#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:35:28 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180791 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/22/2012297.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012297_Fobs loop_ _publ_author_name 'Wang, Zheng' 'Nesterov, Vladimir N.' 'Borbulevych, Oleg Ya.' 'Clark, Ronald D.' 'Antipin, Mikhail Yu.' 'Timofeeva, Tatiana V.' _publ_section_title ; Indole- and carbazole-substituted pyridinium iodide salts: a rare case of conformational isomerism in crystals ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1343 _journal_page_last 1348 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.597 _cell_angle_gamma 90.000 _cell_length_a 7.3189 _cell_length_b 20.9597 _cell_length_c 10.0095 _exptl_crystal_F_000 712.00 _reflns_d_resolution_high 0.7804 _cod_data_source_file bm1458Ibsup3.hkl _cod_data_source_block Ib #BEGIN Tags that were not found in dictionaries: _shelx_title ' 2am in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 307.71 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 19138.26 19815.30 210.47 o 3 0 0 14689.44 16575.98 265.30 o 4 0 0 2524.64 2861.71 129.11 o 5 0 0 3514.99 4090.94 173.33 o 6 0 0 363.72 435.09 80.47 o 7 0 0 269.46 306.01 95.07 o 8 0 0 13.89 -13.81 47.58 o 9 0 0 0.53 -15.03 99.93 o 1 1 0 163.39 186.79 14.02 o 2 1 0 3132.50 3259.88 64.45 o 3 1 0 929.51 937.51 46.07 o 4 1 0 663.05 624.00 47.21 o 5 1 0 1494.09 1709.17 81.18 o 6 1 0 68.96 70.61 31.20 o 7 1 0 296.82 292.82 46.89 o 8 1 0 28.32 14.39 40.66 o 9 1 0 38.91 -21.07 60.85 o 0 2 0 1061.85 983.93 36.70 o 1 2 0 354.22 334.70 14.91 o 2 2 0 386.02 384.60 22.89 o 3 2 0 4.96 -0.21 15.55 o 4 2 0 28.31 29.52 21.39 o 5 2 0 20.42 15.80 22.96 o 6 2 0 0.11 -5.35 24.44 o 7 2 0 12.66 11.39 30.88 o 8 2 0 0.93 -22.50 43.91 o 9 2 0 0.01 -1.00 65.16 o 1 3 0 1288.13 1315.74 34.36 o 2 3 0 33.71 21.75 12.95 o 3 3 0 837.43 871.88 36.60 o 4 3 0 907.39 994.76 46.89 o 5 3 0 1963.17 2182.82 74.44 o 6 3 0 306.87 382.56 47.40 o 7 3 0 234.22 265.98 46.22 o 8 3 0 13.03 15.22 49.39 o 9 3 0 14.71 29.92 50.64 o 2 4 0 26075.38 28619.62 185.50 o 3 4 0 12340.43 13966.72 138.09 o 4 4 0 3810.05 4263.48 88.63 o 5 4 0 2424.17 2400.40 76.23 o 6 4 0 700.17 810.30 55.75 o 7 4 0 129.35 104.93 52.62 o 8 4 0 28.44 46.09 53.11 o 9 4 0 12.41 48.11 49.24 o 1 5 0 2468.47 2605.80 53.64 o 2 5 0 64.63 50.85 22.51 o 3 5 0 2256.55 2345.17 54.52 o 4 5 0 1288.33 1292.99 50.83 o 5 5 0 566.25 639.72 46.24 o 6 5 0 574.51 716.78 59.33 o 7 5 0 98.26 96.62 49.21 o 8 5 0 86.31 140.20 59.40 o 0 6 0 1239.27 1075.43 41.65 o 1 6 0 407.97 428.49 27.89 o 2 6 0 48.10 18.46 19.51 o 3 6 0 441.80 448.15 27.40 o 4 6 0 77.51 54.14 20.39 o 5 6 0 81.12 83.09 26.90 o 6 6 0 34.89 30.08 37.90 o 7 6 0 0.80 -7.44 37.52 o 8 6 0 0.11 -27.38 45.58 o 1 7 0 565.39 520.00 31.06 o 2 7 0 714.43 729.21 38.61 o 3 7 0 909.07 854.21 53.88 o 4 7 0 2221.49 2474.82 63.18 o 5 7 0 595.29 694.28 47.93 o 6 7 0 493.77 629.04 88.43 o 7 7 0 149.33 162.72 52.53 o 8 7 0 1.67 -9.79 46.26 o 0 8 0 19493.88 21358.17 205.54 o 1 8 0 10448.42 10874.05 100.14 o 2 8 0 12573.40 13733.17 225.19 o 3 8 0 5714.48 5902.05 132.30 o 4 8 0 3922.61 3980.36 128.67 o 5 8 0 1633.79 1802.14 93.13 o 6 8 0 83.75 81.80 43.92 o 7 8 0 201.59 201.37 58.97 o 8 8 0 20.75 10.78 50.27 o 1 9 0 14.77 31.55 14.01 o 2 9 0 11.66 -6.37 18.02 o 3 9 0 328.18 261.88 71.63 o 4 9 0 1362.42 1262.32 72.65 o 5 9 0 119.59 119.92 42.51 o 6 9 0 538.02 484.54 70.38 o 7 9 0 72.21 109.23 51.09 o 8 9 0 8.65 -22.22 48.44 o 0 10 0 76.86 80.34 38.03 o 1 10 0 1104.86 953.86 47.26 o 2 10 0 620.25 555.99 41.30 o 3 10 0 171.09 140.84 35.63 o 4 10 0 34.07 10.49 28.95 o 5 10 0 101.20 105.85 42.66 o 6 10 0 4.74 13.84 36.20 o 7 10 0 14.32 40.84 45.70 o 8 10 0 11.80 -6.39 48.10 o 1 11 0 135.62 143.07 21.61 o 2 11 0 939.17 922.00 51.79 o 3 11 0 471.45 519.55 63.67 o 4 11 0 184.36 193.16 44.08 o 5 11 0 168.54 133.07 45.58 o 6 11 0 1.72 12.03 37.11 o 7 11 0 156.60 176.87 87.55 o 8 11 0 0.08 12.97 55.24 o 0 12 0 12216.26 13132.96 228.16 o 1 12 0 6659.95 6545.47 116.01 o 2 12 0 6753.07 7173.05 131.83 o 3 12 0 1471.67 1753.78 88.37 o 4 12 0 1024.99 1098.04 75.21 o 5 12 0 495.51 475.02 65.03 o 6 12 0 140.42 122.84 48.31 o 7 12 0 143.54 156.07 53.54 o 8 12 0 5.31 12.90 48.10 o 1 13 0 100.68 64.79 19.56 o 2 13 0 4.12 8.05 22.05 o 3 13 0 234.86 235.36 50.85 o 4 13 0 274.08 213.87 72.96 o 5 13 0 234.55 209.88 51.18 o 6 13 0 106.55 86.84 47.81 o 7 13 0 9.05 9.49 45.96 o 0 14 0 559.20 578.55 122.92 o 1 14 0 211.64 260.97 29.52 o 2 14 0 0.46 2.51 23.56 o 3 14 0 103.59 156.03 43.65 o 4 14 0 0.54 -0.48 32.79 o 5 14 0 75.18 90.44 45.33 o 6 14 0 22.67 6.90 39.53 o 7 14 0 33.29 18.37 47.79 o 1 15 0 28.64 20.37 19.10 o 2 15 0 8.78 -3.38 23.16 o 3 15 0 1.94 13.12 33.31 o 4 15 0 40.76 18.64 35.05 o 5 15 0 37.40 13.34 36.25 o 6 15 0 16.22 31.20 41.39 o 7 15 0 2.39 -23.21 42.07 o 0 16 0 4070.22 4329.88 128.76 o 1 16 0 4165.18 4486.63 92.15 o 2 16 0 1327.60 1294.05 68.30 o 3 16 0 1404.30 1327.82 73.09 o 4 16 0 227.38 266.07 58.74 o 5 16 0 304.21 374.30 65.97 o 6 16 0 107.79 70.69 46.10 o 7 16 0 35.04 64.97 54.15 o 1 17 0 58.48 53.68 23.83 o 2 17 0 378.15 352.22 48.25 o 3 17 0 58.99 55.88 32.05 o 4 17 0 213.03 120.75 51.29 o 5 17 0 135.57 110.23 50.82 o 6 17 0 29.80 4.41 44.28 o 7 17 0 8.35 -7.13 49.84 o 0 18 0 335.63 433.07 100.37 o 1 18 0 2.37 -11.96 29.39 o 2 18 0 61.09 91.11 36.09 o 3 18 0 90.15 92.98 36.68 o 4 18 0 0.19 -24.03 38.39 o 5 18 0 84.27 110.76 55.02 o 6 18 0 13.62 32.85 45.44 o 1 19 0 47.72 70.46 36.67 o 2 19 0 14.40 20.28 31.77 o 3 19 0 0.32 11.86 32.97 o 4 19 0 122.27 69.86 46.90 o 5 19 0 6.35 -2.64 41.85 o 6 19 0 30.66 7.28 51.17 o 0 20 0 1731.35 1766.98 97.62 o 1 20 0 874.01 1024.68 99.78 o 2 20 0 921.46 963.91 71.29 o 3 20 0 549.64 714.13 72.24 o 4 20 0 203.54 141.72 56.92 o 5 20 0 155.64 164.48 60.62 o 6 20 0 31.74 -9.97 45.96 o 1 21 0 0.56 -5.40 34.45 o 2 21 0 34.40 -3.47 36.31 o 3 21 0 0.52 1.33 35.53 o 4 21 0 54.66 50.79 49.91 o 5 21 0 22.61 -25.78 50.55 o 0 22 0 66.13 96.39 89.32 o 1 22 0 86.39 186.85 49.82 o 2 22 0 109.73 104.87 44.04 o 3 22 0 92.87 63.95 42.91 o 4 22 0 38.60 60.11 51.59 o 5 22 0 19.77 29.95 56.53 o 1 23 0 18.53 30.16 55.34 o 2 23 0 34.26 -1.68 42.84 o 3 23 0 35.12 29.47 43.20 o 4 23 0 14.91 -1.59 53.51 o 0 24 0 592.61 626.11 152.11 o 1 24 0 676.57 960.33 123.50 o 2 24 0 410.65 514.38 75.24 o 3 24 0 244.62 212.83 63.53 o 4 24 0 104.30 81.11 62.17 o 1 25 0 2.52 -66.33 87.55 o 2 25 0 1.42 -49.52 94.62 o 3 25 0 7.75 39.80 84.90 o -9 1 1 0.32 10.14 56.38 o -8 1 1 77.22 64.18 39.72 o -7 1 1 6.02 24.63 38.45 o -6 1 1 691.83 711.01 86.66 o -5 1 1 793.94 711.35 57.92 o -4 1 1 1948.19 2043.62 74.10 o -3 1 1 7657.62 7555.63 343.12 o -2 1 1 7904.65 7682.87 112.15 o -1 1 1 3332.43 3914.07 105.89 o 0 1 1 7.45 10.90 3.84 o 2 1 1 942.45 897.25 33.31 o 3 1 1 329.64 286.83 29.62 o 4 1 1 111.66 72.07 24.06 o 5 1 1 12.29 -16.89 22.92 o 6 1 1 129.91 149.56 38.35 o 7 1 1 0.14 23.50 32.54 o 8 1 1 47.17 51.12 45.06 o -9 2 1 0.06 -10.18 46.44 o -8 2 1 1.24 -42.03 42.03 o -7 2 1 5.29 -8.86 30.29 o -6 2 1 180.26 153.45 40.93 o -5 2 1 335.08 366.32 44.70 o -4 2 1 1376.48 1280.62 65.00 o -3 2 1 5448.17 5627.56 235.23 o -2 2 1 2397.19 2541.58 93.74 o -1 2 1 22401.23 24489.11 176.33 o 0 2 1 120.31 100.40 12.71 o 2 2 1 24621.99 26982.14 496.04 o 3 2 1 8146.23 9166.80 236.63 o 4 2 1 7271.35 7851.67 173.76 o 5 2 1 1236.25 1387.07 64.42 o 6 2 1 762.80 899.03 64.28 o 7 2 1 284.15 338.47 46.60 o 8 2 1 128.55 219.49 58.23 o -9 3 1 6.13 -11.48 50.62 o -8 3 1 61.71 88.83 53.80 o -7 3 1 25.37 18.58 31.75 o -6 3 1 700.72 851.22 59.26 o -5 3 1 369.93 389.30 50.70 o -4 3 1 2335.99 2351.98 78.05 o -3 3 1 3761.91 4156.05 88.16 o -2 3 1 119.93 132.87 19.64 o -1 3 1 6576.81 7269.89 127.45 o 0 3 1 3345.84 3734.99 147.94 o 1 3 1 2488.25 2215.37 69.59 o 2 3 1 405.92 365.50 24.55 o 3 3 1 527.69 511.14 31.62 o 4 3 1 1.44 2.82 19.13 o 5 3 1 0.47 4.55 23.67 o 6 3 1 42.87 38.06 30.40 o 7 3 1 21.43 -17.59 41.43 o 8 3 1 17.11 -3.51 41.40 o -9 4 1 0.97 -4.97 56.28 o -8 4 1 0.09 -30.45 41.58 o -7 4 1 0.39 -29.52 29.52 o -6 4 1 2.44 -16.22 26.13 o -5 4 1 13.18 5.49 21.21 o -4 4 1 41.00 32.58 18.79 o -3 4 1 33.04 40.84 18.48 o -2 4 1 221.52 203.70 21.41 o 0 4 1 20.27 23.42 10.53 o 1 4 1 3.31 28.87 18.48 o 2 4 1 490.07 404.16 23.34 o 3 4 1 38.38 41.11 17.79 o 4 4 1 413.21 376.01 35.45 o 5 4 1 2.28 -6.80 22.28 o 6 4 1 14.00 -8.91 27.79 o 7 4 1 1.83 9.84 42.40 o 8 4 1 1.20 20.37 43.34 o -9 5 1 5.83 12.08 52.62 o -8 5 1 35.58 19.98 48.42 o -7 5 1 8.26 10.43 39.16 o -6 5 1 65.70 72.27 30.82 o -5 5 1 347.24 331.04 37.72 o -4 5 1 2332.40 2396.84 64.66 o -3 5 1 5039.76 5440.02 242.51 o -2 5 1 4885.57 5328.77 119.80 o -1 5 1 3636.38 3672.75 93.15 o 0 5 1 4806.79 5290.73 80.93 o 1 5 1 92.79 72.44 21.65 o 2 5 1 303.94 323.13 36.58 o 3 5 1 1011.28 920.17 37.82 o 4 5 1 179.15 137.88 26.39 o 5 5 1 36.26 36.11 25.39 o 6 5 1 68.95 62.83 42.83 o 7 5 1 24.27 14.15 42.52 o 8 5 1 31.71 -1.93 47.51 o -9 6 1 1.38 6.78 53.40 o -8 6 1 2.68 -24.27 40.04 o -7 6 1 0.61 11.75 39.16 o -6 6 1 174.42 139.69 35.25 o -5 6 1 150.22 138.48 28.74 o -4 6 1 1562.32 1479.58 49.79 o -3 6 1 2865.78 2654.24 67.41 o -2 6 1 12150.09 12944.22 180.42 o 0 6 1 34176.46 38554.83 196.04 o 1 6 1 17926.95 20080.22 500.55 o 2 6 1 15901.31 17557.78 230.37 o 3 6 1 6108.48 6592.15 195.00 o 4 6 1 3721.81 4188.59 136.41 o 5 6 1 1380.78 1473.68 63.49 o 6 6 1 502.89 547.26 72.50 o 7 6 1 371.24 379.35 77.82 o 8 6 1 3.70 -14.64 50.27 o -8 7 1 2.82 -34.22 39.62 o -7 7 1 194.89 215.60 54.07 o -6 7 1 92.43 64.11 37.46 o -5 7 1 1110.88 1131.30 51.76 o -4 7 1 1530.14 1541.58 49.95 o -3 7 1 1185.51 1071.07 42.90 o -2 7 1 9811.84 10192.61 103.48 o -1 7 1 2415.39 2347.91 55.01 o 0 7 1 174.38 191.02 18.45 o 1 7 1 1837.79 1688.02 51.66 o 2 7 1 1025.09 902.82 51.17 o 3 7 1 80.50 95.43 32.20 o 4 7 1 337.35 352.11 34.59 o 5 7 1 100.02 76.86 41.50 o 6 7 1 6.15 14.67 39.34 o 7 7 1 2.68 -6.24 44.81 o 8 7 1 51.18 80.48 58.11 o -8 8 1 86.11 59.22 52.61 o -7 8 1 2.20 -6.43 36.01 o -6 8 1 53.05 17.38 34.68 o -5 8 1 0.78 2.70 21.48 o -4 8 1 63.80 39.73 18.88 o -3 8 1 48.36 39.48 17.49 o -2 8 1 6.43 -5.25 13.23 o -1 8 1 285.39 323.61 25.19 o 0 8 1 395.38 325.35 22.20 o 1 8 1 59.96 50.02 19.65 o 2 8 1 79.59 82.28 28.95 o 3 8 1 2.93 -2.89 24.65 o 4 8 1 72.07 45.02 35.33 o 5 8 1 4.14 3.38 33.75 o 6 8 1 116.87 78.93 44.91 o 7 8 1 11.62 8.81 44.38 o 8 8 1 0.92 -18.05 51.72 o -8 9 1 43.85 37.58 50.65 o -7 9 1 45.80 47.15 44.71 o -6 9 1 193.45 202.53 51.52 o -5 9 1 904.35 923.89 68.17 o -4 9 1 309.32 278.38 27.45 o -3 9 1 1786.30 1782.82 71.97 o -2 9 1 1655.36 1565.44 50.16 o -1 9 1 3209.16 3530.25 62.75 o 0 9 1 1497.45 1722.51 50.80 o 1 9 1 2573.23 2485.04 66.95 o 2 9 1 1383.97 1403.53 68.84 o 3 9 1 4.29 11.56 24.36 o 4 9 1 0.13 3.12 28.74 o 5 9 1 26.63 50.41 38.27 o 6 9 1 87.90 64.08 44.31 o 7 9 1 0.29 26.09 47.51 o 8 9 1 70.11 81.36 61.93 o -8 10 1 26.92 16.74 47.71 o -7 10 1 4.06 -32.94 38.01 o -6 10 1 198.09 158.19 45.31 o -5 10 1 634.22 672.00 69.47 o -4 10 1 561.19 582.84 61.19 o -3 10 1 6787.31 7781.26 186.97 o -2 10 1 4536.78 4667.00 79.72 o 1 10 1 22306.87 24570.41 324.74 o 2 10 1 6129.78 6330.67 187.48 o 3 10 1 7811.36 8881.69 291.83 o 4 10 1 3329.19 3661.56 130.47 o 5 10 1 652.75 829.35 107.00 o 6 10 1 882.91 966.14 113.19 o 7 10 1 10.20 -9.73 43.15 o 8 10 1 32.72 26.13 56.19 o -8 11 1 46.65 40.21 47.13 o -7 11 1 113.25 79.18 44.95 o -6 11 1 128.78 129.47 46.59 o -5 11 1 890.46 844.53 77.82 o -4 11 1 1893.73 1948.49 91.64 o -3 11 1 2833.59 2749.28 217.01 o -2 11 1 2933.80 3163.48 68.82 o -1 11 1 2635.53 2771.07 61.48 o 1 11 1 726.93 744.06 30.90 o 2 11 1 49.85 38.06 23.41 o 3 11 1 0.64 -6.13 27.95 o 4 11 1 135.18 97.72 41.90 o 5 11 1 148.83 96.15 45.33 o 6 11 1 42.31 47.31 42.52 o 7 11 1 27.68 45.45 48.73 o 8 11 1 44.88 11.82 54.98 o -8 12 1 4.10 1.65 50.88 o -7 12 1 5.78 2.55 40.80 o -6 12 1 93.60 95.11 43.82 o -5 12 1 6.82 -6.70 30.91 o -4 12 1 284.56 250.09 47.33 o -3 12 1 1.32 3.99 23.50 o -2 12 1 47.07 31.22 19.66 o -1 12 1 44.99 15.11 16.33 o 0 12 1 143.23 134.82 28.11 o 1 12 1 9.10 -2.25 13.93 o 2 12 1 423.57 333.58 61.90 o 3 12 1 44.85 24.98 31.54 o 4 12 1 22.23 29.62 35.76 o 5 12 1 0.17 5.60 35.91 o 6 12 1 4.21 17.69 43.15 o 7 12 1 6.15 -6.00 42.81 o -8 13 1 54.21 72.57 51.02 o -7 13 1 59.48 103.64 44.30 o -6 13 1 359.50 402.17 64.37 o -5 13 1 488.01 558.01 67.57 o -4 13 1 1264.49 1338.50 80.08 o -3 13 1 936.63 914.93 56.59 o -2 13 1 1130.31 1063.66 45.45 o -1 13 1 973.41 972.61 41.49 o 0 13 1 812.65 762.04 37.93 o 1 13 1 240.82 205.75 24.75 o 2 13 1 2.06 3.17 22.74 o 3 13 1 17.57 28.76 31.98 o 4 13 1 220.42 171.38 47.76 o 5 13 1 21.04 6.95 35.38 o 6 13 1 222.83 188.24 55.77 o 7 13 1 2.97 -11.10 50.01 o -7 14 1 3.87 -24.96 40.80 o -6 14 1 76.26 86.97 42.06 o -5 14 1 428.46 396.53 60.13 o -4 14 1 1532.77 1568.61 87.58 o -3 14 1 1409.05 1287.83 66.41 o -2 14 1 3195.91 3396.51 79.86 o -1 14 1 4609.52 5050.46 92.55 o 0 14 1 6076.34 6485.91 134.72 o 1 14 1 6532.92 6803.57 130.85 o 2 14 1 8577.61 8391.60 268.02 o 3 14 1 3776.37 3813.34 134.79 o 4 14 1 2276.96 2516.20 119.35 o 5 14 1 490.28 444.11 69.63 o 6 14 1 150.52 108.22 50.14 o 7 14 1 85.79 171.52 58.84 o -7 15 1 47.75 77.47 49.05 o -6 15 1 238.65 172.35 52.90 o -5 15 1 340.04 360.85 62.70 o -4 15 1 815.56 843.31 69.11 o -3 15 1 1681.40 1507.61 74.01 o -2 15 1 1163.92 1141.17 51.73 o -1 15 1 1113.46 1117.85 48.45 o 0 15 1 731.10 738.55 41.10 o 1 15 1 225.36 206.83 28.41 o 2 15 1 335.85 285.69 42.49 o 3 15 1 80.66 74.54 38.71 o 4 15 1 9.75 17.24 36.27 o 5 15 1 22.58 36.33 43.09 o 6 15 1 42.15 -16.64 40.24 o 7 15 1 85.38 57.50 52.81 o -7 16 1 0.29 -1.80 44.76 o -6 16 1 13.12 6.69 39.79 o -5 16 1 20.40 27.81 41.55 o -4 16 1 193.71 221.74 52.70 o -3 16 1 362.78 369.16 51.81 o -2 16 1 84.98 71.42 30.49 o -1 16 1 289.30 298.90 35.98 o 0 16 1 177.02 150.99 27.38 o 1 16 1 244.99 227.08 30.63 o 2 16 1 568.46 623.53 61.37 o 3 16 1 1.13 -8.50 31.00 o 4 16 1 95.87 79.34 45.33 o 5 16 1 0.95 4.73 40.67 o 6 16 1 1.69 4.49 48.10 o 7 16 1 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