#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2012671.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012671_Fobs loop_ _publ_author_name 'Naumov, Dmitry Yu.' 'Naumova, Marina I.' 'Kuratieva, Natalia V.' 'Boldyreva, Elena V.' 'Howard, Judith A. K.' _publ_section_title ; Copper(II) hypophosphite: the \a- and \b-forms at 270 and 100K, and the \g-form at 270K ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i55 _journal_page_last i60 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.835 _cell_angle_gamma 90.000 _cell_length_a 7.2186 _cell_length_b 5.3462 _cell_length_c 6.2521 _exptl_crystal_F_000 190.00 _reflns_d_resolution_high 0.7312 _[local]_cod_data_source_file av1101alpha270sup2.hkl _[local]_cod_data_source_block alpha270 #BEGIN Tags that were not found in dictionaries: _shelx_title ' a-Cu(H2PO2)2 in P2(1)/c, T=270K, SMART CCD, FaceABS' _shelx_refln_list_code 4 _shelx_f_calc_maximum 97.84 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 5538.20 6353.08 411.67 o 2 0 0 267.24 298.97 6.10 o 3 0 0 1576.89 1423.26 44.79 o 4 0 0 4498.58 4393.49 79.08 o 5 0 0 252.67 261.13 10.50 o 6 0 0 44.04 50.20 6.33 o 7 0 0 713.29 725.17 23.70 o 8 0 0 1171.05 1183.35 36.00 o 9 0 0 115.90 84.16 11.30 o 1 1 0 767.22 784.05 26.97 o 2 1 0 107.47 137.63 6.06 o 3 1 0 1267.00 1324.75 27.86 o 4 1 0 51.94 51.95 2.83 o 5 1 0 273.31 293.26 7.39 o 6 1 0 28.02 45.27 8.60 o 7 1 0 27.62 10.57 5.93 o 8 1 0 0.80 4.73 4.39 o 9 1 0 18.36 29.90 7.68 o 0 2 0 5980.10 5905.47 149.44 o 1 2 0 1920.51 1900.90 86.99 o 2 2 0 608.81 658.77 20.89 o 3 2 0 2187.49 2109.38 104.12 o 4 2 0 1961.60 1861.11 31.34 o 5 2 0 169.54 176.95 4.15 o 6 2 0 80.19 82.09 5.34 o 7 2 0 856.35 851.32 19.33 o 8 2 0 546.69 575.93 25.77 o 9 2 0 15.66 11.65 12.55 o 1 3 0 130.97 107.99 3.90 o 2 3 0 299.91 334.39 11.11 o 3 3 0 791.23 793.48 17.92 o 4 3 0 7.10 11.45 4.33 o 5 3 0 234.81 244.22 5.68 o 6 3 0 18.62 28.48 6.97 o 7 3 0 34.94 46.83 5.13 o 8 3 0 90.29 115.76 16.29 o 0 4 0 798.24 804.23 33.08 o 1 4 0 436.19 456.89 21.53 o 2 4 0 369.41 369.88 8.26 o 3 4 0 957.98 981.28 28.02 o 4 4 0 1119.01 1127.87 19.50 o 5 4 0 436.46 421.45 9.76 o 6 4 0 195.25 212.44 6.76 o 7 4 0 281.62 287.62 15.02 o 8 4 0 162.17 147.93 12.64 o 1 5 0 249.48 256.76 17.03 o 2 5 0 20.75 27.02 3.15 o 3 5 0 209.25 211.57 6.70 o 4 5 0 42.72 32.49 4.29 o 5 5 0 107.76 118.53 11.11 o 6 5 0 85.39 95.97 7.19 o 7 5 0 74.71 68.76 10.10 o 0 6 0 197.31 207.55 9.94 o 1 6 0 205.11 236.44 17.18 o 2 6 0 190.47 167.92 7.35 o 3 6 0 186.67 192.58 9.56 o 4 6 0 308.52 295.45 11.71 o 5 6 0 351.16 353.11 13.32 o 1 7 0 291.86 274.76 10.13 o 2 7 0 7.45 25.94 6.67 o -9 1 1 151.96 175.34 8.41 o -8 1 1 17.23 11.74 6.95 o -7 1 1 891.14 915.02 20.43 o -6 1 1 2428.61 2350.82 44.98 o -5 1 1 608.65 614.26 9.17 o -4 1 1 136.32 133.79 2.95 o -3 1 1 1829.07 1610.38 21.18 o -2 1 1 2982.24 2895.21 37.10 o -1 1 1 75.85 85.98 2.16 o 0 1 1 1030.74 1055.14 13.61 o 1 1 1 9247.28 9994.18 102.59 o 2 1 1 4600.07 4841.68 77.43 o 3 1 1 571.02 562.29 17.87 o 4 1 1 1374.09 1250.77 29.96 o 5 1 1 2586.74 2466.05 46.39 o 6 1 1 269.34 306.24 21.84 o 7 1 1 16.26 10.51 4.26 o 8 1 1 251.99 248.86 9.32 o 9 1 1 514.92 518.95 14.68 o -9 2 1 122.33 117.85 11.89 o -8 2 1 20.50 22.88 4.80 o -7 2 1 79.25 66.12 13.64 o -6 2 1 13.44 17.85 4.23 o -5 2 1 3.38 4.81 2.41 o -4 2 1 135.54 147.25 5.24 o -3 2 1 212.01 228.71 12.02 o -2 2 1 36.92 34.14 2.27 o -1 2 1 233.47 238.84 5.22 o 0 2 1 134.26 159.10 2.54 o 1 2 1 405.42 493.77 12.35 o 2 2 1 215.14 204.85 3.37 o 3 2 1 140.97 145.51 4.45 o 4 2 1 480.28 493.29 9.09 o 5 2 1 9.60 11.56 2.48 o 6 2 1 46.81 45.32 3.91 o 7 2 1 28.70 33.20 4.78 o 8 2 1 48.04 46.86 6.01 o 9 2 1 38.05 47.37 9.47 o -9 3 1 35.10 36.15 8.67 o -8 3 1 28.96 25.90 6.67 o -7 3 1 618.63 610.76 17.47 o -6 3 1 876.52 849.15 15.51 o -5 3 1 58.35 62.17 6.79 o -4 3 1 173.39 177.65 4.91 o -3 3 1 3106.69 3017.61 39.71 o -2 3 1 3623.18 3441.03 51.75 o -1 3 1 172.61 157.82 6.30 o 0 3 1 221.94 212.40 3.95 o 1 3 1 3359.12 3320.73 72.98 o 2 3 1 2232.62 2210.71 45.15 o 3 3 1 65.33 68.87 5.11 o 4 3 1 145.19 144.08 3.88 o 5 3 1 1316.38 1287.97 18.37 o 6 3 1 715.64 724.47 16.77 o 7 3 1 59.93 56.66 5.29 o 8 3 1 98.51 108.38 6.83 o -8 4 1 27.46 25.77 7.95 o -7 4 1 141.17 141.13 16.02 o -6 4 1 123.29 106.48 8.35 o -5 4 1 182.00 197.15 25.97 o -4 4 1 506.40 513.45 15.84 o -3 4 1 486.14 480.94 8.56 o -2 4 1 647.31 645.67 10.54 o -1 4 1 619.45 621.07 21.04 o 0 4 1 452.08 470.39 10.61 o 1 4 1 198.53 197.42 6.32 o 2 4 1 610.70 607.68 10.04 o 3 4 1 122.51 116.73 6.49 o 4 4 1 540.16 538.05 13.43 o 5 4 1 144.88 130.85 4.93 o 6 4 1 124.27 125.77 4.19 o 7 4 1 5.97 13.53 5.29 o -7 5 1 43.41 43.23 5.71 o -6 5 1 112.03 106.78 10.39 o -5 5 1 275.11 277.86 12.16 o -4 5 1 423.30 419.40 18.94 o -3 5 1 495.94 506.03 9.51 o -2 5 1 669.02 674.11 20.01 o -1 5 1 843.88 809.75 13.29 o 0 5 1 676.79 654.81 11.77 o 1 5 1 260.84 280.12 6.80 o 2 5 1 103.51 122.01 4.68 o 3 5 1 182.08 185.47 7.74 o 4 5 1 300.63 312.42 14.24 o 5 5 1 269.95 251.05 7.95 o 6 5 1 172.12 151.68 6.86 o -5 6 1 146.65 161.87 13.63 o -4 6 1 15.81 19.08 7.36 o -3 6 1 62.89 66.05 9.13 o -2 6 1 88.74 83.15 5.68 o -1 6 1 29.65 29.98 3.82 o 0 6 1 256.57 272.19 11.85 o 1 6 1 73.69 82.39 5.12 o 2 6 1 132.46 143.56 6.08 o 3 6 1 9.73 16.77 7.10 o 4 6 1 111.05 109.18 10.51 o -2 7 1 79.94 69.08 5.17 o -1 7 1 319.70 314.21 11.50 o 0 7 1 253.36 225.52 13.35 o 1 7 1 39.05 27.63 4.86 o 2 7 1 73.69 65.91 7.58 o -9 0 2 655.60 682.78 25.15 o -8 0 2 184.22 214.17 12.99 o -7 0 2 29.06 29.32 6.25 o -6 0 2 1075.14 1101.16 32.51 o -5 0 2 5899.56 6125.05 110.73 o -4 0 2 1920.32 1906.71 35.71 o -3 0 2 4.11 11.05 4.92 o -2 0 2 2941.64 2841.16 51.57 o -1 0 2 9573.05 9965.29 251.23 o 0 0 2 129.10 111.97 3.37 o 1 0 2 790.04 916.87 14.75 o 2 0 2 2104.12 1837.52 49.33 o 3 0 2 6393.14 6748.07 183.81 o 4 0 2 868.92 859.10 17.52 o 5 0 2 129.16 133.05 5.96 o 6 0 2 1318.63 1370.10 63.44 o 7 0 2 823.95 855.68 29.90 o 8 0 2 12.04 18.58 4.97 o -9 1 2 2.59 0.35 6.35 o -8 1 2 94.35 94.85 6.58 o -7 1 2 1.23 14.34 3.76 o -6 1 2 80.91 75.16 5.86 o -5 1 2 37.96 36.40 2.12 o -4 1 2 342.10 354.89 5.39 o -3 1 2 165.68 171.95 3.64 o -2 1 2 1714.13 1857.42 24.36 o -1 1 2 36.82 41.23 2.67 o 0 1 2 800.35 839.25 12.15 o 1 1 2 26.16 35.50 1.89 o 2 1 2 162.50 169.76 2.36 o 3 1 2 39.84 39.10 2.05 o 4 1 2 249.21 262.79 5.47 o 5 1 2 0.32 8.30 2.35 o 6 1 2 93.82 103.43 4.11 o 7 1 2 9.54 16.63 3.91 o 8 1 2 1.07 7.66 4.12 o 9 1 2 0.37 7.02 6.88 o -9 2 2 403.60 408.84 13.92 o -8 2 2 380.41 377.45 22.58 o -7 2 2 43.74 36.44 6.33 o -6 2 2 427.83 416.90 8.88 o -5 2 2 1944.92 1885.29 33.75 o -4 2 2 1247.63 1187.51 19.10 o -3 2 2 465.79 478.84 7.66 o -2 2 2 1977.39 1860.62 24.73 o -1 2 2 2961.48 2705.87 68.70 o 0 2 2 453.00 411.30 5.62 o 1 2 2 453.13 440.77 5.45 o 2 2 2 2627.46 2452.24 47.44 o 3 2 2 2036.24 1952.51 21.00 o 4 2 2 144.64 142.91 3.34 o 5 2 2 250.11 261.68 9.21 o 6 2 2 1264.25 1266.64 22.69 o 7 2 2 436.00 457.62 10.71 o 8 2 2 1.64 9.57 4.23 o -8 3 2 154.15 155.27 7.91 o -7 3 2 61.17 53.62 7.68 o -6 3 2 78.18 79.77 5.06 o -5 3 2 3.32 16.42 5.63 o -4 3 2 224.67 234.55 7.78 o -3 3 2 147.31 147.69 5.40 o -2 3 2 1011.15 1038.61 19.84 o -1 3 2 0.28 8.52 2.55 o 0 3 2 242.73 225.80 3.77 o 1 3 2 61.27 63.07 2.01 o 2 3 2 32.58 34.18 1.76 o 3 3 2 431.39 423.37 7.05 o 4 3 2 179.60 182.52 3.89 o 5 3 2 195.26 188.77 7.32 o 6 3 2 112.58 117.64 8.38 o 7 3 2 31.58 37.07 6.03 o 8 3 2 0.10 2.91 4.93 o -8 4 2 237.55 213.59 10.16 o -7 4 2 106.97 98.15 5.24 o -6 4 2 197.35 194.29 8.10 o -5 4 2 413.01 407.09 19.82 o -4 4 2 262.25 251.96 6.78 o -3 4 2 193.55 191.19 5.56 o -2 4 2 814.31 843.37 23.93 o -1 4 2 1508.41 1501.37 45.85 o 0 4 2 925.99 943.26 35.26 o 1 4 2 735.25 733.91 13.39 o 2 4 2 982.68 999.34 29.45 o 3 4 2 600.59 619.41 14.76 o 4 4 2 98.03 103.82 14.12 o 5 4 2 84.55 73.20 5.14 o 6 4 2 278.22 277.61 9.83 o 7 4 2 188.42 183.06 15.17 o -7 5 2 14.27 16.74 9.22 o -6 5 2 128.20 129.76 8.15 o -5 5 2 2.92 6.54 5.18 o -4 5 2 181.66 193.03 6.12 o -3 5 2 5.82 9.04 5.37 o -2 5 2 223.23 222.61 12.17 o -1 5 2 42.70 34.18 4.97 o 0 5 2 159.29 160.96 7.24 o 1 5 2 145.84 145.77 5.55 o 2 5 2 154.30 165.78 10.24 o 3 5 2 126.79 121.99 6.89 o 4 5 2 51.82 58.47 6.08 o 5 5 2 165.43 160.09 8.44 o 6 5 2 34.82 42.85 10.15 o -5 6 2 101.63 98.50 8.19 o -4 6 2 79.93 67.62 16.05 o -3 6 2 127.48 135.64 5.62 o -2 6 2 240.98 243.10 33.73 o -1 6 2 408.79 455.46 13.85 o 0 6 2 473.64 524.74 28.69 o 1 6 2 296.10 311.76 8.67 o 2 6 2 151.68 163.26 8.69 o 3 6 2 195.15 176.37 21.56 o 4 6 2 197.10 205.93 12.27 o -2 7 2 101.80 121.88 14.87 o -1 7 2 30.62 29.54 7.66 o 0 7 2 166.33 154.04 20.54 o -9 1 3 10.72 7.68 8.80 o -8 1 3 502.95 514.66 34.03 o -7 1 3 703.01 769.05 17.97 o -6 1 3 22.79 33.18 2.79 o -5 1 3 187.29 184.69 6.55 o -4 1 3 2838.64 2802.42 32.95 o -3 1 3 2740.05 2651.26 46.29 o -2 1 3 697.85 680.09 11.36 o -1 1 3 2628.40 2759.21 50.69 o 0 1 3 4787.12 4484.67 83.96 o 1 1 3 781.84 754.84 9.52 o 2 1 3 3.84 5.00 1.44 o 3 1 3 793.55 778.98 9.04 o 4 1 3 1930.95 1892.43 25.48 o 5 1 3 181.01 182.36 5.77 o 6 1 3 19.97 20.80 4.75 o 7 1 3 637.75 655.10 17.06 o 8 1 3 573.75 608.03 40.47 o -9 2 3 17.34 24.92 6.99 o -8 2 3 87.94 81.30 6.26 o -7 2 3 2.07 1.25 3.25 o -6 2 3 70.46 68.61 3.64 o -5 2 3 4.88 6.44 1.88 o -4 2 3 33.46 30.02 2.65 o -3 2 3 203.69 219.48 4.70 o -2 2 3 6.15 9.26 2.03 o -1 2 3 416.95 442.50 10.42 o 0 2 3 46.28 50.54 1.94 o 1 2 3 0.54 5.78 1.42 o 2 2 3 223.33 217.77 4.61 o 3 2 3 126.29 120.40 3.68 o 4 2 3 204.33 197.64 6.00 o 5 2 3 238.30 232.45 6.47 o 6 2 3 27.08 33.71 3.86 o 7 2 3 59.90 55.66 5.73 o 8 2 3 15.54 12.56 5.22 o -8 3 3 587.92 594.95 60.64 o -7 3 3 616.46 607.13 12.68 o -6 3 3 36.59 35.67 4.73 o -5 3 3 181.59 176.87 6.36 o -4 3 3 1937.95 1887.76 42.86 o -3 3 3 1360.76 1303.65 25.73 o -2 3 3 11.43 10.16 2.19 o -1 3 3 251.70 254.96 6.01 o 0 3 3 2561.37 2497.56 34.83 o 1 3 3 1650.35 1588.60 33.58 o 2 3 3 151.49 145.89 4.11 o 3 3 3 363.78 363.90 7.93 o 4 3 3 1153.91 1127.29 16.39 o 5 3 3 399.01 401.44 11.03 o 6 3 3 35.90 35.22 5.73 o 7 3 3 108.57 104.93 7.74 o -7 4 3 162.65 159.64 7.06 o -6 4 3 140.86 141.64 12.12 o -5 4 3 256.06 243.41 8.09 o -4 4 3 83.87 86.80 4.79 o -3 4 3 651.12 651.64 25.00 o -2 4 3 127.10 121.23 8.35 o -1 4 3 859.83 904.78 20.39 o 0 4 3 233.65 243.49 9.72 o 1 4 3 311.81 325.95 7.72 o 2 4 3 6.97 13.26 5.18 o 3 4 3 349.22 339.24 11.93 o 4 4 3 0.77 9.97 8.44 o 5 4 3 185.54 172.51 11.36 o 6 4 3 0.06 5.95 6.09 o -6 5 3 340.63 334.65 11.42 o -5 5 3 325.31 313.20 11.12 o -4 5 3 182.45 182.46 15.98 o -3 5 3 121.30 139.14 7.37 o -2 5 3 187.25 219.30 9.40 o -1 5 3 314.37 303.09 29.23 o 0 5 3 299.00 320.30 12.39 o 1 5 3 293.89 287.30 7.84 o 2 5 3 459.45 435.85 12.51 o 3 5 3 557.05 552.42 20.71 o 4 5 3 319.21 296.22 39.37 o 5 5 3 85.99 82.89 9.89 o -4 6 3 59.09 53.73 6.95 o -3 6 3 79.39 78.04 7.33 o -2 6 3 4.56 10.31 8.84 o -1 6 3 144.23 145.73 9.28 o 0 6 3 2.54 14.52 6.52 o 1 6 3 209.56 222.46 8.24 o 2 6 3 5.11 22.53 12.94 o 3 6 3 192.47 166.70 15.55 o -9 0 4 157.54 168.73 13.36 o -8 0 4 2.02 5.42 6.11 o -7 0 4 774.36 747.53 25.43 o -6 0 4 2084.16 2112.73 33.39 o -5 0 4 41.52 31.59 5.50 o -4 0 4 194.39 190.10 6.60 o -3 0 4 1694.38 1680.12 43.76 o -2 0 4 4559.67 4311.87 118.39 o -1 0 4 594.77 570.95 18.03 o 0 0 4 312.11 294.53 11.66 o 1 0 4 3521.66 3564.24 65.36 o 2 0 4 3138.37 3213.83 116.35 o 3 0 4 91.49 96.15 4.57 o 4 0 4 22.79 29.05 5.64 o 5 0 4 629.94 635.72 21.91 o 6 0 4 292.30 270.37 12.89 o 7 0 4 11.54 5.95 5.48 o -9 1 4 40.06 31.66 6.98 o -8 1 4 19.43 23.55 5.95 o -7 1 4 153.84 145.52 9.39 o -6 1 4 0.01 6.04 3.18 o -5 1 4 108.41 109.93 4.21 o -4 1 4 14.01 22.39 3.92 o -3 1 4 139.85 153.07 4.75 o -2 1 4 115.14 115.53 6.29 o -1 1 4 521.55 552.40 12.64 o 0 1 4 0.79 5.83 2.64 o 1 1 4 293.50 303.57 7.69 o 2 1 4 20.39 16.77 1.79 o 3 1 4 10.29 12.48 2.15 o 4 1 4 14.96 7.47 5.20 o 5 1 4 20.26 19.02 4.29 o 6 1 4 2.73 4.70 4.68 o 7 1 4 8.44 15.74 4.60 o -8 2 4 34.17 43.60 5.52 o -7 2 4 387.79 381.93 8.09 o -6 2 4 932.43 929.53 12.89 o -5 2 4 204.87 204.14 7.45 o -4 2 4 120.87 118.09 7.34 o -3 2 4 1516.52 1487.99 20.76 o -2 2 4 1582.82 1434.95 23.36 o -1 2 4 213.78 211.54 13.26 o 0 2 4 651.34 644.55 10.44 o 1 2 4 2526.80 2429.67 47.37 o 2 2 4 1105.29 1084.46 13.25 o 3 2 4 16.99 17.04 6.10 o 4 2 4 227.10 235.63 8.98 o 5 2 4 960.15 959.28 17.16 o 6 2 4 204.85 207.45 11.92 o 7 2 4 1.48 17.44 9.24 o -8 3 4 10.47 20.80 6.39 o -7 3 4 210.16 209.78 14.56 o -6 3 4 1.12 10.08 3.85 o -5 3 4 80.27 87.41 7.89 o -4 3 4 53.04 54.54 7.92 o -3 3 4 67.65 67.01 4.50 o -2 3 4 368.66 385.79 15.48 o -1 3 4 315.11 317.09 7.75 o 0 3 4 184.74 184.15 4.63 o 1 3 4 183.34 186.34 4.61 o 2 3 4 62.64 65.15 2.48 o 3 3 4 1.75 4.88 2.03 o 4 3 4 324.97 310.49 6.53 o 6 3 4 129.70 113.92 7.60 o -7 4 4 165.87 160.61 9.29 o -6 4 4 410.16 405.32 17.83 o -5 4 4 338.64 347.74 16.69 o -4 4 4 358.01 386.64 11.58 o -3 4 4 758.49 775.78 18.37 o -2 4 4 639.46 640.57 15.87 o -1 4 4 158.99 165.49 6.88 o 0 4 4 152.89 173.10 9.15 o 1 4 4 440.28 454.08 9.87 o 2 4 4 358.17 363.45 15.19 o 3 4 4 138.45 160.03 6.93 o 4 4 4 262.21 265.09 8.86 o 5 4 4 438.49 435.34 18.66 o 6 4 4 178.25 184.05 14.00 o -5 5 4 87.16 72.73 9.36 o -4 5 4 50.93 42.01 5.87 o -3 5 4 117.08 110.86 7.21 o -2 5 4 82.90 79.95 6.80 o -1 5 4 51.54 42.26 18.70 o 0 5 4 205.25 191.72 8.07 o 1 5 4 54.66 56.05 6.10 o 2 5 4 165.84 176.32 15.31 o 3 5 4 5.64 8.29 5.90 o 4 5 4 208.69 219.27 13.60 o -3 6 4 185.21 180.40 9.33 o -2 6 4 224.27 229.29 10.57 o -1 6 4 196.31 184.98 9.59 o 0 6 4 63.09 54.52 6.40 o 1 6 4 34.22 43.89 8.48 o 2 6 4 151.99 163.32 21.95 o -8 1 5 411.26 411.72 17.13 o -7 1 5 55.46 48.33 3.80 o -6 1 5 417.57 403.97 7.31 o -5 1 5 1769.63 1757.47 22.09 o -4 1 5 502.78 504.55 10.30 o -3 1 5 3.18 17.97 5.93 o -2 1 5 685.40 707.26 31.35 o -1 1 5 1735.72 1802.32 47.10 o 0 1 5 194.15 196.35 5.20 o 1 1 5 65.36 57.66 2.96 o 2 1 5 1617.44 1616.24 26.14 o 3 1 5 1680.72 1664.18 41.85 o 4 1 5 72.62 85.81 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