1 33.89 32.33 1.61 o -5 9 1 70.13 66.60 2.36 o -4 9 1 49.67 44.05 2.55 o -3 9 1 159.79 154.34 3.88 o -2 9 1 30.86 35.56 2.11 o -1 9 1 65.62 66.55 2.63 o 0 9 1 38.12 41.27 2.26 o 1 9 1 0.21 0.63 1.40 o 2 9 1 13.86 14.47 1.77 o 3 9 1 28.25 27.39 2.21 o 4 9 1 10.76 17.08 2.00 o 5 9 1 0.83 0.91 1.89 o 6 9 1 1.19 0.54 1.99 o 7 9 1 17.67 16.87 1.85 o -8 10 1 2.19 2.39 0.83 o -7 10 1 32.46 30.75 2.54 o -6 10 1 35.54 36.51 1.66 o -5 10 1 33.74 29.86 1.73 o -4 10 1 2.57 1.89 1.52 o -3 10 1 156.28 147.14 4.23 o -2 10 1 490.22 458.09 7.04 o -1 10 1 0.11 -0.92 1.47 o 0 10 1 235.29 247.39 5.09 o 1 10 1 70.29 66.98 2.90 o 2 10 1 21.48 21.15 2.27 o 3 10 1 329.84 348.27 6.41 o 4 10 1 6.13 9.18 1.95 o 5 10 1 88.65 109.24 3.58 o 6 10 1 82.78 79.61 3.18 o -7 11 1 24.73 20.12 1.09 o -6 11 1 99.93 87.15 2.13 o -4 11 1 16.28 17.97 1.77 o -3 11 1 42.33 39.34 2.58 o -2 11 1 2.71 4.51 1.61 o -1 11 1 9.07 9.22 1.82 o 0 11 1 20.23 19.96 2.07 o 1 11 1 41.56 47.22 2.81 o 2 11 1 95.09 100.86 3.76 o 3 11 1 8.15 7.83 2.00 o 4 11 1 4.12 5.68 1.61 o 5 11 1 1.20 1.13 1.46 o 6 11 1 23.71 26.72 1.91 o -6 12 1 4.90 4.72 0.83 o -5 12 1 7.99 6.82 1.06 o -4 12 1 7.88 8.69 1.81 o -3 12 1 26.25 27.67 2.22 o -2 12 1 83.12 81.63 3.37 o -1 12 1 0.01 2.59 1.53 o 0 12 1 169.53 169.95 4.66 o 1 12 1 128.96 130.69 4.13 o 2 12 1 1.48 1.92 1.62 o 3 12 1 82.60 78.81 3.34 o 4 12 1 0.16 1.38 1.38 o 5 12 1 24.82 27.63 1.96 o -6 13 1 4.17 4.54 0.61 o -5 13 1 14.61 15.76 1.39 o -4 13 1 5.19 4.42 1.47 o -3 13 1 36.77 32.82 2.29 o -2 13 1 96.46 87.56 3.36 o -1 13 1 62.43 63.65 2.99 o 0 13 1 5.80 5.59 1.92 o 1 13 1 0.64 -0.28 1.51 o 2 13 1 52.08 58.75 2.65 o 3 13 1 93.79 97.28 3.14 o -4 14 1 4.70 7.04 1.15 o -3 14 1 60.75 50.84 2.34 o -2 14 1 53.61 49.49 2.34 o -1 14 1 0.50 -0.40 1.43 o 0 14 1 6.02 7.34 1.64 o 1 14 1 47.92 45.95 2.28 o 2 14 1 0.10 0.61 1.27 o -2 15 1 0.80 0.97 1.00 o -1 15 1 1.97 0.85 1.11 o 0 15 1 6.58 5.12 1.27 o 1 15 1 3.09 2.65 1.18 o 2 15 1 7.47 5.86 1.06 o -9 0 2 115.67 105.26 2.57 o -8 0 2 362.93 289.25 4.10 o -7 0 2 17.12 14.75 1.26 o -6 0 2 13.83 10.88 1.05 o -5 0 2 0.22 -0.52 0.74 o -4 0 2 1770.80 1573.11 9.31 o -3 0 2 125.11 109.55 1.89 o -2 0 2 41.88 31.40 1.08 o -1 0 2 172.11 147.75 1.71 o 0 0 2 3087.29 2914.53 13.43 o 1 0 2 2565.64 2365.83 10.43 o 2 0 2 95.63 97.12 1.89 o 3 0 2 341.43 322.62 3.82 o 4 0 2 903.01 1000.58 8.02 o 5 0 2 1347.86 1464.00 11.14 o 6 0 2 358.58 388.20 6.09 o 7 0 2 259.03 267.09 5.40 o 8 0 2 102.92 117.41 3.73 o 9 0 2 120.37 129.63 3.53 o -10 1 2 7.36 6.12 1.19 o -9 1 2 17.71 14.73 0.97 o -8 1 2 163.74 145.42 2.60 o -7 1 2 142.75 124.77 1.83 o -6 1 2 96.21 92.40 1.42 o -5 1 2 2.09 0.52 0.50 o -4 1 2 10.79 8.50 0.81 o -3 1 2 28.57 27.41 0.82 o -2 1 2 82.16 81.22 1.06 o -1 1 2 469.26 471.24 13.74 o 0 1 2 5082.66 4877.36 36.22 o 1 1 2 193.21 173.22 1.48 o 2 1 2 506.56 459.12 6.51 o 3 1 2 134.36 143.31 4.79 o 4 1 2 472.39 494.26 5.12 o 5 1 2 378.30 403.45 3.96 o 6 1 2 37.04 41.33 1.69 o 7 1 2 6.71 7.01 1.33 o 8 1 2 57.99 63.74 4.12 o 9 1 2 0.74 2.22 0.97 o -10 2 2 23.62 19.66 1.13 o -9 2 2 10.72 7.17 1.17 o -8 2 2 80.06 69.95 2.17 o -7 2 2 20.60 20.36 1.48 o -6 2 2 272.37 221.25 10.27 o -5 2 2 474.26 506.92 3.93 o -4 2 2 496.30 502.56 4.82 o -3 2 2 469.18 500.35 4.24 o -2 2 2 730.03 716.71 4.67 o -1 2 2 4446.28 4247.03 18.76 o 0 2 2 13645.56 13247.38 64.28 o 1 2 2 6012.55 6020.92 25.99 o 2 2 2 202.25 230.24 2.91 o 3 2 2 224.65 229.76 3.39 o 4 2 2 15.77 15.09 1.42 o 5 2 2 20.57 25.98 1.80 o 6 2 2 480.49 516.84 7.35 o 7 2 2 0.88 3.09 1.66 o 8 2 2 33.07 37.75 2.52 o 9 2 2 61.02 76.96 2.77 o -10 3 2 142.52 195.32 2.77 o -9 3 2 11.22 12.69 1.30 o -8 3 2 0.48 3.18 2.74 o -7 3 2 740.61 650.98 5.97 o -6 3 2 175.57 158.06 2.97 o -5 3 2 661.17 655.30 8.01 o -4 3 2 494.64 478.25 4.90 o -3 3 2 1166.86 1141.75 7.25 o -2 3 2 1930.36 1825.70 9.21 o -1 3 2 419.55 350.98 3.11 o 0 3 2 6410.83 6253.70 26.78 o 1 3 2 5242.63 5496.81 24.91 o 2 3 2 4.35 7.56 1.09 o 3 3 2 582.92 596.87 5.72 o 4 3 2 64.77 57.13 2.15 o 5 3 2 144.44 146.82 3.60 o 6 3 2 38.11 37.53 2.59 o 7 3 2 195.57 214.69 5.05 o 8 3 2 10.52 11.03 2.03 o 9 3 2 84.83 116.91 3.20 o -10 4 2 10.24 15.10 0.99 o -9 4 2 49.32 39.58 1.63 o -8 4 2 3.97 1.69 1.24 o -7 4 2 2.13 2.07 1.18 o -6 4 2 177.94 156.54 3.08 o -5 4 2 29.27 29.11 1.19 o -4 4 2 401.83 392.48 4.74 o -3 4 2 706.41 754.16 6.02 o -2 4 2 1773.74 1787.74 9.64 o -1 4 2 620.11 615.09 4.69 o 0 4 2 0.76 1.77 0.90 o 1 4 2 43.30 35.76 1.38 o 2 4 2 401.21 415.05 4.29 o 3 4 2 15.42 7.49 1.16 o 4 4 2 24.00 25.40 1.66 o 5 4 2 57.31 77.77 2.89 o 6 4 2 55.87 61.95 3.16 o 7 4 2 0.80 -0.09 1.61 o 8 4 2 24.76 30.23 2.51 o -10 5 2 73.39 63.64 1.65 o -9 5 2 27.83 20.95 1.40 o -8 5 2 248.00 222.73 3.52 o -7 5 2 33.31 32.17 1.77 o -6 5 2 34.79 38.27 1.76 o -5 5 2 240.17 240.52 3.07 o -4 5 2 112.92 113.38 2.78 o -3 5 2 80.70 106.59 2.48 o -2 5 2 1156.47 1273.13 8.26 o -1 5 2 0.30 1.29 0.94 o 0 5 2 1102.25 1041.80 7.03 o 1 5 2 184.96 198.83 3.01 o 2 5 2 783.14 806.49 6.71 o 3 5 2 272.75 294.78 4.40 o 4 5 2 3.62 4.22 1.41 o 5 5 2 300.91 313.10 5.50 o 6 5 2 451.13 501.90 7.53 o 7 5 2 7.90 5.69 2.14 o 8 5 2 2.90 2.31 1.52 o -10 6 2 17.61 15.29 0.87 o -9 6 2 137.24 113.50 3.97 o -8 6 2 0.76 0.39 1.05 o -7 6 2 162.79 151.31 2.96 o -6 6 2 387.21 372.73 7.64 o -5 6 2 10.43 12.05 1.04 o -4 6 2 193.59 160.74 3.39 o -3 6 2 268.66 272.34 4.04 o -2 6 2 410.23 413.59 4.75 o -1 6 2 1455.10 1481.08 9.50 o 0 6 2 485.56 548.59 5.30 o 1 6 2 1288.90 1283.23 9.00 o 2 6 2 68.46 57.14 2.08 o 3 6 2 454.87 488.23 5.94 o 4 6 2 349.09 345.15 5.56 o 5 6 2 838.20 918.59 10.04 o 6 6 2 21.61 21.21 2.38 o 7 6 2 31.40 36.98 2.50 o -9 7 2 74.65 63.02 1.70 o -8 7 2 37.67 30.00 1.73 o -7 7 2 28.26 22.36 1.57 o -6 7 2 26.76 23.76 2.08 o -5 7 2 0.09 -1.10 1.10 o -4 7 2 13.98 11.13 1.60 o -3 7 2 0.91 8.51 1.24 o -2 7 2 87.57 112.72 2.77 o -1 7 2 126.69 129.18 2.88 o 0 7 2 6.78 5.49 1.11 o 1 7 2 219.56 250.44 4.07 o 2 7 2 679.53 742.27 7.48 o 3 7 2 0.03 1.75 1.45 o 4 7 2 175.88 179.08 4.27 o 5 7 2 78.49 83.20 3.51 o 6 7 2 7.97 11.86 2.08 o -9 8 2 30.21 29.24 1.16 o -8 8 2 3.72 5.14 1.69 o -7 8 2 3.80 6.90 1.28 o -6 8 2 39.46 34.81 1.81 o -5 8 2 44.33 42.14 1.78 o -4 8 2 570.58 552.71 7.21 o -3 8 2 323.03 311.64 5.10 o -2 8 2 1.06 1.51 1.16 o -1 8 2 394.92 396.01 5.42 o 0 8 2 284.74 282.44 4.58 o 1 8 2 158.74 153.04 3.49 o 2 8 2 0.59 0.68 1.29 o 3 8 2 9.68 11.34 1.86 o 4 8 2 170.59 182.40 4.50 o 5 8 2 11.06 15.45 2.18 o 6 8 2 99.55 117.49 3.88 o 7 8 2 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