#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/26/2012655.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012655_Fobs loop_ _publ_author_name 'Glidewell, Christopher' 'Low, John N.' 'Skakle, Janet M. S.' 'Wardell, James L.' _publ_section_title ; Hydrogen-bonded molecular ladders in S-(4-nitrophenyl)thioglycolic acid ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o201 _journal_page_last o203 _journal_volume 58 _journal_year 2002 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 73.882 _cell_angle_beta 85.721 _cell_angle_gamma 80.984 _cell_length_a 7.1540 _cell_length_b 7.8750 _cell_length_c 8.0352 _exptl_crystal_F_000 220.00 _reflns_d_resolution_high 0.7691 _[local]_cod_data_source_file sk1535Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1006' _shelx_refln_list_code 4 _shelx_f_calc_maximum 64.06 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1091.63 1125.51 22.74 o 3 0 0 165.89 185.06 5.98 o 4 0 0 88.65 83.03 1.70 o 5 0 0 5.16 4.84 0.37 o 6 0 0 113.63 122.98 2.72 o 7 0 0 188.72 203.13 6.84 o 8 0 0 110.31 107.70 5.78 o 9 0 0 73.82 67.58 5.78 o -9 1 0 2.54 3.57 2.55 o -8 1 0 3.30 2.09 1.07 o -7 1 0 8.50 8.90 0.96 o -6 1 0 268.91 285.28 7.00 o -5 1 0 0.81 0.20 0.34 o -4 1 0 378.84 399.00 7.80 o -3 1 0 21.84 25.39 0.76 o -2 1 0 305.67 272.60 5.47 o -1 1 0 322.48 305.37 8.80 o 1 1 0 22.34 24.75 0.56 o 2 1 0 391.73 398.37 10.01 o 3 1 0 544.81 598.91 13.42 o 4 1 0 218.29 206.59 4.09 o 5 1 0 1.32 1.51 0.30 o 6 1 0 4.57 4.09 0.60 o 7 1 0 0.01 -0.19 0.67 o 8 1 0 71.18 66.24 4.29 o 9 1 0 32.16 32.87 3.25 o -8 2 0 20.12 19.04 1.96 o -7 2 0 1.94 2.30 1.26 o -6 2 0 8.76 8.50 0.98 o -5 2 0 148.55 146.09 3.33 o -4 2 0 4.20 2.17 0.50 o -3 2 0 572.01 553.99 12.63 o -2 2 0 1465.91 1440.24 29.10 o -1 2 0 543.22 525.08 12.90 o 0 2 0 310.70 198.69 13.31 o 1 2 0 115.85 115.50 2.67 o 2 2 0 997.73 950.58 20.95 o 3 2 0 48.13 51.84 1.29 o 4 2 0 194.35 200.40 3.97 o 5 2 0 8.52 8.45 0.60 o 6 2 0 324.68 342.19 7.90 o 7 2 0 5.14 5.11 0.86 o 8 2 0 61.74 57.98 3.96 o 9 2 0 85.58 83.02 5.40 o -8 3 0 3.59 1.52 1.80 o -7 3 0 86.34 84.38 6.51 o -6 3 0 28.72 26.34 1.55 o -5 3 0 165.97 171.88 5.16 o -4 3 0 29.27 27.15 1.01 o -3 3 0 1023.71 1086.66 20.95 o -2 3 0 510.45 549.81 11.84 o 0 3 0 158.17 74.28 5.62 o 1 3 0 16.56 12.45 0.91 o 2 3 0 233.59 225.62 5.53 o 3 3 0 15.88 12.48 0.63 o 4 3 0 53.88 64.58 1.66 o 5 3 0 132.66 152.23 3.60 o 6 3 0 26.62 22.26 1.07 o 7 3 0 19.31 19.10 1.54 o 8 3 0 98.19 111.02 5.69 o 9 3 0 4.21 3.95 1.68 o -7 4 0 602.55 605.34 28.45 o -6 4 0 0.87 0.67 0.59 o -5 4 0 139.66 135.23 3.39 o -4 4 0 38.71 39.54 1.63 o -3 4 0 0.38 0.30 0.23 o -2 4 0 7.61 6.39 0.26 o -1 4 0 68.86 70.82 2.23 o 0 4 0 917.76 902.13 27.10 o 1 4 0 353.60 343.93 7.56 o 2 4 0 10.46 11.16 0.51 o 3 4 0 103.96 102.92 3.45 o 4 4 0 460.95 492.95 10.13 o 5 4 0 6.64 8.49 1.03 o 6 4 0 55.72 60.29 2.02 o 7 4 0 48.45 43.95 2.30 o 8 4 0 39.11 39.20 2.85 o -7 5 0 8.54 10.69 2.55 o -6 5 0 3.92 3.05 1.53 o -5 5 0 46.97 44.02 2.09 o -4 5 0 79.64 79.05 3.52 o -3 5 0 147.82 148.64 3.46 o -2 5 0 0.26 0.00 0.52 o -1 5 0 70.43 68.10 4.40 o 0 5 0 45.62 37.93 1.12 o 1 5 0 595.18 596.34 13.72 o 2 5 0 83.38 84.70 2.67 o 3 5 0 30.68 31.57 1.48 o 4 5 0 98.14 97.54 2.31 o 5 5 0 293.92 309.87 7.22 o 6 5 0 148.63 161.16 5.49 o 7 5 0 44.90 36.76 2.23 o 8 5 0 146.07 149.33 8.16 o -5 6 0 122.49 117.42 9.06 o -4 6 0 9.08 6.83 0.48 o -3 6 0 43.49 21.75 23.06 o -2 6 0 0.85 1.04 0.37 o -1 6 0 216.65 230.73 8.84 o 0 6 0 19.48 19.06 1.04 o 1 6 0 61.34 58.62 2.41 o 2 6 0 1457.90 1434.37 34.56 o 3 6 0 2.65 3.14 0.32 o 4 6 0 549.54 590.05 13.72 o 5 6 0 200.05 206.45 5.36 o 6 6 0 43.14 43.33 2.16 o 7 6 0 118.78 105.67 9.72 o 8 6 0 26.09 25.61 2.76 o -5 7 0 13.73 13.16 1.95 o -4 7 0 2.23 2.71 1.01 o -3 7 0 2.65 2.73 0.65 o -2 7 0 0.10 1.99 1.49 o 1 7 0 172.48 168.27 6.24 o 2 7 0 83.47 91.31 2.89 o 3 7 0 613.17 654.77 19.59 o 4 7 0 10.54 11.16 0.82 o 5 7 0 28.73 26.52 2.05 o 6 7 0 4.53 5.46 1.46 o 7 7 0 7.97 8.98 1.44 o -4 8 0 51.52 43.20 4.92 o -3 8 0 107.45 108.92 7.47 o -2 8 0 90.32 104.19 7.03 o 1 8 0 191.23 193.91 8.46 o 2 8 0 66.07 64.82 2.08 o 3 8 0 263.94 259.90 10.07 o 4 8 0 9.81 9.47 1.10 o 5 8 0 57.00 49.05 3.30 o 6 8 0 6.97 7.23 2.06 o -2 9 0 46.33 52.33 5.01 o -1 9 0 83.06 96.24 7.58 o 3 9 0 11.77 12.68 1.59 o 4 9 0 12.46 11.62 1.59 o -4 -9 1 45.77 44.38 4.25 o -2 -9 1 174.43 183.42 13.84 o -5 -8 1 147.33 153.98 12.49 o -4 -8 1 61.95 65.27 4.97 o -3 -8 1 109.72 111.20 5.08 o -2 -8 1 1.17 2.05 1.03 o -1 -8 1 70.72 66.63 2.91 o 0 -8 1 181.32 195.54 8.38 o 1 -8 1 28.20 21.62 2.07 o 3 -8 1 19.52 22.99 2.51 o -7 -7 1 0.03 -0.26 1.80 o -6 -7 1 10.45 9.35 2.84 o -5 -7 1 328.96 337.65 15.74 o -4 -7 1 104.10 109.65 4.03 o -3 -7 1 58.26 58.58 2.19 o -2 -7 1 30.96 33.08 1.39 o -1 -7 1 16.37 19.26 0.78 o 0 -7 1 25.06 31.45 1.42 o 1 -7 1 16.42 12.27 0.73 o 2 -7 1 40.03 36.59 2.02 o 3 -7 1 4.52 4.39 1.17 o 4 -7 1 233.69 213.87 18.13 o 5 -7 1 1.05 -0.49 1.96 o -7 -6 1 73.21 75.71 4.71 o -6 -6 1 294.20 297.50 12.21 o -5 -6 1 4.76 3.60 0.89 o -4 -6 1 624.92 640.25 20.01 o -3 -6 1 22.10 20.14 1.08 o -2 -6 1 226.20 231.38 4.87 o -1 -6 1 83.42 82.89 2.74 o 0 -6 1 50.21 53.23 1.61 o 1 -6 1 26.08 21.91 0.90 o 2 -6 1 6.51 9.77 0.85 o 3 -6 1 162.40 138.04 5.06 o 4 -6 1 6.17 6.63 0.65 o 5 -6 1 2.59 2.82 0.84 o 6 -6 1 67.77 70.76 6.70 o -8 -5 1 35.03 26.80 3.53 o -7 -5 1 135.15 130.73 6.82 o -6 -5 1 0.76 1.88 0.89 o -5 -5 1 66.32 69.04 2.14 o -4 -5 1 1.00 1.16 0.51 o -3 -5 1 655.80 678.60 12.80 o -2 -5 1 0.96 1.39 0.28 o -1 -5 1 204.83 194.09 5.69 o 0 -5 1 57.92 57.38 1.74 o 1 -5 1 233.24 225.44 5.64 o 2 -5 1 437.10 450.49 10.49 o 3 -5 1 86.78 83.18 2.74 o 4 -5 1 34.23 36.84 1.17 o 5 -5 1 42.69 39.93 1.39 o 6 -5 1 98.00 89.06 4.71 o 7 -5 1 3.75 6.64 2.05 o -8 -4 1 11.30 12.44 2.30 o -7 -4 1 7.46 4.79 1.22 o -6 -4 1 73.86 75.27 3.14 o -5 -4 1 159.39 173.02 4.58 o -4 -4 1 23.67 26.09 1.03 o -3 -4 1 382.80 362.86 7.62 o -2 -4 1 208.07 217.00 4.60 o -1 -4 1 186.57 180.07 4.03 o 0 -4 1 135.77 134.31 3.37 o 1 -4 1 35.04 23.11 0.68 o 2 -4 1 42.29 42.59 1.20 o 3 -4 1 309.05 301.59 9.94 o 4 -4 1 31.71 30.47 1.01 o 5 -4 1 797.67 811.05 22.24 o 6 -4 1 2.07 1.85 1.04 o 7 -4 1 53.35 44.83 4.60 o -8 -3 1 0.13 -0.25 1.07 o -7 -3 1 4.43 3.04 1.44 o -6 -3 1 23.70 21.28 1.13 o -5 -3 1 74.71 81.99 2.29 o -4 -3 1 86.00 83.74 2.05 o -3 -3 1 180.52 186.07 4.95 o -2 -3 1 7.85 5.79 0.35 o -1 -3 1 3274.81 3257.00 106.94 o 0 -3 1 875.92 882.80 23.87 o 1 -3 1 1972.91 1961.39 44.70 o 2 -3 1 129.72 133.12 3.04 o 3 -3 1 228.04 225.10 4.46 o 4 -3 1 23.84 24.10 0.74 o 5 -3 1 135.51 135.33 3.26 o 6 -3 1 45.63 48.66 2.35 o 7 -3 1 80.42 74.67 3.88 o 8 -3 1 471.56 459.22 29.80 o -9 -2 1 10.53 11.13 2.54 o -8 -2 1 132.77 134.15 8.97 o -7 -2 1 35.36 34.37 2.16 o -6 -2 1 132.73 141.49 3.73 o -5 -2 1 1.83 1.54 0.51 o -4 -2 1 481.25 497.00 10.82 o -3 -2 1 196.36 190.99 4.08 o -2 -2 1 96.77 95.60 2.33 o -1 -2 1 652.02 607.72 12.32 o 0 -2 1 2059.11 1946.22 40.89 o 1 -2 1 857.57 811.88 16.00 o 2 -2 1 110.76 134.03 2.93 o 3 -2 1 56.44 55.56 1.26 o 4 -2 1 0.01 0.10 0.22 o 5 -2 1 0.14 0.65 0.28 o 6 -2 1 4.29 4.20 0.55 o 7 -2 1 90.56 82.63 3.80 o 8 -2 1 53.41 46.42 3.31 o -9 -1 1 7.09 6.62 1.59 o -8 -1 1 4.92 5.96 1.44 o -7 -1 1 12.17 10.24 0.96 o -6 -1 1 131.09 136.10 3.58 o -5 -1 1 2.73 5.92 0.65 o -4 -1 1 272.75 272.10 5.51 o -3 -1 1 235.27 214.43 5.45 o -2 -1 1 42.27 35.52 1.03 o -1 -1 1 211.15 191.85 4.12 o 0 -1 1 229.41 206.20 4.25 o 1 -1 1 186.94 180.61 3.89 o 2 -1 1 165.62 170.78 3.73 o 3 -1 1 23.02 20.62 0.55 o 4 -1 1 194.87 203.98 3.99 o 5 -1 1 48.71 42.14 2.55 o 6 -1 1 121.40 118.99 3.49 o 7 -1 1 15.34 16.50 1.36 o 8 -1 1 0.52 0.96 1.11 o -9 0 1 49.22 39.91 5.10 o -8 0 1 85.24 80.70 5.88 o -7 0 1 0.63 0.54 0.40 o -6 0 1 66.97 70.27 2.05 o -5 0 1 22.96 23.36 0.87 o -4 0 1 677.55 722.67 16.15 o -3 0 1 0.04 -0.17 0.32 o -1 0 1 33.50 29.21 0.77 o 1 0 1 565.63 535.32 10.83 o 2 0 1 0.86 1.67 0.25 o 3 0 1 101.43 88.41 1.78 o 4 0 1 84.25 92.57 2.61 o 5 0 1 634.13 693.85 13.33 o 6 0 1 122.56 134.64 3.88 o 7 0 1 279.27 287.75 9.76 o 8 0 1 10.22 9.82 1.80 o 9 0 1 25.20 23.46 2.70 o -8 1 1 175.59 162.67 29.42 o -7 1 1 5.46 5.40 1.22 o -6 1 1 221.10 239.60 5.73 o -5 1 1 0.68 1.01 0.27 o -4 1 1 77.40 65.29 1.74 o -3 1 1 39.89 44.01 1.02 o -2 1 1 96.95 108.15 2.33 o -1 1 1 308.50 295.01 6.46 o 0 1 1 142.51 135.80 11.93 o 2 1 1 99.83 103.39 2.74 o 3 1 1 59.41 59.94 1.27 o 4 1 1 131.01 141.59 2.92 o 5 1 1 27.21 24.95 1.18 o 6 1 1 110.53 107.55 2.84 o 7 1 1 171.53 177.21 7.01 o 8 1 1 3.63 2.82 1.09 o 9 1 1 40.80 36.88 3.26 o -8 2 1 5.81 7.61 3.04 o -7 2 1 64.21 60.28 2.92 o -6 2 1 13.87 13.58 0.87 o -5 2 1 120.79 121.85 2.68 o -4 2 1 428.75 442.48 9.79 o -3 2 1 26.15 24.29 0.67 o -2 2 1 348.30 370.96 6.43 o -1 2 1 0.50 0.49 0.49 o 0 2 1 1230.42 1238.38 50.36 o 1 2 1 606.71 565.31 12.25 o 2 2 1 290.13 277.32 5.91 o 3 2 1 8.38 9.67 0.51 o 4 2 1 776.77 759.64 15.40 o 5 2 1 161.69 161.94 3.55 o 6 2 1 97.73 102.64 2.86 o 7 2 1 160.33 167.15 5.31 o 8 2 1 10.87 10.81 1.44 o 9 2 1 207.62 213.51 12.78 o -8 3 1 22.11 20.53 2.15 o -7 3 1 43.41 43.00 2.51 o -6 3 1 4.66 5.22 0.60 o -5 3 1 276.07 293.62 6.38 o -4 3 1 62.21 62.91 1.98 o -3 3 1 604.79 626.85 11.66 o -2 3 1 330.73 316.60 7.81 o -1 3 1 449.85 442.81 9.96 o 1 3 1 2.66 9.22 0.26 o 2 3 1 83.00 110.64 2.49 o 3 3 1 591.31 637.09 14.15 o 4 3 1 162.35 148.64 4.33 o 5 3 1 82.26 89.89 3.25 o 6 3 1 243.58 265.96 6.97 o 7 3 1 45.08 46.15 2.06 o 8 3 1 77.36 84.05 4.11 o 9 3 1 10.31 13.14 2.31 o -7 4 1 25.41 25.20 2.15 o -6 4 1 37.01 32.60 2.01 o -5 4 1 8.82 7.77 0.51 o -4 4 1 49.48 53.20 1.24 o -3 4 1 14.04 15.43 0.72 o -2 4 1 1281.81 1344.16 47.59 o -1 4 1 247.97 275.50 11.08 o 1 4 1 34.67 36.93 1.05 o 2 4 1 1063.73 1097.62 26.37 o 3 4 1 51.97 49.16 1.20 o 4 4 1 84.34 84.70 1.97 o 5 4 1 167.73 173.59 3.93 o 6 4 1 69.48 63.98 2.00 o 7 4 1 3.00 2.45 0.73 o 8 4 1 96.83 96.69 6.15 o 9 4 1 6.91 10.58 3.02 o -7 5 1 12.90 10.18 2.04 o -6 5 1 0.80 -0.81 1.02 o -5 5 1 62.83 59.74 2.21 o -4 5 1 29.93 28.92 0.83 o -3 5 1 16.35 11.74 4.06 o -2 5 1 88.92 84.73 4.62 o -1 5 1 424.90 474.92 20.65 o 1 5 1 6.68 5.53 0.50 o 2 5 1 263.50 256.74 5.87 o 3 5 1 553.97 566.66 12.07 o 4 5 1 288.11 302.88 7.26 o 5 5 1 12.47 9.89 0.88 o 6 5 1 188.87 182.51 6.44 o 7 5 1 0.99 0.14 0.94 o 8 5 1 15.82 15.12 1.76 o -6 6 1 31.97 29.73 4.11 o -5 6 1 56.50 60.40 5.51 o -4 6 1 8.30 7.34 1.14 o -3 6 1 239.11 244.65 13.33 o -2 6 1 11.46 9.92 1.98 o -1 6 1 79.61 83.65 4.02 o 1 6 1 6.96 6.64 0.26 o 2 6 1 576.41 557.01 12.49 o 3 6 1 311.05 308.40 7.50 o 4 6 1 63.66 65.51 1.73 o 5 6 1 77.39 72.22 2.38 o 6 6 1 86.83 86.89 3.37 o 7 6 1 14.98 14.72 1.59 o 8 6 1 82.78 80.97 5.45 o -5 7 1 0.20 -0.12 0.48 o -4 7 1 9.35 5.85 0.95 o -3 7 1 89.28 101.86 6.92 o -2 7 1 0.18 0.00 0.99 o -1 7 1 201.66 221.49 11.52 o 1 7 1 541.42 532.05 13.88 o 2 7 1 11.80 11.21 0.51 o 3 7 1 284.17 282.69 8.46 o 4 7 1 3.62 4.27 0.66 o 6 7 1 27.16 24.50 2.55 o 7 7 1 50.91 40.26 4.53 o -4 8 1 32.31 31.71 3.91 o -3 8 1 115.30 134.61 8.89 o -2 8 1 0.15 0.49 1.97 o -1 8 1 143.68 159.70 10.49 o 0 8 1 28.41 25.90 2.50 o 2 8 1 2.24 2.39 0.35 o 3 8 1 55.97 53.30 2.17 o 4 8 1 72.51 75.62 3.16 o 5 8 1 23.88 20.70 1.81 o -2 9 1 67.74 70.11 6.44 o -1 9 1 433.12 527.60 35.96 o 0 9 1 3.73 5.48 1.99 o 1 9 1 0.02 2.50 2.00 o 3 9 1 121.32 121.85 8.34 o 4 9 1 1.39 2.63 1.05 o 5 9 1 45.56 46.85 3.66 o -2 -9 2 2.99 2.63 1.06 o -1 -9 2 9.57 12.94 1.56 o -5 -8 2 17.54 17.66 3.12 o -4 -8 2 9.17 10.98 2.09 o -3 -8 2 3.70 3.70 1.06 o -2 -8 2 261.64 298.54 18.23 o -1 -8 2 3.79 4.70 1.05 o 0 -8 2 121.56 120.71 8.41 o 1 -8 2 79.22 75.54 8.14 o 2 -8 2 81.95 81.18 7.68 o -6 -7 2 109.69 109.51 5.68 o -5 -7 2 3.25 -0.44 1.29 o -4 -7 2 81.76 78.53 3.83 o -3 -7 2 0.66 0.35 0.65 o -2 -7 2 94.27 99.96 5.01 o -1 -7 2 26.37 23.52 1.20 o 0 -7 2 116.17 112.77 4.05 o 1 -7 2 0.26 0.39 0.43 o 2 -7 2 399.36 377.21 21.00 o 3 -7 2 18.59 12.70 4.23 o 4 -7 2 103.64 113.63 5.37 o -7 -6 2 7.72 4.63 1.45 o -6 -6 2 143.56 133.39 9.06 o -5 -6 2 2.18 0.69 0.89 o -4 -6 2 378.20 388.93 13.30 o -3 -6 2 9.76 9.50 0.67 o -2 -6 2 97.08 103.69 3.70 o -1 -6 2 22.35 16.52 1.10 o 0 -6 2 32.38 43.26 1.35 o 1 -6 2 150.00 122.64 3.39 o 2 -6 2 14.11 16.64 0.82 o 3 -6 2 0.02 0.08 0.32 o 4 -6 2 113.13 123.94 6.23 o 5 -6 2 0.57 1.01 0.84 o -7 -5 2 78.12 80.59 5.04 o -6 -5 2 9.41 9.08 1.19 o -5 -5 2 540.20 590.15 15.43 o -4 -5 2 20.84 18.04 0.94 o -3 -5 2 251.96 244.67 6.96 o -2 -5 2 111.58 112.07 2.95 o -1 -5 2 158.55 151.14 3.57 o 0 -5 2 623.47 633.09 13.49 o 1 -5 2 72.57 63.24 1.61 o 2 -5 2 35.86 34.42 1.27 o 3 -5 2 64.51 58.51 1.72 o 4 -5 2 185.47 174.06 5.43 o 5 -5 2 0.77 1.17 0.58 o 6 -5 2 10.20 9.78 1.69 o -8 -4 2 1.41 0.29 1.22 o -7 -4 2 114.13 117.51 6.15 o -6 -4 2 42.24 41.33 2.09 o -5 -4 2 212.51 217.69 6.36 o -4 -4 2 18.13 18.75 0.87 o -3 -4 2 156.29 147.04 4.71 o -2 -4 2 153.19 146.29 3.89 o -1 -4 2 36.09 25.24 0.93 o 0 -4 2 41.47 40.23 1.08 o 1 -4 2 249.88 236.41 5.24 o 2 -4 2 91.87 91.02 2.44 o 3 -4 2 552.46 540.32 12.46 o 4 -4 2 17.79 15.65 0.95 o 5 -4 2 4.32 3.97 0.48 o 6 -4 2 82.10 80.88 3.79 o 7 -4 2 0.80 -0.26 2.81 o -7 -3 2 68.19 72.73 3.56 o -6 -3 2 14.44 13.48 1.07 o -5 -3 2 216.66 222.25 5.19 o -4 -3 2 6.99 8.34 0.51 o -3 -3 2 1300.51 1335.06 40.34 o -2 -3 2 502.13 493.42 13.46 o -1 -3 2 1241.64 1270.28 37.08 o 0 -3 2 195.72 197.20 4.31 o 1 -3 2 84.81 89.24 2.41 o 2 -3 2 3.15 4.01 0.26 o 3 -3 2 109.39 105.94 2.71 o 4 -3 2 247.48 248.53 5.92 o 5 -3 2 47.36 46.47 1.52 o 6 -3 2 1235.12 1238.38 60.66 o 7 -3 2 23.19 25.30 1.96 o 8 -3 2 33.63 32.28 2.81 o -8 -2 2 69.78 74.42 4.49 o -7 -2 2 1.84 2.04 1.08 o -6 -2 2 167.58 175.71 6.06 o -5 -2 2 84.01 84.69 3.26 o -4 -2 2 22.18 22.77 0.90 o -3 -2 2 173.37 162.36 3.32 o -2 -2 2 747.32 710.89 14.52 o -1 -2 2 329.60 310.87 6.14 o 0 -2 2 888.71 911.42 23.54 o 1 -2 2 40.74 42.20 1.20 o 2 -2 2 60.96 62.08 1.50 o 3 -2 2 2.42 1.86 0.28 o 4 -2 2 17.04 16.91 0.64 o 5 -2 2 125.00 122.59 2.88 o 6 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