#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2012642.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012642_Fobs loop_ _publ_author_name 'Reuter, Hans' 'Eickmeier, Henning' 'Puff, Heinrich' 'Beckermann, Norbert' 'H\"anssgen, Dieter' _publ_section_title ; Tin--halide compounds. IV. tert-Butyltrichlorotin(IV) ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m217 _journal_page_last m218 _journal_volume 58 _journal_year 2002 _space_group_IT_number 11 _symmetry_space_group_name_Hall '-P 2yb' _symmetry_space_group_name_H-M 'P 1 21/m 1' _cell_angle_alpha 90.000 _cell_angle_beta 112.770 _cell_angle_gamma 90.000 _cell_length_a 7.6320 _cell_length_b 10.3410 _cell_length_c 6.2890 _exptl_crystal_F_000 268.00 _reflns_d_resolution_high 0.8412 _[local]_cod_data_source_file ln1131Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' tert-Butyltrichlorotin(IV)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 116.51 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' '-x, -y, -z' 'x, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 13573.50 13672.88 47.79 o 2 0 0 1603.70 1657.75 5.60 o 3 0 0 2860.45 3086.63 37.51 o 4 0 0 3293.19 3525.48 11.44 o 5 0 0 3088.08 3355.51 12.73 o 6 0 0 1338.30 1350.69 9.05 o 7 0 0 333.54 335.64 5.76 o 8 0 0 45.55 43.15 1.26 o 1 1 0 145.97 179.86 1.10 o 2 1 0 5063.55 4999.56 27.63 o 3 1 0 921.48 1045.78 3.99 o 4 1 0 247.45 255.12 2.62 o 5 1 0 705.61 772.78 4.56 o 6 1 0 1051.78 1147.54 6.49 o 7 1 0 480.50 485.21 4.82 o 8 1 0 87.24 78.80 1.33 o 1 2 0 7350.28 6474.78 28.53 o 2 2 0 11554.10 11652.75 46.10 o 3 2 0 8366.09 9078.99 47.93 o 4 2 0 2298.46 2479.22 6.83 o 5 2 0 620.91 632.09 4.47 o 6 2 0 325.00 348.82 3.83 o 7 2 0 717.17 743.28 5.59 o 8 2 0 476.36 462.53 3.82 o 1 3 0 660.24 566.01 2.61 o 2 3 0 8.95 7.68 0.53 o 3 3 0 1975.68 2026.25 5.56 o 4 3 0 3462.76 3681.66 8.35 o 5 3 0 744.70 814.75 5.07 o 6 3 0 45.78 43.06 0.81 o 7 3 0 119.65 115.24 1.76 o 8 3 0 158.19 149.93 2.17 o 0 4 0 5355.62 5102.95 31.78 o 1 4 0 6559.32 6115.41 37.06 o 2 4 0 7405.52 7285.55 44.00 o 3 4 0 3643.64 3608.66 8.27 o 4 4 0 1541.97 1563.74 5.96 o 5 4 0 839.62 846.44 5.17 o 6 4 0 336.16 331.42 3.98 o 7 4 0 544.41 505.64 3.69 o 1 5 0 1137.44 1313.99 4.97 o 2 5 0 1182.16 1017.24 4.37 o 3 5 0 271.85 256.64 3.06 o 4 5 0 130.45 131.79 2.20 o 5 5 0 187.83 188.27 2.44 o 6 5 0 524.84 509.98 4.94 o 7 5 0 526.67 449.19 3.48 o 0 6 0 9067.25 9181.57 54.76 o 1 6 0 4463.02 4390.34 9.14 o 2 6 0 1124.47 1133.81 5.07 o 3 6 0 712.00 673.57 4.61 o 4 6 0 1396.03 1242.31 6.27 o 5 6 0 1481.58 1423.80 7.23 o 6 6 0 485.95 467.60 5.02 o 7 6 0 143.37 132.40 2.04 o 1 7 0 26.38 24.51 0.68 o 2 7 0 336.04 317.23 3.41 o 3 7 0 206.07 177.21 2.36 o 4 7 0 151.92 139.91 2.26 o 5 7 0 269.27 259.18 3.96 o 6 7 0 301.88 283.94 2.99 o 0 8 0 1333.44 1312.75 5.95 o 1 8 0 1014.99 1002.47 5.63 o 2 8 0 1715.87 1608.99 7.14 o 3 8 0 1989.36 1933.52 8.43 o 4 8 0 609.85 572.09 5.23 o 5 8 0 78.24 77.11 1.44 o 6 8 0 98.46 88.41 1.54 o 1 9 0 149.78 140.39 2.27 o 2 9 0 22.57 23.24 0.72 o 3 9 0 304.92 320.53 4.16 o 4 9 0 299.83 311.28 4.34 o 5 9 0 112.99 122.53 1.97 o 0 10 0 881.84 1025.86 6.57 o 1 10 0 617.99 725.70 5.52 o 2 10 0 521.24 591.01 5.32 o 3 10 0 424.25 455.48 3.50 o 4 10 0 204.60 216.20 2.81 o 1 11 0 78.42 101.03 1.78 o 2 11 0 105.67 125.57 2.14 o 3 11 0 14.56 19.15 0.84 o 0 12 0 443.38 353.19 4.62 o 1 12 0 287.76 267.59 2.90 o -8 0 1 1088.58 1042.01 7.06 o -7 0 1 2420.38 2589.37 13.25 o -6 0 1 3563.39 4005.50 14.78 o -5 0 1 757.75 810.82 6.62 o -4 0 1 37.11 46.72 1.12 o -3 0 1 4132.66 3994.45 40.25 o -2 0 1 8544.86 9398.33 50.94 o -1 0 1 7785.12 7794.56 38.14 o 0 0 1 7582.32 7187.05 25.63 o 1 0 1 1084.01 1143.18 4.64 o 2 0 1 1880.10 2026.12 6.81 o 3 0 1 6573.51 6889.52 62.23 o 4 0 1 6140.94 6606.41 69.68 o 5 0 1 625.55 709.87 6.56 o 6 0 1 0.44 3.73 0.95 o 7 0 1 95.61 96.82 2.28 o -7 1 1 30.44 34.88 0.73 o -6 1 1 352.43 363.05 3.91 o -5 1 1 406.27 404.98 3.58 o -4 1 1 871.83 835.43 3.96 o -3 1 1 7.53 10.97 0.41 o -2 1 1 487.24 427.10 1.98 o -1 1 1 2663.92 2393.08 15.63 o 0 1 1 2680.76 2613.11 11.37 o 1 1 1 375.05 409.91 1.94 o 2 1 1 306.90 318.47 2.44 o 3 1 1 1840.29 2043.61 5.58 o 4 1 1 2823.32 3113.30 7.66 o 5 1 1 2163.92 2301.39 7.89 o 6 1 1 2160.54 2258.54 9.11 o 7 1 1 813.86 732.25 4.07 o -8 2 1 1041.27 984.83 4.72 o -7 2 1 858.31 888.01 6.11 o -6 2 1 1192.40 1314.25 6.45 o -5 2 1 2237.69 2478.21 7.51 o -4 2 1 3557.38 3839.83 8.53 o -3 2 1 3681.72 4027.25 30.67 o -2 2 1 375.47 377.93 2.39 o -1 2 1 1372.67 1455.47 3.67 o 0 2 1 7923.38 7573.02 22.22 o 1 2 1 9301.30 8879.71 40.00 o 2 2 1 6444.20 6601.22 38.46 o 3 2 1 1707.58 1890.08 5.96 o 4 2 1 1083.67 1165.83 5.14 o 5 2 1 746.21 764.69 5.29 o 6 2 1 497.36 503.49 4.91 o 7 2 1 302.28 301.71 3.08 o -8 3 1 176.24 169.43 2.31 o -7 3 1 63.31 67.59 1.24 o -5 3 1 4.13 8.82 0.65 o -4 3 1 499.91 548.73 3.52 o -3 3 1 1924.02 2082.16 5.64 o -2 3 1 1564.25 1463.72 4.20 o -1 3 1 1.99 5.39 0.35 o 0 3 1 1850.89 1599.95 3.30 o 1 3 1 906.86 802.03 3.49 o 2 3 1 4614.89 4650.93 34.89 o 3 3 1 3443.22 3535.44 8.18 o 4 3 1 1282.83 1320.41 5.97 o 5 3 1 424.58 467.93 4.14 o 6 3 1 1092.04 1105.03 6.82 o 7 3 1 1427.85 1277.42 5.38 o -8 4 1 964.00 895.69 4.91 o -7 4 1 989.52 943.68 6.30 o -6 4 1 709.29 690.73 5.03 o -5 4 1 1361.30 1408.86 6.17 o -4 4 1 2532.02 2580.46 7.67 o -3 4 1 2037.18 1966.69 6.09 o -2 4 1 640.80 501.83 3.06 o -1 4 1 2855.42 2939.24 5.98 o 0 4 1 4095.42 4092.38 9.73 o 1 4 1 3704.31 3785.33 7.64 o 2 4 1 3971.05 3669.91 8.35 o 3 4 1 1353.69 1371.70 5.58 o 4 4 1 940.62 896.97 5.33 o 5 4 1 827.78 831.57 5.52 o 6 4 1 325.02 332.63 4.24 o 7 4 1 91.13 93.23 1.71 o -6 5 1 236.75 227.02 2.68 o -5 5 1 556.48 568.55 4.56 o -4 5 1 142.81 152.47 2.02 o -3 5 1 78.43 78.45 1.45 o -2 5 1 9.53 24.91 0.82 o -1 5 1 1313.79 1433.88 5.19 o 0 5 1 898.93 760.32 2.64 o 1 5 1 776.68 608.84 3.38 o 2 5 1 184.58 176.68 2.54 o 3 5 1 379.44 349.48 3.58 o 4 5 1 1545.49 1535.44 6.97 o 5 5 1 1689.27 1648.80 7.78 o 6 5 1 1141.01 1070.24 6.71 o 7 5 1 466.36 417.25 3.63 o -7 6 1 1172.18 1097.65 4.98 o -6 6 1 1240.48 1231.67 7.20 o -5 6 1 454.99 428.89 4.25 o -4 6 1 182.83 163.99 2.27 o -3 6 1 969.63 904.30 4.94 o -2 6 1 2516.57 2630.58 7.04 o -1 6 1 3435.76 3744.25 8.42 o 0 6 1 1565.83 1395.94 3.58 o 1 6 1 313.38 266.19 3.12 o 2 6 1 988.06 900.27 4.93 o 3 6 1 2209.09 2042.88 7.44 o 4 6 1 1820.88 1748.74 7.45 o 5 6 1 291.93 285.34 3.92 o 6 6 1 1.50 11.06 1.09 o -6 7 1 29.61 26.65 0.85 o -5 7 1 84.39 79.41 1.46 o -4 7 1 225.42 215.04 3.00 o -3 7 1 67.50 60.70 0.85 o -1 7 1 317.88 303.75 3.33 o 0 7 1 372.72 361.58 2.60 o 1 7 1 161.46 153.49 2.20 o 2 7 1 278.63 262.99 3.54 o 3 7 1 747.73 667.01 4.94 o 4 7 1 830.18 823.59 5.89 o 5 7 1 533.55 515.52 5.27 o 6 7 1 515.39 458.47 3.80 o -6 8 1 357.61 325.21 3.20 o -5 8 1 627.04 562.30 5.51 o -4 8 1 876.07 845.44 5.96 o -3 8 1 921.20 857.69 5.61 o -2 8 1 185.43 177.19 2.36 o -1 8 1 129.99 131.01 2.19 o 0 8 1 1336.79 1324.56 4.48 o 1 8 1 1942.41 1792.77 7.54 o 2 8 1 917.53 812.25 5.46 o 3 8 1 302.83 292.33 3.97 o 4 8 1 185.25 180.46 2.57 o 5 8 1 108.37 104.22 1.81 o -5 9 1 15.42 15.74 0.81 o -4 9 1 91.38 98.58 1.63 o -3 9 1 327.12 324.73 4.19 o -2 9 1 97.47 105.06 1.68 o -1 9 1 16.81 15.25 0.75 o 0 9 1 0.72 2.96 0.94 o 1 9 1 82.61 90.22 1.69 o 2 9 1 601.49 604.90 5.04 o 3 9 1 664.25 656.08 5.60 o 4 9 1 153.58 153.29 2.20 o 5 9 1 63.25 62.31 1.08 o -5 10 1 157.75 167.29 2.30 o -4 10 1 233.06 263.11 3.10 o -3 10 1 383.85 393.55 4.88 o -2 10 1 256.97 289.94 4.19 o -1 10 1 274.04 339.10 4.28 o 0 10 1 464.19 558.83 3.55 o 1 10 1 367.29 400.90 4.65 o 2 10 1 218.09 228.44 2.89 o 3 10 1 183.10 201.59 2.71 o 4 10 1 213.17 217.01 3.02 o -4 11 1 11.16 64.25 1.20 o -3 11 1 6.67 15.31 0.85 o -1 11 1 137.34 173.35 2.70 o 0 11 1 169.73 231.10 2.91 o 1 11 1 88.43 105.89 1.83 o 2 11 1 19.50 24.03 0.87 o 3 11 1 37.40 36.43 0.91 o -1 12 1 277.24 392.86 3.79 o 0 12 1 104.82 152.93 2.20 o -9 0 2 954.73 883.79 6.91 o -8 0 2 1976.55 1993.62 12.84 o -7 0 2 1505.84 1603.27 10.41 o -6 0 2 1288.85 1480.12 8.95 o -5 0 2 926.90 1064.76 7.14 o -4 0 2 2831.94 2637.49 9.18 o -3 0 2 6536.38 6738.30 56.01 o -2 0 2 2189.17 2241.91 28.68 o -1 0 2 825.78 865.12 6.45 o 0 0 2 2073.15 2308.29 4.63 o 1 0 2 1124.70 1228.90 5.28 o 2 0 2 1031.03 1126.61 5.97 o 3 0 2 213.32 241.92 3.82 o 4 0 2 23.24 35.78 1.06 o 5 0 2 136.31 151.61 3.20 o 7 0 2 100.20 105.05 2.24 o -8 1 2 99.61 97.36 1.62 o -7 1 2 766.59 841.61 5.55 o -6 1 2 1332.19 1439.51 6.23 o -5 1 2 1197.62 1212.76 5.24 o -4 1 2 2913.29 2672.70 6.40 o -3 1 2 5865.84 5616.17 36.44 o -2 1 2 9730.80 10677.20 45.23 o 0 1 2 4200.34 4432.50 20.31 o 1 1 2 1505.33 1519.15 4.81 o 2 1 2 1024.05 1088.21 4.52 o 3 1 2 3578.45 3852.12 8.54 o 4 1 2 1855.98 2044.69 7.43 o 5 1 2 565.09 608.25 4.72 o 6 1 2 736.65 756.38 5.64 o 7 1 2 628.60 586.43 3.97 o -8 2 2 709.46 646.69 4.17 o -7 2 2 1538.96 1581.99 7.62 o -6 2 2 3216.27 3471.18 9.71 o -5 2 2 2548.95 2869.43 8.09 o -4 2 2 1516.93 1697.63 5.65 o -3 2 2 435.87 518.53 3.11 o -2 2 2 104.41 90.65 1.30 o -1 2 2 1461.49 1621.51 4.42 o 0 2 2 674.16 654.00 2.10 o 1 2 2 77.83 99.41 1.36 o 2 2 2 198.99 234.76 2.51 o 3 2 2 9.66 24.23 0.54 o 4 2 2 376.41 384.75 3.75 o 5 2 2 132.77 137.65 2.24 o 6 2 2 9.70 10.17 0.74 o 7 2 2 11.75 6.66 1.06 o -8 3 2 91.66 100.49 1.64 o -7 3 2 58.95 49.95 0.87 o -6 3 2 270.18 240.64 3.60 o -5 3 2 3239.00 3536.79 8.99 o -4 3 2 7522.51 7696.74 51.14 o -3 3 2 2723.03 2651.41 6.37 o -2 3 2 1147.11 961.84 3.82 o -1 3 2 2958.52 3040.64 6.08 o 0 3 2 5093.36 4922.86 10.70 o 1 3 2 6613.70 6147.16 41.38 o 2 3 2 2026.93 2096.77 6.28 o 3 3 2 367.98 383.19 3.74 o 4 3 2 286.19 286.30 3.47 o 5 3 2 1137.88 1147.04 6.49 o 6 3 2 1580.88 1525.28 5.88 o -8 4 2 537.19 486.43 3.92 o -7 4 2 1246.84 1219.70 7.17 o -6 4 2 1833.17 1864.03 7.69 o -5 4 2 1330.06 1410.27 6.17 o -4 4 2 1699.72 1748.51 6.30 o -3 4 2 914.09 844.84 3.98 o -2 4 2 12.12 9.82 0.47 o -1 4 2 722.45 665.15 3.53 o 0 4 2 508.06 472.37 2.08 o 1 4 2 0.82 15.20 0.64 o 2 4 2 10.51 14.36 0.52 o 3 4 2 44.60 47.37 0.85 o 4 4 2 174.45 197.17 2.30 o 5 4 2 25.97 29.61 0.74 o 6 4 2 2.74 4.28 0.93 o -8 5 2 161.44 153.80 2.20 o -7 5 2 590.55 573.63 5.56 o -6 5 2 467.47 457.36 4.38 o -5 5 2 602.85 600.03 4.69 o -4 5 2 1445.65 1393.79 6.13 o -3 5 2 1935.94 1668.86 6.16 o -2 5 2 4523.80 4632.30 9.39 o -1 5 2 5398.17 5223.59 13.99 o 0 5 2 1141.08 1024.18 3.07 o 1 5 2 416.08 360.66 3.37 o 2 5 2 894.99 832.65 4.74 o 3 5 2 1815.60 1739.20 7.43 o 4 5 2 1248.56 1242.63 6.75 o 5 5 2 552.46 519.29 4.98 o 6 5 2 318.28 294.17 3.28 o -7 6 2 804.70 764.76 4.16 o -6 6 2 473.83 458.80 4.98 o -5 6 2 256.82 238.72 2.95 o -4 6 2 1230.11 1128.24 5.98 o -3 6 2 2274.97 2002.53 7.36 o -2 6 2 379.97 350.78 3.58 o -1 6 2 31.65 31.20 0.61 o 0 6 2 80.71 78.32 0.85 o 1 6 2 140.89 120.15 1.95 o 2 6 2 459.63 423.04 3.94 o 3 6 2 126.67 109.46 2.00 o 4 6 2 1.67 5.08 1.05 o 5 6 2 56.66 54.18 0.90 o 6 6 2 2.11 4.86 2.38 o -7 7 2 189.80 183.59 2.78 o -6 7 2 402.14 383.60 4.82 o -5 7 2 478.46 449.50 4.64 o -4 7 2 911.16 838.95 5.55 o -3 7 2 1234.95 1119.48 5.95 o -2 7 2 1511.09 1366.29 6.07 o -1 7 2 1424.24 1320.84 5.97 o 0 7 2 1070.29 1031.59 3.95 o 1 7 2 729.07 676.64 4.98 o 2 7 2 619.43 544.44 4.78 o 3 7 2 907.43 814.80 5.85 o 4 7 2 451.92 424.29 4.78 o 5 7 2 186.64 155.34 2.38 o -6 8 2 850.37 792.30 4.62 o -5 8 2 700.12 663.17 5.63 o -4 8 2 178.13 173.92 2.52 o -3 8 2 56.15 51.31 0.78 o -2 8 2 121.79 112.77 1.89 o -1 8 2 294.52 274.41 3.85 o 0 8 2 245.14 247.66 2.36 o 1 8 2 66.41 52.98 0.89 o 2 8 2 62.04 52.09 0.99 o 3 8 2 22.12 23.70 0.80 o 4 8 2 107.82 92.31 1.44 o 5 8 2 58.39 53.68 1.00 o -6 9 2 87.97 85.36 1.39 o -5 9 2 384.80 400.34 3.55 o -4 9 2 880.20 895.70 6.55 o -3 9 2 592.78 563.91 5.19 o -2 9 2 182.17 205.50 2.55 o -1 9 2 274.49 322.23 4.17 o 0 9 2 988.95 1085.81 4.51 o 1 9 2 938.14 942.39 6.30 o 2 9 2 256.94 280.25 4.12 o 3 9 2 135.93 122.08 1.96 o 4 9 2 122.18 107.17 1.98 o -5 10 2 201.89 215.40 3.01 o -4 10 2 198.75 216.80 3.02 o -3 10 2 151.08 149.43 2.00 o -2 10 2 68.70 51.21 0.88 o 0 10 2 20.21 24.30 0.54 o 1 10 2 12.57 15.09 1.06 o 3 10 2 13.63 10.17 0.83 o -3 11 2 185.57 233.18 3.13 o -2 11 2 445.37 582.88 3.96 o -1 11 2 439.44 570.08 3.91 o 0 11 2 127.78 168.17 2.48 o 1 11 2 42.88 54.78 0.91 o 2 11 2 107.54 129.58 2.02 o -9 0 3 199.42 216.20 4.42 o -8 0 3 59.49 67.03 1.23 o -6 0 3 240.44 274.82 5.21 o -5 0 3 1919.24 1838.83 9.40 o -4 0 3 2391.96 2170.51 8.95 o -3 0 3 38.10 57.03 1.03 o -2 0 3 212.34 244.97 3.42 o -1 0 3 165.60 205.77 2.94 o 1 0 3 196.09 219.11 3.44 o 2 0 3 1167.52 1230.20 7.68 o 3 0 3 2588.05 2738.59 12.20 o 4 0 3 966.77 996.71 8.20 o 5 0 3 143.80 145.61 2.80 o 6 0 3 62.99 57.86 1.56 o -9 1 3 426.78 412.75 3.89 o -8 1 3 624.73 673.23 3.90 o -7 1 3 604.79 680.43 5.35 o -6 1 3 501.76 558.72 4.52 o -5 1 3 1460.28 1610.48 6.59 o -4 1 3 3507.33 3359.71 7.98 o -3 1 3 6325.38 7189.12 45.86 o -2 1 3 7096.89 6868.78 42.67 o -1 1 3 3402.76 3161.12 9.30 o 0 1 3 5785.32 6171.21 29.39 o 1 1 3 5271.88 5460.71 41.86 o 2 1 3 3236.12 3541.13 9.00 o 3 1 3 1954.98 2028.44 7.41 o 4 1 3 466.71 534.61 4.42 o 5 1 3 212.70 235.09 3.14 o 6 1 3 223.13 222.07 2.85 o -8 2 3 161.09 155.50 2.21 o -7 2 3 576.55 617.36 5.09 o -6 2 3 460.30 509.99 4.32 o -5 2 3 64.56 68.38 1.24 o -4 2 3 246.37 280.35 3.20 o -3 2 3 723.41 803.73 3.88 o -2 2 3 973.40 972.96 4.27 o -1 2 3 29.77 28.58 0.44 o 0 2 3 696.12 760.83 2.64 o 1 2 3 943.13 1074.94 5.38 o 3 2 3 237.92 257.43 3.29 o 4 2 3 222.35 229.49 3.52 o 5 2 3 551.15 540.03 5.40 o 6 2 3 408.62 392.45 3.52 o -8 3 3 140.18 132.09 2.04 o -7 3 3 896.19 904.87 6.17 o -6 3 3 1411.32 1514.62 6.92 o -5 3 3 2121.00 2381.52 8.03 o -4 3 3 1692.71 1769.05 6.34 o -3 3 3 1017.74 898.03 4.51 o -2 3 3 4047.90 3923.81 8.64 o -1 3 3 10178.07 9759.06 55.25 o 0 3 3 8606.06 8401.20 37.00 o 1 3 3 1667.66 1597.69 6.02 o 2 3 3 636.08 680.45 4.64 o 3 3 3 1279.85 1304.65 6.43 o 4 3 3 1130.55 1166.08 6.54 o 5 3 3 733.74 701.73 4.35 o -8 4 3 37.52 30.36 0.83 o -7 4 3 369.16 379.31 4.52 o -6 4 3 527.83 551.28 4.81 o -5 4 3 42.79 48.03 0.76 o -4 4 3 210.75 194.54 2.67 o -3 4 3 700.09 630.41 4.12 o -2 4 3 220.40 172.73 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