#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2012673.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012673_Fobs loop_ _publ_author_name 'Naumov, Dmitry Yu.' 'Naumova, Marina I.' 'Kuratieva, Natalia V.' 'Boldyreva, Elena V.' 'Howard, Judith A. K.' _publ_section_title ; Copper(II) hypophosphite: the \a- and \b-forms at 270 and 100K, and the \g-form at 270K ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i55 _journal_page_last i60 _journal_volume 58 _journal_year 2002 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.3259 _cell_length_b 6.2720 _cell_length_c 14.2590 _exptl_crystal_F_000 380.00 _reflns_d_resolution_high 0.7303 _[local]_cod_data_source_file av1101beta270sup4.hkl _[local]_cod_data_source_block beta270 #BEGIN Tags that were not found in dictionaries: _shelx_title ' b-Cu(H2PO2)2 in Pbca, T=270K, SMART CCD, FaceABS' _shelx_refln_list_code 4 _shelx_f_calc_maximum 156.04 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 24349.23 26086.58 462.61 o 4 0 0 3325.59 3396.59 62.67 o 6 0 0 828.27 938.41 21.19 o 2 1 0 532.00 648.12 7.89 o 4 1 0 787.97 777.45 13.95 o 6 1 0 725.25 711.70 25.88 o 0 2 0 10208.32 9787.11 409.62 o 2 2 0 4555.78 4058.66 51.68 o 4 2 0 4723.40 4513.33 69.11 o 6 2 0 1998.35 2008.68 32.66 o 2 3 0 1138.92 1175.37 18.41 o 4 3 0 3843.92 3671.35 79.64 o 6 3 0 355.70 371.49 16.41 o 0 4 0 1071.30 1001.75 27.40 o 2 4 0 719.12 682.35 9.11 o 4 4 0 431.30 465.22 22.12 o 6 4 0 598.61 623.72 39.12 o 2 5 0 672.82 689.91 9.09 o 4 5 0 4.62 7.58 3.91 o 0 6 0 38.42 48.79 4.67 o 2 6 0 823.56 858.19 11.79 o 4 6 0 973.51 997.20 17.99 o 2 7 0 195.13 193.44 11.25 o 4 7 0 315.62 317.55 10.80 o 0 8 0 1824.95 1887.86 54.35 o 2 8 0 2242.62 2268.31 36.79 o 1 1 1 3612.16 3633.56 34.70 o 2 1 1 0.10 11.30 2.05 o 3 1 1 1129.68 1037.12 8.88 o 4 1 1 1389.68 1353.84 14.54 o 5 1 1 2678.95 2525.43 25.69 o 6 1 1 265.76 277.87 7.76 o 7 1 1 1021.18 1019.04 13.64 o 0 2 1 8649.25 8745.07 121.82 o 1 2 1 846.22 887.22 15.63 o 2 2 1 1118.35 1082.72 10.29 o 3 2 1 330.13 324.84 4.35 o 4 2 1 104.50 130.05 3.22 o 5 2 1 401.91 402.66 6.64 o 6 2 1 0.00 23.44 9.81 o 7 2 1 410.29 423.68 21.51 o 1 3 1 14224.59 14203.22 149.93 o 2 3 1 158.99 180.61 3.02 o 3 3 1 4176.13 4219.74 38.72 o 4 3 1 112.62 162.09 6.11 o 5 3 1 1292.56 1379.66 19.25 o 6 3 1 153.16 149.88 4.88 o 0 4 1 592.26 583.44 9.96 o 1 4 1 895.62 900.31 10.18 o 2 4 1 0.04 3.87 3.02 o 3 4 1 267.41 260.54 4.20 o 4 4 1 18.00 32.19 3.41 o 5 4 1 1.80 4.51 3.07 o 6 4 1 29.41 39.10 5.27 o 1 5 1 4992.69 4902.41 44.53 o 2 5 1 280.01 292.34 3.86 o 3 5 1 4867.57 4793.74 42.33 o 4 5 1 771.05 787.86 14.32 o 5 5 1 1401.87 1374.28 51.97 o 0 6 1 280.42 309.87 6.27 o 1 6 1 93.66 99.19 3.35 o 2 6 1 470.14 473.54 5.63 o 3 6 1 780.96 777.12 7.88 o 4 6 1 100.58 109.08 4.20 o 5 6 1 343.20 340.25 8.54 o 1 7 1 1466.21 1453.47 15.80 o 2 7 1 98.89 95.89 3.58 o 3 7 1 1017.86 1000.43 10.54 o 4 7 1 0.49 -0.83 6.60 o 0 8 1 325.91 331.29 26.43 o 1 8 1 0.54 -1.72 5.69 o 2 8 1 113.66 100.06 13.46 o 0 0 2 22693.04 28802.56 1596.80 o 1 0 2 3054.16 3368.70 90.72 o 2 0 2 8038.10 8116.71 88.98 o 3 0 2 518.68 460.59 6.14 o 4 0 2 1755.29 1743.76 41.47 o 5 0 2 1002.37 997.84 14.97 o 6 0 2 784.50 858.19 16.00 o 7 0 2 1253.15 1231.13 22.51 o 1 1 2 5427.48 5393.39 45.28 o 2 1 2 1176.45 1279.44 11.22 o 3 1 2 1044.12 1089.27 10.28 o 4 1 2 122.56 123.08 3.65 o 5 1 2 95.70 96.23 5.56 o 6 1 2 13.76 24.88 5.32 o 7 1 2 79.38 99.32 5.90 o 0 2 2 4565.62 4114.36 46.56 o 1 2 2 1781.60 1943.32 18.92 o 2 2 2 5276.80 4978.24 44.71 o 3 2 2 287.69 292.33 3.61 o 4 2 2 4192.11 3985.54 42.29 o 5 2 2 0.83 7.99 2.61 o 6 2 2 1515.02 1493.20 28.19 o 7 2 2 15.18 12.69 16.07 o 1 3 2 594.59 527.22 6.12 o 2 3 2 215.24 219.97 3.08 o 3 3 2 2718.79 2606.58 24.15 o 4 3 2 58.25 62.75 2.79 o 5 3 2 4.65 7.08 3.77 o 6 3 2 16.35 27.42 7.50 o 0 4 2 7543.34 7198.05 93.81 o 1 4 2 623.98 634.35 6.25 o 2 4 2 4445.13 4365.89 45.88 o 3 4 2 1730.92 1729.33 18.00 o 4 4 2 1362.75 1415.25 18.11 o 5 4 2 848.47 837.06 13.72 o 6 4 2 482.04 486.64 19.61 o 1 5 2 290.91 291.83 4.80 o 2 5 2 40.99 43.86 2.63 o 3 5 2 0.05 11.51 4.07 o 4 5 2 1.47 11.90 6.54 o 5 5 2 119.76 147.47 25.42 o 0 6 2 1660.69 1722.70 27.29 o 1 6 2 184.90 188.53 3.94 o 2 6 2 1715.78 1767.11 16.30 o 3 6 2 92.35 101.01 2.55 o 4 6 2 1168.55 1186.83 16.22 o 5 6 2 76.32 103.32 26.64 o 1 7 2 1207.29 1185.89 14.50 o 2 7 2 20.63 27.86 3.30 o 3 7 2 280.14 272.23 4.88 o 4 7 2 23.36 21.63 8.64 o 0 8 2 725.26 692.37 17.54 o 1 8 2 2.05 0.67 4.04 o 2 8 2 676.84 661.47 16.64 o 1 1 3 19070.41 19426.86 146.80 o 2 1 3 98.50 128.60 1.80 o 3 1 3 11991.01 11932.33 129.91 o 4 1 3 1160.20 1145.58 17.05 o 5 1 3 1716.80 1748.22 18.38 o 6 1 3 186.89 188.67 4.66 o 7 1 3 321.39 307.30 15.43 o 0 2 3 7813.01 8116.40 92.15 o 1 2 3 1543.73 1623.30 27.61 o 2 2 3 623.83 609.62 6.51 o 3 2 3 1539.91 1550.28 14.65 o 4 2 3 20.39 30.67 4.16 o 5 2 3 777.83 772.94 11.08 o 6 2 3 0.06 7.11 3.21 o 7 2 3 353.46 334.82 20.05 o 1 3 3 3475.51 3306.89 37.71 o 2 3 3 8.26 9.80 2.38 o 3 3 3 2188.16 2174.41 21.82 o 4 3 3 13.50 34.00 4.96 o 5 3 3 899.86 965.16 15.18 o 6 3 3 135.76 146.68 6.42 o 0 4 3 413.96 412.06 15.29 o 1 4 3 156.85 158.79 3.31 o 2 4 3 6.56 21.79 5.50 o 3 4 3 17.65 20.07 2.69 o 4 4 3 61.11 70.62 7.04 o 5 4 3 52.21 56.07 7.22 o 6 4 3 88.81 90.61 8.55 o 1 5 3 258.06 249.47 4.67 o 2 5 3 379.55 381.30 5.93 o 3 5 3 481.56 488.51 6.55 o 4 5 3 775.52 745.99 15.39 o 5 5 3 1091.88 1104.41 26.10 o 0 6 3 21.95 18.40 3.54 o 1 6 3 1.45 8.54 8.14 o 2 6 3 283.61 283.04 5.60 o 3 6 3 107.34 112.43 4.04 o 4 6 3 153.75 155.13 6.62 o 5 6 3 212.30 205.39 11.67 o 1 7 3 2088.43 2156.06 36.26 o 2 7 3 229.55 220.73 4.75 o 3 7 3 649.94 644.24 7.56 o 4 7 3 0.01 5.00 5.39 o 0 8 3 408.96 442.01 20.48 o 1 8 3 49.27 53.00 4.18 o 2 8 3 96.87 98.00 8.59 o 0 0 4 1009.37 1131.33 21.01 o 1 0 4 439.02 511.54 13.08 o 2 0 4 2421.15 2604.85 53.17 o 3 0 4 1145.67 1177.29 15.24 o 4 0 4 1388.31 1375.89 23.87 o 5 0 4 77.64 78.00 10.78 o 6 0 4 703.84 710.41 14.11 o 1 1 4 457.21 528.18 4.40 o 2 1 4 407.41 403.09 3.68 o 3 1 4 107.89 126.52 4.38 o 4 1 4 1424.11 1413.43 14.83 o 5 1 4 227.42 224.13 4.15 o 6 1 4 267.25 282.01 10.34 o 7 1 4 2.46 11.45 7.70 o 0 2 4 1263.91 1059.38 22.91 o 1 2 4 658.47 714.72 7.42 o 2 2 4 5411.01 5302.77 47.63 o 3 2 4 392.05 406.51 4.98 o 4 2 4 2795.90 2727.32 41.78 o 5 2 4 3.87 8.26 4.50 o 6 2 4 785.95 766.02 15.63 o 1 3 4 825.54 815.38 8.54 o 2 3 4 18.74 22.97 1.54 o 3 3 4 33.04 36.67 2.62 o 4 3 4 1998.18 1902.94 26.21 o 5 3 4 58.51 53.93 3.95 o 6 3 4 419.12 441.04 11.37 o 0 4 4 15398.16 15448.68 194.42 o 1 4 4 66.00 63.57 3.75 o 2 4 4 9324.07 9071.98 94.03 o 3 4 4 44.02 43.00 2.32 o 4 4 4 2757.87 2732.26 34.88 o 5 4 4 21.17 10.08 10.89 o 6 4 4 486.47 472.98 13.17 o 1 5 4 76.46 73.86 5.35 o 2 5 4 267.80 274.11 4.73 o 3 5 4 0.26 0.41 4.38 o 4 5 4 5.55 14.05 9.01 o 5 5 4 51.34 56.02 5.49 o 0 6 4 5538.04 5730.71 138.53 o 1 6 4 3.78 3.30 2.95 o 2 6 4 2472.58 2556.07 26.05 o 3 6 4 35.76 44.66 3.21 o 4 6 4 1142.48 1144.65 20.41 o 5 6 4 3.60 30.14 14.86 o 1 7 4 1.53 12.27 10.55 o 2 7 4 350.95 347.31 12.31 o 3 7 4 7.91 10.97 2.55 o 0 8 4 252.08 232.69 10.88 o 1 8 4 9.18 0.08 5.87 o 2 8 4 51.26 24.88 10.42 o 1 1 5 11223.54 10746.35 90.49 o 2 1 5 232.13 231.39 3.06 o 3 1 5 10018.88 9885.29 79.00 o 4 1 5 1280.93 1246.72 13.29 o 5 1 5 1212.45 1229.42 27.33 o 6 1 5 247.13 264.58 13.83 o 0 2 5 3024.21 2767.91 75.04 o 1 2 5 974.89 1008.32 10.61 o 2 2 5 929.54 886.91 10.83 o 3 2 5 433.90 428.76 7.95 o 4 2 5 302.02 305.22 5.03 o 5 2 5 260.28 258.95 6.25 o 6 2 5 3.15 2.23 3.08 o 1 3 5 2866.02 2796.45 34.08 o 2 3 5 772.24 785.97 8.53 o 3 3 5 2621.54 2614.70 26.09 o 4 3 5 376.03 389.42 7.57 o 5 3 5 1024.37 1040.06 16.18 o 6 3 5 88.95 93.01 7.40 o 0 4 5 1523.37 1478.38 39.63 o 1 4 5 454.63 427.68 31.26 o 2 4 5 81.71 86.97 6.37 o 3 4 5 59.23 62.90 3.24 o 4 4 5 23.08 31.27 5.72 o 5 4 5 11.31 20.95 9.12 o 6 4 5 10.47 17.48 6.74 o 1 5 5 881.75 893.84 14.14 o 2 5 5 17.11 16.93 5.04 o 3 5 5 422.12 435.09 6.15 o 4 5 5 438.32 447.61 9.59 o 5 5 5 771.18 762.89 12.11 o 0 6 5 1492.46 1468.38 29.52 o 1 6 5 0.29 0.26 3.84 o 2 6 5 803.58 775.55 12.18 o 3 6 5 131.17 127.10 3.68 o 4 6 5 6.05 11.38 9.01 o 1 7 5 1444.22 1417.02 24.64 o 2 7 5 11.86 23.43 8.10 o 3 7 5 512.59 494.90 7.63 o 0 8 5 58.88 61.82 18.82 o 1 8 5 10.41 24.60 7.69 o 0 0 6 6049.49 5995.94 231.49 o 1 0 6 5025.75 5402.48 59.68 o 2 0 6 8208.43 8355.51 170.67 o 3 0 6 3156.26 3184.60 39.04 o 4 0 6 3798.30 3723.08 56.16 o 5 0 6 861.65 856.57 19.01 o 6 0 6 818.10 861.19 43.55 o 1 1 6 45.96 37.97 2.66 o 2 1 6 436.69 475.45 5.83 o 3 1 6 1281.61 1279.80 13.72 o 4 1 6 75.72 86.12 4.11 o 5 1 6 122.43 134.46 7.47 o 6 1 6 6.65 5.91 3.97 o 0 2 6 7781.12 7587.98 104.98 o 1 2 6 29.86 41.31 1.51 o 2 2 6 5897.36 5654.60 45.53 o 3 2 6 135.92 121.90 2.68 o 4 2 6 1839.47 1800.13 26.29 o 5 2 6 6.01 -0.49 5.24 o 6 2 6 551.35 570.41 13.04 o 1 3 6 2999.42 2965.90 31.41 o 2 3 6 30.82 32.97 3.27 o 3 3 6 1513.37 1470.58 18.85 o 4 3 6 4.10 6.68 4.67 o 5 3 6 123.48 125.40 8.36 o 6 3 6 83.58 88.79 6.85 o 0 4 6 1805.49 1794.43 34.33 o 1 4 6 59.31 73.08 2.47 o 2 4 6 1779.38 1744.86 24.89 o 3 4 6 410.61 416.35 6.98 o 4 4 6 1446.05 1481.44 19.23 o 5 4 6 656.91 642.68 16.19 o 6 4 6 773.88 710.53 24.91 o 1 5 6 580.14 571.92 13.51 o 2 5 6 41.66 38.11 3.67 o 3 5 6 21.37 26.47 3.79 o 4 5 6 2.75 -2.39 3.88 o 5 5 6 0.73 6.42 6.53 o 0 6 6 1863.66 1923.59 37.83 o 1 6 6 264.94 255.10 8.46 o 2 6 6 1094.88 1137.82 19.87 o 3 6 6 214.12 212.81 8.55 o 4 6 6 612.58 619.03 10.25 o 1 7 6 680.52 702.75 12.56 o 2 7 6 10.39 9.88 5.29 o 3 7 6 219.62 217.37 8.04 o 0 8 6 1073.04 1070.50 35.29 o 1 1 7 1684.73 1574.30 20.17 o 2 1 7 4.85 6.87 1.40 o 3 1 7 804.96 796.07 7.78 o 4 1 7 849.39 840.83 21.03 o 5 1 7 1318.40 1306.41 17.26 o 6 1 7 48.79 55.67 5.87 o 0 2 7 1813.12 1755.58 37.39 o 1 2 7 666.69 696.20 7.63 o 2 2 7 107.74 108.11 3.77 o 3 2 7 1219.00 1235.28 11.57 o 4 2 7 70.90 72.42 3.63 o 5 2 7 685.36 677.79 10.55 o 6 2 7 32.03 34.03 3.95 o 1 3 7 6207.45 6034.37 77.54 o 2 3 7 334.35 328.55 5.73 o 3 3 7 3765.41 3737.20 38.99 o 4 3 7 73.09 88.24 5.01 o 5 3 7 1506.03 1485.08 35.41 o 6 3 7 31.95 48.64 5.81 o 0 4 7 1314.42 1320.01 33.15 o 1 4 7 29.80 28.21 3.33 o 2 4 7 0.27 -1.78 1.78 o 3 4 7 2.80 1.93 3.49 o 4 4 7 29.21 32.75 3.89 o 5 4 7 24.75 39.92 6.09 o 1 5 7 7057.84 6939.54 79.78 o 2 5 7 4.71 6.28 5.87 o 3 5 7 3141.64 3154.62 31.85 o 4 5 7 209.99 204.02 7.35 o 5 5 7 516.86 512.66 9.66 o 0 6 7 360.38 331.55 13.88 o 1 6 7 4.49 3.53 5.19 o 2 6 7 359.92 362.67 7.24 o 3 6 7 193.89 203.44 5.74 o 4 6 7 3.46 10.92 5.55 o 1 7 7 414.17 406.76 11.83 o 2 7 7 0.02 -3.73 5.05 o 3 7 7 770.97 763.00 15.68 o 0 0 8 19316.07 19184.29 313.60 o 1 0 8 236.08 257.32 4.39 o 2 0 8 8291.03 8010.07 87.67 o 3 0 8 4.31 9.13 5.23 o 4 0 8 4704.19 4499.99 83.09 o 5 0 8 142.95 133.40 12.66 o 6 0 8 1358.03 1371.71 56.40 o 1 1 8 427.69 439.68 5.42 o 2 1 8 983.40 991.82 10.12 o 3 1 8 1.35 -0.65 2.34 o 4 1 8 1331.93 1310.84 16.93 o 5 1 8 14.07 19.21 9.29 o 6 1 8 125.39 127.24 7.75 o 0 2 8 13757.15 13695.49 154.32 o 1 2 8 0.19 3.66 2.41 o 2 2 8 4353.22 4224.71 34.45 o 3 2 8 72.04 71.30 2.98 o 4 2 8 1143.70 1162.94 17.68 o 5 2 8 8.58 14.25 4.10 o 6 2 8 570.11 581.49 13.13 o 1 3 8 70.72 74.68 5.91 o 2 3 8 2.46 2.46 1.95 o 3 3 8 0.73 16.19 1.95 o 4 3 8 1225.08 1201.50 15.91 o 5 3 8 41.43 50.45 5.51 o 6 3 8 530.23 508.72 12.21 o 0 4 8 29.11 31.88 4.51 o 1 4 8 41.33 34.66 3.71 o 2 4 8 147.60 160.50 4.07 o 3 4 8 171.29 171.05 7.00 o 4 4 8 829.41 827.64 17.11 o 5 4 8 82.62 81.11 4.26 o 1 5 8 7.31 -4.84 4.84 o 2 5 8 25.71 28.49 7.71 o 3 5 8 80.05 81.44 3.50 o 4 5 8 13.96 26.06 4.57 o 5 5 8 0.84 7.52 9.36 o 0 6 8 232.93 270.73 9.73 o 1 6 8 9.22 21.61 3.93 o 2 6 8 619.58 666.13 15.94 o 3 6 8 4.22 0.68 5.60 o 4 6 8 385.71 397.15 41.97 o 1 7 8 87.91 83.70 5.76 o 2 7 8 234.97 220.09 11.25 o 1 1 9 3544.83 3444.80 52.20 o 2 1 9 219.06 243.26 3.83 o 3 1 9 583.86 601.92 6.07 o 4 1 9 800.18 802.72 14.92 o 5 1 9 1289.26 1277.87 19.38 o 6 1 9 304.71 319.31 13.96 o 0 2 9 3047.84 3084.09 40.29 o 1 2 9 607.64 632.76 10.10 o 2 2 9 1256.59 1229.85 12.41 o 3 2 9 279.74 283.28 5.38 o 4 2 9 159.11 161.72 5.60 o 5 2 9 56.15 53.82 7.07 o 6 2 9 7.13 27.34 4.64 o 1 3 9 3448.91 3546.09 37.84 o 2 3 9 104.98 106.57 4.39 o 3 3 9 2236.04 2226.60 30.21 o 4 3 9 148.00 130.47 5.63 o 5 3 9 1397.64 1396.17 23.14 o 0 4 9 297.11 298.41 12.34 o 1 4 9 74.93 76.38 3.14 o 2 4 9 81.51 88.10 3.22 o 3 4 9 39.27 36.59 2.72 o 4 4 9 30.74 38.64 5.03 o 5 4 9 4.86 4.22 6.34 o 1 5 9 3702.65 3671.23 44.28 o 2 5 9 290.66 287.42 8.65 o 3 5 9 2013.14 1992.95 25.30 o 4 5 9 551.85 540.78 10.69 o 0 6 9 450.38 451.02 13.09 o 1 6 9 39.38 36.23 4.48 o 2 6 9 350.04 344.05 7.45 o 3 6 9 6.55 2.94 4.12 o 1 7 9 324.85 329.73 10.52 o 2 7 9 25.74 19.66 6.55 o 0 0 10 1115.88 1080.57 14.82 o 1 0 10 1097.90 1149.85 14.27 o 2 0 10 814.38 845.58 12.56 o 3 0 10 952.39 975.13 15.45 o 4 0 10 1811.50 1781.33 35.48 o 5 0 10 507.47 510.37 14.26 o 6 0 10 1418.69 1409.55 42.93 o 1 1 10 576.95 592.40 11.32 o 2 1 10 47.56 45.63 3.83 o 3 1 10 544.30 539.21 6.33 o 4 1 10 3.56 22.18 9.21 o 5 1 10 2.61 18.00 5.01 o 6 1 10 99.76 86.33 6.29 o 0 2 10 6097.66 5919.69 91.13 o 1 2 10 92.60 102.71 3.84 o 2 2 10 2391.60 2363.36 30.46 o 3 2 10 0.47 7.54 1.90 o 4 2 10 702.17 699.13 9.53 o 5 2 10 2.28 -0.92 3.43 o 1 3 10 953.50 965.25 10.86 o 2 3 10 626.51 620.79 8.43 o 3 3 10 803.90 803.21 9.53 o 4 3 10 72.90 68.91 6.36 o 5 3 10 20.81 29.89 7.56 o 0 4 10 2407.66 2377.62 45.57 o 1 4 10 104.75 109.77 4.22 o 2 4 10 2454.15 2431.26 40.46 o 3 4 10 472.17 483.45 9.05 o 4 4 10 1607.98 1582.46 23.30 o 5 4 10 452.79 438.67 13.42 o 1 5 10 279.96 263.85 10.83 o 2 5 10 33.78 31.21 3.17 o 3 5 10 0.08 6.99 3.66 o 4 5 10 135.67 142.40 11.06 o 0 6 10 1337.17 1307.73 27.93 o 1 6 10 128.58 133.35 5.51 o 2 6 10 1308.79 1327.21 18.11 o 3 6 10 118.56 130.32 5.66 o 1 7 10 567.67 534.47 11.11 o 1 1 11 8100.09 7861.64 107.61 o 2 1 11 6.85 7.66 3.98 o 3 1 11 3959.40 3873.88 35.91 o 4 1 11 426.97 412.65 17.73 o 5 1 11 810.07 775.53 13.49 o 0 2 11 908.26 913.52 13.59 o 1 2 11 134.18 137.01 3.97 o 2 2 11 58.79 66.49 3.61 o 3 2 11 587.18 584.42 9.91 o 4 2 11 28.88 37.24 7.49 o 5 2 11 655.36 623.66 11.78 o 1 3 11 445.95 474.91 6.61 o 2 3 11 71.32 80.93 5.94 o 3 3 11 806.31 831.73 14.76 o 4 3 11 4.16 14.89 4.73 o 5 3 11 781.93 783.72 16.25 o 0 4 11 628.73 648.30 15.59 o 1 4 11 110.87 111.51 3.90 o 2 4 11 0.96 24.09 3.30 o 3 4 11 232.96 220.79 10.47 o 4 4 11 1.39 22.24 4.91 o 1 5 11 176.94 176.39 8.46 o 2 5 11 2.85 2.84 5.22 o 3 5 11 119.09 130.65 7.37 o 4 5 11 95.87 90.72 11.12 o 0 6 11 24.00 31.85 12.99 o 1 6 11 89.29 93.98 8.80 o 2 6 11 70.62 81.32 4.29 o 3 6 11 381.80 355.11 15.42 o 0 0 12 318.49 307.14 12.78 o 1 0 12 117.78 114.10 4.53 o 2 0 12 260.56 261.34 7.37 o 3 0 12 35.96 39.46 4.30 o 4 0 12 792.53 815.95 22.38 o 5 0 12 271.13 267.94 15.97 o 1 1 12 568.87 589.07 21.52 o 2 1 12 1.03 2.36 1.72 o 3 1 12 0.83 25.65 4.11 o 4 1 12 259.32 257.22 6.59 o 5 1 12 14.55 18.65 7.91 o 0 2 12 1699.51 1683.20 29.55 o 1 2 12 1.23 5.61 1.87 o 2 2 12 1924.81 1929.22 34.41 o 3 2 12 110.41 108.31 3.49 o 4 2 12 681.88 675.20 20.74 o 5 2 12 17.51 20.04 6.83 o 1 3 12 137.60 154.09 3.84 o 2 3 12 207.14 214.23 4.74 o 3 3 12 19.43 26.37 4.19 o 4 3 12 869.59 882.72 16.45 o 0 4 12 4249.07 4238.14 79.06 o 1 4 12 54.32 55.93 5.13 o 2 4 12 3181.06 3129.67 34.50 o 3 4 12 210.00 201.62 9.48 o 4 4 12 1432.52 1364.64 20.82 o 1 5 12 4.28 4.13 8.45 o 2 5 12 154.38 142.39 7.32 o 3 5 12 53.18 52.13 6.01 o 0 6 12 2395.94 2403.85 47.61 o 1 6 12 19.77 29.05 4.89 o 2 6 12 1166.95 1195.93 16.92 o 1 1 13 2376.10 2488.39 31.80 o 2 1 13 168.83 182.79 6.53 o 3 1 13 2660.22 2617.89 31.05 o 4 1 13 362.85 375.51 11.50 o 5 1 13 418.82 395.65 10.75 o 0 2 13 1786.97 1800.10 29.17 o 1 2 13 122.68 114.18 3.09 o 2 2 13 873.91 868.90 12.86 o 3 2 13 20.76 21.36 8.88 o 4 2 13 63.73 66.93 12.11 o 5 2 13 13.11 17.39 6.29 o 1 3 13 907.00 961.64 16.23 o 2 3 13 26.04 27.25 4.36 o 3 3 13 1035.46 1057.61 15.01 o 4 3 13 105.70 97.99 10.46 o 0 4 13 10.11 5.76 20.47 o 1 4 13 163.85 165.43 9.54 o 2 4 13 20.61 30.75 3.98 o 3 4 13 26.34 35.33 4.92 o 4 4 13 29.60 25.10 9.25 o 1 5 13 674.09 663.86 17.11 o 2 5 13 379.28 365.89 7.07 o 3 5 13 237.11 217.27 19.90 o 0 6 13 281.92 253.67 37.33 o 1 6 13 1.11 -4.60 4.60 o 0 0 14 2719.11 2618.46 71.13 o 1 0 14 126.51 109.76 12.00 o 2 0 14 3337.21 3283.92 65.70 o 3 0 14 143.38 152.44 7.20 o 4 0 14 1247.12 1197.69 36.41 o 5 0 14 327.58 296.09 47.69 o 1 1 14 847.32 841.73 12.03 o 2 1 14 109.92 128.81 5.06 o 3 1 14 154.50 148.30 4.81 o 4 1 14 51.79 58.14 7.47 o 5 1 14 38.69 60.94 15.85 o 0 2 14 1290.30 1331.58 22.74 o 1 2 14 171.60 177.70 5.33 o 2 2 14 1629.12 1672.68 19.65 o 3 2 14 141.13 138.59 4.58 o 4 2 14 789.43 721.16 17.92 o 1 3 14 284.59 299.37 6.20 o 2 3 14 193.51 172.03 9.91 o 3 3 14 567.15 587.22 11.82 o 4 3 14 29.41 15.49 6.03 o 0 4 14 333.92 321.86 11.57 o 1 4 14 130.86 122.24 7.91 o 2 4 14 308.72 322.32 8.42 o 3 4 14 429.58 420.21 10.72 o 1 5 14 7.14 1.16 4.23 o 2 5 14 1.49 3.02 4.27 o 1 1 15 95.58 106.14 13.61 o 2 1 15 40.94 35.15 4.51 o 3 1 15 260.34 267.85 10.08 o 4 1 15 94.47 89.61 11.67 o 0 2 15 351.38 327.83 10.81 o 1 2 15 70.07 84.76 3.57 o 2 2 15 3.91 24.81 5.03 o 3 2 15 408.03 416.47 16.63 o 4 2 15 2.46 4.16 4.97 o 1 3 15 2172.90 2263.97 45.96 o 2 3 15 0.89 -2.38 5.20 o 3 3 15 1203.40 1192.53 26.78 o 0 4 15 33.56 40.85 26.53 o 1 4 15 6.40 11.05 4.89 o 2 4 15 22.54 24.03 7.07 o 3 4 15 37.88 32.82 26.86 o 1 5 15 2142.72 2150.31 73.95 o 0 0 16 5297.96 5319.15 139.40 o 1 0 16 4.37 -3.64 3.64 o 2 0 16 2458.55 2505.18 90.72 o 3 0 16 344.68 349.25 15.31 o 1 1 16 42.29 50.01 10.17 o 2 1 16 4.97 -2.44 4.41 o 3 1 16 23.40 30.04 4.06 o 4 1 16 125.94 118.24 9.91 o 0 2 16 1291.16 1349.74 32.56 o 1 2 16 62.73 56.68 5.12 o 2 2 16 865.61 873.76 13.92 o 3 2 16 14.13 2.97 6.51 o 1 3 16 340.88 324.35 8.84 o 2 3 16 127.04 135.03 5.34 o 3 3 16 1.45 -2.47 3.94 o 0 4 16 82.95 84.07 9.56 o 1 4 16 1.64 -6.49 6.49 o 2 4 16 97.31 110.05 11.37 o 1 1 17 782.96 765.04 13.33 o 2 1 17 199.46 188.00 6.48 o 3 1 17 241.20 239.68 10.94 o 0 2 17 651.50 662.99 17.81 o 1 2 17 27.33 25.13 5.61 o 2 2 17 493.05 493.45 22.20 o 3 2 17 0.65 17.85 16.39 o 1 3 17 887.22 921.04 16.26 o 2 3 17 66.15 75.57 8.48 o 1 4 17 73.32 88.06 12.99 o 0 0 18 570.74 594.15 23.80 o 1 0 18 113.27 118.03 8.56 o 2 0 18 98.56 84.68 12.22 o 1 1 18 92.36 81.70 13.57 o 2 1 18 187.76 188.73 7.31 o 0 2 18 454.73 446.10 30.96 o 1 2 18 6.09 8.83 10.21 o 2 2 18 303.33 294.19 10.83 o