#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/25/2012535.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012535_Fobs loop_ _publ_author_name 'Comerlato, Nadia M.' 'Harrison, William T. A.' 'Howie, R. Alan' 'Low, John Nicolson' 'Silvino, Alexandre C.' 'Wardell, James L.' 'Wardell, Solange M. S. V.' _publ_section_title ; Bis(tetra-n-butylammonium) (a redetermination at 150K) and bis(tetraphenylarsonium) bis(1,3-dithiole-2-thione-4,5-dithiolato)zinc(II) (at 300K) ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m105 _journal_page_last m108 _journal_volume 58 _journal_year 2002 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 73.072 _cell_angle_beta 85.867 _cell_angle_gamma 72.259 _cell_length_a 10.3451 _cell_length_b 15.0563 _cell_length_c 18.8083 _exptl_crystal_F_000 1240.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file tr1005IXsup3.hkl _[local]_cod_data_source_block IX #BEGIN Tags that were not found in dictionaries: _shelx_title ' AsPh4 Zn(DMIT)2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 287.39 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1596.16 2094.16 25.04 o 2 0 0 38114.32 39539.42 328.05 o 3 0 0 19754.01 19790.13 411.14 o 4 0 0 57.71 95.53 27.18 o 5 0 0 10733.49 11327.55 83.21 o 6 0 0 2757.34 2672.46 48.05 o 7 0 0 73.36 67.00 24.47 o 8 0 0 588.13 642.61 53.29 o 9 0 0 70.04 50.42 42.38 o 10 0 0 2.76 34.57 44.27 o 11 0 0 65.73 104.75 49.53 o -11 1 0 68.43 67.21 49.51 o -10 1 0 4.33 8.88 44.27 o -9 1 0 595.08 671.89 56.75 o -8 1 0 552.26 599.73 53.07 o -7 1 0 5423.30 5389.36 101.08 o -6 1 0 455.52 383.56 40.27 o -5 1 0 16365.72 16038.89 196.70 o -4 1 0 12691.01 12511.38 743.39 o -3 1 0 932.22 946.22 48.63 o -2 1 0 612.25 565.52 12.35 o -1 1 0 7386.66 7436.35 62.59 o 0 1 0 925.88 813.60 173.31 o 1 1 0 17550.38 18325.48 174.17 o 2 1 0 8532.93 8492.70 97.25 o 3 1 0 176.00 157.03 31.32 o 4 1 0 3270.24 3489.96 120.33 o 5 1 0 2586.35 2458.55 55.93 o 6 1 0 40.65 62.40 20.46 o 7 1 0 5728.33 5419.91 84.62 o 8 1 0 418.20 437.94 50.67 o 9 1 0 497.73 535.53 58.79 o 10 1 0 139.48 186.62 47.64 o 11 1 0 51.94 33.07 45.37 o -11 2 0 71.57 75.29 50.39 o -10 2 0 99.14 159.29 48.66 o -9 2 0 766.20 813.90 59.02 o -8 2 0 15.07 0.02 42.32 o -7 2 0 389.43 425.13 45.99 o -6 2 0 1658.66 1678.23 66.76 o -5 2 0 2863.70 2834.05 81.87 o -4 2 0 1506.73 1436.27 45.28 o -3 2 0 4334.35 4362.16 46.53 o -2 2 0 5039.53 5350.70 93.30 o -1 2 0 4309.54 4427.61 99.38 o 0 2 0 23502.90 24134.73 260.30 o 1 2 0 24865.82 24601.18 211.53 o 2 2 0 7973.77 8224.02 103.29 o 3 2 0 1764.66 1756.01 55.49 o 4 2 0 1792.43 1914.88 59.06 o 5 2 0 15476.30 15394.48 249.17 o 6 2 0 490.17 391.03 47.25 o 7 2 0 735.28 733.20 32.66 o 8 2 0 1927.91 1812.10 47.49 o 9 2 0 5.35 -10.41 40.92 o 10 2 0 518.63 602.53 55.62 o 11 2 0 7.30 -40.70 43.39 o 12 2 0 8.73 1.85 48.84 o -10 3 0 3.13 0.76 46.15 o -9 3 0 35.35 39.43 43.08 o -8 3 0 614.73 630.06 53.43 o -7 3 0 1172.06 1158.42 90.11 o -6 3 0 4210.81 4076.11 122.53 o -5 3 0 311.07 327.15 35.83 o -4 3 0 3060.27 2877.78 62.15 o -3 3 0 2760.77 2967.94 38.79 o -2 3 0 13167.54 12983.25 170.94 o -1 3 0 6.25 34.52 18.06 o 0 3 0 1842.54 1864.20 29.65 o 1 3 0 10344.66 10855.47 160.71 o 2 3 0 2389.57 2477.43 66.48 o 3 3 0 6349.85 6153.18 102.75 o 4 3 0 1515.47 1698.87 63.74 o 5 3 0 383.34 397.40 31.01 o 6 3 0 1832.75 1788.88 70.33 o 7 3 0 959.88 959.14 70.88 o 8 3 0 20.09 5.79 25.19 o 9 3 0 150.24 191.08 48.27 o 10 3 0 188.05 228.42 47.95 o 11 3 0 248.36 308.12 54.19 o 12 3 0 313.34 384.11 58.39 o -10 4 0 0.87 -0.12 46.67 o -9 4 0 769.02 803.77 61.80 o -8 4 0 573.24 619.44 54.73 o -7 4 0 1470.56 1483.73 65.79 o -6 4 0 1018.60 1026.90 53.90 o -5 4 0 581.30 595.40 43.65 o -4 4 0 8926.50 8804.19 128.72 o -3 4 0 1475.62 1586.18 33.86 o -2 4 0 20.38 18.13 18.23 o -1 4 0 2200.03 2234.84 37.75 o 0 4 0 587.89 557.04 30.45 o 1 4 0 9410.07 9621.25 131.87 o 2 4 0 343.69 377.85 30.69 o 3 4 0 14.67 9.89 34.61 o 4 4 0 7734.69 8193.25 138.46 o 5 4 0 3214.62 3282.91 95.60 o 6 4 0 160.89 119.25 28.78 o 7 4 0 278.46 277.19 35.78 o 8 4 0 796.05 774.88 49.05 o 9 4 0 144.34 144.04 38.96 o 10 4 0 10.13 13.20 45.23 o 11 4 0 130.46 219.34 51.32 o 12 4 0 31.10 -11.36 57.42 o -10 5 0 6.73 29.94 45.50 o -9 5 0 36.02 44.04 44.17 o -8 5 0 1040.04 1038.62 61.72 o -7 5 0 1085.69 1052.04 59.53 o -6 5 0 584.76 560.98 48.40 o -5 5 0 2305.94 2079.25 107.14 o -4 5 0 726.39 704.12 45.50 o -3 5 0 4488.18 4179.85 87.09 o -2 5 0 3836.67 3764.88 171.05 o -1 5 0 141.98 139.67 20.84 o 0 5 0 7750.08 7535.02 125.82 o 1 5 0 4215.46 4387.83 101.10 o 2 5 0 604.67 643.92 37.36 o 3 5 0 28118.91 28118.14 515.30 o 4 5 0 904.50 823.06 57.69 o 5 5 0 43.30 70.33 41.76 o 6 5 0 6887.20 6643.83 146.15 o 7 5 0 104.72 63.73 31.42 o 8 5 0 116.67 168.04 36.81 o 9 5 0 723.89 669.68 51.07 o 10 5 0 10.17 8.71 36.02 o 11 5 0 31.51 41.30 50.16 o 12 5 0 0.07 -12.54 48.97 o -9 6 0 389.76 393.08 54.58 o -8 6 0 653.62 660.34 56.84 o -7 6 0 28.43 59.68 38.92 o -6 6 0 456.84 433.77 48.32 o -5 6 0 1026.50 1091.13 64.56 o -4 6 0 6785.11 6807.08 108.32 o -3 6 0 55.12 12.25 33.24 o -2 6 0 14602.65 14339.54 291.75 o -1 6 0 26312.14 26086.21 193.95 o 0 6 0 1812.59 1807.66 74.17 o 1 6 0 5425.99 5237.81 115.38 o 2 6 0 35.79 107.86 43.12 o 3 6 0 859.49 957.32 43.51 o 4 6 0 1044.81 1095.58 66.48 o 5 6 0 310.48 251.09 51.65 o 6 6 0 2409.32 2441.71 98.35 o 7 6 0 2.19 37.36 52.75 o 8 6 0 365.21 375.83 42.06 o 9 6 0 80.92 70.82 34.85 o 10 6 0 392.33 375.67 53.02 o 11 6 0 191.69 280.05 47.71 o 12 6 0 185.33 226.37 74.72 o -9 7 0 2.39 12.99 44.88 o -8 7 0 533.53 529.47 55.58 o -7 7 0 42.37 55.48 40.66 o -6 7 0 2438.47 2356.47 79.30 o -5 7 0 195.71 157.01 43.18 o -4 7 0 29.75 35.06 40.04 o -3 7 0 1473.13 1520.37 61.00 o -2 7 0 5709.58 5346.36 92.06 o -1 7 0 935.45 1003.24 71.15 o 0 7 0 1656.77 1541.73 80.22 o 1 7 0 19748.61 20176.54 251.64 o 2 7 0 526.37 465.38 57.14 o 3 7 0 20663.90 19602.38 253.29 o 4 7 0 9351.96 9430.38 132.69 o 5 7 0 2905.58 2767.53 102.75 o 6 7 0 2430.60 2555.45 106.04 o 7 7 0 16.14 -2.20 56.59 o 8 7 0 940.25 977.45 82.42 o 9 7 0 2.98 -15.18 33.77 o 10 7 0 18.26 21.90 37.30 o 11 7 0 55.66 50.98 40.44 o 12 7 0 75.72 25.82 66.48 o -8 8 0 100.90 143.48 46.32 o -7 8 0 0.29 -4.11 40.40 o -6 8 0 465.09 487.22 50.90 o -5 8 0 11.42 -10.19 41.77 o -4 8 0 6431.51 6368.16 242.58 o -3 8 0 72.86 81.64 41.30 o -2 8 0 1443.18 1358.82 58.42 o -1 8 0 4196.46 4071.90 124.72 o 0 8 0 498.35 556.58 64.28 o 1 8 0 7169.41 7136.13 156.59 o 2 8 0 91.75 82.97 50.55 o 3 8 0 324.62 344.74 52.25 o 4 8 0 3245.49 3050.43 86.54 o 5 8 0 1469.87 1432.81 58.46 o 6 8 0 116.97 173.07 60.44 o 7 8 0 1040.02 923.06 83.51 o 8 8 0 3.97 -32.42 54.94 o 9 8 0 14.56 22.44 35.08 o 10 8 0 50.86 45.41 37.20 o 11 8 0 0.84 14.83 64.28 o 12 8 0 10.22 -0.55 67.58 o -8 9 0 131.94 94.70 46.60 o -7 9 0 319.86 327.07 52.17 o -6 9 0 915.85 883.11 60.67 o -5 9 0 10.03 37.67 39.95 o -4 9 0 235.00 232.48 45.94 o -3 9 0 2129.46 2100.49 73.59 o -2 9 0 1194.95 1224.60 61.74 o -1 9 0 2113.48 1980.73 103.29 o 0 9 0 54.47 28.02 54.94 o 1 9 0 3820.01 3755.97 124.17 o 2 9 0 3341.09 3327.41 120.33 o 3 9 0 1418.03 1323.60 84.06 o 4 9 0 272.69 306.55 44.29 o 5 9 0 103.11 96.14 40.01 o 6 9 0 380.06 349.21 46.15 o 7 9 0 0.32 -31.36 32.44 o 8 9 0 725.55 708.78 79.12 o 9 9 0 603.85 634.05 80.77 o 10 9 0 1138.59 1237.34 101.10 o 11 9 0 413.60 435.16 79.67 o -7 10 0 0.54 -16.85 43.03 o -6 10 0 33.70 48.25 43.56 o -5 10 0 1546.63 1674.47 82.14 o -4 10 0 307.85 284.23 47.74 o -3 10 0 150.73 215.48 53.02 o -2 10 0 379.78 339.00 71.43 o -1 10 0 1351.97 1463.16 103.84 o 0 10 0 556.60 577.46 79.12 o 1 10 0 4739.36 4351.57 146.15 o 2 10 0 37.77 28.02 67.03 o 3 10 0 89.62 106.04 63.19 o 4 10 0 8191.42 7227.89 178.57 o 5 10 0 1128.26 1090.06 63.71 o 6 10 0 3683.60 3655.83 96.52 o 7 10 0 156.76 160.93 44.29 o 8 10 0 708.67 780.03 57.23 o 9 10 0 110.51 98.90 64.83 o 10 10 0 50.22 68.68 66.48 o 11 10 0 112.89 76.37 69.23 o -6 11 0 1298.93 1458.36 78.16 o -5 11 0 28.53 46.95 42.90 o -4 11 0 26.52 46.79 44.66 o -3 11 0 1373.66 1485.14 99.45 o -2 11 0 120.09 107.14 63.19 o 0 11 0 2453.83 2427.43 123.62 o 1 11 0 3176.90 3238.95 140.11 o 2 11 0 7067.25 7396.56 192.30 o 3 11 0 865.11 863.72 86.81 o 4 11 0 932.16 858.78 87.36 o 5 11 0 1063.91 1050.99 75.17 o 6 11 0 927.47 829.14 60.98 o 7 11 0 6.08 19.32 39.97 o 8 11 0 403.27 283.96 45.80 o 9 11 0 1.48 23.03 43.68 o 10 11 0 2.59 -3.63 40.32 o 11 11 0 9.19 23.56 37.22 o -5 12 0 870.10 873.25 66.20 o -4 12 0 34.76 84.61 64.83 o -3 12 0 372.11 410.43 74.72 o -2 12 0 81.47 147.80 70.33 o -1 12 0 590.86 515.37 80.22 o 0 12 0 1596.74 1620.30 111.54 o 1 12 0 348.54 292.30 79.12 o 2 12 0 603.20 600.54 86.81 o 3 12 0 2.66 36.81 67.58 o 4 12 0 243.57 278.57 72.53 o 5 12 0 491.26 429.66 72.53 o 6 12 0 491.23 455.03 52.62 o 7 12 0 637.39 661.98 58.45 o 8 12 0 201.12 236.55 46.04 o 9 12 0 115.07 66.27 43.64 o 10 12 0 336.29 347.53 52.63 o -4 13 0 11.09 1.10 64.28 o -3 13 0 331.56 440.65 83.51 o -2 13 0 128.86 231.31 74.72 o -1 13 0 1693.29 1790.08 117.58 o 0 13 0 55.22 28.02 63.19 o 1 13 0 302.15 346.15 80.22 o 2 13 0 2779.59 2528.52 128.57 o 3 13 0 673.92 854.93 91.21 o 5 13 0 438.24 466.47 79.67 o 6 13 0 380.74 390.10 76.92 o 7 13 0 675.05 664.07 58.85 o 8 13 0 115.32 128.56 47.19 o 9 13 0 54.41 31.54 44.47 o 10 13 0 1.20 -5.15 41.18 o -3 14 0 626.52 849.98 100.00 o -2 14 0 111.43 126.37 72.53 o -1 14 0 51.00 42.31 69.78 o 0 14 0 1113.56 1093.39 102.20 o 1 14 0 4.32 54.39 68.13 o 2 14 0 16.10 -10.99 65.38 o 3 14 0 0.58 6.04 62.64 o 4 14 0 257.29 176.92 70.88 o 5 14 0 37.69 59.34 61.54 o 6 14 0 180.48 212.08 70.88 o 7 14 0 155.57 168.13 71.98 o 8 14 0 2.53 -18.87 58.35 o 9 14 0 36.80 54.14 46.77 o -2 15 0 189.02 231.31 79.67 o -1 15 0 735.87 846.14 102.20 o 0 15 0 22.99 -9.89 74.72 o 1 15 0 42.82 63.74 79.67 o 2 15 0 71.99 50.00 74.17 o 3 15 0 15.33 46.70 69.23 o 4 15 0 18.08 19.78 65.93 o 5 15 0 27.31 29.12 64.83 o 6 15 0 23.22 22.53 62.64 o 7 15 0 198.03 207.14 73.62 o 8 15 0 131.86 84.61 72.53 o 0 16 0 279.85 292.85 84.06 o 1 16 0 85.94 54.39 76.37 o 2 16 0 111.36 197.80 81.32 o 3 16 0 261.94 326.37 88.46 o 4 16 0 347.69 273.07 80.22 o 5 16 0 51.60 106.04 74.72 o 6 16 0 183.54 155.49 75.27 o 7 16 0 22.79 -36.81 62.64 o 3 17 0 37.37 -35.16 71.43 o 4 17 0 17.55 -4.40 71.43 o 5 17 0 119.79 266.48 89.01 o -7 -16 1 192.55 115.38 71.98 o -6 -16 1 209.65 222.52 79.12 o -5 -16 1 3.36 -68.68 68.68 o -4 -16 1 473.55 367.58 83.51 o -3 -16 1 42.99 -68.13 68.13 o -2 -16 1 1047.74 1151.08 119.23 o -1 -16 1 128.57 152.74 76.37 o 0 -16 1 8.90 16.48 72.53 o -8 -15 1 1.17 -39.01 64.28 o -7 -15 1 11.33 -23.08 62.64 o -6 -15 1 809.86 898.33 103.29 o -5 -15 1 1206.05 1129.10 109.89 o -4 -15 1 78.22 9.34 69.78 o -3 -15 1 0.12 -9.89 65.38 o -2 -15 1 57.58 49.45 73.62 o -1 -15 1 892.44 960.42 103.29 o 0 -15 1 212.28 108.24 75.27 o 1 -15 1 483.77 640.65 97.80 o 2 -15 1 154.90 308.24 82.97 o -9 -14 1 54.41 29.85 44.38 o -8 -14 1 1032.24 934.05 102.20 o -7 -14 1 180.15 187.36 72.53 o -6 -14 1 1060.54 1058.77 101.10 o -5 -14 1 316.77 351.09 77.47 o -4 -14 1 2.43 7.14 66.48 o -3 -14 1 2360.59 2180.73 127.47 o -2 -14 1 33.68 32.97 67.03 o -1 -14 1 269.05 304.39 79.67 o 0 -14 1 171.91 225.27 81.87 o 1 -14 1 100.89 72.53 71.98 o 2 -14 1 126.08 146.70 76.92 o 3 -14 1 20.08 51.10 71.43 o -10 -13 1 630.15 624.47 64.30 o -9 -13 1 2.30 -34.37 44.09 o -8 -13 1 999.49 1100.34 101.92 o -7 -13 1 1533.17 1579.64 112.64 o -6 -13 1 100.91 54.94 60.99 o -5 -13 1 1017.86 1019.21 96.15 o -4 -13 1 1316.08 1199.98 101.10 o -3 -13 1 4.69 20.33 64.83 o -2 -13 1 0.93 22.53 70.33 o -1 -13 1 1422.74 1269.21 104.39 o 0 -13 1 42.32 51.65 67.58 o 1 -13 1 1049.95 902.18 97.25 o 2 -13 1 1.06 45.60 68.13 o 3 -13 1 102.43 48.90 64.83 o 4 -13 1 63.84 23.63 64.83 o -10 -12 1 27.05 34.46 44.66 o -9 -12 1 7.01 -18.81 41.73 o -8 -12 1 1066.40 1093.40 67.59 o -7 -12 1 176.11 119.19 42.82 o -6 -12 1 306.75 241.75 70.88 o -5 -12 1 447.34 419.22 71.43 o -4 -12 1 49.10 20.33 66.48 o -3 -12 1 4985.11 4580.13 161.54 o -2 -12 1 546.35 574.71 80.22 o -1 -12 1 2298.53 2201.61 124.17 o 0 -12 1 880.63 960.97 96.15 o 1 -12 1 92.24 140.11 67.03 o 2 -12 1 629.34 652.73 83.51 o 3 -12 1 15.77 -40.11 65.38 o 4 -12 1 16.10 29.12 62.64 o 5 -12 1 43.49 24.72 59.34 o -11 -11 1 42.00 95.18 48.35 o -10 -11 1 1135.79 1118.19 68.57 o -9 -11 1 106.35 146.52 57.14 o -8 -11 1 248.61 189.05 43.90 o -7 -11 1 460.22 446.86 50.10 o -6 -11 1 34.78 11.11 41.55 o -5 -11 1 2016.59 1755.46 109.34 o -4 -11 1 486.53 491.20 75.82 o -3 -11 1 28.01 53.85 65.93 o -2 -11 1 2450.46 2644.46 125.27 o -1 -11 1 123.88 92.31 71.98 o 0 -11 1 135.90 196.15 72.53 o 1 -11 1 86.29 84.06 70.33 o 2 -11 1 0.33 21.98 60.99 o 3 -11 1 5.49 9.89 63.74 o 4 -11 1 230.18 293.40 71.43 o 5 -11 1 115.48 76.48 45.25 o 6 -11 1 7.12 -6.07 42.60 o -11 -10 1 22.59 20.88 62.64 o -10 -10 1 877.64 946.86 74.29 o -9 -10 1 1363.43 1410.52 82.14 o -8 -10 1 244.85 212.79 42.21 o -7 -10 1 2111.66 2015.08 77.11 o -6 -10 1 865.87 775.24 79.67 o -5 -10 1 19.53 0.90 39.32 o -4 -10 1 211.89 166.48 63.19 o -3 -10 1 7195.35 6636.14 171.97 o -2 -10 1 147.70 184.61 69.23 o -1 -10 1 160.59 208.24 70.88 o 0 -10 1 380.77 418.12 81.87 o 1 -10 1 462.63 495.05 80.22 o 2 -10 1 46.26 4.94 65.38 o 3 -10 1 1055.32 1114.26 90.11 o 4 -10 1 1158.77 1247.06 67.09 o 5 -10 1 718.32 725.27 58.06 o 6 -10 1 215.07 165.31 46.18 o 7 -10 1 2.57 -14.08 42.06 o -11 -9 1 5.49 9.34 64.28 o -10 -9 1 1445.99 1526.81 79.67 o -9 -9 1 462.98 468.12 74.72 o -8 -9 1 983.83 984.17 50.43 o -7 -9 1 46.44 18.28 35.16 o -6 -9 1 1758.50 1863.09 79.39 o -5 -9 1 2098.31 1985.97 70.51 o -4 -9 1 1469.83 1398.41 89.28 o -3 -9 1 67.98 68.13 54.94 o -2 -9 1 1398.48 1507.66 91.76 o -1 -9 1 298.12 284.06 64.83 o 0 -9 1 1233.62 1249.98 88.46 o 1 -9 1 612.17 767.02 84.06 o 2 -9 1 122.34 179.12 67.03 o 3 -9 1 908.03 973.08 61.56 o 4 -9 1 113.85 118.36 44.42 o 5 -9 1 56.28 84.63 42.16 o 6 -9 1 340.23 323.75 50.03 o 7 -9 1 35.04 61.88 44.49 o -11 -8 1 202.57 199.45 70.33 o -10 -8 1 456.97 486.15 51.00 o -9 -8 1 171.11 119.23 63.74 o -8 -8 1 886.46 865.37 80.77 o -7 -8 1 2024.51 1902.71 99.45 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