#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2012299.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012299_Fobs loop_ _publ_author_name 'Wang, Zheng' 'Nesterov, Vladimir N.' 'Borbulevych, Oleg Ya.' 'Clark, Ronald D.' 'Antipin, Mikhail Yu.' 'Timofeeva, Tatiana V.' _publ_section_title ; Indole- and carbazole-substituted pyridinium iodide salts: a rare case of conformational isomerism in crystals ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1343 _journal_page_last 1348 _journal_volume 57 _journal_year 2001 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 82.272 _cell_angle_beta 87.363 _cell_angle_gamma 87.417 _cell_length_a 7.5536 _cell_length_b 16.0464 _cell_length_c 16.2948 _exptl_crystal_F_000 880.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file bm1458IIIsup5.hkl _[local]_cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' vlad in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 308.24 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 5123.89 6052.46 78.83 o 2 0 0 2956.59 3327.83 77.95 o 3 0 0 16816.00 19261.49 241.37 o 4 0 0 8003.02 8283.27 175.38 o 5 0 0 896.94 816.68 66.88 o 6 0 0 800.01 758.22 73.52 o 7 0 0 1504.33 1627.84 135.08 o 8 0 0 130.16 157.72 40.13 o -9 1 0 92.81 103.19 54.03 o -8 1 0 52.45 89.02 50.93 o -7 1 0 942.12 849.20 57.36 o -6 1 0 236.38 157.14 33.16 o -5 1 0 738.53 697.91 43.37 o -4 1 0 424.71 386.20 45.62 o -3 1 0 186.13 127.99 29.23 o -2 1 0 17864.07 21144.19 223.66 o -1 1 0 1624.40 1650.34 27.61 o 1 1 0 20.82 21.07 9.65 o 2 1 0 20675.02 23648.26 225.43 o 3 1 0 928.53 878.68 50.93 o 4 1 0 51.62 36.76 31.00 o 5 1 0 57.07 52.70 34.54 o 6 1 0 454.10 428.27 57.13 o 7 1 0 1110.35 1026.45 58.36 o 8 1 0 68.54 56.93 42.52 o 9 1 0 232.63 163.94 45.46 o -9 2 0 845.05 815.35 92.12 o -8 2 0 818.67 787.01 81.93 o -7 2 0 826.15 769.29 73.08 o -6 2 0 349.73 345.02 39.77 o -5 2 0 6815.90 7011.92 125.04 o -4 2 0 7391.49 7677.92 187.56 o -3 2 0 1807.74 1640.02 48.55 o -2 2 0 2290.10 2455.35 62.00 o -1 2 0 9151.83 10390.49 186.23 o 0 2 0 8500.68 7855.44 334.16 o 1 2 0 1037.88 1146.85 19.36 o 2 2 0 17597.33 19769.25 146.61 o 3 2 0 10989.30 11208.08 170.95 o 4 2 0 2364.39 2039.93 85.92 o 5 2 0 1432.23 1488.95 58.30 o 6 2 0 1613.84 1774.42 82.60 o 7 2 0 1686.23 1638.69 87.47 o 8 2 0 471.35 377.77 38.16 o 9 2 0 309.95 322.43 56.47 o -9 3 0 285.86 255.54 65.55 o -8 3 0 562.29 484.52 71.30 o -7 3 0 921.65 851.66 77.95 o -6 3 0 591.67 573.02 44.10 o -5 3 0 1270.25 1169.26 52.58 o -4 3 0 902.85 820.88 41.81 o -3 3 0 3625.43 3325.74 65.31 o -2 3 0 5474.66 5794.62 85.48 o -1 3 0 7945.80 7900.17 120.02 o 1 3 0 63.95 42.64 10.48 o 2 3 0 2056.41 2044.60 32.76 o 3 3 0 226.48 185.51 23.77 o 4 3 0 2490.24 2362.18 127.11 o 5 3 0 3467.12 3556.40 87.69 o 6 3 0 1138.96 1097.85 56.99 o 7 3 0 153.45 110.10 32.04 o 8 3 0 205.00 159.44 38.65 o 9 3 0 290.11 322.24 51.62 o -9 4 0 109.98 116.04 58.90 o -8 4 0 34.44 43.85 44.73 o -7 4 0 326.83 253.77 55.80 o -6 4 0 1934.01 2113.14 78.42 o -5 4 0 2164.57 2101.69 69.53 o -4 4 0 47.89 34.66 24.33 o -3 4 0 4137.11 4301.39 74.04 o -2 4 0 8490.85 9048.79 290.53 o -1 4 0 16442.28 15152.41 186.90 o 1 4 0 4673.66 4855.14 73.75 o 2 4 0 15599.00 17537.58 255.18 o 3 4 0 2627.96 2544.10 69.90 o 4 4 0 1269.40 1260.26 37.38 o 5 4 0 3843.38 3839.33 106.96 o 6 4 0 891.92 818.35 39.34 o 7 4 0 2.33 -3.15 28.59 o 8 4 0 911.08 855.78 62.44 o 9 4 0 272.05 311.30 50.56 o -9 5 0 72.81 39.42 54.92 o -8 5 0 524.16 413.65 68.20 o -7 5 0 392.77 430.93 69.09 o -6 5 0 180.44 142.33 49.38 o -5 5 0 18.68 2.88 25.68 o -4 5 0 2245.80 2178.50 61.93 o -3 5 0 7781.84 8060.40 240.04 o -2 5 0 128.45 96.06 22.81 o -1 5 0 10165.22 9848.87 162.98 o 0 5 0 21436.41 23787.13 139.53 o 1 5 0 494.87 435.59 19.07 o 2 5 0 1501.10 1630.81 30.07 o 3 5 0 4597.89 4789.52 125.20 o 4 5 0 2034.06 1926.52 71.71 o 5 5 0 520.63 475.04 29.84 o 6 5 0 711.13 625.27 47.89 o 7 5 0 720.39 708.42 54.02 o 8 5 0 481.37 493.92 53.97 o 9 5 0 54.54 52.70 59.79 o -9 6 0 7.22 2.21 55.36 o -8 6 0 54.43 12.40 48.27 o -7 6 0 1179.38 1127.58 97.88 o -6 6 0 698.91 549.18 68.20 o -5 6 0 427.74 378.24 36.07 o -4 6 0 3.90 24.68 23.77 o -3 6 0 2668.40 2585.06 57.67 o -2 6 0 7635.79 8051.64 170.07 o -1 6 0 3669.71 3850.88 108.06 o 0 6 0 2504.48 2387.32 44.38 o 1 6 0 2551.34 2369.98 40.32 o 2 6 0 3096.80 3104.86 43.97 o 3 6 0 441.73 363.44 30.10 o 4 6 0 501.57 478.10 25.86 o 5 6 0 414.48 397.65 28.11 o 6 6 0 484.84 413.36 43.50 o 7 6 0 486.02 398.18 45.61 o 8 6 0 100.58 115.37 38.82 o -9 7 0 92.31 91.23 59.35 o -8 7 0 548.75 550.51 84.59 o -7 7 0 798.35 732.97 86.81 o -6 7 0 9.22 -18.60 42.96 o -5 7 0 2757.90 3033.76 140.84 o -4 7 0 4097.10 4279.32 82.89 o -3 7 0 1519.54 1369.84 81.93 o -2 7 0 1149.86 1019.08 69.98 o -1 7 0 15392.79 15711.33 243.14 o 0 7 0 9075.14 9389.57 186.85 o 1 7 0 295.89 372.30 21.13 o 2 7 0 8818.87 8910.06 153.89 o 3 7 0 11455.00 12668.79 310.58 o 4 7 0 2681.10 2746.89 77.32 o 5 7 0 377.87 357.49 39.28 o 6 7 0 1201.57 1169.52 63.05 o 7 7 0 1266.10 1339.27 72.90 o 8 7 0 103.57 105.18 40.55 o 9 7 0 168.41 188.23 69.09 o -8 8 0 441.72 458.83 79.28 o -7 8 0 247.98 248.90 62.00 o -6 8 0 165.75 153.24 52.70 o -5 8 0 1196.53 1097.47 90.35 o -4 8 0 861.32 850.78 77.50 o -3 8 0 2.65 -9.30 33.22 o -2 8 0 87.16 40.75 33.66 o -1 8 0 1275.04 1354.78 77.50 o 0 8 0 1341.82 1136.33 37.19 o 1 8 0 435.37 407.73 23.47 o 2 8 0 177.95 140.17 16.94 o 3 8 0 640.67 608.39 24.59 o 4 8 0 825.63 754.13 48.66 o 5 8 0 17.48 22.75 28.51 o 6 8 0 703.68 629.04 52.20 o 7 8 0 231.19 235.14 43.41 o 8 8 0 10.36 1.28 37.20 o 9 8 0 108.75 124.45 65.99 o -8 9 0 276.67 341.02 75.73 o -7 9 0 101.46 91.68 57.13 o -6 9 0 1075.38 1072.67 101.42 o -5 9 0 2868.00 2965.11 144.38 o -4 9 0 771.74 736.07 76.62 o -3 9 0 1001.58 906.58 76.62 o -2 9 0 13397.85 13794.52 262.19 o -1 9 0 6872.21 6870.02 179.37 o 0 9 0 869.36 808.14 34.92 o 1 9 0 8089.51 7906.19 91.40 o 2 9 0 13812.67 14069.92 319.03 o 3 9 0 2648.87 2714.06 45.44 o 4 9 0 128.29 123.99 37.65 o 5 9 0 3438.00 3730.22 107.39 o 6 9 0 2082.36 2344.29 90.55 o 7 9 0 54.25 61.16 36.89 o 8 9 0 243.63 201.96 68.65 o -8 10 0 9.08 -15.94 56.25 o -7 10 0 53.68 54.03 53.15 o -6 10 0 360.98 385.75 72.63 o -5 10 0 297.10 289.65 60.68 o -4 10 0 107.98 89.91 50.05 o -3 10 0 334.53 263.96 52.70 o -2 10 0 239.24 216.57 47.39 o -1 10 0 564.52 532.35 58.46 o 0 10 0 97.59 111.31 30.11 o 1 10 0 0.03 0.06 17.77 o 2 10 0 238.13 181.34 35.03 o 3 10 0 0.57 -5.06 26.53 o 4 10 0 148.37 104.16 33.72 o 5 10 0 32.47 47.56 33.20 o 6 10 0 74.77 59.65 35.64 o 7 10 0 9.42 23.03 36.95 o 8 10 0 102.46 115.15 68.20 o -8 11 0 198.16 163.42 64.22 o -7 11 0 287.73 297.62 71.30 o -6 11 0 1211.58 1446.90 118.69 o -5 11 0 214.03 219.23 58.90 o -4 11 0 439.32 325.96 60.23 o -3 11 0 5222.92 5598.50 190.44 o -2 11 0 5448.25 5442.16 178.93 o -1 11 0 289.94 234.29 47.83 o 0 11 0 3545.33 3541.73 99.11 o 1 11 0 9943.19 10073.48 166.11 o 2 11 0 3754.72 3627.46 103.19 o 3 11 0 74.70 76.00 32.01 o 4 11 0 5241.30 5656.91 132.83 o 5 11 0 2249.50 2339.57 92.00 o 6 11 0 114.09 92.05 38.33 o 7 11 0 33.49 38.51 41.43 o 8 11 0 412.41 438.90 91.23 o -7 12 0 380.99 392.40 88.13 o -6 12 0 110.13 101.86 56.69 o -5 12 0 268.12 251.56 62.00 o -4 12 0 1505.07 1477.91 112.94 o -3 12 0 0.88 -13.73 39.42 o -2 12 0 1752.65 1630.70 107.62 o -1 12 0 2639.02 2447.82 120.91 o 0 12 0 850.71 706.68 52.70 o 1 12 0 416.18 331.94 41.49 o 2 12 0 1492.26 1323.87 68.35 o 3 12 0 2920.92 3043.35 101.13 o 4 12 0 45.53 29.09 32.82 o 5 12 0 26.01 11.87 34.79 o 6 12 0 329.76 297.10 48.78 o 7 12 0 160.67 139.95 71.30 o 8 12 0 79.94 77.95 75.29 o -7 13 0 439.84 480.97 88.58 o -6 13 0 31.30 49.16 57.13 o -5 13 0 2.12 20.82 48.27 o -4 13 0 1009.81 1032.36 100.53 o -3 13 0 2352.09 2411.95 138.18 o -2 13 0 622.97 573.09 73.08 o -1 13 0 643.75 598.78 70.42 o 0 13 0 3645.10 3975.37 243.81 o 1 13 0 1960.89 1772.06 79.95 o 2 13 0 586.93 466.42 50.44 o 3 13 0 1587.33 1578.32 78.92 o 4 13 0 575.54 543.22 52.89 o 5 13 0 166.18 154.73 41.98 o 6 13 0 169.20 156.80 76.84 o 7 13 0 503.62 521.28 95.66 o -6 14 0 539.46 520.39 91.23 o -5 14 0 527.63 527.92 83.26 o -4 14 0 214.45 217.90 63.78 o -3 14 0 106.57 58.90 47.83 o -2 14 0 414.58 305.15 62.45 o -1 14 0 536.52 484.96 70.86 o 0 14 0 96.21 92.37 36.50 o 1 14 0 2373.59 2324.03 94.39 o 2 14 0 939.71 1002.11 67.40 o 3 14 0 127.61 104.13 37.87 o 4 14 0 20.93 15.08 35.84 o 5 14 0 581.48 605.33 59.88 o 6 14 0 858.92 960.17 109.84 o 7 14 0 92.17 27.02 71.30 o -6 15 0 100.46 143.05 69.09 o -5 15 0 468.13 399.92 80.16 o -4 15 0 538.64 511.09 83.26 o -3 15 0 147.41 98.32 53.15 o -2 15 0 351.52 216.13 57.57 o -1 15 0 425.73 407.45 69.09 o 0 15 0 1439.35 1504.28 81.43 o 1 15 0 118.90 138.85 41.93 o 2 15 0 449.37 345.51 50.68 o 3 15 0 402.11 398.65 63.33 o 4 15 0 1525.79 1455.43 83.61 o 5 15 0 1.65 -17.51 39.01 o 6 15 0 211.77 273.70 89.46 o 7 15 0 121.21 108.95 82.38 o -5 16 0 184.62 225.87 74.40 o -4 16 0 390.29 388.41 79.72 o -3 16 0 1184.76 1372.50 120.02 o -2 16 0 2227.00 2404.42 146.15 o -1 16 0 96.03 69.09 46.95 o 0 16 0 1579.89 1632.47 120.02 o 1 16 0 2927.00 3227.38 118.98 o 2 16 0 1660.77 1857.59 94.33 o 3 16 0 214.25 185.63 46.48 o 4 16 0 1286.43 1173.96 80.21 o 5 16 0 697.14 650.27 67.69 o 6 16 0 13.06 18.60 75.29 o -5 17 0 69.64 45.17 67.32 o -4 17 0 0.00 9.74 59.79 o -3 17 0 1.75 -12.40 51.82 o -2 17 0 200.71 208.60 66.88 o -1 17 0 193.94 200.63 62.45 o 0 17 0 185.91 197.53 59.35 o 1 17 0 54.05 65.77 40.74 o 2 17 0 112.52 127.63 45.21 o 3 17 0 158.63 87.94 44.94 o 4 17 0 0.02 33.13 42.61 o 5 17 0 11.97 -52.26 72.63 o -4 18 0 835.12 854.77 110.28 o -3 18 0 986.54 1192.24 121.35 o -2 18 0 118.99 116.92 59.79 o -1 18 0 258.97 239.16 67.76 o 0 18 0 2212.67 2503.18 155.90 o 1 18 0 1239.93 1300.88 86.15 o 2 18 0 238.75 227.03 51.49 o 3 18 0 1161.85 1144.05 84.86 o 4 18 0 1037.38 1057.97 82.46 o 5 18 0 260.20 336.15 96.99 o -3 19 0 77.50 16.83 65.55 o -2 19 0 76.71 52.26 62.45 o -1 19 0 79.73 108.06 61.12 o 0 19 0 9.13 67.76 58.90 o 1 19 0 94.22 89.19 48.69 o 2 19 0 13.85 33.57 45.50 o 3 19 0 0.61 -12.41 49.33 o 4 19 0 5.35 -37.65 73.52 o -2 20 0 174.40 163.42 73.52 o -1 20 0 745.57 845.91 108.51 o 0 20 0 1073.38 1031.04 117.81 o 1 20 0 41.72 52.26 67.32 o 2 20 0 1012.82 1280.03 94.73 o -2 -20 1 661.62 737.35 96.99 o -1 -20 1 1032.71 1036.16 85.89 o 0 -20 1 184.62 221.00 76.18 o 1 -20 1 203.89 144.38 69.53 o -4 -19 1 35.10 57.13 75.29 o -3 -19 1 4.68 -48.72 71.30 o -2 -19 1 69.12 75.53 46.90 o -1 -19 1 2.19 11.63 46.19 o 0 -19 1 15.08 33.66 59.35 o 1 -19 1 33.99 52.70 58.46 o 2 -19 1 17.95 20.37 58.90 o 3 -19 1 16.05 35.43 63.78 o -4 -18 1 10.93 16.39 73.08 o -3 -18 1 606.34 580.94 67.66 o -2 -18 1 1404.24 1649.97 164.53 o -1 -18 1 708.69 644.85 66.39 o 0 -18 1 156.29 211.70 65.10 o 1 -18 1 1007.09 1069.12 111.16 o 2 -18 1 942.23 885.33 104.52 o 3 -18 1 30.07 7.97 55.80 o 4 -18 1 366.12 379.11 86.36 o -5 -17 1 71.12 46.06 77.06 o -4 -17 1 134.72 168.74 80.60 o -3 -17 1 12.76 35.47 42.66 o -2 -17 1 194.95 165.94 47.35 o -1 -17 1 793.46 765.61 66.38 o 0 -17 1 405.38 325.52 70.42 o 1 -17 1 1.47 31.89 48.27 o 2 -17 1 274.90 195.75 62.89 o 3 -17 1 257.94 252.00 69.53 o 4 -17 1 509.75 368.92 80.16 o 5 -17 1 63.83 81.93 62.89 o -6 -16 1 279.29 303.82 95.22 o -5 -16 1 103.13 96.99 77.06 o -4 -16 1 344.82 304.23 53.60 o -3 -16 1 2383.58 2461.87 107.88 o -2 -16 1 1127.90 1042.26 74.61 o -1 -16 1 6.51 8.30 38.46 o 0 -16 1 949.21 904.71 75.73 o 1 -16 1 2066.20 2093.51 135.52 o 2 -16 1 268.78 216.57 63.78 o 3 -16 1 408.16 325.52 76.18 o 4 -16 1 547.00 590.81 87.69 o 5 -16 1 85.33 57.57 63.78 o -6 -15 1 408.33 343.68 88.13 o -5 -15 1 1071.25 1057.61 117.81 o -4 -15 1 766.46 662.16 62.35 o -3 -15 1 1.17 16.27 37.43 o -2 -15 1 2376.94 2452.65 111.61 o -1 -15 1 2670.39 2708.15 105.30 o 0 -15 1 145.21 122.66 38.84 o 1 -15 1 1301.06 1294.55 105.85 o 2 -15 1 757.10 675.84 83.26 o 3 -15 1 699.20 581.51 84.59 o 4 -15 1 104.35 91.68 57.13 o 5 -15 1 145.90 136.85 65.55 o 6 -15 1 342.17 341.02 80.60 o -7 -14 1 172.22 166.08 78.83 o -6 -14 1 72.03 77.95 68.20 o -5 -14 1 238.21 200.88 46.59 o -4 -14 1 999.08 932.12 67.77 o -3 -14 1 16.51 21.81 34.57 o -2 -14 1 98.57 74.98 37.07 o -1 -14 1 987.63 935.29 63.80 o 0 -14 1 2098.23 2160.48 100.98 o 1 -14 1 27.03 19.49 41.19 o 2 -14 1 124.81 52.26 50.05 o 3 -14 1 140.30 100.53 52.26 o 4 -14 1 421.11 321.98 71.30 o 5 -14 1 3.72 27.90 55.36 o 6 -14 1 155.40 161.21 66.88 o -7 -13 1 3.84 27.46 68.65 o -6 -13 1 1183.08 1269.31 125.78 o -5 -13 1 353.13 313.28 49.47 o -4 -13 1 73.48 83.93 35.96 o -3 -13 1 3748.26 3915.02 118.04 o -2 -13 1 4794.42 5121.13 141.28 o -1 -13 1 35.21 8.50 22.94 o 0 -13 1 695.53 638.01 52.90 o 1 -13 1 4949.51 5222.05 183.35 o 2 -13 1 6191.82 6938.23 224.10 o 3 -13 1 49.61 52.26 47.39 o 4 -13 1 276.43 170.07 57.57 o 5 -13 1 775.14 870.27 98.32 o 6 -13 1 427.27 439.78 81.05 o 7 -13 1 351.62 334.82 78.39 o -8 -12 1 33.39 62.45 72.63 o -7 -12 1 22.23 -1.33 64.22 o -6 -12 1 59.39 31.89 59.79 o -5 -12 1 472.41 476.31 60.23 o -4 -12 1 128.41 97.71 35.59 o -3 -12 1 2695.98 2747.79 94.27 o -2 -12 1 326.87 332.33 42.46 o -1 -12 1 1.77 4.95 20.86 o 0 -12 1 533.62 512.97 34.74 o 1 -12 1 152.50 120.02 42.52 o 2 -12 1 1945.39 1946.92 114.26 o 3 -12 1 1026.43 942.46 87.25 o 4 -12 1 763.62 736.07 85.03 o 5 -12 1 1543.00 1379.14 114.26 o 6 -12 1 2.19 27.46 50.93 o 7 -12 1 42.84 -10.63 56.69 o -8 -11 1 45.13 77.50 69.98 o -7 -11 1 1837.90 2072.26 149.25 o -6 -11 1 493.79 495.82 54.03 o -5 -11 1 169.76 165.95 39.36 o -4 -11 1 1902.74 1911.85 79.80 o -3 -11 1 5697.68 5995.86 130.59 o -2 -11 1 4537.95 4567.83 87.56 o -1 -11 1 21.97 10.01 20.29 o 0 -11 1 8428.93 8575.16 115.01 o 1 -11 1 3953.25 3911.56 148.81 o 2 -11 1 47.66 29.23 38.09 o 3 -11 1 1438.00 1393.76 98.76 o 4 -11 1 2755.56 2972.64 147.48 o 5 -11 1 1589.74 1605.01 116.92 o 6 -11 1 105.55 116.92 53.15 o 7 -11 1 1446.62 1550.98 131.54 o 8 -11 1 274.45 333.05 82.82 o -8 -10 1 0.60 -18.16 58.90 o -7 -10 1 68.91 18.60 55.80 o -6 -10 1 105.73 98.11 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