#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:38:41 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180794 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/25/2012533.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012533_Fobs loop_ _publ_author_name 'Moisan, Lionel' 'Le Borgne, Thierry' 'Thu\'ery, Pierre' 'Ephritikhine, Michel' _publ_section_title ; An ion pair formed by protonated Fe(cp*py)~2~ and the octanuclear cluster U~8~Cl~24~O~4~(cp*py)~2~ [cp*py is tetramethyl-5-(2-pyridyl)cyclopentadiene] ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m98 _journal_page_last m101 _journal_volume 58 _journal_year 2002 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 61.128 _cell_angle_beta 70.648 _cell_angle_gamma 83.316 _cell_length_a 14.3894 _cell_length_b 15.9758 _cell_length_c 16.0646 _exptl_crystal_F_000 2040.00 _reflns_d_resolution_high 0.8200 _cod_data_source_file tr1004Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' (I) in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 508.70 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2189.20 1854.38 204.71 o 3 0 0 6051.02 5265.89 256.45 o 4 0 0 7981.16 7520.77 595.16 o 5 0 0 101921.62 108976.58 4305.06 o 6 0 0 36210.02 38575.13 1525.15 o 7 0 0 832.80 1583.08 444.37 o 8 0 0 21300.15 17674.20 3347.27 o 9 0 0 5259.32 5289.02 366.98 o 10 0 0 327.20 218.69 399.44 o 11 0 0 6464.26 7055.33 1058.50 o 12 0 0 8585.24 9556.10 764.42 o 13 0 0 2546.78 2073.55 467.70 o 14 0 0 331.66 197.35 368.92 o 15 0 0 1357.50 1459.74 459.20 o 16 0 0 3175.35 2720.94 728.19 o -16 1 0 1188.62 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