#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/26/2012672.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012672_Fobs loop_ _publ_author_name 'Naumov, Dmitry Yu.' 'Naumova, Marina I.' 'Kuratieva, Natalia V.' 'Boldyreva, Elena V.' 'Howard, Judith A. K.' _publ_section_title ; Copper(II) hypophosphite: the \a- and \b-forms at 270 and 100K, and the \g-form at 270K ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i55 _journal_page_last i60 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.709 _cell_angle_gamma 90.000 _cell_length_a 7.2079 _cell_length_b 5.3216 _cell_length_c 6.2121 _exptl_crystal_F_000 190.00 _reflns_d_resolution_high 0.7317 _[local]_cod_data_source_file av1101alpha100sup3.hkl _[local]_cod_data_source_block alpha100 #BEGIN Tags that were not found in dictionaries: _shelx_title ' a-Cu(H2PO2)2 in P2(1)/c, T=100K, SMART CCD, FaceABS' _shelx_refln_list_code 4 _shelx_f_calc_maximum 99.91 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 5513.68 6184.15 202.25 o 2 0 0 252.30 292.84 14.75 o 3 0 0 1750.58 1661.78 32.40 o 4 0 0 5047.34 4995.06 132.54 o 5 0 0 268.09 283.30 10.88 o 6 0 0 64.40 66.03 7.83 o 7 0 0 1022.84 1013.86 31.14 o 8 0 0 1848.14 1914.07 54.63 o 9 0 0 223.93 230.60 13.75 o 1 1 0 742.85 752.87 12.05 o 2 1 0 122.01 156.36 8.94 o 3 1 0 1370.39 1446.65 29.53 o 4 1 0 61.46 59.77 2.76 o 5 1 0 331.93 336.52 10.21 o 6 1 0 39.00 32.27 4.26 o 7 1 0 36.17 37.58 5.10 o 8 1 0 2.43 5.65 4.38 o 9 1 0 41.17 31.15 6.77 o 0 2 0 6242.65 6488.68 313.73 o 1 2 0 1971.14 1941.68 71.38 o 2 2 0 637.63 680.14 21.92 o 3 2 0 2445.67 2479.19 87.65 o 4 2 0 2333.26 2167.11 44.25 o 5 2 0 215.42 221.47 4.89 o 6 2 0 119.97 122.21 5.96 o 7 2 0 1298.64 1275.84 26.68 o 8 2 0 863.98 882.75 20.65 o 9 2 0 29.19 35.84 13.55 o 1 3 0 143.29 115.68 4.33 o 2 3 0 317.97 348.97 19.10 o 3 3 0 886.27 889.15 18.36 o 4 3 0 5.85 11.02 5.15 o 5 3 0 299.85 299.03 8.99 o 6 3 0 17.78 18.07 3.59 o 7 3 0 39.47 40.53 13.24 o 8 3 0 160.79 163.88 8.04 o 0 4 0 985.24 1002.67 43.35 o 1 4 0 496.75 518.51 18.98 o 2 4 0 413.91 405.77 11.30 o 3 4 0 1270.59 1272.93 54.23 o 4 4 0 1574.16 1567.26 25.71 o 5 4 0 603.69 590.12 16.74 o 6 4 0 316.35 316.03 7.32 o 7 4 0 546.98 525.45 20.83 o 8 4 0 301.78 285.58 17.21 o 1 5 0 345.81 345.05 14.15 o 2 5 0 21.47 36.62 6.04 o 3 5 0 255.61 248.88 6.03 o 4 5 0 76.09 80.90 10.27 o 5 5 0 172.81 182.41 7.28 o 6 5 0 142.68 152.58 12.21 o 7 5 0 126.68 116.04 9.92 o 0 6 0 356.21 358.72 16.88 o 1 6 0 311.21 304.53 9.48 o 2 6 0 259.49 243.37 6.90 o 3 6 0 325.26 296.69 8.82 o 4 6 0 561.80 551.84 13.78 o 5 6 0 573.87 555.57 13.64 o 1 7 0 547.48 518.49 11.57 o 2 7 0 12.70 12.79 8.53 o -9 1 1 303.14 293.61 10.54 o -8 1 1 33.68 41.94 9.73 o -7 1 1 1208.63 1306.69 27.36 o -6 1 1 3117.58 3128.07 58.75 o -5 1 1 747.90 756.31 10.99 o -4 1 1 155.38 143.44 5.18 o -3 1 1 1892.01 1689.38 27.55 o -2 1 1 3127.53 2979.53 38.14 o -1 1 1 89.24 97.92 3.15 o 0 1 1 1005.04 995.99 18.60 o 1 1 1 9381.40 9775.72 100.29 o 2 1 1 4884.16 4962.50 64.82 o 3 1 1 653.58 636.84 22.52 o 4 1 1 1631.65 1508.98 56.77 o 5 1 1 3260.68 3204.72 93.76 o 6 1 1 358.21 403.01 10.62 o 7 1 1 21.58 17.63 4.93 o 8 1 1 422.53 405.75 12.33 o 9 1 1 934.85 942.15 22.36 o -9 2 1 203.27 217.87 21.83 o -8 2 1 37.47 39.25 13.17 o -7 2 1 104.47 110.53 13.61 o -6 2 1 26.96 40.14 10.85 o -5 2 1 0.37 4.84 3.71 o -4 2 1 154.99 153.29 4.03 o -3 2 1 215.19 218.68 5.76 o -2 2 1 34.45 39.25 3.57 o -1 2 1 237.21 236.94 4.30 o 0 2 1 161.74 203.46 4.68 o 1 2 1 475.56 572.24 9.81 o 2 2 1 230.29 222.93 3.26 o 3 2 1 140.65 153.34 3.12 o 4 2 1 519.43 536.50 9.69 o 5 2 1 14.88 11.27 3.83 o 6 2 1 49.04 55.64 7.24 o 7 2 1 44.15 40.00 8.92 o 8 2 1 66.22 68.52 24.85 o 9 2 1 84.25 80.20 11.66 o -8 3 1 33.77 32.62 8.06 o -7 3 1 891.80 892.25 20.90 o -6 3 1 1305.48 1311.85 22.08 o -5 3 1 82.25 89.68 4.99 o -4 3 1 186.59 202.97 5.40 o -3 3 1 3681.60 3514.57 45.91 o -2 3 1 4343.10 4233.64 86.08 o -1 3 1 201.55 190.31 8.21 o 0 3 1 234.33 225.10 11.55 o 1 3 1 3843.78 3688.25 64.57 o 2 3 1 2555.20 2516.93 67.20 o 3 3 1 56.09 53.29 1.96 o 4 3 1 174.55 180.29 6.49 o 5 3 1 1861.16 1876.65 25.73 o 6 3 1 1053.26 1012.76 22.35 o 7 3 1 96.93 106.99 16.37 o 8 3 1 204.12 184.82 8.26 o -8 4 1 49.69 62.38 9.15 o -7 4 1 243.84 242.59 14.84 o -6 4 1 168.31 170.73 7.51 o -5 4 1 261.37 284.37 15.22 o -4 4 1 622.09 621.05 12.49 o -3 4 1 619.38 616.95 10.33 o -2 4 1 743.45 770.63 12.16 o -1 4 1 742.54 745.85 11.78 o 0 4 1 533.95 543.76 10.03 o 1 4 1 242.27 231.27 7.74 o 2 4 1 750.80 752.53 15.22 o 3 4 1 177.46 188.28 8.68 o 4 4 1 687.77 703.24 16.31 o 5 4 1 199.04 191.08 7.86 o 6 4 1 212.56 207.99 6.55 o 7 4 1 16.51 42.54 8.69 o -7 5 1 70.21 59.03 6.40 o -6 5 1 213.56 214.92 8.31 o -5 5 1 423.97 409.10 12.64 o -4 5 1 577.90 572.72 12.60 o -3 5 1 745.77 761.62 12.74 o -2 5 1 982.30 985.96 25.10 o -1 5 1 1057.17 1026.54 19.61 o 0 5 1 865.03 842.77 12.13 o 1 5 1 409.22 408.19 8.26 o 2 5 1 154.20 171.20 10.32 o 3 5 1 224.65 211.37 8.22 o 4 5 1 454.20 437.44 12.29 o 5 5 1 471.77 479.95 11.33 o 6 5 1 288.88 267.84 8.79 o -5 6 1 278.59 235.79 12.57 o -4 6 1 22.36 12.23 6.41 o -3 6 1 108.79 126.87 11.51 o -2 6 1 137.67 139.94 11.85 o -1 6 1 51.66 63.56 4.69 o 0 6 1 412.09 429.14 16.53 o 1 6 1 128.94 135.53 5.69 o 2 6 1 214.89 218.05 8.44 o 3 6 1 22.26 15.21 9.88 o 4 6 1 172.57 165.96 9.58 o 5 6 1 5.15 8.07 8.74 o -2 7 1 148.59 139.89 41.21 o -1 7 1 513.44 519.92 13.11 o 0 7 1 432.39 406.46 14.76 o 1 7 1 92.88 103.66 10.90 o -9 0 2 1067.70 1055.19 34.76 o -8 0 2 311.78 340.76 16.72 o -7 0 2 40.83 55.55 6.12 o -6 0 2 1269.99 1319.30 37.91 o -5 0 2 6992.51 7040.92 126.91 o -4 0 2 2303.45 2241.62 41.64 o -3 0 2 4.34 8.32 2.54 o -2 0 2 2861.93 2725.49 49.52 o -1 0 2 9982.16 10584.47 266.64 o 0 0 2 172.94 141.86 3.89 o 1 0 2 869.76 989.85 15.05 o 2 0 2 2115.31 1818.82 27.19 o 3 0 2 7265.05 7625.00 111.32 o 4 0 2 1060.43 1055.88 59.55 o 5 0 2 167.63 170.39 9.72 o 6 0 2 1908.03 2057.50 40.30 o 7 0 2 1363.95 1437.51 87.12 o 8 0 2 28.55 22.32 5.55 o -9 1 2 4.10 7.51 4.76 o -8 1 2 152.06 163.32 8.25 o -7 1 2 4.06 2.77 5.60 o -6 1 2 99.09 101.87 4.61 o -5 1 2 35.90 35.55 2.98 o -4 1 2 377.16 406.86 5.98 o -3 1 2 153.14 156.76 3.54 o -2 1 2 1807.60 1960.23 35.12 o -1 1 2 53.66 64.61 2.55 o 0 1 2 803.95 834.95 11.44 o 1 1 2 32.15 37.98 1.15 o 2 1 2 168.20 181.23 2.55 o 3 1 2 49.60 49.64 2.44 o 4 1 2 340.08 361.66 7.86 o 5 1 2 0.09 9.97 4.37 o 6 1 2 136.56 140.30 7.54 o 7 1 2 18.95 27.43 7.27 o 8 1 2 2.45 6.93 3.47 o -9 2 2 676.48 678.20 25.97 o -8 2 2 640.26 637.31 25.31 o -7 2 2 66.99 73.54 10.48 o -6 2 2 528.95 500.19 10.43 o -5 2 2 2370.06 2384.39 31.73 o -4 2 2 1466.30 1487.55 23.44 o -3 2 2 490.60 517.28 8.12 o -2 2 2 2098.07 1995.70 26.43 o -1 2 2 3328.88 3117.80 40.33 o 0 2 2 529.33 488.20 5.78 o 1 2 2 486.58 491.12 6.47 o 2 2 2 2948.22 2804.84 42.05 o 3 2 2 2457.40 2348.55 25.05 o 4 2 2 182.11 183.97 6.43 o 5 2 2 337.67 355.26 17.07 o 6 2 2 1869.40 1905.49 39.08 o 7 2 2 702.68 718.51 26.44 o 8 2 2 3.44 5.47 10.05 o -8 3 2 236.43 232.83 19.71 o -7 3 2 96.55 79.63 11.76 o -6 3 2 94.44 97.58 4.41 o -5 3 2 2.82 5.49 5.23 o -4 3 2 262.08 283.35 6.58 o -3 3 2 146.82 139.31 7.46 o -2 3 2 1135.81 1143.21 18.58 o -1 3 2 1.17 3.76 1.55 o 0 3 2 281.86 265.14 4.63 o 1 3 2 54.20 58.11 2.85 o 2 3 2 35.30 34.91 2.92 o 3 3 2 517.25 526.17 14.88 o 4 3 2 270.44 272.93 4.81 o 5 3 2 219.91 222.96 5.65 o 6 3 2 159.74 167.64 11.39 o 7 3 2 45.94 40.20 7.45 o 8 3 2 0.26 8.29 8.82 o -8 4 2 488.81 485.02 17.23 o -7 4 2 165.34 169.26 11.56 o -6 4 2 256.10 229.02 12.56 o -5 4 2 594.34 561.71 14.32 o -4 4 2 359.86 365.69 18.22 o -3 4 2 211.40 224.78 8.42 o -2 4 2 997.47 1011.10 22.05 o -1 4 2 1956.67 1950.32 30.94 o 0 4 2 1129.06 1111.95 23.57 o 1 4 2 907.80 891.41 34.79 o 2 4 2 1382.35 1394.95 47.76 o 3 4 2 867.25 909.98 35.87 o 4 4 2 117.05 108.93 6.57 o 5 4 2 120.85 110.96 10.51 o 6 4 2 491.97 483.96 18.88 o 7 4 2 331.87 305.72 14.73 o -7 5 2 25.22 10.81 7.39 o -6 5 2 209.21 204.93 9.31 o -4 5 2 264.36 255.91 14.73 o -3 5 2 2.55 4.50 3.51 o -2 5 2 280.46 285.07 8.06 o -1 5 2 64.49 66.58 8.77 o 0 5 2 244.12 244.73 6.30 o 1 5 2 179.97 194.00 14.15 o 2 5 2 220.94 212.63 8.29 o 3 5 2 181.89 190.65 8.62 o 4 5 2 88.23 89.27 7.11 o 5 5 2 262.17 258.79 9.26 o 6 5 2 53.45 87.11 10.44 o -5 6 2 220.23 213.26 9.15 o -4 6 2 152.43 168.84 8.31 o -3 6 2 173.92 188.85 7.00 o -2 6 2 375.52 380.61 12.51 o -1 6 2 682.94 717.28 25.99 o 0 6 2 688.33 722.28 19.04 o 1 6 2 420.75 396.48 19.84 o 2 6 2 279.27 267.66 10.01 o 3 6 2 359.48 349.71 33.77 o 4 6 2 321.28 333.91 26.00 o -1 7 2 58.14 70.69 8.40 o 0 7 2 343.79 307.88 18.26 o -9 1 3 15.92 25.49 5.46 o -8 1 3 695.62 678.27 25.32 o -7 1 3 999.61 988.52 34.41 o -6 1 3 36.63 41.28 2.76 o -5 1 3 198.22 191.50 4.17 o -4 1 3 3151.74 3182.21 37.17 o -3 1 3 3122.46 3036.51 39.55 o -2 1 3 738.78 726.44 17.57 o -1 1 3 2721.20 2707.32 40.37 o 0 1 3 5267.85 5031.59 89.06 o 1 1 3 958.33 917.14 12.99 o 2 1 3 4.22 10.63 2.02 o 3 1 3 909.30 880.48 10.07 o 4 1 3 2473.40 2410.97 31.95 o 5 1 3 256.18 268.59 7.04 o 6 1 3 31.20 22.13 4.29 o 7 1 3 1089.84 1042.34 24.04 o 8 1 3 1138.29 1156.12 39.77 o -9 2 3 27.86 25.94 7.64 o -8 2 3 130.04 126.84 13.04 o -7 2 3 0.83 8.08 3.54 o -6 2 3 85.65 88.89 4.68 o -5 2 3 12.84 10.71 2.07 o -4 2 3 46.94 40.80 3.74 o -3 2 3 227.89 240.99 5.11 o -2 2 3 2.75 6.67 5.69 o -1 2 3 412.86 441.90 13.46 o 0 2 3 51.01 52.08 1.69 o 1 2 3 0.16 4.13 1.32 o 2 2 3 251.00 255.35 5.72 o 3 2 3 152.99 156.58 5.79 o 4 2 3 263.13 265.50 5.47 o 5 2 3 361.97 367.61 17.90 o 6 2 3 24.94 12.59 4.13 o 7 2 3 82.40 73.86 6.38 o 8 2 3 32.47 45.09 15.43 o -8 3 3 966.23 917.21 39.47 o -7 3 3 1061.89 1049.81 21.97 o -6 3 3 61.67 64.64 7.53 o -5 3 3 192.12 189.84 6.00 o -4 3 3 2398.47 2442.20 68.66 o -3 3 3 1772.13 1742.89 27.64 o -2 3 3 9.51 14.27 6.47 o -1 3 3 233.94 240.47 7.33 o 0 3 3 3043.29 2989.60 43.68 o 1 3 3 2052.51 1996.44 51.47 o 2 3 3 178.48 168.93 3.78 o 3 3 3 494.09 506.37 15.67 o 4 3 3 1738.24 1783.36 24.70 o 5 3 3 633.45 638.23 15.24 o 6 3 3 57.40 75.70 6.37 o 7 3 3 199.44 209.23 9.40 o -7 4 3 238.30 230.37 7.61 o -6 4 3 233.91 241.99 11.68 o -5 4 3 326.61 323.77 10.15 o -4 4 3 139.29 136.78 7.94 o -3 4 3 796.75 804.64 24.21 o -2 4 3 207.32 201.85 5.70 o -1 4 3 988.45 1024.02 22.57 o 0 4 3 297.86 303.93 7.74 o 1 4 3 430.43 432.12 16.93 o 2 4 3 24.94 21.96 2.74 o 3 4 3 464.70 455.16 24.76 o 4 4 3 2.15 7.35 5.05 o 5 4 3 326.11 308.71 14.54 o -6 5 3 563.24 534.07 14.43 o -5 5 3 481.15 474.28 13.24 o -4 5 3 306.58 323.33 11.25 o -3 5 3 200.71 192.38 14.40 o -2 5 3 226.66 263.55 10.25 o -1 5 3 416.29 431.50 29.38 o 0 5 3 469.72 516.63 19.92 o 1 5 3 417.45 438.76 18.85 o 2 5 3 631.59 636.78 15.94 o 3 5 3 924.51 981.10 58.04 o 4 5 3 595.76 640.68 16.86 o 5 5 3 148.12 142.18 13.06 o -4 6 3 125.92 99.34 18.31 o -3 6 3 130.13 120.02 9.96 o -2 6 3 16.04 17.08 6.62 o -1 6 3 219.09 231.25 11.01 o 0 6 3 4.27 3.99 5.30 o 1 6 3 401.47 432.91 13.68 o 2 6 3 0.71 4.87 7.85 o 3 6 3 310.82 334.88 14.34 o -9 0 4 335.96 405.16 21.51 o -8 0 4 3.10 3.64 5.78 o -7 0 4 958.47 923.19 29.22 o -6 0 4 2794.85 2878.99 44.43 o -5 0 4 89.18 98.67 4.66 o -4 0 4 277.25 277.07 7.73 o -3 0 4 1701.19 1714.30 32.79 o -2 0 4 5245.86 5065.21 91.66 o -1 0 4 705.63 668.52 20.35 o 0 0 4 288.34 285.99 9.51 o 1 0 4 3976.22 3812.95 80.22 o 2 0 4 4072.32 3928.53 134.95 o 3 0 4 150.78 140.93 12.74 o 4 0 4 24.47 32.65 6.70 o 5 0 4 901.72 906.60 29.35 o 6 0 4 506.67 578.90 21.82 o 7 0 4 22.65 21.04 7.46 o -9 1 4 72.28 61.16 6.64 o -8 1 4 25.16 13.57 8.73 o -7 1 4 227.40 217.34 6.87 o -6 1 4 0.83 6.43 2.94 o -5 1 4 134.05 132.73 3.87 o -4 1 4 8.93 15.32 4.61 o -3 1 4 162.86 169.45 5.63 o -2 1 4 110.11 114.04 3.89 o -1 1 4 625.10 646.15 20.04 o 0 1 4 0.86 5.56 3.27 o 1 1 4 330.61 335.52 5.88 o 2 1 4 28.24 34.48 3.66 o 3 1 4 17.66 18.72 3.45 o 4 1 4 18.34 10.70 5.89 o 5 1 4 39.57 20.53 9.92 o 7 1 4 24.23 12.46 5.28 o -8 2 4 54.07 51.79 13.78 o -7 2 4 517.17 507.27 9.68 o -6 2 4 1301.55 1305.43 24.03 o -5 2 4 303.41 311.96 6.66 o -4 2 4 127.03 133.35 6.70 o -3 2 4 1746.63 1623.82 22.39 o -2 2 4 1976.85 1849.06 41.36 o -1 2 4 251.77 258.70 6.43 o 0 2 4 679.23 667.82 10.05 o 1 2 4 3010.38 2880.46 38.34 o 2 2 4 1472.84 1443.53 20.72 o 3 2 4 23.91 30.35 3.09 o 4 2 4 314.59 319.39 11.47 o 5 2 4 1518.37 1509.65 41.12 o 6 2 4 369.93 389.19 19.08 o 7 2 4 2.77 19.13 6.87 o -8 3 4 13.76 7.40 10.07 o -7 3 4 312.57 297.40 14.28 o -6 3 4 4.18 13.69 4.74 o -5 3 4 108.91 123.95 4.97 o -4 3 4 49.67 57.92 3.89 o -3 3 4 88.77 96.98 4.76 o -2 3 4 415.20 411.78 15.41 o -1 3 4 436.81 427.60 9.51 o 0 3 4 163.95 162.63 4.56 o 1 3 4 224.06 222.58 4.11 o 2 3 4 80.51 82.43 3.99 o 3 3 4 0.01 2.08 2.62 o 4 3 4 440.77 429.59 8.67 o 5 3 4 28.31 19.82 15.44 o 6 3 4 227.01 238.31 12.43 o -7 4 4 250.10 259.94 49.53 o -6 4 4 677.84 647.82 24.49 o -5 4 4 527.33 527.79 21.39 o -4 4 4 472.60 503.06 14.02 o -3 4 4 1057.21 1092.53 24.17 o -2 4 4 943.30 968.80 21.81 o -1 4 4 203.62 224.31 17.71 o 0 4 4 180.66 182.64 10.61 o 1 4 4 633.64 681.90 14.98 o 2 4 4 517.47 556.09 15.62 o 3 4 4 170.83 175.83 7.86 o 4 4 4 422.74 448.07 13.49 o 5 4 4 860.44 889.10 29.89 o 6 4 4 373.52 340.52 15.46 o -6 5 4 10.65 20.20 11.49 o -5 5 4 156.76 197.35 12.72 o -4 5 4 58.93 51.94 12.68 o -3 5 4 182.78 178.59 9.12 o -2 5 4 112.20 124.34 7.66 o -1 5 4 90.59 75.37 6.33 o 0 5 4 279.11 281.55 10.10 o 1 5 4 86.01 95.82 5.27 o 2 5 4 292.23 326.29 21.14 o 3 5 4 27.45 33.51 11.36 o 4 5 4 322.12 319.77 11.34 o -3 6 4 318.81 340.76 18.01 o -2 6 4 414.15 407.86 39.04 o -1 6 4 318.43 334.32 12.14 o 0 6 4 104.03 104.34 11.86 o 1 6 4 77.83 89.50 13.29 o 2 6 4 283.27 289.72 16.11 o -8 1 5 706.19 723.53 19.57 o -7 1 5 95.26 96.41 12.04 o -6 1 5 503.11 513.91 9.93 o -5 1 5 2274.56 2307.05 28.92 o -4 1 5 733.45 723.10 15.20 o -3 1 5 3.86 13.21 5.34 o -2 1 5 740.20 740.36 26.95 o -1 1 5 2158.32 2152.64 41.32 o 0 1 5 269.99 265.51 5.68 o 1 1 5 57.02 56.16 3.46 o 2 1 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