#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/23/2012321.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012321_Fobs loop_ _publ_author_name 'Wilson, Claire' 'Clark, J. Stephen' 'Bate, Andrea L.' 'Blake, Alexander J.' 'Grinter, Trevor' 'Teat, Simon J.' _publ_section_title ; Diels--Alder adducts of medium-ring carbocyclic dienes prepared by rearrangement of catalytically generated cyclic oxonium ylides ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1326 _journal_page_last 1329 _journal_volume 57 _journal_year 2001 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.149 _cell_angle_gamma 90.000 _cell_length_a 27.6658 _cell_length_b 5.0662 _cell_length_c 22.7925 _exptl_crystal_F_000 1312.00 _reflns_d_resolution_high 0.7393 _[local]_cod_data_source_file gg1070IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' bzhpme in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 303.34 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 82260.17 86889.78 596.70 o 6 0 0 3988.63 3742.97 28.73 o 8 0 0 7325.29 7925.24 54.46 o 10 0 0 47.00 40.70 5.98 o 12 0 0 6872.73 6547.51 238.80 o 14 0 0 1666.35 1511.19 18.55 o 16 0 0 72.87 57.46 8.98 o 18 0 0 14574.27 13467.28 496.75 o 20 0 0 307.51 203.49 11.37 o 22 0 0 5865.88 5695.86 75.41 o 24 0 0 430.06 423.73 23.34 o 26 0 0 1211.15 1068.91 32.32 o 28 0 0 25.99 25.14 17.36 o 30 0 0 1453.20 1419.03 38.90 o 32 0 0 164.85 196.90 21.55 o 34 0 0 843.66 921.68 36.51 o 1 1 0 39003.54 41986.06 351.91 o 3 1 0 27218.02 28685.16 198.10 o 5 1 0 7265.97 8278.35 47.88 o 7 1 0 22240.16 22444.08 131.07 o 9 1 0 3114.52 3298.89 44.29 o 11 1 0 12673.34 12434.29 103.54 o 13 1 0 1792.18 2059.41 17.36 o 15 1 0 3468.59 3456.30 22.74 o 17 1 0 546.30 451.86 8.98 o 19 1 0 0.15 20.95 7.18 o 21 1 0 5257.88 5041.10 37.11 o 23 1 0 1843.21 1770.94 23.94 o 25 1 0 53.04 21.55 8.98 o 27 1 0 9.51 -17.36 11.37 o 29 1 0 328.57 297.45 16.16 o 31 1 0 232.46 232.22 16.16 o 33 1 0 62.02 73.61 14.36 o 0 2 0 34822.41 38064.14 220.84 o 2 2 0 3347.07 3616.09 34.11 o 4 2 0 1522.64 1703.31 39.50 o 6 2 0 3353.08 3766.31 23.34 o 8 2 0 2081.93 1985.80 20.35 o 10 2 0 39.81 11.37 5.98 o 12 2 0 185.47 146.03 7.18 o 14 2 0 4688.86 4881.91 27.53 o 16 2 0 182.08 139.45 6.58 o 18 2 0 3113.00 2896.71 27.53 o 20 2 0 90.60 65.83 9.58 o 22 2 0 3872.80 3620.28 34.71 o 24 2 0 970.53 948.61 17.95 o 26 2 0 69.75 89.18 8.98 o 28 2 0 66.22 69.43 8.98 o 30 2 0 3.08 -1.20 10.17 o 32 2 0 531.30 516.50 19.75 o 34 2 0 236.82 286.68 24.54 o 1 3 0 714.60 769.66 15.56 o 3 3 0 0.00 -4.79 8.98 o 5 3 0 405.80 489.57 32.32 o 7 3 0 147.50 137.05 8.98 o 9 3 0 97.82 119.10 7.78 o 11 3 0 878.09 808.56 15.56 o 13 3 0 2572.33 2603.44 29.33 o 15 3 0 402.18 477.60 19.75 o 17 3 0 1205.00 1179.03 28.13 o 19 3 0 793.05 758.89 21.55 o 21 3 0 1394.81 1296.34 25.14 o 23 3 0 55.90 55.66 10.17 o 25 3 0 259.50 205.88 11.97 o 27 3 0 484.07 479.39 18.55 o 29 3 0 47.05 71.82 10.77 o 31 3 0 83.68 94.56 14.96 o 0 4 0 2758.96 2991.27 44.29 o 2 4 0 1.63 10.77 10.77 o 4 4 0 3018.75 3149.27 32.32 o 6 4 0 58.93 78.40 11.97 o 8 4 0 595.99 587.12 13.77 o 10 4 0 2984.04 2982.29 28.13 o 12 4 0 21.35 49.67 9.58 o 14 4 0 5113.82 5202.70 46.68 o 16 4 0 349.54 362.09 16.76 o 18 4 0 157.18 169.97 13.77 o 20 4 0 719.32 690.66 20.35 o 22 4 0 42.09 47.88 13.17 o 24 4 0 298.83 287.28 16.76 o 26 4 0 0.01 1.20 13.17 o 28 4 0 11.05 37.71 19.75 o 1 5 0 94.83 102.94 13.17 o 3 5 0 176.22 190.32 14.36 o 5 5 0 289.92 311.22 15.56 o 7 5 0 114.32 242.99 11.97 o 9 5 0 127.29 126.88 10.77 o 11 5 0 876.66 892.35 22.14 o 13 5 0 127.45 118.50 13.77 o 15 5 0 6.75 4.19 13.17 o 17 5 0 11.02 85.58 14.36 o 19 5 0 0.03 15.56 13.17 o 21 5 0 376.39 357.90 18.55 o 0 6 0 195.22 151.42 20.95 o 2 6 0 58.92 37.11 13.17 o 4 6 0 17.40 8.38 13.17 o 6 6 0 16.12 32.32 10.77 o 8 6 0 12.11 17.95 13.17 o 10 6 0 189.54 180.15 16.16 o 12 6 0 180.02 178.95 15.56 o -33 1 1 11.61 10.17 12.57 o -31 1 1 74.64 56.26 13.17 o -29 1 1 54.28 28.73 11.97 o -27 1 1 63.16 61.64 9.58 o -25 1 1 112.58 102.34 10.17 o -23 1 1 354.50 334.56 14.96 o -21 1 1 1671.82 1662.01 17.36 o -19 1 1 2993.34 2905.68 34.71 o -17 1 1 229.78 195.71 7.78 o -15 1 1 1318.97 1329.25 16.76 o -13 1 1 2417.58 2571.12 20.95 o -11 1 1 3821.81 3927.31 27.53 o -9 1 1 157.81 286.68 11.37 o -7 1 1 0.10 36.51 10.77 o -5 1 1 30546.18 29940.79 268.12 o -3 1 1 62.47 42.49 4.19 o -1 1 1 199.98 181.94 5.98 o 1 1 1 381.70 407.57 7.78 o 3 1 1 27105.67 27528.87 144.84 o 5 1 1 4205.05 3973.99 21.55 o 7 1 1 13140.44 12497.13 55.66 o 9 1 1 12.35 6.58 4.79 o 11 1 1 3168.87 3227.67 24.54 o 13 1 1 6.27 19.15 7.78 o 15 1 1 1358.91 1467.50 14.36 o 17 1 1 15.24 7.18 5.39 o 19 1 1 872.49 841.48 11.97 o 21 1 1 75.81 66.43 10.17 o 23 1 1 196.85 191.52 11.37 o 25 1 1 33.11 4.79 11.37 o 27 1 1 136.63 87.98 12.57 o 29 1 1 117.43 74.21 12.57 o 31 1 1 53.69 25.14 13.17 o 33 1 1 58.86 52.07 14.36 o -32 2 1 144.45 135.86 14.96 o -30 2 1 68.70 48.48 10.77 o -28 2 1 121.27 92.77 8.98 o -26 2 1 0.01 -11.37 7.78 o -24 2 1 1026.61 983.32 19.15 o -22 2 1 1511.16 1491.44 22.74 o -20 2 1 1899.81 1834.98 20.95 o -18 2 1 5055.33 5096.76 41.30 o -16 2 1 25.18 26.93 5.39 o -14 2 1 374.62 409.37 13.77 o -12 2 1 0.13 12.57 7.18 o -10 2 1 96.48 105.93 8.38 o -8 2 1 5586.62 5906.52 49.08 o -6 2 1 122.30 116.71 7.18 o -4 2 1 21716.09 22754.10 149.02 o -2 2 1 186.72 163.39 8.98 o 0 2 1 49.87 125.08 10.77 o 2 2 1 1104.28 1134.74 14.96 o 4 2 1 153.84 171.77 11.97 o 6 2 1 22.95 28.13 5.39 o 8 2 1 6833.56 7306.40 38.90 o 10 2 1 1254.08 1365.16 13.77 o 12 2 1 6156.31 6448.76 52.07 o 14 2 1 2027.74 1799.67 22.74 o 16 2 1 687.07 660.14 10.77 o 18 2 1 9311.49 9442.42 69.43 o 20 2 1 247.63 236.40 10.17 o 22 2 1 760.80 706.82 16.76 o 24 2 1 565.68 541.64 14.36 o 26 2 1 414.62 422.54 11.97 o 28 2 1 103.94 110.72 10.77 o 30 2 1 108.26 125.08 11.97 o 32 2 1 220.57 242.99 17.36 o -31 3 1 70.10 88.58 11.97 o -29 3 1 44.96 42.49 10.77 o -27 3 1 98.02 104.74 11.97 o -25 3 1 3.59 5.39 9.58 o -23 3 1 1.61 1.20 10.77 o -21 3 1 27.29 27.53 10.77 o -19 3 1 1133.40 1126.96 28.13 o -17 3 1 1.56 27.53 8.98 o -15 3 1 3166.12 3252.81 42.49 o -13 3 1 465.31 602.68 32.32 o -11 3 1 266.14 271.12 10.77 o -9 3 1 344.24 375.85 11.97 o -7 3 1 628.31 652.36 14.96 o -5 3 1 5017.69 5102.15 37.11 o -3 3 1 722.55 866.02 16.16 o -1 3 1 17.02 14.96 9.58 o 1 3 1 46.46 20.35 9.58 o 3 3 1 1974.88 2127.64 22.74 o 5 3 1 953.84 946.22 32.92 o 7 3 1 2161.12 2327.54 32.32 o 9 3 1 116.08 143.04 7.78 o 11 3 1 72.43 83.79 7.78 o 13 3 1 218.39 313.01 16.16 o 15 3 1 2101.52 2144.40 48.48 o 17 3 1 944.57 998.29 29.92 o 19 3 1 118.99 103.54 11.97 o 21 3 1 345.46 368.07 14.36 o 23 3 1 524.62 502.73 15.56 o 25 3 1 100.54 101.74 10.77 o 27 3 1 154.09 173.56 12.57 o 29 3 1 571.96 617.64 17.95 o 31 3 1 139.44 153.21 23.94 o -28 4 1 115.45 123.29 21.55 o -26 4 1 120.53 103.54 14.36 o -24 4 1 1.68 4.79 12.57 o -22 4 1 19.15 31.72 12.57 o -20 4 1 303.25 311.22 15.56 o -18 4 1 0.64 15.56 11.97 o -16 4 1 435.94 475.20 17.36 o -14 4 1 1062.71 1231.70 19.75 o -12 4 1 8.94 41.30 9.58 o -10 4 1 1629.80 1636.88 20.35 o -8 4 1 38.44 29.33 8.98 o -6 4 1 345.36 395.60 14.96 o -4 4 1 1165.19 1252.05 29.33 o -2 4 1 879.57 980.93 19.15 o 0 4 1 137.98 201.69 13.17 o 2 4 1 12.99 10.17 11.37 o 4 4 1 95.59 181.94 12.57 o 6 4 1 641.41 636.80 14.36 o 8 4 1 1517.59 1523.16 19.15 o 10 4 1 277.98 443.48 16.16 o 12 4 1 959.20 999.48 21.55 o 14 4 1 585.88 804.37 20.95 o 16 4 1 329.57 310.02 16.16 o 18 4 1 628.50 621.24 19.15 o 20 4 1 159.54 195.11 14.96 o 22 4 1 43.26 45.49 13.17 o 24 4 1 34.31 58.65 13.77 o 26 4 1 48.45 69.43 14.96 o -23 5 1 338.84 332.76 25.74 o -21 5 1 475.54 485.98 20.35 o -19 5 1 32.89 17.36 13.17 o -17 5 1 1336.01 1337.63 27.53 o -15 5 1 18.86 22.14 12.57 o -13 5 1 28.89 76.61 12.57 o -11 5 1 194.81 247.78 12.57 o -9 5 1 7.37 22.74 9.58 o -7 5 1 596.02 553.61 14.96 o -5 5 1 69.95 77.21 13.17 o -3 5 1 16.65 44.29 11.97 o -1 5 1 0.32 -5.98 11.97 o 1 5 1 798.93 723.58 19.15 o 3 5 1 722.71 696.65 19.15 o 5 5 1 295.02 363.29 16.16 o 7 5 1 2859.48 2723.74 28.13 o 9 5 1 26.75 43.09 10.17 o 11 5 1 336.17 333.96 16.16 o 13 5 1 207.00 240.00 15.56 o 15 5 1 2.38 -2.99 13.17 o 17 5 1 52.80 50.27 14.36 o 19 5 1 163.06 154.41 15.56 o 21 5 1 128.58 157.40 16.16 o -14 6 1 65.35 103.54 20.35 o -12 6 1 12.29 31.12 13.17 o -10 6 1 146.48 150.22 15.56 o -8 6 1 197.72 186.73 12.57 o -6 6 1 108.75 118.50 11.97 o -4 6 1 1.59 8.98 13.77 o -2 6 1 76.76 89.18 13.77 o 0 6 1 81.14 80.80 13.77 o 2 6 1 6.53 8.98 12.57 o 4 6 1 106.88 88.58 13.77 o 6 6 1 65.59 64.04 13.77 o 8 6 1 10.46 16.16 13.17 o 10 6 1 43.36 64.04 14.36 o 12 6 1 7.22 52.67 18.55 o -34 0 2 32.33 1.20 19.15 o -32 0 2 59.64 52.67 19.15 o -30 0 2 110.23 70.62 19.15 o -28 0 2 61.15 31.72 16.76 o -26 0 2 255.35 208.28 13.77 o -24 0 2 998.42 940.23 30.52 o -22 0 2 235.59 217.85 11.97 o -20 0 2 599.61 654.15 25.14 o -18 0 2 4951.59 4709.54 189.72 o -16 0 2 8878.50 9304.17 55.66 o -14 0 2 128.63 225.03 10.17 o -12 0 2 17260.08 17540.63 348.92 o -10 0 2 16798.95 16824.23 159.20 o -8 0 2 24581.80 23266.41 162.19 o -6 0 2 1326.66 1221.52 12.57 o -4 0 2 2050.83 1981.61 10.77 o -2 0 2 209.49 232.81 3.59 o 0 0 2 24354.65 19624.58 147.83 o 2 0 2 789.79 671.51 11.37 o 4 0 2 227.69 230.42 5.39 o 6 0 2 22969.23 22379.44 89.18 o 8 0 2 2058.01 2261.11 20.35 o 10 0 2 10338.75 10404.20 66.43 o 12 0 2 1601.60 1302.32 15.56 o 14 0 2 21387.42 22098.75 478.79 o 16 0 2 159.53 157.40 8.98 o 18 0 2 4958.02 4643.71 85.58 o 20 0 2 116.83 55.06 8.98 o 22 0 2 2639.43 2684.24 44.89 o 24 0 2 847.53 748.71 27.53 o 26 0 2 1372.96 1316.09 35.31 o 28 0 2 2.15 0.00 16.76 o 30 0 2 675.72 670.31 30.52 o 32 0 2 75.97 102.34 21.55 o -33 1 2 0.89 4.79 12.57 o -31 1 2 236.30 254.36 16.76 o -29 1 2 259.84 219.65 15.56 o -27 1 2 2980.72 2884.14 42.49 o -25 1 2 150.92 141.84 11.37 o -23 1 2 5224.84 5008.79 51.47 o -21 1 2 13.23 22.14 5.98 o -19 1 2 4695.99 4676.62 42.49 o -17 1 2 64.33 104.14 6.58 o -15 1 2 239.12 217.25 7.18 o -13 1 2 502.22 498.54 10.17 o -11 1 2 3161.08 3438.34 28.13 o -9 1 2 21382.34 22063.44 128.08 o -7 1 2 13146.17 13400.25 91.57 o -5 1 2 1025.08 991.70 31.12 o -3 1 2 2634.46 2499.90 18.55 o -1 1 2 18787.92 18257.62 113.12 o 1 1 2 19532.44 19246.33 65.24 o 3 1 2 63284.36 67427.39 362.69 o 5 1 2 23701.74 24317.36 122.69 o 7 1 2 3383.85 3569.41 19.75 o 9 1 2 1485.08 1383.12 14.96 o 11 1 2 7927.48 8746.97 36.51 o 13 1 2 7506.75 7482.96 37.71 o 15 1 2 19.98 22.74 5.39 o 17 1 2 323.99 242.39 6.58 o 19 1 2 5476.37 5583.34 38.90 o 21 1 2 184.05 140.05 8.38 o 23 1 2 59.95 55.06 7.78 o 25 1 2 191.35 172.37 13.77 o 27 1 2 52.31 32.92 11.97 o 29 1 2 74.14 49.67 13.17 o 31 1 2 3.33 0.00 13.17 o 33 1 2 713.17 789.41 33.52 o -32 2 2 104.96 79.00 14.36 o -30 2 2 117.59 102.94 9.58 o -28 2 2 9.79 -15.56 7.78 o -26 2 2 125.78 104.74 9.58 o -24 2 2 1.16 11.37 10.77 o -22 2 2 548.36 534.45 18.55 o -20 2 2 391.64 440.49 15.56 o -18 2 2 2550.79 2586.09 25.74 o -16 2 2 655.76 663.13 13.17 o -14 2 2 840.03 888.76 20.35 o -12 2 2 783.13 794.20 15.56 o -10 2 2 2349.51 2503.50 49.67 o -8 2 2 1.03 20.35 10.17 o -6 2 2 284.95 311.22 12.57 o -4 2 2 1390.53 1238.28 33.52 o -2 2 2 852.86 920.48 46.08 o 0 2 2 734.23 675.10 12.57 o 2 2 2 22.86 6.58 5.98 o 4 2 2 9177.35 9922.41 92.77 o 6 2 2 132.45 94.56 5.39 o 8 2 2 4744.22 5248.18 29.33 o 10 2 2 204.90 216.65 7.18 o 12 2 2 315.02 362.69 17.95 o 14 2 2 183.42 144.84 7.78 o 16 2 2 1464.05 1474.09 19.15 o 18 2 2 993.81 989.91 23.94 o 20 2 2 0.01 -3.59 7.18 o 22 2 2 216.68 183.14 10.17 o 24 2 2 396.30 360.29 10.77 o 26 2 2 348.63 375.25 11.37 o 28 2 2 145.54 158.00 11.97 o 30 2 2 642.08 669.11 17.95 o 32 2 2 171.70 183.74 16.76 o -31 3 2 283.12 308.82 17.36 o -29 3 2 133.73 110.12 11.97 o -27 3 2 158.14 137.05 12.57 o -25 3 2 6.61 4.79 9.58 o -23 3 2 467.66 520.09 20.35 o -21 3 2 21.27 38.90 11.37 o -19 3 2 566.78 563.78 22.74 o -17 3 2 347.21 372.86 13.17 o -15 3 2 3250.08 3155.85 57.46 o -13 3 2 6259.98 6652.25 154.41 o -11 3 2 83.67 153.21 8.98 o -9 3 2 284.72 336.35 10.17 o -7 3 2 151.85 200.50 12.57 o -5 3 2 24.72 149.62 13.17 o -3 3 2 6095.36 7138.82 45.49 o -1 3 2 5.65 74.81 10.17 o 1 3 2 604.71 730.16 14.96 o 3 3 2 4118.52 4301.37 32.92 o 5 3 2 996.07 1146.11 20.35 o 7 3 2 111.05 127.48 8.98 o 9 3 2 113.46 110.72 6.58 o 11 3 2 80.08 162.19 9.58 o 13 3 2 2134.37 2218.01 35.31 o 15 3 2 1159.29 1172.45 27.53 o 17 3 2 946.53 968.96 22.14 o 19 3 2 482.41 484.18 14.36 o 21 3 2 320.32 284.88 11.97 o 23 3 2 19.25 14.36 9.58 o 25 3 2 103.22 83.19 10.77 o 27 3 2 305.12 344.13 14.36 o 29 3 2 1071.44 1036.59 25.74 o 31 3 2 73.88 99.35 21.55 o -28 4 2 60.83 79.00 20.35 o -26 4 2 9.76 16.76 13.17 o -24 4 2 6.71 10.17 12.57 o -22 4 2 1.57 -1.20 11.37 o -20 4 2 100.04 111.92 13.17 o -18 4 2 477.52 414.76 16.76 o -16 4 2 90.70 123.89 10.77 o -14 4 2 668.94 697.84 14.96 o -12 4 2 789.82 837.89 15.56 o -10 4 2 718.45 794.20 14.96 o -8 4 2 2.89 23.34 8.98 o -6 4 2 72.10 111.32 13.17 o -4 4 2 1817.04 1908.59 25.74 o -2 4 2 278.63 328.57 13.77 o 0 4 2 237.21 278.90 13.77 o 2 4 2 1047.62 1139.53 20.35 o 4 4 2 724.42 737.34 17.36 o 6 4 2 32.74 34.11 8.98 o 8 4 2 1971.91 1966.05 21.55 o 10 4 2 5390.46 5264.94 38.30 o 12 4 2 1846.43 1855.93 28.13 o 14 4 2 1386.13 1459.13 26.33 o 16 4 2 1.62 13.77 12.57 o 18 4 2 8.17 38.30 12.57 o 20 4 2 355.06 340.54 16.76 o 22 4 2 93.63 108.93 14.36 o 24 4 2 254.65 286.08 17.36 o 26 4 2 349.26 417.75 19.75 o -23 5 2 438.64 478.20 28.13 o -21 5 2 89.05 114.31 14.96 o -19 5 2 1.30 1.20 13.17 o -17 5 2 0.00 85.58 14.36 o -15 5 2 38.85 58.65 13.17 o -13 5 2 1166.26 1086.86 20.95 o -11 5 2 779.86 713.40 16.16 o -9 5 2 435.77 463.83 16.16 o -7 5 2 612.44 654.15 19.75 o -5 5 2 25.81 91.57 13.17 o -3 5 2 577.23 567.37 17.95 o -1 5 2 136.43 139.45 13.77 o 1 5 2 1.97 25.74 11.37 o 3 5 2 0.55 24.54 11.97 o 5 5 2 1106.82 1042.57 19.75 o 7 5 2 136.46 301.04 13.77 o 9 5 2 497.90 453.06 17.95 o 11 5 2 0.71 17.95 11.97 o 13 5 2 322.39 289.07 16.16 o 15 5 2 12.33 10.17 13.17 o 17 5 2 17.21 23.94 13.77 o 19 5 2 109.14 109.52 15.56 o 21 5 2 67.32 86.78 20.35 o -14 6 2 389.42 369.27 25.14 o -12 6 2 270.62 177.15 15.56 o -10 6 2 17.00 22.14 10.77 o -8 6 2 445.18 408.77 14.96 o -6 6 2 417.21 447.07 19.75 o -4 6 2 51.30 68.23 13.77 o -2 6 2 439.65 400.99 17.95 o 0 6 2 294.48 270.52 16.16 o 2 6 2 111.76 95.16 13.77 o 4 6 2 65.33 47.88 10.77 o 6 6 2 5.52 -5.39 13.17 o 8 6 2 102.57 117.90 14.96 o 10 6 2 0.11 1.80 13.17 o 12 6 2 229.89 241.19 23.34 o -35 1 3 432.30 431.51 28.13 o -33 1 3 68.62 76.61 13.77 o -31 1 3 675.92 590.11 20.35 o -29 1 3 219.53 188.53 13.17 o -27 1 3 31.85 20.35 13.17 o -25 1 3 679.75 657.74 16.16 o -23 1 3 652.88 603.28 14.96 o -21 1 3 779.44 693.05 11.97 o -19 1 3 2354.17 2323.95 23.34 o -17 1 3 1966.66 1894.23 23.94 o -15 1 3 98.37 141.24 7.78 o -13 1 3 455.31 472.21 7.78 o -11 1 3 6064.25 6199.79 44.29 o -9 1 3 5897.17 6222.53 44.89 o -7 1 3 30472.46 30337.00 177.15 o -5 1 3 92014.31 90645.91 404.58 o -3 1 3 1461.88 1298.73 18.55 o -1 1 3 15618.50 15436.92 88.58 o 1 1 3 2799.83 2709.98 17.95 o 3 1 3 148.98 118.50 5.98 o 5 1 3 2125.99 2061.21 13.77 o 7 1 3 1769.66 1746.40 11.97 o 9 1 3 15317.73 15567.39 108.93 o 11 1 3 5068.22 5251.77 26.93 o 13 1 3 355.85 324.38 8.38 o 15 1 3 3830.73 3736.99 22.74 o 17 1 3 46.42 61.05 6.58 o 19 1 3 1337.84 1222.72 16.16 o 21 1 3 424.06 352.51 10.17 o 23 1 3 180.95 191.52 10.77 o 25 1 3 660.80 564.38 18.55 o 27 1 3 88.39 55.66 13.17 o 29 1 3 101.63 129.27 14.36 o 31 1 3 0.20 4.79 13.17 o 33 1 3 19.56 66.43 20.95 o -32 2 3 181.78 145.43 14.96 o -30 2 3 106.33 79.60 10.77 o -28 2 3 120.71 104.14 8.98 o -26 2 3 173.86 143.64 10.17 o -24 2 3 1689.89 1613.54 23.34 o -22 2 3 4104.63 4008.70 35.91 o -20 2 3 2745.97 2668.08 34.71 o -18 2 3 378.83 439.89 14.96 o -16 2 3 420.02 435.70 10.77 o -14 2 3 2697.78 2700.40 31.12 o -12 2 3 145.75 194.51 10.17 o 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