#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2012271.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012271_Fobs loop_ _publ_author_name 'Glidewell, Christopher' 'Low, John N.' 'McWilliam, Susan A.' 'Skakle, Janet M. S.' 'Wardell, James L.' _publ_section_title ; Hydrogen bonding in nitroaniline analogues: a three-dimensional framework in 2-amino-6-nitro-1,3-benzothiazole ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1209 _journal_page_last 1211 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.252 _cell_angle_gamma 90.000 _cell_length_a 3.7715 _cell_length_b 15.6399 _cell_length_c 13.3484 _exptl_crystal_F_000 400.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file gg1076Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' jl221' _shelx_refln_list_code 4 _shelx_f_calc_maximum 178.07 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, z+1/2' '-x, -y, -z' '-x-1/2, y-1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10.54 13.62 3.07 o 4 0 0 562.59 472.16 53.00 o 1 1 0 2530.33 2352.61 156.19 o 2 1 0 143.46 121.53 5.83 o 3 1 0 105.89 85.12 18.38 o 4 1 0 44.66 57.07 19.45 o 1 2 0 10208.54 10103.23 197.73 o 2 2 0 115.75 105.64 7.73 o 3 2 0 444.42 445.71 22.77 o 4 2 0 9.06 -2.91 16.64 o 1 3 0 401.60 377.19 13.84 o 2 3 0 254.59 256.48 9.32 o 3 3 0 0.25 -0.77 2.42 o 4 3 0 90.79 56.82 24.75 o 0 4 0 3546.69 3309.17 132.04 o 1 4 0 85.05 74.74 6.69 o 2 4 0 9.85 9.65 1.84 o 3 4 0 29.37 33.26 6.31 o 4 4 0 360.68 282.02 39.34 o 1 5 0 193.90 233.11 10.81 o 2 5 0 0.22 1.27 2.29 o 3 5 0 562.80 598.89 24.16 o 4 5 0 5.08 3.61 6.17 o 0 6 0 1008.26 987.28 39.64 o 1 6 0 1100.07 1187.83 34.43 o 2 6 0 24.35 24.12 3.20 o 3 6 0 26.23 26.60 3.70 o 4 6 0 406.85 419.26 48.89 o 1 7 0 30.89 45.26 4.19 o 2 7 0 0.87 1.21 2.84 o 3 7 0 274.72 286.74 10.70 o 4 7 0 168.93 146.39 20.22 o 0 8 0 910.66 989.51 45.98 o 1 8 0 1291.13 1349.95 41.59 o 2 8 0 54.49 59.46 5.32 o 3 8 0 230.74 243.24 10.96 o 4 8 0 4.77 -5.66 33.97 o 1 9 0 179.72 211.98 10.52 o 2 9 0 366.09 376.33 23.30 o 3 9 0 104.76 117.89 8.77 o 4 9 0 2.11 -30.46 30.46 o 0 10 0 361.88 330.57 19.96 o 1 10 0 0.13 -5.30 5.30 o 2 10 0 93.52 97.73 8.66 o 3 10 0 140.07 115.56 8.99 o 4 10 0 125.43 85.51 32.70 o 1 11 0 374.35 397.07 16.89 o 2 11 0 397.29 405.77 17.81 o 3 11 0 101.63 141.03 16.09 o 4 11 0 60.17 29.19 45.98 o 0 12 0 260.48 252.44 26.94 o 1 12 0 146.57 136.22 11.36 o 2 12 0 101.36 103.68 12.64 o 3 12 0 862.52 952.10 40.40 o 1 13 0 11.23 8.66 12.07 o 2 13 0 354.58 384.87 22.43 o 3 13 0 241.94 229.44 18.34 o 0 14 0 834.96 797.70 49.21 o 1 14 0 67.82 80.62 9.16 o 2 14 0 26.47 15.43 10.09 o 3 14 0 218.95 268.73 36.90 o 1 15 0 14.16 5.43 9.87 o 2 15 0 0.23 2.30 12.62 o 3 15 0 56.46 71.14 21.79 o 0 16 0 300.15 373.86 49.20 o 1 16 0 548.82 466.76 29.86 o 2 16 0 3.38 15.22 14.03 o 3 16 0 154.73 130.04 70.53 o 1 17 0 104.49 97.65 20.29 o 2 17 0 21.33 43.82 24.40 o 0 18 0 123.11 96.93 38.75 o 1 18 0 133.67 137.46 41.10 o 2 18 0 17.95 48.65 18.17 o 1 19 0 2.40 9.78 22.15 o 0 20 0 224.71 230.17 70.57 o -3 0 1 59.52 29.28 19.13 o -1 0 1 3892.18 3454.94 154.33 o 1 0 1 506.34 414.98 12.45 o 3 0 1 173.68 166.63 22.84 o -4 1 1 180.05 150.97 23.36 o -3 1 1 0.11 6.36 11.05 o -2 1 1 157.77 142.14 7.14 o -1 1 1 474.61 450.55 29.24 o 1 1 1 3849.85 3781.94 73.74 o 2 1 1 806.27 788.28 29.75 o 3 1 1 228.57 245.48 11.43 o 4 1 1 9.26 -0.07 22.61 o -4 2 1 46.93 22.47 18.39 o -3 2 1 124.71 97.81 15.91 o -2 2 1 82.28 91.29 12.64 o -1 2 1 394.69 374.52 75.94 o 0 2 1 188.81 201.45 5.70 o 1 2 1 5394.45 5315.78 128.33 o 2 2 1 81.54 80.02 3.83 o 3 2 1 6.66 0.55 4.65 o 4 2 1 99.09 110.75 25.37 o -4 3 1 17.89 20.73 17.75 o -3 3 1 154.37 146.67 6.41 o -2 3 1 611.93 621.64 29.55 o -1 3 1 18.53 21.28 1.88 o 0 3 1 1923.66 1991.09 46.29 o 1 3 1 4.99 13.48 1.90 o 2 3 1 395.45 427.24 14.47 o 3 3 1 74.48 70.28 7.75 o 4 3 1 0.32 -16.17 16.17 o -4 4 1 103.07 89.68 27.01 o -3 4 1 443.06 448.81 26.24 o -2 4 1 153.04 168.51 6.72 o -1 4 1 248.69 213.50 5.82 o 0 4 1 2195.02 2249.32 55.23 o 1 4 1 250.53 224.83 6.18 o 2 4 1 213.02 212.99 6.92 o 3 4 1 382.63 374.29 12.94 o 4 4 1 3.48 1.61 7.86 o -4 5 1 57.21 67.32 23.22 o -3 5 1 152.61 147.18 9.94 o -2 5 1 1404.43 1448.10 45.30 o -1 5 1 40.21 51.05 3.95 o 0 5 1 127.71 120.46 5.66 o 1 5 1 42.64 34.15 3.18 o 2 5 1 477.80 470.59 15.60 o 3 5 1 9.74 9.99 2.73 o 4 5 1 19.19 23.09 9.52 o -4 6 1 192.94 179.69 17.79 o -3 6 1 204.25 215.95 10.03 o -2 6 1 0.60 2.75 3.97 o -1 6 1 2086.37 2092.62 58.19 o 0 6 1 2004.03 2215.48 60.68 o 1 6 1 515.14 540.18 15.11 o 2 6 1 72.17 88.90 5.03 o 3 6 1 189.68 164.13 10.63 o 4 6 1 215.59 186.50 22.18 o -4 7 1 27.55 42.54 18.59 o -3 7 1 200.13 222.67 9.38 o -2 7 1 39.73 35.99 5.26 o -1 7 1 1171.33 1155.06 69.53 o 0 7 1 116.87 137.76 6.34 o 1 7 1 1937.94 2197.21 54.43 o 2 7 1 532.34 592.31 14.64 o 3 7 1 167.38 164.25 9.65 o 4 7 1 10.18 -23.82 23.82 o -4 8 1 268.53 258.97 34.79 o -3 8 1 69.87 68.05 7.22 o -2 8 1 48.66 52.46 6.01 o -1 8 1 0.37 -3.52 3.52 o 0 8 1 4965.72 5612.71 129.21 o 1 8 1 114.58 133.06 7.48 o 2 8 1 97.56 105.35 6.67 o 3 8 1 77.01 66.11 6.97 o 4 8 1 59.71 79.26 41.88 o -4 9 1 19.82 45.99 20.35 o -3 9 1 34.68 37.77 6.07 o -2 9 1 160.21 151.29 9.74 o -1 9 1 14.99 17.56 4.30 o 0 9 1 257.00 258.15 15.35 o 1 9 1 1830.17 2066.65 56.75 o 2 9 1 183.09 166.66 8.66 o 3 9 1 77.72 84.59 7.13 o 4 9 1 8.80 -5.66 32.80 o -4 10 1 71.16 71.35 24.89 o -3 10 1 184.08 193.13 11.45 o -2 10 1 63.78 76.52 8.56 o -1 10 1 145.76 160.59 11.12 o 0 10 1 238.90 264.01 12.78 o 1 10 1 682.63 714.30 22.50 o 2 10 1 98.18 83.05 7.49 o 3 10 1 128.08 110.71 9.78 o -4 11 1 151.50 115.66 26.31 o -3 11 1 130.11 128.61 10.76 o -2 11 1 393.35 391.25 17.47 o -1 11 1 59.59 54.94 6.97 o 0 11 1 79.22 98.37 9.73 o 1 11 1 11.13 12.74 7.34 o 2 11 1 281.71 299.08 14.48 o 3 11 1 47.90 37.46 7.70 o 4 11 1 0.07 26.94 50.56 o -3 12 1 0.02 2.63 8.17 o -2 12 1 117.81 104.52 10.99 o -1 12 1 414.04 405.05 17.07 o 0 12 1 462.59 460.89 19.81 o 1 12 1 1.14 6.12 7.79 o 2 12 1 1.46 0.75 6.31 o 3 12 1 333.37 344.69 21.64 o -3 13 1 540.79 583.12 33.18 o -2 13 1 460.81 450.65 30.25 o -1 13 1 497.82 468.89 23.92 o 0 13 1 70.48 64.49 8.71 o 1 13 1 33.87 38.77 10.26 o 2 13 1 173.29 148.72 10.30 o 3 13 1 159.35 199.01 24.43 o -3 14 1 19.80 18.76 22.74 o -2 14 1 331.89 350.24 27.32 o -1 14 1 0.04 -3.61 8.58 o 0 14 1 103.55 94.04 12.89 o 1 14 1 38.86 38.64 13.33 o 2 14 1 132.65 105.34 12.26 o 3 14 1 54.91 55.41 16.52 o -3 15 1 343.63 319.62 31.48 o -2 15 1 74.99 82.26 14.11 o -1 15 1 94.82 86.27 12.47 o 0 15 1 99.62 77.19 15.76 o 1 15 1 2.37 12.81 9.15 o 2 15 1 147.76 168.11 15.85 o 3 15 1 113.12 134.96 28.61 o -3 16 1 0.02 3.32 33.97 o -2 16 1 0.74 4.41 13.03 o -1 16 1 354.09 360.63 36.56 o 0 16 1 112.08 114.04 24.39 o 1 16 1 91.99 79.13 14.98 o 2 16 1 13.26 -0.93 12.46 o -2 17 1 137.85 155.55 30.75 o -1 17 1 148.32 107.16 19.42 o 0 17 1 33.19 7.52 24.79 o 1 17 1 155.51 188.91 29.33 o 2 17 1 112.12 127.76 23.83 o -2 18 1 9.19 -0.95 41.39 o -1 18 1 10.61 55.70 28.55 o 0 18 1 643.49 662.56 47.23 o 1 18 1 0.51 -19.54 25.67 o 2 18 1 1.05 -6.71 16.91 o -1 19 1 169.29 176.07 33.62 o 0 19 1 17.28 -15.98 52.57 o 1 19 1 157.06 116.36 46.02 o 0 20 1 17.19 24.60 29.45 o -4 0 2 141.62 125.14 33.29 o 0 0 2 1272.27 1123.31 26.00 o 2 0 2 875.72 950.68 23.37 o 4 0 2 50.89 29.97 27.62 o -4 1 2 107.80 102.67 23.72 o -3 1 2 329.73 259.16 36.70 o -2 1 2 2042.79 1907.93 263.41 o -1 1 2 332.52 319.77 27.01 o 0 1 2 2957.26 2663.80 45.43 o 1 1 2 31708.45 28007.88 590.92 o 2 1 2 3951.97 3823.98 56.98 o 3 1 2 250.10 255.61 17.37 o 4 1 2 9.35 -12.69 16.88 o -4 2 2 52.28 74.58 31.48 o -3 2 2 75.34 54.35 12.98 o -2 2 2 107.61 76.26 16.33 o -1 2 2 169.50 153.71 4.21 o 0 2 2 2322.03 2339.36 38.32 o 1 2 2 58.40 53.81 2.23 o 2 2 2 458.28 469.24 10.65 o 3 2 2 17.54 14.60 3.47 o 4 2 2 21.85 26.30 22.12 o -4 3 2 33.48 33.75 18.39 o -3 3 2 699.87 692.32 21.19 o -2 3 2 511.79 466.89 20.30 o -1 3 2 1660.22 1776.74 34.74 o 0 3 2 347.43 338.45 8.36 o 1 3 2 1077.67 987.12 19.10 o 2 3 2 1495.79 1394.02 37.86 o 3 3 2 19.74 17.99 2.97 o 4 3 2 6.70 4.60 8.59 o -4 4 2 51.20 55.61 19.66 o -3 4 2 3.71 3.71 2.78 o -2 4 2 283.28 297.63 18.98 o -1 4 2 704.96 726.40 18.49 o 0 4 2 31.26 33.55 2.87 o 1 4 2 46.62 48.31 3.35 o 2 4 2 20.30 19.55 3.45 o 3 4 2 0.79 -2.89 2.89 o 4 4 2 124.26 100.62 12.39 o -4 5 2 18.66 29.43 17.75 o -3 5 2 643.98 668.15 31.76 o -2 5 2 26.95 26.84 3.71 o -1 5 2 943.91 917.05 37.95 o 0 5 2 0.03 2.53 2.73 o 1 5 2 584.43 566.44 13.39 o 2 5 2 219.67 234.67 8.74 o 3 5 2 308.03 313.97 14.23 o 4 5 2 0.00 -5.33 10.92 o -4 6 2 114.18 112.81 11.13 o -3 6 2 50.57 49.80 4.90 o -2 6 2 626.93 686.45 23.65 o -1 6 2 13.65 19.47 3.04 o 0 6 2 55.03 76.11 5.39 o 1 6 2 2.92 0.37 3.39 o 2 6 2 598.70 648.51 19.59 o 3 6 2 40.04 46.93 4.92 o 4 6 2 243.35 194.35 43.24 o -4 7 2 21.37 12.81 12.08 o -3 7 2 306.99 328.49 12.38 o -2 7 2 1179.11 1239.92 34.39 o -1 7 2 14.36 12.23 3.74 o 0 7 2 304.86 376.23 12.20 o 1 7 2 2.88 2.12 3.91 o 2 7 2 1710.91 1775.78 40.95 o 3 7 2 92.98 86.40 7.80 o 4 7 2 0.01 -0.06 6.25 o -4 8 2 401.03 364.62 35.25 o -3 8 2 11.02 16.24 4.43 o -2 8 2 37.90 42.32 5.49 o -1 8 2 159.52 135.60 7.24 o 0 8 2 634.20 699.56 19.64 o 1 8 2 241.05 254.17 10.03 o 2 8 2 30.01 35.50 5.30 o 3 8 2 21.98 22.88 6.57 o 4 8 2 2.26 12.75 34.51 o -4 9 2 119.27 84.18 18.45 o -3 9 2 37.72 57.18 6.63 o -2 9 2 133.88 121.93 8.51 o -1 9 2 1078.77 1082.71 35.55 o 0 9 2 14.30 16.72 5.37 o 1 9 2 392.85 387.89 17.94 o 2 9 2 335.81 341.30 11.78 o 3 9 2 25.38 30.79 6.40 o 4 9 2 22.32 21.24 17.57 o -4 10 2 2.51 15.81 18.16 o -3 10 2 300.74 316.78 14.30 o -2 10 2 111.67 120.73 9.00 o -1 10 2 12.88 14.32 6.28 o 0 10 2 552.70 558.37 18.70 o 1 10 2 201.90 225.24 12.98 o 2 10 2 37.20 42.71 6.48 o 3 10 2 9.58 5.53 5.84 o 4 10 2 229.19 202.47 30.60 o -4 11 2 12.89 11.32 24.89 o -3 11 2 121.70 113.34 11.92 o -2 11 2 892.25 936.28 44.77 o -1 11 2 1140.10 1156.64 31.71 o 0 11 2 0.12 5.45 6.16 o 1 11 2 70.11 54.72 8.85 o 2 11 2 3.64 0.04 5.74 o 3 11 2 37.22 58.50 8.89 o 4 11 2 175.25 192.98 39.69 o -3 12 2 14.29 4.86 10.14 o -2 12 2 208.01 207.58 12.96 o -1 12 2 1593.54 1639.91 64.29 o 0 12 2 343.91 366.22 18.56 o 1 12 2 66.26 61.26 9.90 o 2 12 2 0.05 0.84 6.35 o 3 12 2 260.28 245.43 18.69 o -3 13 2 7.52 9.94 11.82 o -2 13 2 2165.38 2273.31 120.69 o -1 13 2 139.12 108.75 9.91 o 0 13 2 0.93 -4.44 7.68 o 1 13 2 0.01 6.85 8.31 o 2 13 2 359.63 351.85 19.18 o 3 13 2 25.56 26.19 13.40 o -3 14 2 27.26 50.06 17.91 o -2 14 2 175.48 181.70 21.40 o -1 14 2 8.18 11.56 6.80 o 0 14 2 7.85 4.26 9.38 o 1 14 2 78.34 75.58 11.39 o 2 14 2 29.04 20.33 12.13 o 3 14 2 0.83 -3.30 14.29 o -3 15 2 384.63 366.73 48.12 o -2 15 2 1.35 -1.94 12.95 o -1 15 2 187.65 199.65 22.74 o 0 15 2 214.85 158.64 16.82 o 1 15 2 652.27 732.36 39.05 o 2 15 2 63.71 62.56 13.32 o 3 15 2 112.04 122.35 40.27 o -2 16 2 0.17 -4.32 29.32 o -1 16 2 3.70 -5.36 8.57 o 0 16 2 40.34 39.21 18.19 o 1 16 2 2.39 14.95 12.98 o 2 16 2 4.90 -0.92 23.43 o -2 17 2 306.74 297.80 50.52 o -1 17 2 0.03 -19.43 19.43 o 0 17 2 53.64 63.49 29.63 o 1 17 2 28.87 29.95 39.68 o 2 17 2 421.48 441.18 41.63 o -2 18 2 14.84 61.84 55.74 o -1 18 2 111.42 111.15 31.42 o 0 18 2 42.78 50.92 23.11 o 1 18 2 80.15 91.05 19.03 o 2 18 2 11.85 -6.67 20.69 o -1 19 2 146.30 170.10 41.14 o 0 19 2 0.39 -18.69 19.40 o 1 19 2 69.57 37.55 34.34 o 0 20 2 126.51 157.27 51.20 o -3 0 3 1478.88 1193.52 74.77 o -1 0 3 6.79 2.32 2.44 o 1 0 3 2149.51 1992.88 42.10 o 3 0 3 61.97 69.75 7.58 o -4 1 3 7.43 2.15 20.31 o -3 1 3 39.95 36.80 20.11 o -2 1 3 1454.94 1532.34 49.03 o -1 1 3 44.36 34.01 1.75 o 0 1 3 1272.62 1208.28 18.39 o 1 1 3 12.35 7.08 1.75 o 2 1 3 2593.43 2559.50 39.13 o 3 1 3 104.51 98.29 5.05 o 4 1 3 0.31 6.32 8.74 o -4 2 3 176.54 144.04 24.59 o -3 2 3 94.01 91.76 20.11 o -2 2 3 81.91 89.81 8.37 o -1 2 3 38.56 41.83 2.14 o 0 2 3 364.68 346.36 6.84 o 1 2 3 321.03 311.80 5.72 o 2 2 3 2292.49 2380.94 39.67 o 3 2 3 512.26 531.05 16.20 o 4 2 3 102.93 107.18 10.49 o -4 3 3 2.55 21.27 17.35 o -3 3 3 428.65 453.66 16.67 o -2 3 3 104.98 103.88 4.34 o -1 3 3 3856.34 3897.53 77.51 o 0 3 3 332.48 328.41 7.04 o 1 3 3 1784.53 1715.61 33.56 o 2 3 3 459.50 492.13 12.04 o 3 3 3 907.51 933.74 32.83 o 4 3 3 2.62 -0.75 10.20 o -4 4 3 82.95 93.28 25.16 o -3 4 3 16.53 18.07 3.64 o -2 4 3 0.68 -1.14 2.50 o -1 4 3 1894.17 2064.51 40.33 o 0 4 3 286.19 311.25 8.09 o 1 4 3 37.22 32.36 3.42 o 2 4 3 4.56 4.26 2.74 o 3 4 3 177.91 163.71 7.34 o 4 4 3 63.12 53.62 12.10 o -4 5 3 116.42 98.79 34.07 o -3 5 3 3.31 6.86 4.97 o -2 5 3 3468.76 3795.96 90.36 o -1 5 3 0.12 0.76 2.14 o 0 5 3 355.44 384.13 9.21 o 1 5 3 0.23 -1.75 2.24 o 2 5 3 1360.77 1392.47 40.47 o 3 5 3 37.56 38.32 4.71 o 4 5 3 8.04 7.31 4.17 o -4 6 3 79.09 60.02 13.39 o -3 6 3 5.95 0.73 2.25 o -2 6 3 294.64 334.49 10.78 o -1 6 3 577.38 638.71 15.09 o 0 6 3 18.10 19.04 3.61 o 1 6 3 223.74 196.78 7.69 o 2 6 3 25.19 21.90 4.29 o 3 6 3 253.54 274.49 12.36 o 4 6 3 4.65 3.93 6.60 o -4 7 3 131.81 130.54 14.32 o -3 7 3 1023.49 1144.47 27.55 o -2 7 3 32.27 34.32 4.21 o -1 7 3 303.52 330.92 13.70 o 0 7 3 337.59 374.27 18.15 o 1 7 3 2976.32 3274.48 75.38 o 2 7 3 134.32 138.43 9.45 o 3 7 3 0.10 4.06 5.16 o 4 7 3 5.80 3.90 20.16 o -4 8 3 83.12 106.40 16.11 o -3 8 3 11.31 10.76 4.49 o -2 8 3 0.13 2.38 3.93 o -1 8 3 0.02 -3.88 5.01 o 0 8 3 350.53 385.00 14.59 o 1 8 3 589.41 641.50 19.00 o 2 8 3 456.39 471.40 22.82 o 3 8 3 5.70 5.27 5.25 o 4 8 3 88.97 95.88 16.40 o -4 9 3 59.46 57.01 18.25 o -3 9 3 30.07 24.94 4.85 o -2 9 3 870.46 960.89 33.43 o -1 9 3 152.42 125.56 8.56 o 0 9 3 16.84 16.86 7.42 o 1 9 3 836.87 947.25 24.92 o 2 9 3 397.37 384.71 12.59 o 3 9 3 58.76 59.44 7.99 o 4 9 3 25.72 49.49 38.26 o -4 10 3 2.51 15.91 20.50 o -3 10 3 194.03 203.26 10.89 o -2 10 3 22.17 15.44 7.35 o -1 10 3 45.37 48.98 6.26 o 0 10 3 174.88 202.01 12.55 o 1 10 3 103.58 94.81 9.38 o 2 10 3 153.14 147.32 8.42 o 3 10 3 87.14 83.38 7.64 o 4 10 3 21.30 20.64 13.20 o -4 11 3 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