#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/24/2012485.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012485_Fobs loop_ _publ_author_name 'Castro, Jes\'us' 'P\'erez Lourido, Paulo' 'Sousa-Pedrares, Antonio' 'Labisbal, Elena' 'Carabel, Maximiliano' 'Garc\'ia-V\'azquez, Jos\'e Arturo' _publ_section_title ; catena-Poly[[[tetrakis(1-methylimidazole-\kN^3^)copper(II)]-\m^2^-sulfato-\k^2^O:O'] acetonitrile hemisolvate sesquihydrate] ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m65 _journal_page_last m67 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.650 _cell_angle_gamma 90.000 _cell_length_a 18.6227 _cell_length_b 14.2708 _cell_length_c 17.5255 _exptl_crystal_F_000 2232.00 _reflns_d_resolution_high 0.7502 _[local]_cod_data_source_file bm1479Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title MeImCuII _shelx_refln_list_code 4 _shelx_f_calc_maximum 590.91 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 110.91 -0.91 12.44 o 2 0 0 207666.88 182111.03 5018.86 o 3 0 0 77.82 92.80 17.38 o 4 0 0 7111.27 7353.26 160.73 o 5 0 0 5106.61 4967.06 104.74 o 6 0 0 10584.08 11424.48 227.50 o 7 0 0 1607.05 1697.16 43.73 o 8 0 0 841.01 669.78 24.92 o 9 0 0 13794.33 14446.71 286.14 o 10 0 0 5084.58 4625.07 142.18 o 11 0 0 1041.76 1011.05 33.19 o 12 0 0 8149.45 7949.26 164.42 o 13 0 0 30.14 17.11 25.45 o 14 0 0 20869.87 21465.26 617.96 o 15 0 0 628.84 678.92 49.03 o 16 0 0 2728.56 2761.41 107.25 o 17 0 0 3006.99 3017.31 115.45 o 18 0 0 250.69 318.89 42.36 o 19 0 0 3265.49 3588.75 134.90 o 20 0 0 1849.39 1929.30 90.37 o 21 0 0 2660.04 2856.77 117.34 o 22 0 0 645.69 661.81 57.77 o 23 0 0 1782.73 1699.67 89.63 o 24 0 0 505.51 491.53 56.45 o 1 1 0 5878.59 4143.24 293.38 o 2 1 0 912.61 962.19 19.67 o 3 1 0 10272.39 10989.43 154.26 o 4 1 0 340.19 417.41 13.12 o 5 1 0 7903.34 7686.99 110.65 o 6 1 0 992.53 1068.44 22.36 o 7 1 0 390.95 434.74 19.20 o 8 1 0 755.04 723.33 16.09 o 9 1 0 5888.34 6498.86 96.01 o 10 1 0 115.43 81.40 10.51 o 11 1 0 1872.47 1960.23 35.82 o 12 1 0 396.51 495.11 24.38 o 13 1 0 245.23 195.71 22.43 o 14 1 0 39.88 61.57 20.05 o 15 1 0 1797.23 1842.12 68.75 o 16 1 0 2033.65 1968.65 60.38 o 17 1 0 1033.06 1048.40 43.57 o 18 1 0 402.28 387.52 45.80 o 19 1 0 1591.70 1692.88 59.04 o 20 1 0 798.65 841.63 72.78 o 21 1 0 1015.48 1048.74 48.02 o 22 1 0 239.17 228.41 31.45 o 23 1 0 34.27 52.71 28.65 o 24 1 0 14.19 -24.91 24.91 o 0 2 0 2587.55 2769.34 52.85 o 1 2 0 12535.13 11871.23 170.46 o 2 2 0 4306.29 4406.57 60.70 o 3 2 0 2556.82 2686.41 39.83 o 4 2 0 111.88 71.05 8.90 o 5 2 0 3032.75 3000.53 48.17 o 6 2 0 612.25 627.80 19.77 o 7 2 0 7085.62 6945.09 101.62 o 8 2 0 4652.17 4752.12 72.62 o 9 2 0 3931.40 3941.07 62.08 o 10 2 0 2366.77 2262.03 34.96 o 11 2 0 1533.96 1643.15 27.80 o 12 2 0 28.50 19.99 12.91 o 13 2 0 1944.22 1940.78 56.68 o 14 2 0 193.71 169.06 24.64 o 15 2 0 13.06 7.59 18.76 o 16 2 0 841.23 821.46 66.08 o 17 2 0 2640.08 2612.43 73.71 o 18 2 0 56.57 80.16 25.74 o 19 2 0 918.06 901.45 43.28 o 20 2 0 17.50 8.69 31.16 o 21 2 0 348.75 311.01 33.75 o 22 2 0 70.32 70.59 27.90 o 23 2 0 49.52 29.43 27.47 o 24 2 0 133.53 75.98 30.68 o 1 3 0 14101.83 14469.45 206.76 o 2 3 0 330.43 419.20 12.12 o 3 3 0 73.70 81.47 8.31 o 4 3 0 6232.64 6479.06 87.07 o 5 3 0 4707.90 4245.02 59.87 o 6 3 0 77.83 115.48 18.66 o 7 3 0 4692.11 4521.26 69.50 o 8 3 0 20134.34 20545.29 284.39 o 9 3 0 3736.55 3719.26 59.46 o 10 3 0 3631.53 3670.29 59.11 o 11 3 0 8378.36 8976.25 130.41 o 12 3 0 5128.64 4875.23 93.91 o 13 3 0 540.14 523.55 29.94 o 14 3 0 12589.58 12729.81 267.16 o 15 3 0 2334.31 2137.78 62.45 o 16 3 0 384.94 430.60 37.17 o 17 3 0 1262.41 1290.75 48.12 o 18 3 0 136.10 84.59 25.09 o 19 3 0 2964.02 2957.49 83.45 o 20 3 0 1211.95 1299.87 51.84 o 21 3 0 3553.26 3817.75 111.65 o 22 3 0 584.42 623.54 40.36 o 23 3 0 924.28 925.52 104.38 o 24 3 0 253.78 283.50 34.56 o 0 4 0 183190.61 159609.69 2591.02 o 1 4 0 5.37 18.71 7.85 o 2 4 0 42285.73 40674.05 567.96 o 3 4 0 12573.82 12322.52 158.98 o 4 4 0 24384.95 23755.90 299.91 o 5 4 0 1631.14 1393.94 25.26 o 6 4 0 8714.67 8442.35 112.17 o 7 4 0 165.25 116.78 10.65 o 8 4 0 4723.41 4559.23 65.06 o 9 4 0 789.79 821.80 21.23 o 10 4 0 675.39 778.46 31.93 o 11 4 0 67.79 122.42 12.53 o 12 4 0 3751.74 3695.21 71.38 o 13 4 0 286.29 265.46 24.43 o 14 4 0 6023.26 6002.73 136.51 o 15 4 0 410.00 389.66 30.51 o 16 4 0 1027.71 1041.37 105.52 o 17 4 0 4134.62 4044.71 101.50 o 18 4 0 1819.38 1902.21 60.88 o 19 4 0 5679.96 5734.73 142.18 o 20 4 0 230.56 237.85 30.60 o 21 4 0 1704.39 1733.44 134.96 o 22 4 0 6.40 21.12 37.78 o 23 4 0 1516.29 1706.27 91.18 o 24 4 0 160.09 231.47 72.63 o 1 5 0 3338.56 3253.82 49.04 o 2 5 0 16271.53 15388.65 220.76 o 3 5 0 9.92 -1.33 7.55 o 4 5 0 711.24 596.28 19.20 o 5 5 0 564.34 659.03 16.72 o 6 5 0 2884.39 3093.15 46.78 o 7 5 0 1.91 21.17 9.48 o 8 5 0 36.58 57.86 10.36 o 9 5 0 661.30 798.86 21.17 o 10 5 0 2735.20 2831.21 48.60 o 11 5 0 2242.34 2341.36 42.36 o 12 5 0 4926.94 5179.87 74.33 o 13 5 0 4202.96 4371.71 74.13 o 14 5 0 773.47 842.31 38.34 o 15 5 0 576.78 537.46 27.04 o 16 5 0 43.80 7.68 17.44 o 17 5 0 73.61 81.38 24.90 o 18 5 0 170.65 201.28 25.95 o 19 5 0 596.47 674.01 45.98 o 20 5 0 278.63 320.97 66.18 o 21 5 0 594.95 622.45 43.07 o 22 5 0 3.63 30.15 29.19 o 23 5 0 672.51 651.96 66.69 o 0 6 0 5427.47 5691.35 102.56 o 1 6 0 20649.89 22392.65 263.50 o 2 6 0 3619.82 3470.97 57.48 o 3 6 0 24482.42 24749.28 350.29 o 4 6 0 78.55 38.34 9.14 o 5 6 0 23143.79 23707.34 300.25 o 6 6 0 231.60 300.97 13.00 o 7 6 0 23235.46 22811.07 289.80 o 8 6 0 940.28 852.60 20.37 o 9 6 0 1967.43 1801.78 53.93 o 10 6 0 1869.84 1963.46 34.54 o 11 6 0 4693.56 4462.33 65.50 o 12 6 0 290.70 324.38 15.26 o 13 6 0 206.05 205.34 16.71 o 14 6 0 451.08 511.45 27.16 o 15 6 0 628.26 537.33 27.74 o 16 6 0 327.60 289.85 23.77 o 17 6 0 1653.57 1427.78 55.74 o 18 6 0 97.50 92.76 27.16 o 19 6 0 260.87 276.27 32.63 o 20 6 0 12.74 38.34 28.51 o 21 6 0 85.08 88.03 34.09 o 22 6 0 43.59 95.10 31.12 o 23 6 0 68.43 67.68 30.64 o 1 7 0 1202.98 1275.98 25.43 o 2 7 0 598.12 619.09 21.19 o 3 7 0 3217.88 3406.51 57.39 o 4 7 0 1171.43 1253.31 38.37 o 5 7 0 21.28 60.21 9.85 o 6 7 0 161.15 198.98 11.95 o 7 7 0 911.01 1115.12 23.44 o 8 7 0 17993.07 19546.81 250.39 o 9 7 0 56.93 87.36 13.52 o 10 7 0 3364.11 3398.07 52.48 o 11 7 0 37.88 34.35 11.32 o 12 7 0 1428.10 1447.70 36.68 o 13 7 0 89.64 113.15 19.03 o 14 7 0 819.79 768.46 39.58 o 15 7 0 1439.01 1321.24 69.19 o 16 7 0 1459.12 1429.10 55.18 o 17 7 0 7.16 9.86 24.91 o 18 7 0 2.92 13.11 36.04 o 19 7 0 679.79 635.30 41.38 o 20 7 0 77.33 63.64 28.58 o 21 7 0 399.11 321.72 37.78 o 22 7 0 255.29 247.65 35.71 o 23 7 0 417.34 467.38 42.52 o 0 8 0 276.47 335.38 17.11 o 1 8 0 6191.07 6197.29 87.86 o 2 8 0 7115.29 7328.69 111.74 o 3 8 0 4350.02 3771.50 63.05 o 4 8 0 92.59 104.84 13.30 o 5 8 0 9048.68 8847.84 133.32 o 6 8 0 1867.14 1729.64 41.09 o 7 8 0 7873.13 7941.84 121.36 o 8 8 0 25.09 21.33 14.91 o 9 8 0 8608.60 8513.49 141.83 o 10 8 0 1206.17 1321.10 31.56 o 11 8 0 1170.77 1029.81 32.81 o 12 8 0 549.87 493.14 20.92 o 13 8 0 323.18 341.54 48.40 o 14 8 0 2682.78 2533.61 101.89 o 15 8 0 1828.75 1891.78 64.63 o 16 8 0 2058.52 2041.88 68.57 o 17 8 0 1927.63 1950.43 67.81 o 18 8 0 266.87 312.98 34.11 o 19 8 0 2559.53 2239.80 75.45 o 20 8 0 12.16 62.77 27.85 o 21 8 0 1213.52 1024.85 52.32 o 22 8 0 73.16 121.63 33.70 o 1 9 0 250.27 253.84 16.60 o 2 9 0 3128.09 2986.31 61.31 o 3 9 0 43.59 74.68 12.47 o 4 9 0 1416.63 1628.74 34.39 o 5 9 0 2491.12 2396.78 45.27 o 6 9 0 360.75 380.45 24.87 o 7 9 0 2290.99 2304.13 49.47 o 8 9 0 38.74 44.59 13.34 o 9 9 0 3876.92 3622.20 63.23 o 10 9 0 5839.41 5652.12 91.45 o 11 9 0 29.51 61.82 14.80 o 12 9 0 11718.83 11825.35 177.01 o 13 9 0 599.51 602.71 36.61 o 14 9 0 3393.30 3369.65 94.29 o 15 9 0 1484.95 1511.45 56.92 o 16 9 0 3134.75 3140.08 91.51 o 17 9 0 2557.38 2806.68 85.85 o 18 9 0 96.78 125.86 32.33 o 19 9 0 1264.66 1282.56 56.25 o 20 9 0 12.54 -0.30 27.88 o 21 9 0 283.53 276.18 49.45 o 0 10 0 225.49 235.06 35.58 o 1 10 0 384.04 514.01 29.68 o 2 10 0 1.64 15.84 17.61 o 3 10 0 2931.54 2851.95 60.18 o 4 10 0 106.54 79.97 13.74 o 5 10 0 3101.87 3155.05 56.37 o 6 10 0 384.12 312.23 36.67 o 7 10 0 8144.23 8124.98 148.46 o 8 10 0 84.77 64.12 14.86 o 9 10 0 2318.82 2224.14 52.36 o 10 10 0 27.22 -2.60 13.82 o 11 10 0 7255.77 7223.60 140.54 o 12 10 0 623.00 579.45 27.93 o 13 10 0 1023.57 937.60 34.30 o 14 10 0 3258.16 3221.51 91.60 o 15 10 0 397.54 397.88 46.29 o 16 10 0 1245.78 1311.86 53.86 o 17 10 0 396.96 366.73 35.88 o 18 10 0 77.63 5.51 25.89 o 19 10 0 18.63 21.29 26.36 o 20 10 0 308.51 318.45 36.67 o 21 10 0 411.71 420.73 40.21 o 1 11 0 1186.67 1245.93 36.76 o 2 11 0 4974.93 4816.62 143.27 o 3 11 0 5170.95 5343.46 104.68 o 4 11 0 1457.49 1395.71 49.81 o 5 11 0 9997.32 9876.40 173.92 o 6 11 0 2004.06 2013.03 47.59 o 7 11 0 947.78 892.00 28.00 o 8 11 0 13.32 -11.38 15.39 o 9 11 0 3976.11 3830.43 77.93 o 10 11 0 12.27 23.35 21.58 o 11 11 0 1776.92 1634.93 38.31 o 12 11 0 198.15 207.79 22.30 o 13 11 0 9.86 16.42 17.84 o 14 11 0 305.68 286.55 32.59 o 15 11 0 882.22 875.22 54.25 o 16 11 0 768.68 796.18 52.08 o 17 11 0 1196.38 1167.55 59.13 o 18 11 0 1196.13 1330.89 69.60 o 19 11 0 361.93 397.71 80.48 o 20 11 0 502.26 461.49 70.94 o 0 12 0 1057.17 1102.60 51.76 o 1 12 0 1319.83 1378.17 42.86 o 2 12 0 940.66 914.47 41.19 o 3 12 0 4426.18 4353.63 87.10 o 4 12 0 285.34 270.23 29.04 o 5 12 0 5332.52 5434.41 104.53 o 6 12 0 1496.33 1636.63 44.60 o 7 12 0 1917.94 1896.98 79.36 o 8 12 0 53.53 79.00 19.66 o 9 12 0 3354.50 3395.05 73.08 o 10 12 0 1584.88 1612.87 44.95 o 11 12 0 3467.54 3345.73 81.86 o 12 12 0 203.18 255.11 23.48 o 13 12 0 2336.41 2286.00 95.64 o 14 12 0 44.02 42.17 68.43 o 15 12 0 727.18 753.62 42.61 o 16 12 0 5.17 19.50 25.35 o 17 12 0 80.05 39.90 27.80 o 18 12 0 13.05 20.78 27.95 o 19 12 0 93.05 166.83 33.08 o 1 13 0 884.52 798.23 53.40 o 2 13 0 85.99 116.45 20.06 o 3 13 0 1485.31 1445.17 52.53 o 4 13 0 298.22 260.25 24.70 o 5 13 0 1400.09 1252.56 66.21 o 6 13 0 88.58 82.51 20.20 o 7 13 0 1169.61 1275.83 40.12 o 8 13 0 414.21 390.77 26.56 o 9 13 0 2863.47 2802.05 130.87 o 10 13 0 137.54 143.19 28.12 o 11 13 0 80.07 79.51 25.74 o 12 13 0 484.82 443.44 35.36 o 13 13 0 15.09 15.92 24.74 o 14 13 0 1392.63 1580.26 95.79 o 15 13 0 186.03 299.03 59.33 o 16 13 0 508.54 634.90 67.60 o 17 13 0 1360.19 1417.44 60.34 o 18 13 0 4.06 31.09 30.32 o 0 14 0 442.02 365.18 43.41 o 1 14 0 1235.92 1045.94 39.74 o 2 14 0 793.06 693.55 31.83 o 3 14 0 433.78 418.91 28.13 o 4 14 0 1397.82 1400.86 52.15 o 5 14 0 807.57 760.11 39.25 o 6 14 0 1625.34 1596.24 67.69 o 7 14 0 223.51 172.14 22.35 o 8 14 0 1524.62 1420.76 43.55 o 9 14 0 59.73 31.58 20.22 o 10 14 0 225.88 187.00 25.46 o 11 14 0 349.91 341.63 32.17 o 12 14 0 1010.90 1044.27 49.53 o 13 14 0 939.71 917.18 48.91 o 14 14 0 595.41 495.91 60.35 o 15 14 0 533.80 462.12 61.98 o 16 14 0 492.95 572.99 67.67 o 1 15 0 87.42 73.83 24.64 o 2 15 0 53.42 63.07 21.11 o 3 15 0 809.04 781.38 34.59 o 4 15 0 0.68 -12.68 18.93 o 5 15 0 534.69 524.99 30.09 o 6 15 0 95.00 81.73 31.54 o 7 15 0 691.43 735.86 33.25 o 8 15 0 486.35 487.62 41.41 o 9 15 0 9.02 3.57 20.61 o 10 15 0 171.31 174.68 32.35 o 11 15 0 103.67 114.60 23.40 o 12 15 0 1152.06 1252.96 71.79 o 13 15 0 9.24 16.75 28.18 o 14 15 0 1191.24 1478.09 96.40 o 15 15 0 497.50 471.88 63.60 o 0 16 0 1208.53 1188.14 67.91 o 1 16 0 28.87 64.10 25.95 o 2 16 0 453.64 462.63 56.22 o 3 16 0 904.29 961.75 38.06 o 4 16 0 21.47 31.52 20.69 o 5 16 0 915.01 943.99 38.27 o 6 16 0 329.00 302.89 27.50 o 7 16 0 243.15 257.94 30.90 o 8 16 0 949.00 1074.92 42.33 o 9 16 0 835.54 910.32 38.25 o 10 16 0 228.97 218.07 28.82 o 11 16 0 397.99 429.00 39.89 o 12 16 0 4.45 9.93 36.22 o 13 16 0 53.85 79.16 48.12 o 1 17 0 327.79 290.43 59.25 o 2 17 0 50.76 45.50 25.93 o 3 17 0 696.95 744.83 41.67 o 4 17 0 193.49 165.70 25.40 o 5 17 0 85.28 80.98 34.62 o 6 17 0 67.53 16.80 22.08 o 7 17 0 208.99 211.27 29.51 o 8 17 0 38.41 29.42 26.51 o 9 17 0 89.21 76.04 23.68 o 10 17 0 47.28 23.83 27.73 o 11 17 0 645.68 720.70 47.16 o 0 18 0 232.67 286.36 48.39 o 1 18 0 66.92 48.83 26.94 o 2 18 0 743.54 702.50 79.53 o 3 18 0 8.28 -24.29 24.29 o 4 18 0 484.73 450.91 32.43 o 5 18 0 78.73 34.35 34.01 o 6 18 0 539.53 525.88 33.47 o 7 18 0 153.83 210.78 30.08 o -24 1 1 491.97 472.23 39.02 o -23 1 1 577.16 517.30 39.21 o -22 1 1 1209.42 1178.42 53.49 o -21 1 1 668.25 663.58 39.85 o -20 1 1 3540.47 3431.80 93.01 o -19 1 1 321.35 325.73 33.77 o -18 1 1 2162.89 2103.32 64.99 o -17 1 1 255.09 199.19 25.89 o -16 1 1 434.59 462.21 53.01 o -15 1 1 2891.19 2930.61 77.85 o -14 1 1 775.32 680.24 46.59 o -13 1 1 424.18 430.45 26.88 o -12 1 1 149.87 171.19 21.43 o -11 1 1 5355.27 5172.11 92.33 o -10 1 1 433.90 453.60 16.18 o -9 1 1 1247.40 1543.02 29.29 o -8 1 1 1823.45 1723.82 31.39 o -7 1 1 253.97 191.37 10.73 o -6 1 1 5118.84 5164.52 76.90 o -5 1 1 2086.02 2016.59 34.51 o -4 1 1 8111.34 8083.54 115.49 o -3 1 1 7069.10 6984.54 100.52 o -2 1 1 79.14 61.65 7.90 o -1 1 1 670.89 770.38 24.99 o 0 1 1 201.52 203.28 8.49 o 1 1 1 521.67 615.58 21.07 o 2 1 1 4427.56 4510.88 132.81 o 3 1 1 6752.28 7068.22 116.89 o 4 1 1 1786.08 1747.37 31.10 o 5 1 1 19187.48 18669.60 258.04 o 6 1 1 115.62 68.65 9.60 o 7 1 1 89.32 158.86 9.67 o 8 1 1 158.73 278.13 11.58 o 9 1 1 688.86 534.14 16.73 o 10 1 1 5696.74 5952.46 89.40 o 11 1 1 21813.07 22322.84 308.97 o 12 1 1 2326.42 2349.23 41.79 o 13 1 1 1612.42 1638.24 51.09 o 14 1 1 1199.87 1151.81 42.58 o 15 1 1 189.06 170.00 27.02 o 16 1 1 2081.88 2244.37 92.81 o 17 1 1 29.25 -10.25 19.19 o 18 1 1 1209.60 1200.33 48.21 o 19 1 1 64.70 52.82 24.99 o 20 1 1 3046.01 3058.73 85.95 o 21 1 1 1236.23 1314.00 161.12 o 22 1 1 2615.61 2820.55 84.48 o 23 1 1 679.41 650.01 61.03 o 24 1 1 1285.76 1334.18 57.20 o -24 2 1 446.31 531.46 41.59 o -23 2 1 780.25 819.14 45.51 o -22 2 1 3041.87 3189.76 145.64 o -21 2 1 984.72 954.07 68.84 o -20 2 1 2716.80 2651.30 77.69 o -19 2 1 1112.13 1224.59 85.53 o -18 2 1 6319.17 6195.65 148.59 o -17 2 1 317.23 279.85 44.93 o -16 2 1 1957.12 1919.64 59.69 o -15 2 1 303.77 266.92 26.51 o -14 2 1 3658.05 3691.44 91.28 o -13 2 1 1081.44 1052.77 39.21 o -12 2 1 2765.38 2488.61 51.23 o -11 2 1 585.58 707.85 18.94 o -10 2 1 37520.23 37256.48 448.54 o -9 2 1 3910.81 3943.87 86.75 o -8 2 1 9281.15 7862.34 113.99 o -7 2 1 8874.87 9072.97 129.91 o -6 2 1 128941.77 119883.93 1614.03 o -5 2 1 12742.19 13119.50 183.57 o -4 2 1 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