#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/23/2012320.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012320_Fobs loop_ _publ_author_name 'Wilson, Claire' 'Clark, J. Stephen' 'Bate, Andrea L.' 'Blake, Alexander J.' 'Grinter, Trevor' 'Teat, Simon J.' _publ_section_title ; Diels--Alder adducts of medium-ring carbocyclic dienes prepared by rearrangement of catalytically generated cyclic oxonium ylides ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1326 _journal_page_last 1329 _journal_volume 57 _journal_year 2001 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 69.955 _cell_angle_beta 83.957 _cell_angle_gamma 79.806 _cell_length_a 7.4878 _cell_length_b 10.1793 _cell_length_c 11.0220 _exptl_crystal_F_000 328.00 _reflns_d_resolution_high 0.7397 _[local]_cod_data_source_file gg1070Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' cyhpme in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 112.46 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 3144.61 3116.14 22.54 o 2 0 0 33.32 35.21 0.41 o 3 0 0 876.91 871.22 5.24 o 4 0 0 51.28 54.72 0.77 o 5 0 0 3.12 3.78 0.47 o 6 0 0 36.03 33.30 0.97 o 7 0 0 85.33 86.72 1.63 o 8 0 0 13.50 12.20 0.99 o 9 0 0 24.38 26.13 1.43 o -9 1 0 4.82 5.10 0.88 o -8 1 0 15.03 15.29 0.88 o -7 1 0 133.35 130.32 2.04 o -6 1 0 0.11 0.41 0.44 o -5 1 0 477.69 488.84 3.78 o -4 1 0 37.82 30.99 0.80 o -3 1 0 310.13 320.49 2.87 o -2 1 0 1907.26 1869.90 6.98 o -1 1 0 1236.84 1287.82 5.77 o 0 1 0 1022.59 975.06 5.05 o 1 1 0 563.37 543.42 2.29 o 2 1 0 1194.99 1257.58 5.22 o 3 1 0 716.93 684.86 3.67 o 4 1 0 22.04 21.38 0.50 o 5 1 0 640.71 631.88 3.84 o 6 1 0 579.86 563.39 3.92 o 7 1 0 35.64 33.53 1.35 o 8 1 0 16.62 13.63 1.02 o 9 1 0 5.56 7.37 0.94 o -9 2 0 9.36 9.69 1.05 o -8 2 0 75.88 76.54 1.77 o -7 2 0 164.28 161.36 2.35 o -6 2 0 239.46 226.81 2.54 o -5 2 0 53.47 46.63 1.08 o -4 2 0 6.81 5.16 0.47 o -3 2 0 1665.26 1791.70 7.23 o -2 2 0 2386.09 2563.89 8.25 o -1 2 0 4066.51 4092.13 16.67 o 0 2 0 2763.08 2619.44 9.96 o 1 2 0 797.01 771.06 3.59 o 2 2 0 2914.12 2995.86 11.81 o 3 2 0 427.15 457.19 2.65 o 4 2 0 11.77 15.09 0.47 o 5 2 0 163.33 159.24 1.43 o 6 2 0 57.22 60.76 1.60 o 7 2 0 141.90 132.12 2.54 o 8 2 0 36.67 34.22 1.46 o 9 2 0 33.18 36.12 1.66 o -9 3 0 2.51 4.53 1.35 o -8 3 0 10.16 8.31 0.77 o -7 3 0 112.77 109.88 2.15 o -6 3 0 73.46 69.73 1.46 o -5 3 0 44.32 33.08 0.97 o -4 3 0 5.27 4.58 0.47 o -3 3 0 38.37 46.03 0.91 o -2 3 0 53.42 43.60 0.63 o -1 3 0 386.68 371.24 1.82 o 0 3 0 281.95 273.12 1.55 o 1 3 0 10.78 8.61 0.25 o 2 3 0 1127.43 1191.16 4.91 o 3 3 0 119.35 113.08 0.99 o 4 3 0 205.84 194.48 1.68 o 5 3 0 2.67 2.92 0.44 o 6 3 0 13.74 14.21 0.91 o 7 3 0 242.34 228.30 3.37 o 8 3 0 35.62 37.80 1.55 o 9 3 0 0.37 0.69 0.66 o -8 4 0 118.02 120.89 2.32 o -7 4 0 2.48 2.87 0.58 o -6 4 0 7.69 6.82 0.63 o -5 4 0 30.14 25.97 0.91 o -4 4 0 209.61 186.92 2.07 o -3 4 0 64.71 67.69 1.13 o -2 4 0 723.05 751.50 3.34 o -1 4 0 531.58 541.29 2.59 o 0 4 0 280.04 277.37 1.68 o 1 4 0 888.93 913.33 3.97 o 2 4 0 210.42 235.48 1.46 o 3 4 0 68.02 78.53 0.83 o 4 4 0 0.42 0.03 0.33 o 5 4 0 345.15 348.64 2.87 o 6 4 0 67.73 59.79 1.24 o 7 4 0 35.47 32.86 1.35 o 8 4 0 15.08 16.17 1.10 o 9 4 0 39.70 42.08 1.79 o -8 5 0 63.95 67.47 1.82 o -7 5 0 31.32 32.56 1.21 o -6 5 0 4.49 3.64 0.58 o -5 5 0 1.93 1.88 0.50 o -4 5 0 29.14 27.70 0.91 o -3 5 0 26.20 31.57 0.88 o -2 5 0 115.40 119.84 1.21 o -1 5 0 0.64 0.36 0.28 o 0 5 0 10.46 15.12 0.47 o 1 5 0 0.71 0.50 0.30 o 2 5 0 0.22 0.47 0.25 o 3 5 0 35.45 40.01 0.63 o 4 5 0 269.66 276.12 2.46 o 5 5 0 2.62 2.98 0.44 o 6 5 0 0.20 0.14 0.41 o 7 5 0 10.99 9.55 0.88 o 8 5 0 16.75 17.71 1.16 o 9 5 0 134.40 142.13 4.50 o -7 6 0 9.84 12.80 1.16 o -6 6 0 1.17 0.36 0.69 o -5 6 0 6.35 8.03 0.86 o -4 6 0 0.00 0.69 0.44 o -3 6 0 514.61 505.39 3.61 o -2 6 0 426.51 407.36 2.81 o -1 6 0 117.27 121.49 1.24 o 0 6 0 60.18 69.04 0.91 o 1 6 0 0.32 1.10 0.30 o 2 6 0 240.28 231.89 1.55 o 3 6 0 84.64 86.39 1.16 o 4 6 0 100.74 91.00 1.46 o 5 6 0 21.97 22.16 0.83 o 6 6 0 58.38 44.23 1.19 o 7 6 0 44.31 40.04 1.52 o 8 6 0 22.06 28.03 1.41 o 9 6 0 0.73 1.46 1.05 o -7 7 0 2.44 4.30 1.35 o -6 7 0 0.10 -0.14 0.69 o -5 7 0 59.95 61.28 1.90 o -4 7 0 22.94 20.58 1.13 o -3 7 0 11.66 11.20 0.86 o -2 7 0 356.91 348.31 2.95 o -1 7 0 121.18 121.46 1.66 o 0 7 0 0.79 0.36 0.39 o 1 7 0 0.07 -0.25 0.36 o 2 7 0 13.50 15.34 0.66 o 3 7 0 1.77 1.41 0.36 o 4 7 0 13.56 14.18 0.61 o 5 7 0 0.40 0.17 0.41 o 6 7 0 3.62 6.54 0.61 o 7 7 0 0.85 0.36 0.44 o 8 7 0 19.87 25.22 1.41 o 9 7 0 9.18 13.52 1.68 o -6 8 0 60.64 61.75 2.15 o -5 8 0 6.96 6.37 0.88 o -4 8 0 37.72 36.28 1.49 o -3 8 0 320.17 318.95 4.03 o -2 8 0 6.15 4.99 0.69 o -1 8 0 2.88 2.51 0.50 o 0 8 0 102.96 98.53 1.68 o 1 8 0 0.01 0.06 0.39 o 2 8 0 0.04 -0.19 0.50 o 3 8 0 2.27 1.60 0.58 o 4 8 0 75.17 65.97 1.46 o 5 8 0 199.87 168.92 2.43 o 6 8 0 46.63 43.57 1.63 o 7 8 0 1.03 0.77 0.61 o -5 9 0 88.56 90.01 2.51 o -4 9 0 31.34 32.31 1.49 o -3 9 0 38.18 39.29 1.55 o -2 9 0 68.25 65.15 1.85 o -1 9 0 36.34 32.61 1.08 o 0 9 0 47.95 44.98 1.19 o 1 9 0 91.72 93.90 3.01 o 2 9 0 57.08 51.05 1.63 o 3 9 0 2.76 2.15 0.63 o 4 9 0 0.09 -0.39 0.52 o 5 9 0 25.02 18.79 0.94 o 6 9 0 2.81 1.96 0.55 o 7 9 0 22.28 23.29 1.13 o -4 10 0 2.12 1.57 0.75 o -3 10 0 9.12 9.55 0.94 o -2 10 0 2.70 2.01 0.72 o -1 10 0 85.83 93.71 1.82 o 0 10 0 0.83 1.52 0.61 o 1 10 0 26.91 28.06 1.32 o 2 10 0 100.99 94.81 2.32 o 3 10 0 34.28 34.52 1.49 o 4 10 0 5.93 7.51 0.86 o 5 10 0 3.44 4.28 0.77 o 6 10 0 0.01 -0.19 0.52 o -3 11 0 11.18 9.46 1.05 o -2 11 0 8.32 6.15 1.27 o -1 11 0 2.77 2.32 1.08 o 0 11 0 165.93 172.87 3.23 o 1 11 0 18.67 19.89 1.24 o 2 11 0 0.54 0.47 0.63 o 3 11 0 62.61 62.39 2.04 o 4 11 0 0.45 0.39 0.69 o 5 11 0 18.86 21.11 1.35 o 0 12 0 11.52 12.97 1.21 o 1 12 0 3.03 3.09 0.83 o 2 12 0 123.97 140.81 4.50 o 3 12 0 2.40 3.86 0.86 o -2 -12 1 25.36 27.15 2.21 o -1 -12 1 5.07 5.90 0.99 o 0 -12 1 32.12 34.38 2.35 o -4 -11 1 9.67 9.30 1.02 o -3 -11 1 13.52 12.31 1.08 o -2 -11 1 9.68 9.99 0.99 o -1 -11 1 70.74 75.99 2.21 o 0 -11 1 4.61 4.25 0.83 o 1 -11 1 0.61 -0.36 1.05 o 2 -11 1 38.96 40.20 2.46 o -6 -10 1 0.08 -0.50 0.55 o -5 -10 1 0.04 0.03 0.66 o -4 -10 1 10.04 10.18 0.99 o -3 -10 1 1.48 1.55 0.63 o -2 -10 1 53.11 52.07 1.77 o -1 -10 1 13.00 13.16 0.99 o 0 -10 1 72.91 73.23 2.01 o 1 -10 1 72.11 77.73 3.04 o 2 -10 1 4.31 3.78 0.75 o 3 -10 1 1.23 1.41 0.72 o 4 -10 1 21.71 23.48 1.41 o -7 -9 1 3.52 2.37 1.13 o -6 -9 1 31.18 35.18 1.30 o -5 -9 1 43.94 48.45 1.43 o -4 -9 1 3.85 3.12 0.66 o -3 -9 1 106.35 102.78 2.35 o -2 -9 1 86.67 76.74 1.99 o -1 -9 1 520.46 495.54 5.08 o 0 -9 1 55.17 52.81 1.66 o 1 -9 1 11.29 10.24 0.72 o 2 -9 1 137.65 149.31 3.97 o 3 -9 1 0.97 0.25 0.61 o 4 -9 1 9.45 9.16 0.94 o 5 -9 1 0.71 -0.33 0.72 o -8 -8 1 14.45 15.78 1.68 o -7 -8 1 3.83 5.08 0.66 o -6 -8 1 42.69 37.69 1.24 o -5 -8 1 1.59 1.24 0.41 o -4 -8 1 49.03 46.27 1.27 o -3 -8 1 24.36 23.62 1.13 o -2 -8 1 93.88 86.31 1.99 o -1 -8 1 281.45 254.16 3.34 o 0 -8 1 771.03 755.14 6.21 o 1 -8 1 5.51 3.97 0.52 o 2 -8 1 3.65 3.92 0.66 o 3 -8 1 29.56 27.32 1.24 o 4 -8 1 86.61 93.49 2.32 o 5 -8 1 26.90 27.46 1.43 o 6 -8 1 68.43 75.96 3.28 o -8 -7 1 0.00 -0.39 0.63 o -7 -7 1 11.35 10.49 0.75 o -6 -7 1 0.11 0.33 0.41 o -5 -7 1 50.59 45.72 1.21 o -4 -7 1 29.30 22.24 0.75 o -3 -7 1 2.96 3.53 0.44 o -2 -7 1 77.75 78.72 1.38 o -1 -7 1 157.07 154.60 1.52 o 0 -7 1 84.75 83.41 1.21 o 1 -7 1 403.44 391.52 2.62 o 2 -7 1 4.15 2.65 0.47 o 3 -7 1 5.92 5.10 0.69 o 4 -7 1 0.61 0.30 0.55 o 5 -7 1 438.49 446.12 5.30 o 6 -7 1 6.89 6.71 0.91 o 7 -7 1 13.10 13.85 1.68 o -8 -6 1 1.81 1.90 0.69 o -7 -6 1 8.66 10.54 0.94 o -6 -6 1 1.59 0.44 0.41 o -5 -6 1 7.68 5.82 0.55 o -4 -6 1 69.67 79.05 1.41 o -3 -6 1 162.46 168.62 1.71 o -2 -6 1 601.12 634.12 3.95 o -1 -6 1 176.08 171.68 1.49 o 0 -6 1 1052.53 1083.41 6.29 o 1 -6 1 17.98 16.25 0.52 o 2 -6 1 503.72 516.87 3.37 o 3 -6 1 0.01 -0.28 0.39 o 4 -6 1 0.04 -0.22 0.44 o 5 -6 1 81.37 84.68 1.68 o 6 -6 1 3.38 3.04 0.75 o 7 -6 1 4.73 5.85 0.94 o -9 -5 1 2.28 2.35 1.10 o -8 -5 1 0.07 0.25 0.58 o -7 -5 1 12.28 13.22 0.97 o -6 -5 1 9.43 11.59 0.69 o -5 -5 1 274.19 305.10 3.64 o -4 -5 1 225.59 216.38 2.40 o -3 -5 1 0.21 0.58 0.33 o -2 -5 1 87.83 78.42 0.80 o -1 -5 1 0.00 0.63 0.30 o 0 -5 1 0.01 0.75 0.39 o 1 -5 1 14.48 20.47 0.52 o 2 -5 1 319.24 333.66 2.65 o 3 -5 1 326.34 336.58 3.17 o 4 -5 1 827.82 823.24 5.02 o 5 -5 1 211.82 212.02 3.34 o 6 -5 1 31.69 31.51 1.10 o 7 -5 1 0.05 -0.39 0.52 o 8 -5 1 1.64 1.85 0.86 o -9 -4 1 25.72 31.29 1.57 o -8 -4 1 39.13 42.38 1.66 o -7 -4 1 10.80 11.23 0.91 o -6 -4 1 7.99 8.50 0.61 o -5 -4 1 0.01 0.94 0.50 o -4 -4 1 40.03 35.60 0.88 o -3 -4 1 434.98 434.51 3.26 o -2 -4 1 2244.97 2349.22 10.49 o -1 -4 1 513.16 534.64 2.73 o 0 -4 1 351.54 327.56 2.32 o 1 -4 1 16.75 21.88 0.52 o 2 -4 1 28.36 22.54 0.55 o 3 -4 1 14.78 14.79 0.50 o 4 -4 1 81.44 77.59 1.35 o 5 -4 1 282.16 270.55 3.81 o 6 -4 1 30.11 29.97 1.05 o 7 -4 1 150.47 143.46 2.90 o 8 -4 1 1.35 1.27 0.66 o -9 -3 1 44.34 45.23 1.82 o -8 -3 1 51.94 52.29 1.82 o -7 -3 1 47.62 47.46 1.60 o -6 -3 1 0.19 -0.22 0.52 o -5 -3 1 91.52 97.02 1.46 o -4 -3 1 0.59 0.69 0.39 o -3 -3 1 2384.58 2591.48 15.73 o -2 -3 1 22.68 23.32 0.61 o -1 -3 1 436.52 440.47 1.96 o 0 -3 1 704.62 746.81 3.67 o 1 -3 1 711.83 761.57 3.20 o 2 -3 1 1089.61 1115.86 6.51 o 3 -3 1 252.06 246.65 1.60 o 4 -3 1 866.01 894.68 5.22 o 5 -3 1 25.58 26.43 0.88 o 6 -3 1 72.19 70.14 1.46 o 7 -3 1 27.74 25.91 1.05 o 8 -3 1 0.72 0.39 0.55 o 9 -3 1 21.85 20.97 1.41 o -9 -2 1 27.94 28.95 1.52 o -8 -2 1 2.55 2.26 0.69 o -7 -2 1 24.58 19.76 1.10 o -6 -2 1 37.58 34.52 1.27 o -5 -2 1 46.12 43.73 0.77 o -4 -2 1 69.69 83.50 0.94 o -3 -2 1 4442.05 4763.91 18.68 o -2 -2 1 1672.47 1696.31 12.83 o -1 -2 1 67.92 76.49 0.63 o 0 -2 1 3.54 3.20 0.22 o 1 -2 1 14.87 19.32 0.36 o 2 -2 1 20.58 13.60 0.39 o 3 -2 1 60.83 66.11 0.75 o 4 -2 1 12.69 20.28 0.72 o 5 -2 1 30.74 32.31 0.94 o 6 -2 1 101.39 106.51 1.79 o 7 -2 1 33.42 34.57 1.16 o 8 -2 1 37.51 35.37 1.24 o 9 -2 1 8.37 7.17 0.69 o -9 -1 1 9.95 8.36 0.99 o -8 -1 1 18.84 20.17 1.19 o -7 -1 1 74.01 69.64 1.88 o -6 -1 1 213.28 194.48 2.18 o -5 -1 1 10.89 11.06 0.44 o -4 -1 1 532.37 548.80 2.84 o -3 -1 1 31.36 38.69 0.58 o -2 -1 1 4.29 3.01 0.22 o -1 -1 1 1.03 0.44 0.25 o 0 -1 1 722.36 728.68 3.23 o 1 -1 1 429.26 443.03 1.93 o 2 -1 1 1225.03 1260.37 5.63 o 3 -1 1 12.56 13.47 0.58 o 4 -1 1 0.87 0.47 0.39 o 5 -1 1 0.06 0.25 0.39 o 6 -1 1 136.64 137.85 1.93 o 7 -1 1 0.01 -0.08 0.44 o 8 -1 1 7.71 6.10 0.69 o 9 -1 1 2.48 1.43 0.72 o -9 0 1 41.92 41.39 1.77 o -8 0 1 61.19 61.45 1.93 o -7 0 1 23.48 19.70 1.10 o -6 0 1 526.60 533.10 3.86 o -5 0 1 41.40 40.42 0.94 o -4 0 1 16.81 22.13 0.50 o -3 0 1 1796.88 1872.96 6.21 o -2 0 1 320.88 331.86 1.66 o -1 0 1 1640.50 1649.82 5.66 o 0 0 1 117.11 113.38 1.27 o 1 0 1 329.18 327.56 1.79 o 2 0 1 979.40 984.16 5.93 o 3 0 1 937.98 955.05 3.92 o 4 0 1 333.53 336.94 2.62 o 5 0 1 113.61 97.76 1.43 o 6 0 1 0.00 -0.03 0.41 o 7 0 1 3.96 4.17 0.58 o 8 0 1 12.48 12.09 0.69 o 9 0 1 35.92 36.84 1.66 o -9 1 1 0.93 0.08 0.69 o -8 1 1 6.35 6.40 0.83 o -7 1 1 1.76 1.08 0.52 o -6 1 1 15.71 14.51 0.75 o -5 1 1 199.66 200.27 1.85 o -4 1 1 0.92 1.46 0.36 o -3 1 1 0.37 0.55 0.25 o -2 1 1 7200.24 6933.77 59.46 o -1 1 1 1316.41 1376.45 5.71 o 0 1 1 97.01 94.04 0.66 o 1 1 1 2572.10 2504.29 13.38 o 2 1 1 1210.18 1184.46 5.79 o 3 1 1 8.08 7.56 0.33 o 4 1 1 0.04 0.00 0.25 o 5 1 1 3.64 2.48 0.39 o 6 1 1 130.49 115.48 1.68 o 7 1 1 21.63 21.08 0.88 o 8 1 1 30.72 33.61 1.43 o 9 1 1 4.85 6.35 0.88 o -9 2 1 2.64 2.87 0.83 o -8 2 1 6.90 6.95 0.72 o -7 2 1 181.90 178.66 2.48 o -6 2 1 39.28 33.80 1.05 o -5 2 1 216.65 195.06 2.21 o -4 2 1 65.93 77.04 1.21 o -3 2 1 1058.41 1099.50 7.17 o -2 2 1 413.20 419.91 2.87 o -1 2 1 1625.80 1625.98 9.33 o 0 2 1 541.98 583.32 3.70 o 1 2 1 235.39 227.67 1.16 o 2 2 1 818.61 830.91 3.61 o 3 2 1 245.22 255.57 1.63 o 4 2 1 229.35 213.82 1.52 o 5 2 1 62.94 61.45 0.97 o 6 2 1 294.12 284.90 2.65 o 7 2 1 269.43 267.54 5.16 o 8 2 1 0.01 0.06 0.58 o 9 2 1 30.75 30.93 1.52 o -8 3 1 26.47 29.14 1.19 o -7 3 1 1.43 0.72 0.50 o -6 3 1 24.80 23.59 0.91 o -5 3 1 198.11 210.40 2.32 o -4 3 1 5.66 5.79 0.50 o -3 3 1 162.25 163.57 1.19 o -2 3 1 19.78 16.25 0.44 o -1 3 1 382.49 376.12 1.96 o 0 3 1 22.60 20.72 0.33 o 1 3 1 4556.16 4503.13 22.79 o 2 3 1 30.09 31.98 0.50 o 3 3 1 133.69 150.08 1.24 o 4 3 1 525.91 537.02 3.45 o 5 3 1 310.17 310.31 2.15 o 6 3 1 23.94 19.73 0.99 o 7 3 1 30.20 29.28 1.27 o 8 3 1 0.35 0.08 0.58 o 9 3 1 1.99 1.79 0.72 o -8 4 1 3.43 2.98 0.66 o -7 4 1 33.37 31.15 1.16 o -6 4 1 0.14 -0.39 0.47 o -5 4 1 67.39 61.31 1.32 o -4 4 1 623.89 657.35 4.19 o -3 4 1 309.57 333.30 2.54 o -2 4 1 26.86 19.18 0.50 o -1 4 1 362.97 342.15 1.96 o 0 4 1 163.28 162.30 1.19 o 1 4 1 8.19 9.82 0.33 o 2 4 1 1005.02 1004.66 3.70 o 3 4 1 434.37 475.92 2.40 o 4 4 1 2.64 5.71 0.39 o 5 4 1 437.85 427.47 3.15 o 6 4 1 35.58 34.22 0.97 o 7 4 1 1.63 1.71 0.61 o 8 4 1 9.47 9.38 0.91 o 9 4 1 15.52 14.68 1.13 o -8 5 1 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o 5 5 13 13.33 13.47 1.63 o -2 6 13 0.19 0.33 0.63 o -1 6 13 4.85 5.05 0.86 o 0 6 13 28.16 27.90 1.46 o 1 6 13 0.57 0.19 0.63 o 2 6 13 5.93 5.44 0.86 o 3 6 13 19.69 21.85 1.35 o 4 6 13 12.20 13.11 1.13 o 5 6 13 19.72 18.29 1.79 o -3 7 13 6.57 3.81 1.30 o -2 7 13 74.56 73.34 2.29 o -1 7 13 10.89 12.89 1.10 o 0 7 13 2.77 2.43 0.77 o 1 7 13 70.47 66.22 2.18 o 2 7 13 1.20 1.74 0.72 o 3 7 13 22.19 24.06 1.41 o 4 7 13 0.02 0.80 1.08 o 5 7 13 2.67 2.07 1.08 o -1 8 13 0.00 0.33 0.75 o 0 8 13 24.23 24.64 1.43 o 1 8 13 22.76 22.41 1.38 o 2 8 13 28.32 30.44 1.57 o 3 8 13 13.68 12.33 1.13 o -1 2 14 7.64 8.36 1.43 o 0 2 14 4.94 4.33 1.27 o 1 2 14 15.61 16.42 1.77 o 2 2 14 6.52 5.77 0.91 o 3 2 14 98.10 111.03 4.08 o 1 3 14 16.21 16.56 1.74 o 2 3 14 24.84 29.06 2.21 o 3 3 14 18.81 21.41 1.41 o 0 4 14 4.68 6.68 1.35 o 1 4 14 13.09 17.02 1.27 o 2 4 14 77.84 80.52 2.43 o 3 4 14 12.26 8.50 1.57 o 0 5 14 16.30 14.27 1.63 o 1 5 14 88.92 96.55 3.70 o 2 5 14 26.17 26.21 2.10 o -1 6 14 22.94 26.68 2.15 o 0 6 14 57.74 60.65 2.98 o 1 6 14 11.46 11.62 1.55 o 2 6 14 36.70 38.77 2.48 o