#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:39:14 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180795 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/26/2012665.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012665_Fobs loop_ _publ_author_name 'Daran, Jean-Claude' 'Lemoine, Pascale' 'Viossat, Bernard' _publ_section_title ; Bis(isoquinoline-1-carboxylato-\k^2^O,N)(1,10-phenanthroline-\k^2^N,N')zinc(II) dimethylformamide sesquisolvate ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m210 _journal_page_last m212 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.219 _cell_angle_gamma 90.000 _cell_length_a 17.0766 _cell_length_b 12.7466 _cell_length_c 14.4217 _exptl_crystal_F_000 1448.00 _reflns_d_resolution_high 0.8054 _cod_data_source_file tr1009Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 183.81 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8718.44 9863.58 114.14 o 6 0 0 11449.36 11777.02 95.14 o 8 0 0 14248.48 15645.81 196.50 o 9 0 0 33785.63 35749.41 380.58 o 10 0 0 3833.53 4362.98 42.70 o 11 0 0 16692.31 18039.45 401.19 o 12 0 0 1110.75 1175.87 34.41 o 13 0 0 3830.72 3911.00 47.17 o 14 0 0 7017.16 7308.24 63.29 o 15 0 0 859.29 984.48 15.73 o 16 0 0 3974.71 4121.84 115.24 o 17 0 0 546.88 553.86 30.38 o 18 0 0 2604.07 2629.80 189.91 o 19 0 0 397.08 321.73 16.85 o 20 0 0 983.30 949.16 45.83 o 2 1 0 49.88 82.04 19.07 o 3 1 0 1396.97 1210.05 22.50 o 4 1 0 1582.61 1686.60 23.49 o 5 1 0 1955.13 1762.12 24.00 o 6 1 0 1304.33 1352.76 17.41 o 7 1 0 10188.20 10173.36 83.57 o 8 1 0 5767.65 6153.75 93.77 o 9 1 0 2449.07 2342.96 30.69 o 10 1 0 1429.67 1224.67 16.27 o 11 1 0 3135.05 3148.88 41.56 o 12 1 0 540.04 511.56 12.13 o 13 1 0 2.48 -6.53 10.23 o 14 1 0 1297.15 1262.88 19.26 o 15 1 0 7.91 -4.29 11.11 o 16 1 0 191.61 193.98 11.34 o 17 1 0 368.58 347.71 11.77 o 18 1 0 219.62 202.27 14.95 o 19 1 0 265.37 272.05 13.20 o 20 1 0 73.18 41.48 12.01 o 21 1 0 164.21 288.78 22.54 o 0 2 0 2624.88 3543.49 62.96 o 2 2 0 8671.35 9031.10 170.82 o 3 2 0 3069.99 3117.79 82.88 o 4 2 0 11746.60 12027.31 205.58 o 5 2 0 6383.31 6543.18 111.34 o 6 2 0 116.47 92.50 13.35 o 7 2 0 3507.71 3399.77 33.38 o 8 2 0 2317.50 2100.08 17.47 o 9 2 0 8424.16 8485.91 95.11 o 10 2 0 843.44 928.17 22.16 o 11 2 0 1122.57 1236.37 14.49 o 12 2 0 1335.17 1318.14 15.13 o 13 2 0 3655.96 3697.55 20.79 o 14 2 0 1185.22 1181.65 16.07 o 15 2 0 87.30 99.07 10.53 o 16 2 0 971.10 1038.79 14.89 o 17 2 0 34.50 41.41 11.88 o 18 2 0 523.82 529.68 26.51 o 19 2 0 3.71 8.26 12.12 o 20 2 0 38.01 13.72 11.06 o 21 2 0 55.55 123.45 22.36 o 2 3 0 10936.95 12350.61 210.03 o 3 3 0 3985.77 3675.41 53.26 o 4 3 0 678.97 681.68 20.53 o 5 3 0 204.82 147.83 14.42 o 6 3 0 5321.74 4870.89 37.83 o 7 3 0 4806.35 4630.96 43.11 o 8 3 0 9844.09 9878.56 116.29 o 9 3 0 1259.29 1104.22 20.05 o 10 3 0 3680.43 3538.91 19.29 o 11 3 0 43.70 40.47 10.03 o 12 3 0 2119.35 2268.45 41.31 o 13 3 0 461.23 441.47 11.64 o 14 3 0 4088.14 4232.53 26.61 o 15 3 0 713.75 742.42 12.57 o 16 3 0 1929.78 2071.69 15.54 o 17 3 0 364.51 409.32 14.20 o 18 3 0 1322.80 1309.07 13.24 o 19 3 0 387.46 383.63 10.52 o 20 3 0 100.50 89.32 12.09 o 2 4 0 2204.83 1976.71 29.03 o 3 4 0 105.63 69.05 15.21 o 4 4 0 1992.07 1734.11 25.42 o 5 4 0 1799.03 1569.31 36.41 o 6 4 0 668.74 565.87 14.76 o 7 4 0 16936.86 17311.94 184.78 o 8 4 0 1570.99 1545.96 17.46 o 9 4 0 5190.64 5160.68 51.56 o 10 4 0 2.07 20.65 11.86 o 11 4 0 2396.62 2358.46 22.03 o 12 4 0 611.97 631.87 18.17 o 13 4 0 871.83 930.19 13.46 o 14 4 0 1845.01 1881.97 16.07 o 15 4 0 2314.29 2408.29 24.90 o 16 4 0 277.66 327.35 11.17 o 17 4 0 595.31 627.45 18.23 o 18 4 0 412.05 459.08 11.86 o 19 4 0 103.56 91.16 12.09 o 20 4 0 48.76 23.79 12.78 o 1 5 0 6.17 32.79 19.46 o 2 5 0 3.78 11.90 17.13 o 3 5 0 1457.37 1581.34 31.81 o 4 5 0 713.14 693.22 18.56 o 5 5 0 94.96 97.20 14.36 o 6 5 0 213.42 196.81 13.47 o 7 5 0 445.45 400.94 12.44 o 8 5 0 2585.21 2685.86 22.13 o 9 5 0 460.23 492.55 14.34 o 10 5 0 62.89 80.78 13.93 o 11 5 0 645.96 615.56 13.06 o 12 5 0 377.40 360.76 13.25 o 13 5 0 215.43 204.02 10.76 o 14 5 0 40.64 31.08 11.44 o 15 5 0 121.30 141.08 12.82 o 16 5 0 172.46 168.94 13.45 o 17 5 0 73.34 80.92 12.87 o 18 5 0 7.17 0.57 9.89 o 19 5 0 20.04 7.68 10.94 o 0 6 0 5693.89 5709.62 48.52 o 1 6 0 44.00 42.61 15.71 o 2 6 0 19577.93 21782.93 180.34 o 3 6 0 3521.35 3493.30 60.08 o 4 6 0 3253.29 3064.40 61.12 o 5 6 0 953.28 805.44 14.28 o 6 6 0 2237.81 2163.33 32.79 o 7 6 0 476.93 439.88 13.37 o 8 6 0 1052.54 967.67 15.10 o 9 6 0 4861.61 4936.93 64.25 o 10 6 0 2.07 13.92 13.64 o 11 6 0 2494.88 2481.96 32.38 o 12 6 0 620.14 635.58 18.84 o 13 6 0 52.99 48.81 9.61 o 14 6 0 635.44 675.41 18.81 o 15 6 0 54.08 67.95 12.33 o 16 6 0 613.83 607.05 12.49 o 17 6 0 6.99 17.48 9.95 o 18 6 0 37.87 50.97 9.88 o 19 6 0 60.47 65.52 22.58 o 1 7 0 24856.08 28632.09 160.50 o 2 7 0 5130.59 5523.58 79.39 o 3 7 0 9512.48 10129.26 173.06 o 4 7 0 348.08 294.86 17.65 o 5 7 0 1579.22 1508.97 19.13 o 6 7 0 6309.01 6492.18 61.55 o 7 7 0 1198.21 1241.82 16.68 o 8 7 0 6853.29 6872.82 146.83 o 9 7 0 590.07 536.53 12.26 o 10 7 0 4508.50 4551.37 65.81 o 11 7 0 54.66 53.08 11.14 o 12 7 0 85.29 86.86 11.81 o 13 7 0 698.09 734.18 12.78 o 14 7 0 1451.04 1613.67 25.12 o 15 7 0 1052.84 1114.80 19.22 o 16 7 0 243.81 248.48 11.41 o 17 7 0 195.75 195.90 9.92 o 18 7 0 183.79 179.98 10.14 o 0 8 0 2402.67 2594.32 35.47 o 1 8 0 1028.11 1114.65 19.37 o 2 8 0 58.17 111.96 15.37 o 3 8 0 956.95 1040.20 19.66 o 4 8 0 530.32 492.81 16.12 o 5 8 0 139.33 164.05 14.49 o 6 8 0 470.88 504.34 13.17 o 7 8 0 247.64 220.29 12.04 o 8 8 0 1700.39 1683.30 16.87 o 9 8 0 318.26 290.13 12.01 o 10 8 0 0.10 -5.07 11.61 o 11 8 0 38.97 52.71 14.16 o 12 8 0 142.44 156.25 15.17 o 13 8 0 163.83 193.17 12.02 o 14 8 0 11.26 12.23 11.63 o 15 8 0 5.15 -0.61 11.40 o 16 8 0 18.96 -12.01 12.01 o 17 8 0 150.34 150.95 12.07 o 18 8 0 54.61 124.17 27.21 o 1 9 0 180.72 188.24 15.07 o 2 9 0 56.81 63.94 15.68 o 3 9 0 260.31 295.44 16.48 o 4 9 0 243.64 246.22 14.81 o 5 9 0 554.78 555.55 15.54 o 6 9 0 88.38 90.65 13.54 o 7 9 0 3.30 8.13 12.05 o 8 9 0 105.69 96.90 11.35 o 9 9 0 350.57 368.45 12.75 o 10 9 0 1362.01 1328.55 16.14 o 11 9 0 7.13 22.56 13.54 o 12 9 0 555.88 557.86 13.66 o 13 9 0 36.59 34.95 11.20 o 14 9 0 421.58 419.57 11.91 o 15 9 0 96.25 78.27 10.58 o 16 9 0 2.06 -1.70 10.79 o 17 9 0 190.27 153.60 11.86 o 0 10 0 7030.36 7200.88 49.12 o 1 10 0 180.28 197.90 14.52 o 2 10 0 2239.65 2331.80 23.08 o 3 10 0 1907.73 2030.13 21.87 o 4 10 0 391.05 402.94 15.15 o 5 10 0 3094.74 2997.88 41.61 o 6 10 0 211.86 232.99 13.80 o 7 10 0 833.18 794.62 16.20 o 8 10 0 106.99 102.13 11.94 o 9 10 0 2508.73 2654.90 40.96 o 10 10 0 261.67 243.62 13.88 o 11 10 0 719.68 761.39 22.37 o 12 10 0 82.64 87.88 12.64 o 13 10 0 697.30 701.42 18.67 o 14 10 0 72.58 73.98 11.18 o 15 10 0 99.15 75.00 11.99 o 16 10 0 458.47 477.82 12.66 o 1 11 0 547.83 567.32 21.01 o 2 11 0 44.19 46.18 14.24 o 3 11 0 14.91 9.95 14.60 o 4 11 0 62.18 61.83 14.22 o 5 11 0 251.40 269.73 12.58 o 6 11 0 337.00 308.21 13.86 o 7 11 0 60.26 55.52 13.84 o 8 11 0 922.10 932.83 15.93 o 9 11 0 3.30 1.15 14.36 o 10 11 0 769.84 782.39 18.97 o 11 11 0 122.08 108.51 12.68 o 12 11 0 293.51 284.70 17.08 o 13 11 0 80.11 97.60 15.37 o 14 11 0 276.60 263.82 12.05 o 15 11 0 277.02 348.16 11.90 o 0 12 0 440.44 446.94 28.58 o 1 12 0 12.12 20.94 16.64 o 2 12 0 396.50 430.90 17.16 o 3 12 0 26.44 33.31 16.26 o 4 12 0 174.08 180.12 16.62 o 5 12 0 69.32 67.67 14.17 o 6 12 0 98.90 106.57 12.29 o 7 12 0 46.51 60.42 11.39 o 8 12 0 175.54 177.63 13.72 o 9 12 0 52.90 63.15 13.72 o 10 12 0 84.59 67.83 13.48 o 11 12 0 79.52 81.83 14.72 o 12 12 0 20.06 22.96 10.15 o 13 12 0 76.81 67.12 12.84 o 1 13 0 1093.12 1143.47 20.83 o 2 13 0 148.25 151.55 16.77 o 3 13 0 924.02 970.22 20.36 o 4 13 0 311.93 295.01 14.88 o 5 13 0 519.77 515.72 16.00 o 6 13 0 266.78 291.27 14.35 o 7 13 0 176.86 193.39 15.59 o 8 13 0 221.53 213.02 14.57 o 9 13 0 234.62 217.78 15.30 o 10 13 0 366.50 347.40 14.41 o 11 13 0 64.89 47.49 13.99 o 0 14 0 365.21 354.41 25.70 o 1 14 0 107.08 104.01 16.12 o 2 14 0 988.62 1006.23 22.26 o 3 14 0 249.65 227.61 14.69 o 4 14 0 268.66 263.92 15.32 o 5 14 0 272.78 275.82 14.53 o 6 14 0 128.06 125.48 15.32 o 7 14 0 297.62 286.94 15.42 o 8 14 0 43.33 32.83 13.51 o 9 14 0 231.75 225.15 17.52 o 1 15 0 117.36 109.58 17.97 o 2 15 0 3.17 2.90 13.78 o 3 15 0 67.19 64.97 15.07 o 4 15 0 20.57 11.22 15.84 o 5 15 0 87.95 75.58 17.42 o 6 15 0 104.35 120.69 17.49 o -20 1 1 9.69 0.40 11.82 o -19 1 1 217.18 241.47 14.42 o -18 1 1 13.43 16.56 12.85 o -17 1 1 962.68 978.72 21.76 o -16 1 1 209.03 234.13 12.60 o -15 1 1 536.04 504.59 10.93 o -14 1 1 11.19 24.19 12.25 o -13 1 1 810.08 864.92 13.21 o -12 1 1 2999.71 3083.86 50.17 o -11 1 1 783.00 848.98 14.37 o -10 1 1 1901.09 1799.70 28.08 o -9 1 1 1597.80 1625.78 18.06 o -8 1 1 9625.43 9730.82 160.68 o -7 1 1 1205.50 1067.96 13.50 o -6 1 1 4306.58 4377.01 54.43 o -5 1 1 1183.27 967.26 19.04 o -3 1 1 8623.85 9069.84 81.87 o -2 1 1 4089.25 4025.71 67.52 o 0 1 1 7205.36 7616.93 107.89 o 1 1 1 9602.16 10108.72 221.86 o 2 1 1 540.26 537.44 23.85 o 3 1 1 12943.75 13555.15 245.20 o 4 1 1 128.86 182.11 28.19 o 5 1 1 16610.58 18236.70 414.15 o 6 1 1 19973.91 19771.03 245.81 o 7 1 1 37.52 63.15 14.44 o 8 1 1 11666.30 12428.78 141.99 o 9 1 1 6.79 16.15 14.19 o 10 1 1 4490.93 4278.64 80.26 o 11 1 1 1198.72 1132.06 23.21 o 12 1 1 1905.97 1847.86 34.33 o 13 1 1 1297.19 1342.27 21.31 o 14 1 1 1853.51 1857.34 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12.99 o 10 2 1 673.22 589.28 12.31 o 11 2 1 3976.84 3992.03 69.37 o 12 2 1 1294.83 1406.91 12.68 o 13 2 1 854.78 861.01 15.97 o 14 2 1 556.95 634.56 26.30 o 15 2 1 221.59 227.81 10.72 o 16 2 1 883.93 960.44 15.06 o 17 2 1 248.16 228.44 12.62 o 18 2 1 1456.58 1494.84 24.28 o 19 2 1 1.03 11.08 9.94 o 20 2 1 453.38 441.32 10.84 o -20 3 1 338.12 288.35 35.28 o -19 3 1 104.13 91.69 12.54 o -18 3 1 180.93 156.11 13.04 o -17 3 1 0.84 22.99 12.17 o -16 3 1 238.75 246.35 13.29 o -15 3 1 85.51 90.01 9.85 o -14 3 1 73.83 80.27 10.62 o -13 3 1 471.97 450.04 10.97 o -12 3 1 847.71 867.04 13.27 o -11 3 1 6.53 16.54 10.41 o -10 3 1 42.42 40.90 11.38 o -9 3 1 14.49 20.39 10.73 o -8 3 1 303.16 260.50 11.58 o -7 3 1 13.23 11.59 10.19 o -6 3 1 149.09 178.82 12.00 o -5 3 1 3075.32 2876.05 44.51 o -4 3 1 848.40 814.20 18.62 o -3 3 1 781.99 897.18 25.97 o 0 3 1 8424.95 9995.44 63.61 o 1 3 1 11777.50 13769.18 220.58 o 2 3 1 7.88 43.82 20.74 o 3 3 1 7622.30 8034.34 169.84 o 4 3 1 3187.59 3164.49 58.28 o 5 3 1 521.43 451.95 15.95 o 6 3 1 108.21 67.30 13.99 o 7 3 1 605.75 599.50 16.77 o 8 3 1 286.59 297.72 12.18 o 9 3 1 1976.93 1923.48 22.94 o 10 3 1 3.27 -0.81 11.25 o 11 3 1 36.59 43.59 10.42 o 12 3 1 653.61 630.92 12.07 o 13 3 1 5.55 2.37 9.91 o 14 3 1 3.27 1.04 10.52 o 15 3 1 109.80 95.61 11.11 o 16 3 1 223.55 246.92 15.38 o 17 3 1 792.75 814.48 13.04 o 18 3 1 0.20 -6.34 10.37 o 19 3 1 3.93 21.57 9.25 o 20 3 1 112.25 99.48 11.45 o -20 4 1 108.46 83.48 21.39 o -19 4 1 426.50 423.73 13.83 o -18 4 1 2.80 1.81 10.68 o -17 4 1 497.56 546.68 15.01 o -16 4 1 16.50 16.64 11.77 o -15 4 1 123.30 117.11 11.15 o -14 4 1 252.76 267.58 10.55 o -13 4 1 17.52 28.77 9.78 o -12 4 1 882.91 863.37 11.92 o -11 4 1 29.00 40.69 10.37 o -10 4 1 196.14 233.50 10.98 o -9 4 1 307.43 343.27 12.22 o -8 4 1 702.74 622.06 13.41 o -7 4 1 61.71 66.62 10.97 o -6 4 1 209.14 214.84 13.03 o -5 4 1 35.98 41.96 14.85 o -4 4 1 560.96 640.04 17.91 o -3 4 1 384.91 411.95 18.47 o -2 4 1 6327.87 6793.03 55.82 o 0 4 1 532.31 474.00 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5 2 23.42 48.28 11.68 o 11 5 2 162.90 181.72 17.13 o 12 5 2 140.08 137.83 13.40 o 13 5 2 224.21 219.50 12.33 o 14 5 2 234.72 255.53 12.61 o 15 5 2 224.89 231.66 13.89 o 16 5 2 79.42 58.36 10.25 o 17 5 2 130.67 131.65 11.09 o 18 5 2 16.27 -11.24 11.24 o 19 5 2 108.00 83.08 11.94 o -19 6 2 241.54 227.23 14.83 o -18 6 2 127.93 101.37 11.44 o -17 6 2 165.01 153.04 10.52 o -16 6 2 110.52 94.19 12.09 o -15 6 2 247.58 249.88 12.19 o -14 6 2 34.25 39.64 15.57 o -13 6 2 3902.37 3852.86 22.45 o -12 6 2 44.44 42.50 9.02 o -11 6 2 95.84 127.51 9.05 o -10 6 2 2201.52 2136.82 26.45 o -9 6 2 718.85 754.26 19.83 o -8 6 2 3579.34 3469.12 30.61 o -7 6 2 533.87 644.05 15.99 o -6 6 2 7015.95 6969.88 59.24 o -5 6 2 17.89 8.94 12.85 o -4 6 2 2060.95 2033.27 20.12 o -3 6 2 4451.32 4493.14 36.58 o -2 6 2 4317.75 4369.28 28.84 o -1 6 2 2613.24 2263.40 35.64 o 0 6 2 1720.66 1931.08 31.91 o 1 6 2 1813.02 1684.70 29.98 o 2 6 2 1024.20 1040.89 18.98 o 3 6 2 16051.77 17353.37 327.32 o 4 6 2 3059.97 3731.66 48.00 o 5 6 2 2475.68 2223.12 30.83 o 6 6 2 1574.92 1648.59 33.85 o 7 6 2 708.29 612.53 15.91 o 8 6 2 593.83 546.71 14.12 o 9 6 2 1897.18 1916.55 28.92 o 10 6 2 3800.78 3814.21 69.84 o 11 6 2 3784.80 3675.47 59.34 o 12 6 2 38.63 33.44 10.95 o 13 6 2 164.92 165.88 12.97 o 14 6 2 1851.24 1863.50 28.32 o 15 6 2 172.51 194.64 12.45 o 16 6 2 1093.91 1121.68 16.39 o 17 6 2 191.88 188.48 10.50 o 18 6 2 932.64 859.42 21.21 o 19 6 2 311.51 283.94 31.26 o -18 7 2 480.96 389.49 22.26 o -17 7 2 58.62 56.22 9.51 o -16 7 2 865.23 917.98 15.96 o -15 7 2 212.51 228.09 12.53 o -14 7 2 2485.18 2589.03 33.59 o -13 7 2 322.89 335.56 14.73 o -12 7 2 564.58 531.35 14.25 o -11 7 2 3463.58 3435.55 39.91 o -10 7 2 1.06 22.47 10.71 o -9 7 2 3794.93 3667.10 24.79 o -8 7 2 323.99 305.88 12.23 o -7 7 2 2148.24 2011.15 17.51 o -6 7 2 409.75 349.03 12.63 o -5 7 2 250.80 175.84 14.97 o -4 7 2 2677.27 2688.91 27.98 o -3 7 2 4467.49 4494.97 41.67 o -2 7 2 7906.97 7617.03 93.71 o -1 7 2 792.55 906.07 18.76 o 0 7 2 1672.93 1583.98 25.83 o 1 7 2 3064.68 3028.11 28.52 o 2 7 2 4842.54 4573.69 51.27 o 3 7 2 15.35 6.48 14.26 o 4 7 2 2127.36 1892.93 26.42 o 5 7 2 249.95 215.34 13.63 o 6 7 2 2360.81 2233.01 45.88 o 7 7 2 2023.03 2030.18 53.73 o 8 7 2 355.01 279.08 13.12 o 9 7 2 484.01 409.73 20.28 o 10 7 2 857.41 872.06 19.91 o 11 7 2 409.24 417.27 12.94 o 12 7 2 59.65 54.25 12.45 o 13 7 2 195.12 209.72 13.88 o 14 7 2 51.78 52.69 13.08 o 15 7 2 837.30 910.19 14.86 o 16 7 2 7.11 15.48 11.26 o 17 7 2 787.84 823.43 29.10 o 18 7 2 280.84 284.73 11.54 o -18 8 2 3.23 41.46 16.51 o -17 8 2 50.01 50.96 10.94 o -16 8 2 102.35 120.40 10.25 o -15 8 2 97.73 93.30 11.17 o -14 8 2 240.14 256.64 12.06 o -13 8 2 27.81 46.67 11.14 o -12 8 2 224.72 244.61 13.56 o -11 8 2 219.50 229.70 12.13 o -10 8 2 951.84 916.28 16.43 o -9 8 2 126.82 131.06 10.91 o -8 8 2 852.77 891.49 13.79 o -7 8 2 830.27 815.81 13.89 o -6 8 2 2160.77 2099.51 17.94 o -5 8 2 1738.24 1810.98 20.62 o -4 8 2 4.68 13.16 15.73 o -3 8 2 1227.09 1181.45 19.81 o -2 8 2 617.84 690.62 20.34 o -1 8 2 10084.93 10641.85 78.44 o 0 8 2 1458.98 1627.22 27.68 o 1 8 2 911.02 808.17 18.10 o 2 8 2 97.54 88.15 17.46 o 3 8 2 137.19 155.97 17.27 o 4 8 2 84.66 82.76 16.31 o 5 8 2 475.05 424.45 16.58 o 6 8 2 130.11 126.90 15.42 o 7 8 2 268.91 252.13 13.99 o 8 8 2 481.16 500.28 14.70 o 9 8 2 454.70 424.03 15.52 o 10 8 2 175.96 159.23 13.32 o 11 8 2 97.02 78.59 14.23 o 12 8 2 14.13 9.14 13.49 o 13 8 2 413.07 415.56 15.23 o 14 8 2 320.20 348.14 13.55 o 15 8 2 12.24 24.13 14.57 o 16 8 2 282.87 274.55 12.64 o 17 8 2 403.79 362.94 13.86 o -17 9 2 55.48 49.60 11.98 o -16 9 2 246.19 226.52 11.08 o -15 9 2 13.77 15.15 10.51 o -14 9 2 263.20 250.06 11.57 o -13 9 2 1.90 -0.56 11.27 o -12 9 2 2254.46 2368.40 22.58 o -11 9 2 856.17 962.96 17.09 o -10 9 2 463.49 452.21 15.26 o -9 9 2 9.21 17.85 9.19 o -8 9 2 96.90 127.88 11.63 o -7 9 2 1980.27 2020.20 18.04 o -6 9 2 314.06 289.43 13.50 o -5 9 2 653.94 726.08 16.14 o -4 9 2 170.64 146.53 15.39 o -3 9 2 618.39 606.81 16.09 o -2 9 2 15.09 17.65 14.31 o -1 9 2 823.73 838.95 21.29 o 0 9 2 5.66 12.92 15.82 o 1 9 2 784.76 807.56 16.68 o 2 9 2 127.74 127.63 17.16 o 3 9 2 26.82 33.22 15.57 o 4 9 2 1604.92 1589.45 25.70 o 5 9 2 7.79 9.49 12.26 o 6 9 2 224.39 204.17 12.69 o 7 9 2 112.13 80.34 10.55 o 8 9 2 1516.07 1393.60 25.29 o 9 9 2 82.25 112.49 11.97 o 10 9 2 309.76 341.71 13.47 o 11 9 2 944.19 951.35 18.22 o 12 9 2 1119.72 1147.30 17.13 o 13 9 2 631.49 616.19 15.35 o 14 9 2 161.53 182.11 13.99 o 15 9 2 1011.10 992.59 15.84 o 16 9 2 93.17 92.82 11.86 o -16 10 2 33.94 51.36 22.45 o -15 10 2 423.70 381.78 16.06 o -14 10 2 497.78 503.15 12.82 o -13 10 2 1480.30 1548.81 17.22 o -12 10 2 3025.25 3212.60 28.60 o -11 10 2 214.91 230.21 12.01 o -10 10 2 1066.38 1174.23 22.44 o -9 10 2 157.96 125.54 12.35 o -8 10 2 2244.88 2159.52 29.39 o -7 10 2 41.41 31.10 11.17 o -6 10 2 1909.75 1949.11 27.06 o -5 10 2 566.11 542.82 14.83 o -4 10 2 2634.04 2656.44 21.35 o -3 10 2 1897.36 1940.83 20.63 o -2 10 2 17.31 24.45 15.98 o -1 10 2 2649.58 2585.43 49.26 o 0 10 2 30.90 31.62 17.95 o 1 10 2 2533.02 2529.03 49.57 o 2 10 2 0.08 7.06 13.25 o 3 10 2 4453.12 4388.24 26.95 o 4 10 2 788.81 827.40 17.49 o 5 10 2 1684.51 1746.98 39.53 o 6 10 2 5066.85 5095.13 48.53 o 7 10 2 558.13 553.71 16.27 o 8 10 2 2664.44 2725.93 41.85 o 9 10 2 106.62 82.83 12.98 o 10 10 2 2497.70 2718.41 69.14 o 11 10 2 17.49 10.86 12.99 o 12 10 2 2066.74 2112.48 30.77 o 13 10 2 151.78 154.22 11.79 o 14 10 2 857.13 820.86 16.40 o 15 10 2 259.95 240.49 13.46 o -14 11 2 553.21 543.82 14.05 o -13 11 2 1481.33 1420.75 24.21 o -12 11 2 16.73 15.71 11.34 o -11 11 2 1088.45 1145.41 17.24 o -10 11 2 9.66 12.46 10.55 o -9 11 2 1096.52 1111.08 14.92 o -8 11 2 463.14 474.16 13.01 o -7 11 2 1307.59 1346.55 29.99 o -6 11 2 197.82 189.52 14.32 o -5 11 2 237.24 247.13 12.50 o -4 11 2 1206.33 1225.05 19.05 o -3 11 2 736.62 740.42 18.38 o -2 11 2 3500.38 3408.78 63.69 o -1 11 2 2110.97 2039.98 77.73 o 0 11 2 605.32 605.51 18.77 o 1 11 2 55.93 48.68 17.76 o 2 11 2 368.10 381.72 16.80 o 3 11 2 753.92 719.33 17.52 o 4 11 2 71.06 89.60 13.93 o 5 11 2 555.11 575.72 17.63 o 6 11 2 9.78 9.36 17.60 o 7 11 2 1093.95 1104.59 26.98 o 8 11 2 74.62 85.68 16.63 o 9 11 2 136.34 164.56 16.22 o 10 11 2 6.37 2.74 13.65 o 11 11 2 452.68 452.26 13.87 o 12 11 2 20.42 17.64 13.04 o 13 11 2 180.30 186.25 13.81 o 14 11 2 6.60 15.21 13.69 o -13 12 2 6.69 9.09 15.78 o -12 12 2 0.92 6.59 9.08 o -11 12 2 193.52 165.67 11.35 o -10 12 2 45.28 50.72 9.83 o -9 12 2 24.22 5.25 10.96 o -8 12 2 2.22 11.83 11.83 o -7 12 2 88.75 94.03 12.27 o -6 12 2 37.98 36.07 13.09 o -5 12 2 4.97 8.99 14.38 o -4 12 2 262.19 290.77 14.10 o -3 12 2 126.84 158.41 17.58 o -2 12 2 648.76 635.88 21.40 o -1 12 2 163.85 118.67 54.16 o 0 12 2 231.37 248.29 26.05 o 1 12 2 103.55 140.32 25.14 o 2 12 2 53.76 58.94 19.86 o 3 12 2 13.16 14.69 19.35 o 4 12 2 93.23 100.37 18.75 o 5 12 2 1.04 1.83 15.01 o 6 12 2 200.53 213.48 14.96 o 7 12 2 0.74 14.20 14.09 o 8 12 2 2.06 10.31 13.81 o 9 12 2 0.05 4.64 14.87 o 10 12 2 126.73 131.73 15.03 o 11 12 2 31.36 33.97 13.05 o 12 12 2 1.28 4.33 9.90 o 13 12 2 31.96 32.76 14.87 o -11 13 2 2302.50 2151.19 34.28 o -10 13 2 120.56 107.76 10.72 o -9 13 2 115.05 126.50 10.86 o -8 13 2 113.01 83.50 10.63 o -7 13 2 1362.77 1303.14 16.60 o -6 13 2 492.57 532.82 16.59 o -5 13 2 2033.34 2003.09 23.83 o -4 13 2 1297.16 1203.32 22.84 o -3 13 2 320.99 334.61 19.19 o -2 13 2 804.26 792.75 20.65 o -1 13 2 233.95 234.72 23.13 o 0 13 2 2192.94 2111.97 174.28 o 1 13 2 179.05 196.24 24.79 o 2 13 2 791.84 863.39 26.31 o 3 13 2 60.61 58.10 23.12 o 4 13 2 1665.75 1785.14 91.39 o 5 13 2 470.40 456.88 19.73 o 6 13 2 122.07 143.73 17.15 o 7 13 2 301.90 294.59 16.72 o 8 13 2 239.74 218.11 14.21 o 9 13 2 265.88 270.14 13.33 o 10 13 2 10.52 17.59 12.61 o 11 13 2 404.74 413.34 22.69 o -9 14 2 77.37 56.65 13.60 o -8 14 2 370.84 340.22 13.93 o -7 14 2 275.46 247.23 11.58 o -6 14 2 717.25 722.89 17.29 o -5 14 2 235.56 222.42 16.26 o -4 14 2 1804.78 1679.22 72.28 o -3 14 2 2371.43 2113.61 29.49 o -2 14 2 10.61 20.80 20.87 o -1 14 2 792.24 772.51 20.55 o 0 14 2 99.03 105.78 21.74 o 1 14 2 1082.20 1061.92 47.92 o 2 14 2 51.31 45.17 21.51 o 3 14 2 1400.45 1400.77 30.87 o 4 14 2 61.21 72.85 21.68 o 5 14 2 1438.64 1352.60 25.95 o 6 14 2 279.27 232.86 16.46 o 7 14 2 217.70 235.35 16.89 o 8 14 2 215.32 222.88 18.26 o 9 14 2 65.55 71.30 21.73 o -5 15 2 264.86 285.86 25.03 o -4 15 2 7.84 19.44 23.30 o -3 15 2 228.98 195.52 26.76 o -2 15 2 683.79 554.84 40.19 o -1 15 2 21.55 18.27 19.85 o 0 15 2 7.76 29.24 19.65 o 1 15 2 1.49 2.17 16.33 o 2 15 2 92.84 85.48 24.28 o 3 15 2 0.00 -4.20 23.83 o 4 15 2 223.47 239.04 25.54 o 5 15 2 22.36 16.13 19.97 o -20 1 3 121.40 83.20 13.20 o -19 1 3 65.36 54.10 12.38 o -18 1 3 622.39 692.08 13.54 o -17 1 3 1244.80 1296.45 16.28 o -16 1 3 1561.93 1582.28 36.70 o -15 1 3 1507.27 1564.85 25.75 o -14 1 3 19.62 30.45 13.63 o -13 1 3 4281.37 4293.27 54.37 o -12 1 3 30.20 36.46 13.84 o -11 1 3 3352.30 3231.84 36.99 o -10 1 3 7.18 39.27 11.56 o -9 1 3 716.72 637.72 15.06 o -8 1 3 3896.17 3874.50 55.81 o -7 1 3 4289.05 4283.76 43.98 o -6 1 3 3482.26 3035.14 19.99 o -5 1 3 7137.33 6917.18 35.06 o -4 1 3 1821.28 1863.35 21.97 o -3 1 3 2292.74 2576.61 43.17 o -2 1 3 69.41 65.63 19.45 o -1 1 3 19.05 54.51 23.94 o 1 1 3 5.97 71.27 20.63 o 2 1 3 5892.61 6081.70 93.94 o 3 1 3 92.02 116.17 26.73 o 4 1 3 4907.91 5103.78 45.54 o 5 1 3 2693.34 2465.48 21.28 o 6 1 3 883.96 843.89 16.12 o 7 1 3 5330.03 5009.94 90.11 o 8 1 3 1022.38 1142.41 23.60 o 9 1 3 6060.48 5509.33 52.44 o 10 1 3 90.35 70.92 13.42 o 11 1 3 3084.40 3008.06 31.48 o 12 1 3 293.72 284.54 13.15 o 13 1 3 1910.56 1971.71 19.56 o 14 1 3 1042.73 1077.38 22.63 o 15 1 3 634.51 579.44 13.25 o 16 1 3 2514.95 2527.87 27.66 o 17 1 3 1.97 23.12 9.75 o 18 1 3 1030.48 1065.42 18.04 o 19 1 3 1.14 10.68 9.86 o 20 1 3 388.85 389.36 21.00 o -20 2 3 187.47 196.84 23.45 o -19 2 3 497.40 494.05 16.14 o -18 2 3 985.22 999.61 29.42 o -17 2 3 1073.35 1097.52 17.61 o -16 2 3 545.72 593.28 17.08 o -15 2 3 486.10 529.17 19.20 o -14 2 3 8127.55 8121.67 38.30 o -13 2 3 530.07 522.44 13.54 o -12 2 3 1797.07 1806.04 14.24 o -11 2 3 143.40 182.39 17.41 o -10 2 3 5365.47 4940.88 18.92 o -9 2 3 1888.90 1716.84 17.82 o -8 2 3 2053.23 1959.20 19.99 o -7 2 3 9628.52 8960.57 69.36 o -6 2 3 1164.24 1091.13 18.76 o -5 2 3 7846.59 7604.56 73.78 o -4 2 3 5.28 39.29 14.83 o -3 2 3 15641.16 15279.86 197.12 o -2 2 3 1351.54 1453.33 33.21 o -1 2 3 421.61 450.85 24.21 o 0 2 3 15196.06 17112.41 467.46 o 1 2 3 11923.63 12461.76 183.26 o 2 2 3 5466.95 5239.49 36.20 o 3 2 3 322.73 315.59 22.57 o 4 2 3 616.59 467.06 17.31 o 5 2 3 2019.69 1850.83 40.31 o 6 2 3 123.47 67.40 16.44 o 7 2 3 641.19 677.97 17.28 o 8 2 3 3300.54 3000.86 23.90 o 9 2 3 901.66 1136.35 16.26 o 10 2 3 1600.07 1513.97 33.97 o 11 2 3 165.54 178.67 11.39 o 12 2 3 3875.38 3775.79 36.60 o 13 2 3 10.57 7.32 9.92 o 14 2 3 1022.09 1023.77 18.54 o 15 2 3 823.53 876.44 13.71 o 16 2 3 798.24 827.97 18.57 o 17 2 3 3106.79 3018.49 39.54 o 18 2 3 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